CN109567209A - A kind of preparation method of collagen Gly-His-Lys - Google Patents
A kind of preparation method of collagen Gly-His-Lys Download PDFInfo
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- CN109567209A CN109567209A CN201811643109.1A CN201811643109A CN109567209A CN 109567209 A CN109567209 A CN 109567209A CN 201811643109 A CN201811643109 A CN 201811643109A CN 109567209 A CN109567209 A CN 109567209A
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- 102000008186 Collagen Human genes 0.000 title claims abstract description 50
- 108010035532 Collagen Proteins 0.000 title claims abstract description 50
- 229920001436 collagen Polymers 0.000 title claims abstract description 50
- MVORZMQFXBLMHM-QWRGUYRKSA-N Gly-His-Lys Chemical compound NCCCC[C@@H](C(O)=O)NC(=O)[C@@H](NC(=O)CN)CC1=CN=CN1 MVORZMQFXBLMHM-QWRGUYRKSA-N 0.000 title claims abstract description 31
- 108010038983 glycyl-histidyl-lysine Proteins 0.000 title claims abstract description 31
- 238000002360 preparation method Methods 0.000 title claims abstract description 27
- 229920002261 Corn starch Polymers 0.000 claims abstract description 26
- 239000008120 corn starch Substances 0.000 claims abstract description 26
- 229940099112 cornstarch Drugs 0.000 claims abstract description 26
- 102000004190 Enzymes Human genes 0.000 claims abstract description 22
- 108090000790 Enzymes Proteins 0.000 claims abstract description 22
- 239000002002 slurry Substances 0.000 claims abstract description 16
- 238000000034 method Methods 0.000 claims abstract description 14
- 239000000843 powder Substances 0.000 claims abstract description 13
- 208000007976 Ketosis Diseases 0.000 claims abstract description 9
- 239000002131 composite material Substances 0.000 claims abstract description 9
- 150000002584 ketoses Chemical class 0.000 claims abstract description 9
- 238000010438 heat treatment Methods 0.000 claims abstract description 8
- 239000000463 material Substances 0.000 claims abstract description 8
- 108090000765 processed proteins & peptides Proteins 0.000 claims abstract description 8
- 238000001694 spray drying Methods 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 102000004196 processed proteins & peptides Human genes 0.000 claims abstract description 3
- 229920002472 Starch Polymers 0.000 claims description 25
- 235000019698 starch Nutrition 0.000 claims description 25
- 239000008107 starch Substances 0.000 claims description 25
- 239000000839 emulsion Substances 0.000 claims description 23
- 229920000881 Modified starch Polymers 0.000 claims description 16
- 239000013049 sediment Substances 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000012153 distilled water Substances 0.000 claims description 7
- 238000004945 emulsification Methods 0.000 claims description 6
- 238000005119 centrifugation Methods 0.000 claims description 5
- 238000010792 warming Methods 0.000 claims description 5
- 229940100486 rice starch Drugs 0.000 claims description 2
- 239000006210 lotion Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 4
- 230000003712 anti-aging effect Effects 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 235000013361 beverage Nutrition 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 240000008042 Zea mays Species 0.000 description 5
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 5
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 5
- 235000005822 corn Nutrition 0.000 description 5
- 235000013601 eggs Nutrition 0.000 description 5
- 230000007071 enzymatic hydrolysis Effects 0.000 description 3
- 238000006047 enzymatic hydrolysis reaction Methods 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 206010013786 Dry skin Diseases 0.000 description 1
- 102000016942 Elastin Human genes 0.000 description 1
- 108010014258 Elastin Proteins 0.000 description 1
- 235000002710 Ilex cornuta Nutrition 0.000 description 1
- 241001310146 Ilex cornuta Species 0.000 description 1
- 102000007547 Laminin Human genes 0.000 description 1
- 108010085895 Laminin Proteins 0.000 description 1
- 235000010326 Osmanthus heterophyllus Nutrition 0.000 description 1
- 208000037656 Respiratory Sounds Diseases 0.000 description 1
- 101710172711 Structural protein Proteins 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 210000002808 connective tissue Anatomy 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 229920002549 elastin Polymers 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 102000004169 proteins and genes Human genes 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 230000009758 senescence Effects 0.000 description 1
- 230000037394 skin elasticity Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 230000001256 tonic effect Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/17—Amino acids, peptides or proteins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L19/00—Products from fruits or vegetables; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/125—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives containing carbohydrate syrups; containing sugars; containing sugar alcohols; containing starch hydrolysates
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The present invention relates to solid beverages, more particularly to a kind of preparation method of collagen Gly-His-Lys, the method includes the following steps: by weight, by 58-62 parts of collagen peptides, 2-8 parts of ketoses, 8-12 parts of cornstarch, 12-18 portions of fructus lyciis, 8-12 parts of composite enzymes, 1-5 portions of six sugar of shell, 0.01-1 parts of procyanidine are sequentially placed into container, and heating stirs evenly；The above-mentioned material stirred evenly is emulsified, slurry is obtained；Powder is made in spray drying after the slurry homogeneous, obtains collagen Gly-His-Lys.Present invention process is simple, at low cost, and Production Time is short, high-efficient, and collagen absorption is good, and absorptivity can reach 90% or more, increases the Collage Activitv in skin, has and moisturizes the skin, the effect of anti-aging.
Description
Technical field
The present invention relates to collagen Gly-His-Lys, and in particular to a kind of preparation method of collagen Gly-His-Lys.
Background technique
The skin corium of skin collagen rich in, the clear gum that collagen is made of 3 strands of spiral fibers
Substance is the main structural protein in connective tissue, their orderly aligned and elastin laminin interaction connection shapes are webbed
Structure supports the plentiful of skin just as the reinforcement frame of building.The retractility of collagen maintains skin elasticity
With automatic restorable performance.Collagen also adsorbs a large number of water molecules, prevents moisture from evaporating, and skin water is kept to moisten gloss.
Collagen accounts for the 70-80% of skin dry weight, is both important feature ingredient and indispensable nutritional agents and the protection of skin
Agent.
There are many kinds of the methods of replenishing collagen at present, for example eat collagen-rich food pig's feet, pigskin, fish more
Skin, oral collagen tonic etc..But due to that can be filtered out greatly by the digestive system of people, and it can really reach skin
And the amount to work is very limited, therefore, process is lengthy, and efficiency is also relatively low.
Summary of the invention
Technical problems based on background technology, the invention proposes a kind of preparation methods of collagen Gly-His-Lys.This
Invention increases the Collage Activitv in skin, has and moisturizes the skin, the effect of anti-aging.
A kind of preparation method of collagen Gly-His-Lys proposed by the present invention, the method includes the following steps: by weight,
By 58-62 parts of collagen peptides, 2-8 parts of ketoses, 8-12 parts of cornstarch, 12-18 portions of fructus lyciis, 8-12 parts of composite enzymes,
1-5 portions of six sugar of shell, 0.01-1 parts of procyanidine are sequentially placed into container, heat up, stir evenly；By the above-mentioned material stirred evenly
It is emulsified, obtains slurry；Powder is made in spray drying after the slurry homogeneous, obtains collagen Gly-His-Lys.
Preferably, the cornstarch be modified corn starch, the modified corn starch the preparation method comprises the following steps: to corn
Distilled water is added in starch and obtains starch emulsion；Complex enzyme, water-bath are added into starch emulsion, centrifugal treating will obtain
Sediment carry out microwave irradiation, pulverize and sieve, obtain modified corn starch.
Preferably, the mass fraction of the starch emulsion is 12-20wt%.
Preferably, the additional amount of the complex enzyme is 0.08-0.15 times of starch emulsion quality.
Preferably, the temperature of the water-bath is 40-50 DEG C, time 22-26h.
Preferably, in the operation of the centrifugal treating, centrifugal rotational speed 2000-2500r/min, centrifugation time 15-
25min。
Preferably, in the operation of the microwave irradiation, irradiation can be 15-22W/g, irradiation time 10-20min.
Preferably, described to pulverize and sieve to crushed 150-200 mesh.
Preferably, the heating is to be warming up to 75-85 DEG C.
Preferably, the temperature of the emulsification is 70-80 DEG C.
The primary raw material of collagen Gly-His-Lys of the present invention includes collagen, ketose, cornstarch, Chinese holly
Qi, composite enzyme, six sugar of shell, procyanidine, present invention process is simple, and at low cost, Production Time is short, high-efficient, and collagen
Absorbing proteins are good, and absorptivity can reach 90% or more, increase the Collage Activitv in skin, have and moisturize the skin, and delay senescence
Effect.The present invention is modified processing to cornstarch, into cornstarch be added distilled water obtain starch emulsion, then to
Complex enzyme water-bath is added in starch emulsion, cornstarch is digested, corn starch granules surface is degraded after enzymatic hydrolysis,
Particle shape becomes round and smooth, and occurs with a little crackle, and complex enzyme modifying function is milder, can reach micropore by enzymatic hydrolysis
The purpose of change, and the particle shape of cornstarch can be preferably kept, while effectively increasing rising for cornstarch and pasting temperature, change
The transparency of kind cornstarch, and then help to improve thermal stability and organoleptic quality of the invention；Then to the jade after enzymatic hydrolysis
Obtained sediment is carried out microwave irradiation, after microwave radiation, leads to the further of corn starch granules by rice starch centrifugal treating
Degradation, making it dissolve property increases, viscosity reduces, and then improves mobility and dissolubility of the invention；In addition, microwave irradiation can
Aggravate the free water loss speed in cornstarch, and then improves the drying effect of sediment.
Specific embodiment
In the following, technical solution of the present invention is described in detail by specific embodiment.
Embodiment 1
A kind of preparation method of collagen Gly-His-Lys, the method includes the following steps: by weight, by 58 portions of collagen eggs
White peptide, 8 parts of ketoses, 8 parts of cornstarch, 18 portions of fructus lyciis, 8 parts of composite enzymes, 5 parts of shells, six sugar, 0.01 part of procyanidine according to
Secondary to be put into container, heating stirs evenly；The above-mentioned material stirred evenly is emulsified, slurry is obtained；The slurry is equal
Powder is made in spray drying after matter, obtains collagen Gly-His-Lys.
Embodiment 2
A kind of preparation method of collagen Gly-His-Lys, the method includes the following steps: by weight, by 62 portions of collagen eggs
White peptide, 2 parts of ketoses, 12 parts of cornstarch, 12 portions of fructus lyciis, 12 parts of composite enzymes, 1 portion of six sugar of shell, 1 part of procyanidine is successively
It is put into container, heats up, stir evenly；The above-mentioned material stirred evenly is emulsified, slurry is obtained；By the slurry homogeneous
Powder is made in spray drying afterwards, obtains collagen Gly-His-Lys；
Wherein, the cornstarch be modified corn starch, the modified corn starch the preparation method comprises the following steps: to corn form sediment
Distilled water is added in powder and obtains starch emulsion；Complex enzyme, water-bath, centrifugal treating, by what is obtained are added into starch emulsion
Sediment carries out microwave irradiation, pulverizes and sieves, obtains modified corn starch.
Embodiment 3
A kind of preparation method of collagen Gly-His-Lys, the method includes the following steps: by weight, by 60 portions of collagen eggs
White peptide, 5 parts of ketoses, 10 parts of cornstarch, 15 portions of fructus lyciis, 10 parts of composite enzymes, 3 portions of six sugar of shell, 0.05 part of procyanidine
It is sequentially placed into container, heats up, stir evenly；The above-mentioned material stirred evenly is emulsified, slurry is obtained；By the slurry
Powder is made in spray drying after homogeneous, obtains collagen Gly-His-Lys；
Wherein, the cornstarch be modified corn starch, the modified corn starch the preparation method comprises the following steps: to corn form sediment
Distilled water is added in powder and obtains starch emulsion；Complex enzyme, water-bath, centrifugal treating, by what is obtained are added into starch emulsion
Sediment carries out microwave irradiation, pulverizes and sieves, obtains modified corn starch；
The mass fraction of the starch emulsion is 15wt%；
The additional amount of the complex enzyme is 0.1 times of starch emulsion quality；
The temperature of the water-bath is 45 DEG C, and the time is for 24 hours；
In the operation of the centrifugal treating, centrifugal rotational speed 2300r/min, centrifugation time 20min；
In the operation of the microwave irradiation, irradiation can be 19W/g, irradiation time 15min；
It is described to pulverize and sieve to crushed 170 meshes；
The heating is to be warming up to 80 DEG C；
The temperature of the emulsification is 75 DEG C.
Embodiment 4
A kind of preparation method of collagen Gly-His-Lys, the method includes the following steps: by weight, by 59 portions of collagen eggs
White peptide, 3 parts of ketoses, 9 parts of cornstarch, 13 portions of fructus lyciis, 9 parts of composite enzymes, 2 parts of shells, six sugar, 0.03 part of procyanidine according to
Secondary to be put into container, heating stirs evenly；The above-mentioned material stirred evenly is emulsified, slurry is obtained；The slurry is equal
Powder is made in spray drying after matter, obtains collagen Gly-His-Lys；
Wherein, the cornstarch be modified corn starch, the modified corn starch the preparation method comprises the following steps: to corn form sediment
Distilled water is added in powder and obtains starch emulsion；Complex enzyme, water-bath, centrifugal treating, by what is obtained are added into starch emulsion
Sediment carries out microwave irradiation, pulverizes and sieves, obtains modified corn starch；
The mass fraction of the starch emulsion is 12wt%；
The additional amount of the complex enzyme is 0.15 times of starch emulsion quality；
The temperature of the water-bath is 40 DEG C, time 26h；
In the operation of the centrifugal treating, centrifugal rotational speed 2000r/min, centrifugation time 25min；
In the operation of the microwave irradiation, irradiation can be 15W/g, irradiation time 20min；
It is described to pulverize and sieve to crushed 150 meshes；
The heating is to be warming up to 85 DEG C；
The temperature of the emulsification is 70 DEG C.
Embodiment 5
A kind of preparation method of collagen Gly-His-Lys, the method includes the following steps: by weight, by 61 portions of collagen eggs
White peptide, 7 parts of ketoses, 11 parts of cornstarch, 17 portions of fructus lyciis, 11 parts of composite enzymes, 4 portions of six sugar of shell, 0.07 part of procyanidine
It is sequentially placed into container, heats up, stir evenly；The above-mentioned material stirred evenly is emulsified, slurry is obtained；By the slurry
Powder is made in spray drying after homogeneous, obtains collagen Gly-His-Lys；
Wherein, the cornstarch be modified corn starch, the modified corn starch the preparation method comprises the following steps: to corn form sediment
Distilled water is added in powder and obtains starch emulsion；Complex enzyme, water-bath, centrifugal treating, by what is obtained are added into starch emulsion
Sediment carries out microwave irradiation, pulverizes and sieves, obtains modified corn starch；
The mass fraction of the starch emulsion is 20wt%；
The additional amount of the complex enzyme is 0.08 times of starch emulsion quality；
The temperature of the water-bath is 50 DEG C, time 22h；
In the operation of the centrifugal treating, centrifugal rotational speed 2500r/min, centrifugation time 15min；
In the operation of the microwave irradiation, irradiation can be 22W/g, irradiation time 10min；
It is described to pulverize and sieve to crushed 200 meshes；
The heating is to be warming up to 75 DEG C；
The temperature of the emulsification is 80 DEG C.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Anyone skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (10)
1. a kind of preparation method of collagen Gly-His-Lys, which is characterized in that the method includes the following steps: by weight, will
58-62 parts of collagen peptides, 2-8 parts of ketoses, 8-12 parts of cornstarch, 12-18 portions of fructus lyciis, 8-12 parts of composite enzymes, 1-5
Six sugar of part shell, 0.01-1 parts of procyanidine are sequentially placed into container, heat up, stir evenly；By the above-mentioned material stirred evenly into
Row emulsification, obtains slurry；Powder is made in spray drying after the slurry homogeneous, obtains collagen Gly-His-Lys.
2. the preparation method of collagen Gly-His-Lys according to claim 1, which is characterized in that the cornstarch is modified beautiful
Rice starch, the modified corn starch the preparation method comprises the following steps: into cornstarch be added distilled water obtain starch emulsion；To starch
Complex enzyme, water-bath are added in lotion, obtained sediment is carried out microwave irradiation, pulverizes and sieves, changed by centrifugal treating
Property cornstarch.
3. the preparation method of collagen Gly-His-Lys according to claim 2, which is characterized in that the quality of the starch emulsion point
Number is 12-20wt%.
4. the preparation method of collagen Gly-His-Lys according to Claims 2 or 3, which is characterized in that the addition of the complex enzyme
Amount is 0.08-0.15 times of starch emulsion quality.
5. the preparation method of collagen Gly-His-Lys according to Claims 2 or 3, which is characterized in that the temperature of the water-bath
Degree is 40-50 DEG C, time 22-26h.
6. the preparation method of collagen Gly-His-Lys according to Claims 2 or 3, which is characterized in that the behaviour of the centrifugal treating
In work, centrifugal rotational speed 2000-2500r/min, centrifugation time 15-25min.
7. the preparation method of collagen Gly-His-Lys according to Claims 2 or 3, which is characterized in that the behaviour of the microwave irradiation
In work, irradiation can be 15-22W/g, irradiation time 10-20min.
8. the preparation method of collagen Gly-His-Lys according to Claims 2 or 3, which is characterized in that described to pulverize and sieve as powder
It is broken to cross 150-200 mesh.
9. the preparation method of collagen Gly-His-Lys according to claim 1 or claim 2, which is characterized in that the heating is to be warming up to
75-85℃。
10. the preparation method of collagen Gly-His-Lys according to claim 1 or claim 2, which is characterized in that the temperature of the emulsification is
70-80℃。
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811643109.1A CN109567209A (en) | 2018-12-29 | 2018-12-29 | A kind of preparation method of collagen Gly-His-Lys |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811643109.1A CN109567209A (en) | 2018-12-29 | 2018-12-29 | A kind of preparation method of collagen Gly-His-Lys |
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| CN109567209A true CN109567209A (en) | 2019-04-05 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111802552A (en) * | 2020-06-29 | 2020-10-23 | 微肽科技(海南)有限公司 | Formula and preparation method of noni collagen peptide solid beverage |
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