CN110339113A - A kind of peach colloidal solution and its preparation method and application - Google Patents
A kind of peach colloidal solution and its preparation method and application Download PDFInfo
- Publication number
- CN110339113A CN110339113A CN201910661725.8A CN201910661725A CN110339113A CN 110339113 A CN110339113 A CN 110339113A CN 201910661725 A CN201910661725 A CN 201910661725A CN 110339113 A CN110339113 A CN 110339113A
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- Prior art keywords
- peach
- colloidal solution
- peach gum
- gum
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/82—Preparation or application process involves sonication or ultrasonication
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Dermatology (AREA)
- Microbiology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Mycology (AREA)
- Botany (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention belongs to peach gum processing technique fields, disclose a kind of preparation method of peach colloidal solution, include the following steps: that (1) chooses the peach that the age of tree is 2 years or more and collects peach gum；(2) peach gum being collected into is cleaned into removal impurity, and the sterilization processing in autoclave with clear water；Then, drying, micronization processes obtain peach gum micro mist；(3) obtained peach gum micro mist is soaked in water, and ammonium hydroxide is added and adjusts pure water to pH7-8, heating is completely dissolved peach gum, then carries out ultrasonic reaction；(4) hydrogen peroxide is added into peach gum solution to be stirred, then adds active carbon, is placed in thermostat water bath, carry out supersonic oscillations；(5) the peach gum mixed solution that step (4) obtains is centrifuged, obtained supernatant liquor is handled 1 time through step (4) again, filters to obtain peach colloidal solution.The peach colloidal solution active constituent content prepared by the method for the invention is high, is suitable for production facial mask, has effects that moisturizing, whitening.
Description
Technical field
The invention belongs to peach gum processing technique field, it is related to a kind of peach colloidal solution and its preparation method and application.
Background technique
Peach gum, is the colloid vitrina being secreted in the barks such as rosaceous plant peach or mountain peach, outer likeness in form amber,
Main group becomes galactolipin, rhamnose and phlorose aldehydic acid etc., contains carbon water chemistry object, fat, protein and plant collagen
Albumen.Peach gum acts on the equal nonhazardous of people and animals, and medical, medicinal and edible etc. value with higher, traditional medicine think peach
Glue can control the illnesss such as urolithiasis, blood strangury, dysentery, diabetes, sore rash be black；In addition, peach gum can do peptone colloidality food, edibility food
The edible products such as product preservative film, beverage additive can also do medical supersonic conductive agent, and do ink, coating, printing and dyeing industry and help
Agent etc. is widely used in the fields such as food, medicine and industry.
Peach gum extract has good moistening effect, and moisturizing principle is similar to hyaluronic acid, has good moisturizing
Effect.Therefore, in cosmetic field, peach gum extract is multi-purpose to make emulsifier, thickener, moisturising actives and skin anti-inflammatory object
Matter.But using peach gum as primary raw material be applied to the report in mask product there is presently no, therefore research and development can be used for facial mask
Peach colloidal solution and prepare facial mask with it and have great importance.
Summary of the invention
The technical problem to be solved by the present invention is to overcome drawbacks described above, provide the preparation method and its preparation of a kind of peach colloidal solution
Methods and applications.
In order to solve the above-mentioned technical problem, the technical solution of the present invention is as follows:
A kind of preparation method of peach colloidal solution, includes the following steps:
(1) peach that the age of tree is 2 years or more is chosen, inverted triangle mouth is cut at trunk, and place collection vessel in incision,
For collecting peach gum；
(2) peach gum being collected into is cleaned into removal impurity, and the sterilization processing in autoclave with clear water；Then, drying,
Micronization processes obtain peach gum micro mist；
(3) obtained peach gum micro mist is soaked in water, and ammonium hydroxide is added and adjusts pure water to pH7-8, heating keeps peach gum complete
Then fully dissolved carries out ultrasonic reaction；
(4) hydrogen peroxide is added into peach gum solution to be stirred, then adds active carbon, is placed in thermostat water bath
In, carry out supersonic oscillations；
(5) the peach gum mixed solution that step (4) obtains is centrifuged, by obtained supernatant liquor again through step
(4) it handles 1 time, filters to obtain peach colloidal solution.
Preferably, step (2) sterilization temperature is 70-80 DEG C, sterilizing time 10-15min.
Preferably, the mass ratio of peach gum micro mist described in step (3) and water is 1:100-160.
Preferably, heating temperature described in step (3) is 65-75 DEG C.
Preferably, ultrasonic power described in step (3) is 200-500W, and ultrasonic temperature is 40-60 DEG C, and the reaction time is
30-50min。
Preferably, the mass percentage concentration of hydrogen peroxide described in step (4) is 10-15%.
Preferably, it is 20-30kHz, ultrasonic time 5-10min that supersonic oscillations described in step (4), which are supersonic frequency,.
A kind of peach colloidal solution is also disclosed in another object of the present invention, and the method as described in above-mentioned technical proposal is prepared.
It is of the invention to provide a kind of above-mentioned peach colloidal solution in one aspect and preparing the application in peach colloidal solution facial mask.
Compared with prior art the beneficial effects of the present invention are:
The present invention is by carrying out extraction processing to peach gum raw material, so that preferably to enter peach gum raw material thin for internal moisture
Inside cell wall, in conjunction with ultrasonic grind processing, effectively the cell wall inside peach gum raw material can be removed, at centrifugation
Reason, improves the purity of peach gum；Hydrogen peroxide is made by alkali protective effect using hydrogen peroxide and the dual decoloration of active carbon simultaneously
The structure of peach gum molecule will not be damaged in removal peach gum intermolecular stress and bleaching process, while active carbon can adsorb peach
Color component and fine impurity in glue play the role of impurity elimination of decolourizing, and improve peach gum purity, contain the consolidating for peach colloidal solution of preparation
Amount is high.
The peach colloidal solution prepared by the method for the invention is used to prepare facial mask, has the effect of moisturizing, whitening, tender skin, makes flesh
Skin keeps water tender glossy.
Specific embodiment
Specific embodiments of the present invention will be further explained below.It should be noted that for these implementations
The explanation of mode is used to help understand the present invention, but and does not constitute a limitation of the invention.In addition, invention described below
Technical characteristic involved in each embodiment can be combined with each other as long as they do not conflict with each other.
Embodiment 1
A kind of preparation method of peach colloidal solution, includes the following steps:
(1) peach that the age of tree is 2 years or more is chosen, inverted triangle mouth is cut at trunk, and place collection vessel in incision,
For collecting peach gum；
(2) peach gum being collected into is cleaned into removal impurity with clear water, and in 70 DEG C of sterilization 15min in autoclave；Then,
Drying, micronization processes obtain peach gum micro mist；
(3) obtained peach gum micro mist is soaked in water, wherein the mass ratio of peach gum micro mist and water is 1:100, and is added
Ammonium hydroxide adjusts pure water to pH=8, and 65 DEG C of heating is completely dissolved peach gum, then the anti-50min of ultrasound at 200W, 40 DEG C；
(4) it is that 10% hydrogen peroxide is stirred that mass percentage concentration is added into peach gum solution, then adds activity
Charcoal is placed in thermostat water bath, the sonic oscillation 10min in the case where ultrasonic power is 20kHz；
(5) the peach gum mixed solution that step (4) obtains is centrifuged, by obtained supernatant liquor again through step
(4) it handles 1 time, filters to obtain peach colloidal solution.
Embodiment 2
A kind of preparation method of peach colloidal solution, includes the following steps:
(1) peach that the age of tree is 2 years or more is chosen, inverted triangle mouth is cut at trunk, and place collection vessel in incision,
For collecting peach gum；
(2) peach gum being collected into is cleaned into removal impurity with clear water, and in 75 DEG C of sterilization 12min in autoclave；Then,
Drying, micronization processes obtain peach gum micro mist；
(3) obtained peach gum micro mist is soaked in water, wherein the mass ratio of peach gum micro mist and water is 1:120, and is added
Ammonium hydroxide adjusts pure water to pH=7.5, and 70 DEG C of heating is completely dissolved peach gum, then the anti-40min of ultrasound at 300W, 50 DEG C；
(4) it is that 12% hydrogen peroxide is stirred that mass percentage concentration is added into peach gum solution, then adds activity
Charcoal is placed in thermostat water bath, the sonic oscillation 8min in the case where ultrasonic power is 25kHz；
(5) the peach gum mixed solution that step (4) obtains is centrifuged, by obtained supernatant liquor again through step
(4) it handles 1 time, filters to obtain peach colloidal solution.
Embodiment 3
A kind of preparation method of peach colloidal solution, includes the following steps:
(1) peach that the age of tree is 2 years or more is chosen, inverted triangle mouth is cut at trunk, and place collection vessel in incision,
For collecting peach gum；
(2) peach gum being collected into is cleaned into removal impurity with clear water, and in 78 DEG C of sterilization 12min in autoclave；Then,
Drying, micronization processes obtain peach gum micro mist；
(3) obtained peach gum micro mist is soaked in water, wherein the mass ratio of peach gum micro mist and water is 1:150, and is added
Ammonium hydroxide adjusts pure water to pH=8, and 72 DEG C of heating is completely dissolved peach gum, then the anti-45min of ultrasound at 400W, 45 DEG C；
(4) it is that 13% hydrogen peroxide is stirred that mass percentage concentration is added into peach gum solution, then adds activity
Charcoal is placed in thermostat water bath, the sonic oscillation 6min in the case where ultrasonic power is 28kHz；
(5) the peach gum mixed solution that step (4) obtains is centrifuged, by obtained supernatant liquor again through step
(4) it handles 1 time, filters to obtain peach colloidal solution.
Embodiment 4
A kind of preparation method of peach colloidal solution, includes the following steps:
(1) peach that the age of tree is 2 years or more is chosen, inverted triangle mouth is cut at trunk, and place collection vessel in incision,
For collecting peach gum；
(2) peach gum being collected into is cleaned into removal impurity with clear water, and in 80 DEG C of sterilization 10min in autoclave；Then,
Drying, micronization processes obtain peach gum micro mist；
(3) obtained peach gum micro mist is soaked in water, wherein the mass ratio of peach gum micro mist and water is 1:160, and is added
Ammonium hydroxide adjusts pure water to pH=8, and 75 DEG C of heating is completely dissolved peach gum, then the anti-30min of ultrasound at 500W, 60 DEG C；
(4) it is that 15% hydrogen peroxide is stirred that mass percentage concentration is added into peach gum solution, then adds activity
Charcoal is placed in thermostat water bath, the sonic oscillation 5min in the case where ultrasonic power is 30kHz；
(5) the peach gum mixed solution that step (4) obtains is centrifuged, by obtained supernatant liquor again through step
(4) it handles 1 time, filters to obtain peach colloidal solution.
The above are present pre-ferred embodiments, it is only applicable to the principle for helping to understand the embodiment of the present invention；Meanwhile for this
The those skilled in the art in field, according to the present embodiment, there will be changes in terms of specific embodiments and scope of application, comprehensive
Upper described, the contents of this specification are not to be construed as limiting the invention.
Claims (9)
1. a kind of preparation method of peach colloidal solution, characterized by the following steps:
(1) peach that the age of tree is 2 years or more is chosen, inverted triangle mouth is cut at trunk, and place collection vessel in incision, is used for
Collect peach gum；
(2) peach gum being collected into is cleaned into removal impurity, and the sterilization processing in autoclave with clear water；Then, drying, micro mist
Change processing, obtains peach gum micro mist；
(3) obtained peach gum micro mist is soaked in water, and ammonium hydroxide is added and adjusts pure water to pH7-8, heating keeps peach gum completely molten
Solution, then carries out ultrasonic reaction；
(4) hydrogen peroxide is added into peach gum solution to be stirred, then adds active carbon, is placed in thermostat water bath, into
Row supersonic oscillations；
(5) the peach gum mixed solution that step (4) obtains is centrifuged, by obtained supernatant liquor again through step (4) at
Reason 1 time, filters to obtain peach colloidal solution.
2. the preparation method of peach colloidal solution according to claim 1, it is characterised in that: step (2) sterilization temperature is 70-
80 DEG C, sterilizing time 10-15min.
3. the preparation method of peach colloidal solution according to claim 1, it is characterised in that: peach gum micro mist described in step (3) with
The mass ratio of water is 1:100-160.
4. the preparation method of peach colloidal solution according to claim 1, it is characterised in that: heating temperature described in step (3) is
65-75℃。
5. the preparation method of peach colloidal solution according to claim 1, it is characterised in that: ultrasonic power described in step (3) is
200-500W, ultrasonic temperature are 40-60 DEG C, reaction time 30-50min.
6. the preparation method of peach colloidal solution according to claim 1, it is characterised in that: hydrogen peroxide described in step (4)
Mass percentage concentration is 10-15%.
7. the preparation method of peach colloidal solution according to claim 1, it is characterised in that: supersonic oscillations described in step (4)
It is 20-30kHz, ultrasonic time 5-10min for supersonic frequency.
8. a kind of peach colloidal solution by the described in any item method preparations of claim 1-7.
9. a kind of peach colloidal solution according to any one of claims 8 is preparing the application in peach colloidal solution facial mask.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910661725.8A CN110339113A (en) | 2019-07-22 | 2019-07-22 | A kind of peach colloidal solution and its preparation method and application |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910661725.8A CN110339113A (en) | 2019-07-22 | 2019-07-22 | A kind of peach colloidal solution and its preparation method and application |
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| CN110339113A true CN110339113A (en) | 2019-10-18 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112315816A (en) * | 2020-10-28 | 2021-02-05 | 瞿小强 | Preparation method of natural peach gum mask |
| CN115517371A (en) * | 2022-08-10 | 2022-12-27 | 中国农业科学院农产品加工研究所 | Low-viscosity peach gum polysaccharide solution and preparation method and application thereof |
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| CN101433309A (en) * | 2008-12-18 | 2009-05-20 | 福州大学 | Method for decolorizing peach gum hydrolysate |
| CN106109354A (en) * | 2016-08-25 | 2016-11-16 | 青岛海澄知识产权事务有限公司 | A kind of preparation method of peach colloidal solution |
| CN106309216A (en) * | 2016-08-25 | 2017-01-11 | 青岛海澄知识产权事务有限公司 | Peach gum mask |
| CN107383234A (en) * | 2017-09-29 | 2017-11-24 | 贵州爽口达食品开发有限公司 | A kind of extraction process of peach gum polysaccharide |
| CN107400175A (en) * | 2017-08-02 | 2017-11-28 | 杨俊� | A kind of preparation method of high-purity peach gum |
| CN108329738A (en) * | 2018-04-04 | 2018-07-27 | 河北青竹画材科技有限公司 | Peach colloidal solution and preparation method thereof |
| CN109172384A (en) * | 2018-09-26 | 2019-01-11 | 南京中医药大学 | A kind of peach blossom face paste formula facial mask and preparation method thereof |
| CN109575151A (en) * | 2018-12-10 | 2019-04-05 | 宁波工程学院 | A kind of preparation method of peach gum Polysaccharides |
-
2019
- 2019-07-22 CN CN201910661725.8A patent/CN110339113A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101433309A (en) * | 2008-12-18 | 2009-05-20 | 福州大学 | Method for decolorizing peach gum hydrolysate |
| CN106109354A (en) * | 2016-08-25 | 2016-11-16 | 青岛海澄知识产权事务有限公司 | A kind of preparation method of peach colloidal solution |
| CN106309216A (en) * | 2016-08-25 | 2017-01-11 | 青岛海澄知识产权事务有限公司 | Peach gum mask |
| CN107400175A (en) * | 2017-08-02 | 2017-11-28 | 杨俊� | A kind of preparation method of high-purity peach gum |
| CN107383234A (en) * | 2017-09-29 | 2017-11-24 | 贵州爽口达食品开发有限公司 | A kind of extraction process of peach gum polysaccharide |
| CN108329738A (en) * | 2018-04-04 | 2018-07-27 | 河北青竹画材科技有限公司 | Peach colloidal solution and preparation method thereof |
| CN109172384A (en) * | 2018-09-26 | 2019-01-11 | 南京中医药大学 | A kind of peach blossom face paste formula facial mask and preparation method thereof |
| CN109575151A (en) * | 2018-12-10 | 2019-04-05 | 宁波工程学院 | A kind of preparation method of peach gum Polysaccharides |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112315816A (en) * | 2020-10-28 | 2021-02-05 | 瞿小强 | Preparation method of natural peach gum mask |
| CN115517371A (en) * | 2022-08-10 | 2022-12-27 | 中国农业科学院农产品加工研究所 | Low-viscosity peach gum polysaccharide solution and preparation method and application thereof |
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Application publication date: 20191018 |
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