CN109566596A - A kind of anticorrosion treatment technology of ox horn - Google Patents
A kind of anticorrosion treatment technology of ox horn Download PDFInfo
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- CN109566596A CN109566596A CN201811464980.5A CN201811464980A CN109566596A CN 109566596 A CN109566596 A CN 109566596A CN 201811464980 A CN201811464980 A CN 201811464980A CN 109566596 A CN109566596 A CN 109566596A
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N1/00—Preservation of bodies of humans or animals, or parts thereof
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- A—HUMAN NECESSITIES
- A45—HAND OR TRAVELLING ARTICLES
- A45D—HAIRDRESSING OR SHAVING EQUIPMENT; EQUIPMENT FOR COSMETICS OR COSMETIC TREATMENTS, e.g. FOR MANICURING OR PEDICURING
- A45D24/00—Hair combs for care of the hair; Accessories therefor
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
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- General Health & Medical Sciences (AREA)
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Abstract
The present invention is a kind of anticorrosion treatment technology of ox horn, the present invention uses and ox horn is first spontaneously dried depoling, carried out disinfection cleaning with disinfection cleaning solution again, except degerm, spot and angle core residue, then ox horn is put into impregnating fluid and carries out infusion, make impregnating fluid liquid uniform fold ox horn surface, moisture, insect pest, bacterium can effectively be completely cut off, play and help ox horn storage, extend ox horn storage time, it prevents ox horn to be damaged by insects, while can play the role of effectively removing stink, the fishy smell of ox horn.
Description
Technical field:
The present invention relates to the processing technique fields of ox horn, and in particular to a kind of anticorrosion treatment technology of ox horn.
Background technique:
Ox horn is one kind of Chinese medicine in itself, carries according to Compendium of Material Medica: " ox horn, acid are salty, refrigerant, nontoxic ".Therefore ox horn system
Product have certain health-care effect.It was occurred as soon as before very early with ox horn and makees comb, horn comb is using ox horn as raw material system
A kind of comb made.Good horn comb feel is gentle as beautiful, and thick and solid, ox horn color is mellow and full, good hand touch, does not play electrostatic.Use ox horn
It combs one's hair for several times, massage brain scalp and head nerves can be played, promoted blood circulation, the work of relaxation of tension and tired mood
With.It may be said that the use of ox horn is very extensive.
Ox horn is needed to clean ox horn raw material, be sterilized, the pretreatment such as taste removal before manufacturing into horn-ware,
Excessive to avoid the horn-ware taste of production, situations such as addling, therefore the pretreatment of ox horn is to influence horn-ware into quality
Measure an important step.
Summary of the invention:
The technical problem to be solved by the present invention lies in overcoming the defects of the prior art, provides a kind of preservative treatment of ox horn
Technique.
The following technical solution is employed for the technical problems to be solved by the invention to realize:
A kind of anticorrosion treatment technology of ox horn, which is characterized in that processing step is as follows:
(1) ox horn raw material is put at shady and cool, dry and is dried in the shade naturally 3-8 days, make angle core water loss, volume becomes smaller;
(2) the angle core in the dried ox horn of step 1 is removed;
(3) by the osteocomma of the ox horn removal root after removal angle core, trifle is sawn into according to ox horn size and shape;
(4) ox horn for handling step 3 well is put into disinfection cleaning solution, uses frequency for 20kHz, and power is the super of 800W
Sound wave carries out cleaning 20-40 minutes, and cleaning temperature is 45-55 degree;
(5) ox horn for handling step 4 well is rinsed well with clear water, is drained away the water;
(6) position addled is rasped away by the ox horn file that step 5 is handled well, then is polished smooth ox horn with sand paper;
(7) impregnating fluid is heated to 60 degree, the ox horn that step 6 is handled well is put into carry out infusion, keeps the temperature at 60-
70 degree, and be stirred continuously, the infusion time is 20-40 minutes;
(8) ox horn for handling step 7 well takes out, and wipes extra impregnating fluid.
Further, the disinfection cleaning solution is by following parts by weight at being grouped as: 80-120 parts of water, hydrogen peroxide 20-
40 parts, 5-15 parts of sodium carbonate peroxide, 5-15 parts of microcrystalline cellulose, 4-8 parts of pectin, 2% 4-8 parts of oxalic acid, 4-8 parts of active carbon.
Further, the impregnating fluid is by following parts by weight at being grouped as: 100-120 parts of paraffin, yellow cinnamon leaf 10-20
Part, 10-20 parts of folium artemisiae argyi, 10-15 parts of grape seed oil, 5-10 parts of active carbon, 5-10 parts of modified starch;Its production method are as follows: will be fragrant
Camphor tree leaf is mixed with folium artemisiae argyi, is broken into slurries with wall-breaking machine, is added in grape seed oil after slurries are filtered, and is carried out heating stirring and is endured
It boils, continues stirring infusion 5-10 minutes when temperature, which rises to 100-120, to be spent, obtain mixture I;Active carbon and modified starch are mixed
Conjunction carries out being gradually warmed up grinding, grinds after twenty minutes, the microwave treatment 10-15min under microwave frequency 2450MHz, power 600W,
Obtain mixtures II;Heating paraffin is melted, 60-70 degree is kept the temperature at, mixture I, II are added, after mixing evenly, is used
Ultrasonication 30min, then carry out insulated and stirred 10-20 minutes with the blender of 1000-1200r/min, that is, it can be made into.
Further, the ultrasonication is divided into tri- ranks of supersonic frequency 25-30kHz, 20-25kHz, 15-20kHz
Section, each stage are respectively handled 10 minutes.
The modified starch is made of starch, polyglutamic acid, chitosan, palm oil modification, production method are as follows: will form sediment
Powder is mixed with polyglutamic acid, heating grinding is carried out with the speed of 5 DEG C/min, after grinding 10-20 minutes, inwardly with 60d/min
Speed instill palm oil, continue grinding 10-20 minute, the absolute alcohol and shell that 3 times of parts by weight are added after the completion of grinding gather
Sugar stirs evenly, and is put into microwave processing equipment, is spaced microwave treatment under microwave frequency 2400MHz, power 500W, interval
Time is 10 minutes, and each microwave treatment 5 minutes is carried out continuously 5 times, and mixture obtained is sent into freeze drier, is done
Micro mist is made through micronizer to get modified starch in dry obtained solid.
The beneficial effects of the present invention are:
1, the present invention is using first spontaneously drying depoling for ox horn, then is carried out disinfection cleaning with disinfection cleaning solution, except degerm,
Spot and angle core residue, then ox horn is put into impregnating fluid and carries out infusion, make impregnating fluid liquid uniform fold ox horn surface, it can
Effectively isolation moisture, insect pest, bacterium plays and helps ox horn storage, extends ox horn storage time, prevent ox horn to be damaged by insects, together
When can play the role of effectively removing stink, the fishy smell of ox horn;
2, disinfection cleaning solution of the present invention is with water, hydrogen peroxide, sodium carbonate peroxide, microcrystalline cellulose, pectin, 2% oxalic acid, activity
Charcoal is made of raw material, materials safety, mild, effective, i.e., will not cause to corrode to ox horn, while effectively to the residual on ox horn
Spot is cleaned, and active carbon is added and plays increase adsorptivity, adsorbs stink, pectin is added in fishy smell, microcrystalline cellulose plays increasing
Add viscous stickiness, enhance cleaning effect, dilute oxalic acid that low concentration is added plays the role of softening spot;
3, using paraffin as primary raw material, non-toxic and safe environmental protection is added yellow cinnamon leaf, folium artemisiae argyi, plays anti-anti-corrosion wax liquor of the present invention
Only insect is corroded, and improves the effect of smell, while grape seed oil one side is added and reinforces insect prevention effective component in yellow cinnamon leaf and folium artemisiae argyi
Diffusion, on the one hand prevent ox horn oxidation it is dry and cracked, enhance the protective effect to ox horn, be also added into active carbon and increase absorption
Effect, has added modified starch, has increased caking property, be stained on impregnating fluid preferably on ox horn, further increases to extraneous tide
The isolation of gas, pest, it is more preferable to the anti-corrosion effect of ox horn.
Specific embodiment:
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Embodiment 1:
A kind of anticorrosion treatment technology of ox horn, which is characterized in that processing step is as follows:
(1) ox horn raw material is put at shady and cool, dry and is dried in the shade naturally 3 days, make angle core water loss, volume becomes smaller;
(2) the angle core in the dried ox horn of step 1 is removed;
(3) by the osteocomma of the ox horn removal root after removal angle core, trifle is sawn into according to ox horn size and shape;
(4) ox horn for handling step 3 well is put into disinfection cleaning solution, uses frequency for 20kHz, and power is the super of 800W
Sound wave carries out cleaning 20 minutes, and cleaning temperature is 45 degree;
(5) ox horn for handling step 4 well is rinsed well with clear water, is drained away the water;
(6) position addled is rasped away by the ox horn file that step 5 is handled well, then is polished smooth ox horn with sand paper;
(7) impregnating fluid is heated to 60 degree, the ox horn that step 6 is handled well is put into carry out infusion, keeps the temperature at 60
Degree, and be stirred continuously, the infusion time is 20 minutes;
(8) ox horn for handling step 7 well takes out, and wipes extra impregnating fluid.
Further, the disinfection cleaning solution is by following parts by weight at being grouped as: 80 parts of water, 20 parts of hydrogen peroxide, and mistake
5 parts of oxygen sodium carbonate, 5 parts of microcrystalline cellulose, 4 parts of pectin, 2% 4 parts of oxalic acid, 4 parts of active carbon.
Further, the impregnating fluid is by following parts by weight at being grouped as: 100 parts of paraffin, 10 parts of yellow cinnamon leaf, folium artemisiae argyi
10 parts, 10 parts of grape seed oil, 5 parts of active carbon, 5 parts of modified starch;Its production method are as follows: mix yellow cinnamon leaf with folium artemisiae argyi, with broken
Wall machine is broken into slurries, is added in grape seed oil after slurries are filtered, and heating stirring infusion is carried out, when temperature rises to 100 degree
Shi Jixu is stirred infusion 5 minutes, obtains mixture I;Active carbon is mixed with modified starch and be gradually warmed up grinding, grinds 20 points
Zhong Hou, the microwave treatment 10min under microwave frequency 2450MHz, power 600W, obtains mixtures II;Heating paraffin is melted, it will be warm
Degree is maintained at 60 degree, mixture I, II is added, after mixing evenly, with ultrasonication 30min, then stirring with 1000r/min
It mixes machine to carry out insulated and stirred 10 minutes, that is, can be made into.
Further, the ultrasonication is divided into supersonic frequency 25kHz, 20kHz, 15kHz three phases, each stage
Each processing 10 minutes.
The modified starch is made of starch, polyglutamic acid, chitosan, palm oil modification, production method are as follows: will form sediment
Powder is mixed with polyglutamic acid, is carried out heating grinding with the speed of 5 DEG C/min, is ground after ten minutes, inwardly with the speed of 60d/min
Degree instills palm oil, continues grinding 10 minutes, the absolute alcohol and chitosan of 3 times of parts by weight, stirring are added after the completion of grinding
Uniformly, it is put into microwave processing equipment, microwave treatment, interval time 10 is spaced under microwave frequency 2400MHz, power 500W
Minute, each microwave treatment 5 minutes is carried out continuously 5 times, and mixture obtained is sent into freeze drier, and dry gained is solid
Micro mist is made through micronizer to get modified starch in body.
Embodiment 2:
A kind of anticorrosion treatment technology of ox horn, which is characterized in that processing step is as follows:
(1) ox horn raw material is put at shady and cool, dry and is dried in the shade naturally 6 days, make angle core water loss, volume becomes smaller;
(2) the angle core in the dried ox horn of step 1 is removed;
(3) by the osteocomma of the ox horn removal root after removal angle core, trifle is sawn into according to ox horn size and shape;
(4) ox horn for handling step 3 well is put into disinfection cleaning solution, uses frequency for 20kHz, and power is the super of 800W
Sound wave carries out cleaning 30 minutes, and cleaning temperature is 50 degree;
(5) ox horn for handling step 4 well is rinsed well with clear water, is drained away the water;
(6) position addled is rasped away by the ox horn file that step 5 is handled well, then is polished smooth ox horn with sand paper;
(7) impregnating fluid is heated to 60 degree, the ox horn that step 6 is handled well is put into carry out infusion, keeps the temperature at 65
Degree, and be stirred continuously, the infusion time is 30 minutes;
(8) ox horn for handling step 7 well takes out, and wipes extra impregnating fluid.
Further, the disinfection cleaning solution is by following parts by weight at being grouped as: 100 parts of water, 30 parts of hydrogen peroxide, and mistake
10 parts of oxygen sodium carbonate, 10 parts of microcrystalline cellulose, 6 parts of pectin, 2% 6 parts of oxalic acid, 6 parts of active carbon.
Further, the impregnating fluid is by following parts by weight at being grouped as: 110 parts of paraffin, 15 parts of yellow cinnamon leaf, folium artemisiae argyi
15 parts, 13 parts of grape seed oil, 8 parts of active carbon, 8 parts of modified starch;Its production method are as follows: mix yellow cinnamon leaf with folium artemisiae argyi, with broken
Wall machine is broken into slurries, is added in grape seed oil after slurries are filtered, and heating stirring infusion is carried out, when temperature rises to 110 degree
Shi Jixu is stirred infusion 8 minutes, obtains mixture I;Active carbon is mixed with modified starch and be gradually warmed up grinding, grinds 20 points
Zhong Hou, the microwave treatment 13min under microwave frequency 2450MHz, power 600W, obtains mixtures II;Heating paraffin is melted, it will be warm
Degree is maintained at 65 degree, mixture I, II is added, after mixing evenly, with ultrasonication 30min, then stirring with 1100r/min
It mixes machine to carry out insulated and stirred 15 minutes, that is, can be made into.
Further, the ultrasonication is divided into supersonic frequency 28kHz, 23kHz, 18kHz three phases, each stage
Each processing 10 minutes.
The modified starch is made of starch, polyglutamic acid, chitosan, palm oil modification, production method are as follows: will form sediment
Powder is mixed with polyglutamic acid, heating grinding is carried out with the speed of 5 DEG C/min, after grinding 15 minutes, inwardly with the speed of 60d/min
Degree instills palm oil, continues grinding 15 minutes, the absolute alcohol and chitosan of 3 times of parts by weight, stirring are added after the completion of grinding
Uniformly, it is put into microwave processing equipment, microwave treatment, interval time 10 is spaced under microwave frequency 2400MHz, power 500W
Minute, each microwave treatment 5 minutes is carried out continuously 5 times, and mixture obtained is sent into freeze drier, and dry gained is solid
Micro mist is made through micronizer to get modified starch in body.
Embodiment 3:
A kind of anticorrosion treatment technology of ox horn, which is characterized in that processing step is as follows:
(1) ox horn raw material is put at shady and cool, dry and is dried in the shade naturally 8 days, make angle core water loss, volume becomes smaller;
(2) the angle core in the dried ox horn of step 1 is removed;
(3) by the osteocomma of the ox horn removal root after removal angle core, trifle is sawn into according to ox horn size and shape;
(4) ox horn for handling step 3 well is put into disinfection cleaning solution, uses frequency for 20kHz, and power is the super of 800W
Sound wave carries out cleaning 40 minutes, and cleaning temperature is 55 degree;
(5) ox horn for handling step 4 well is rinsed well with clear water, is drained away the water;
(6) position addled is rasped away by the ox horn file that step 5 is handled well, then is polished smooth ox horn with sand paper;
(7) impregnating fluid is heated to 60 degree, the ox horn that step 6 is handled well is put into carry out infusion, keeps the temperature at 70
Degree, and be stirred continuously, the infusion time is 40 minutes;
(8) ox horn for handling step 7 well takes out, and wipes extra impregnating fluid.
Further, the disinfection cleaning solution is by following parts by weight at being grouped as: 120 parts of water, 40 parts of hydrogen peroxide, and mistake
15 parts of oxygen sodium carbonate, 15 parts of microcrystalline cellulose, 8 parts of pectin, 2% 8 parts of oxalic acid, 8 parts of active carbon.
Further, the impregnating fluid is by following parts by weight at being grouped as: 120 parts of paraffin, 20 parts of yellow cinnamon leaf, folium artemisiae argyi
20 parts, 15 parts of grape seed oil, 10 parts of active carbon, 10 parts of modified starch;Its production method are as follows: yellow cinnamon leaf is mixed with folium artemisiae argyi, is used
Wall-breaking machine is broken into slurries, is added in grape seed oil after slurries are filtered, and heating stirring infusion is carried out, when temperature rises to 120
Continue stirring infusion 10 minutes when spending, obtains mixture I;Active carbon is mixed with modified starch and be gradually warmed up grinding, is ground
After twenty minutes, the microwave treatment 15min under microwave frequency 2450MHz, power 600W, obtains mixtures II;Heating paraffin is melted,
70 degree are kept the temperature at, mixture I, II are added, after mixing evenly, with ultrasonication 30min, then uses 1200r/min
Blender carry out insulated and stirred 20 minutes, that is, can be made into.
Further, the ultrasonication is divided into supersonic frequency 30kHz, 25kHz, 20kHz three phases, each stage
Each processing 10 minutes.
The modified starch is made of starch, polyglutamic acid, chitosan, palm oil modification, production method are as follows: will form sediment
Powder is mixed with polyglutamic acid, is carried out heating grinding with the speed of 5 DEG C/min, is ground after twenty minutes, inwardly with the speed of 60d/min
Degree instills palm oil, continues grinding 20 minutes, the absolute alcohol and chitosan of 3 times of parts by weight, stirring are added after the completion of grinding
Uniformly, it is put into microwave processing equipment, microwave treatment, interval time 10 is spaced under microwave frequency 2400MHz, power 500W
Minute, each microwave treatment 5 minutes is carried out continuously 5 times, and mixture obtained is sent into freeze drier, and dry gained is solid
Micro mist is made through micronizer to get modified starch in body.
Control group 1:
This control group content and 2 content of embodiment are essentially identical, and something in common no longer repeats, the difference is that: it does not adopt
It is cleaned with disinfection cleaning solution, is cleaned using clear water.
Control group 2:
This control group content and 2 content of embodiment are essentially identical, and something in common no longer repeats, the difference is that: it uses
It after disinfection cleaning solution cleans up, directly dries, does not use impregnating fluid infusion.
Control group 3:
Commercially available ox horn.
The obtained ox horn of above-described embodiment 1-3 and comparative example 1-3 is compared, the results are shown in Table 1:
Table 1
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (4)
1. a kind of anticorrosion treatment technology of ox horn, which is characterized in that processing step is as follows:
(1) ox horn raw material is put at shady and cool, dry and is dried in the shade naturally 3-8 days, make angle core water loss, volume becomes smaller;
(2) the angle core in the dried ox horn of step 1 is removed;
(3) by the osteocomma of the ox horn removal root after removal angle core, trifle is sawn into according to ox horn size and shape;
(4) ox horn for handling step 3 well is put into disinfection cleaning solution, uses frequency for 20kHz, and power is the ultrasonic wave of 800W
Cleaning 20-40 minutes is carried out, cleaning temperature is 45-55 degree;
(5) ox horn for handling step 4 well is rinsed well with clear water, is drained away the water;
(6) position addled is rasped away by the ox horn file that step 5 is handled well, then is polished smooth ox horn with sand paper;
(7) impregnating fluid is heated to 60 degree, the ox horn that step 6 is handled well is put into carry out infusion, keeps the temperature at 60-70
Degree, and be stirred continuously, the infusion time is 20-40 minutes;
(8) ox horn for handling step 7 well takes out, and wipes extra impregnating fluid.
2. the anticorrosion treatment technology of ox horn according to claim 1, which is characterized in that the disinfection cleaning solution is by following heavy
Amount number at being grouped as: 80-120 parts of water, 20-40 parts of hydrogen peroxide, 5-15 parts of sodium carbonate peroxide, 5-15 parts of microcrystalline cellulose,
4-8 parts of pectin, 2% 4-8 parts of oxalic acid, 4-8 parts of active carbon.
3. the anticorrosion treatment technology of ox horn according to claim 1, which is characterized in that the impregnating fluid is by following parts by weight
It is several at being grouped as: 100-120 parts of paraffin, 10-20 parts of yellow cinnamon leaf, 10-20 parts of folium artemisiae argyi, 10-15 parts of grape seed oil, active carbon 5-
10 parts, 5-10 parts of modified starch;Its production method are as follows: yellow cinnamon leaf is mixed with folium artemisiae argyi, is broken into slurries with wall-breaking machine, by slurries
It is added in grape seed oil after filtering, carries out heating stirring infusion, continue to stir infusion 5-10 when temperature, which rises to 100-120, to be spent
Minute, obtain mixture I;Active carbon is mixed with modified starch and be gradually warmed up grinding, is ground after twenty minutes, in microwave frequency
Microwave treatment 10-15min under 2450MHz, power 600W, obtains mixtures II;Heating paraffin is melted, 60- is kept the temperature at
70 degree, mixture I, II are added, after mixing evenly, with ultrasonication 30min, then the blender with 1000-1200r/min
It carries out insulated and stirred 10-20 minutes, that is, can be made into.
4. the anticorrosion treatment technology of ox horn according to claim 3, which is characterized in that the ultrasonication is divided into ultrasound
Frequency 25-30kHz, 20-25kHz, 15-20kHz three phases, each stage are respectively handled 10 minutes.
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Citations (4)
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---|---|---|---|---|
CN1398550A (en) * | 2002-08-29 | 2003-02-26 | 周至春 | Synthesis of animal's horn and hoof raw material |
CN1621247A (en) * | 2005-01-07 | 2005-06-01 | 许玉奇 | Making process of embossment board picture with animal horns and bones |
TW200816917A (en) * | 2007-11-26 | 2008-04-16 | Lungyen Life Service Co Ltd | Anticorrosive compound for body remains and the preparation method and application of the same |
CN108610926A (en) * | 2018-05-22 | 2018-10-02 | 天长市双丰文化用品有限公司 | A kind of anticorrosive paint for easel |
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2018
- 2018-12-03 CN CN201811464980.5A patent/CN109566596A/en not_active Withdrawn
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1398550A (en) * | 2002-08-29 | 2003-02-26 | 周至春 | Synthesis of animal's horn and hoof raw material |
CN1621247A (en) * | 2005-01-07 | 2005-06-01 | 许玉奇 | Making process of embossment board picture with animal horns and bones |
TW200816917A (en) * | 2007-11-26 | 2008-04-16 | Lungyen Life Service Co Ltd | Anticorrosive compound for body remains and the preparation method and application of the same |
CN108610926A (en) * | 2018-05-22 | 2018-10-02 | 天长市双丰文化用品有限公司 | A kind of anticorrosive paint for easel |
Non-Patent Citations (4)
Title |
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于淑池: "《生物源拮抗物质的提取及应用》", 31 March 2016, 北京理工大学出版社 * |
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