CN109498474A - A kind of salubrious three-phase Emulsified sunscreen cosmetic and preparation method thereof - Google Patents
A kind of salubrious three-phase Emulsified sunscreen cosmetic and preparation method thereof Download PDFInfo
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- CN109498474A CN109498474A CN201811516549.0A CN201811516549A CN109498474A CN 109498474 A CN109498474 A CN 109498474A CN 201811516549 A CN201811516549 A CN 201811516549A CN 109498474 A CN109498474 A CN 109498474A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/06—Emulsions
- A61K8/066—Multiple emulsions, e.g. water-in-oil-in-water
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/85—Polyesters
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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Abstract
The present invention proposes a kind of salubrious three-phase Emulsified sunscreen cosmetic and preparation method thereof, realizes excellent sun-screening function by three-phase emulsifying manner of W/O/W and provides salubrious skin sense, is effectively improved the universal sticky disadvantage of sunscreen product.The component of sunscreen cosmetic is: 5% to 15% grease, 0.5% to 1% surfactant, 10% to 20% polyalcohol, 10% to 20% sun-screening agent, 0.1% to 1% thickener, and surplus is water；Preparation method is: dispersing surfactant and sun-screening agent in grease and is heated to 80-85 DEG C, insulated and stirred is uniformly mixed to it, is stirred for being cooled to 40-42 DEG C, be kept the temperature spare；Polyalcohol, thickener are dispersed in water and are heated to 80-90 DEG C, insulated and stirred is uniformly mixed to it, is stirred for being cooled to 40-42 DEG C, be kept the temperature spare；It is slowly pumped into aqueous mixture by aqueous mixture high-speed stirred obtained, then by oil mixture obtained, homogeneous scrapes uneven Material, is stirred for homogeneous several minutes, discharges after being cooled to 30-35 DEG C.
Description
Technical field
The present invention relates to a kind of salubrious three-phase Emulsified sunscreen cosmetics and preparation method thereof.
Background technique
Excessive ultraviolet light has damage to skin in atmosphere, and skin quality is caused to be deteriorated, to take into account antiultraviolet damage and day
There are the cosmetics with sun-proof function in the prior art in normal makeups dual requirements, and this kind of cosmetics is by shielding or absorbs
Ultraviolet light is to play mitigation because solarization causes the effect of skin injury.Due to being added to sun-prevention component, existing sunscreen product
Generally existing sticky disadvantage, user experience are bad.
Summary of the invention
To overcome defect existing in the prior art, the present invention propose a kind of salubrious three-phase Emulsified sunscreen cosmetic and
Preparation method realizes excellent sun-screening function by three-phase emulsifying manner of W/O/W, and is capable of providing salubrious skin
Sense is effectively improved the universal sticky disadvantage of sunscreen product, and particular technique content is as follows:
A kind of salubrious three-phase Emulsified sunscreen cosmetic, component include: 5% to 15% grease, 0.5% to 1%
Surfactant, 10% to 20% polyalcohol, 10% to 20% sun-screening agent, 0.1% to 1% thickener, surplus is
Water.Specifically, the grease include carbonic acid dioctyl ester, the poly- trimethicone of diphenyl silicon phenyl, isohexadecane,
C12-15 alcohol benzoic ether, isononyl isononanoate, caprylic/capric triglyceride, Parleam one of work as, two kinds or
It is a variety of.The surfactant selects polyethers silicone oil emulsification agent of the HLB between 3 to 5, including the poly- diformazan of lauryl PEG-9
Base silica ethyl dimethyl silicone polymer, cetyl PEG/PPG-10/1 dimethyl silicone polymer, PEG-10 polydimethylsiloxanes
Alkane, PEG-9 dimethyl silicone polymer one of work as, two or more.The polyalcohol includes dipropylene glycol, glycerol, isoamyl
Glycol, propylene glycol, 1,3-PD, sorbierite one of work as, two or more.The sun-screening agent include physical sunscreen agent and
Chemical sun, the physical sunscreen agent include titanium dioxide, and the chemical sun includes diethylamino hydroxyl Benzoylbenzene first
The own ester of acid, Octocrilene, butylmethoxydibenzoylmethane, ethylhexyl methoxy cinnamate, double-ethylhexylphenol
Methylamino benzene piperazine one of works as, two or more.The thickener include Sodium Polyacrylate, carbomer, acrylic acid (ester) class/
C10-30 alkylol acrylamide acid esters cross-linked polymer one of works as, two or more.
A kind of preparation method of salubrious three-phase Emulsified sunscreen cosmetic, it includes:
Step 1, it in a reservoir disperses the surfactant of selected dosage and sun-screening agent in grease, and is heated to 80-
It 85 DEG C, is uniformly mixed to it within insulated and stirred 10 to 15 minutes, is stirred for being cooled to 40-42 DEG C, keep the temperature spare；
Step 2, the polyalcohol of selected dosage, thickener are dispersed in water by another extracting container, are heated to 80-90 DEG C, heat preservation
It is uniformly mixed to it within stirring 20 to 30 minutes, is stirred for being cooled to 40-42 DEG C, keep the temperature spare；
Step 3, to the aqueous mixture high-speed stirred prepared in step 2, then the oil mixture prepared in step 1 delayed
Slow filtering is pumped into aqueous mixture, subsequent homogeneous 5-10 minutes, is scraped uneven Material, is stirred for homogeneous 5-10 minutes, cold
But to discharging after 30-35 DEG C.
Compared with prior art, sun-proof result of the invention, salubrious sense and stability are significantly improved.
One) sun-proof result
This product effectively expands defensible ultra-violet bands range by the way that physics and chemical sun is applied in combination,
Make product that all there is excellent ultraviolet protection effect in the wide in range ultraviolet range of range, avoids skin tanning and sunburn.
Oil is mutually that continuous phase can mix more compared with common oil-in-water type emulsified type in Water-In-Oil phase in this product
Heavy wool soluble sunscreen obtains higher ultraviolet protection ability.Meanwhile when smearing after outer aqueous phase demulsification, in skin surface
The low oil film of water penetration is remained, even if contacting because washing, perspiring etc. with water, it is also difficult to generation emulsifies again, reach excellent sweat proof,
Water-fast effect, to realize excellent sun-screening function.
Two) salubrious sense
W/O/W three-phase emulsifies structure while the salubrious sense of touch for maintaining oil-in-water type emulsion type as feature,
Using the emulsifier and grease that skin sense is salubriouser, not sticky interior Water-In-Oil phase is formed, is overcome because mixing a large amount of oils generations
Sticky feeling.In addition, making product be applied to the ion on skin surface and skin using the thickener intolerant to ion in outer aqueous phase
When being in contact, faster, salubrious sense is become apparent from for demulsification.
Three) stability
Polyalcohol reduces the freezing point of inner aqueous phase since the polyhydroxy structure of itself is easy to happen aquation, enhancing
The stabilization of product at low temperature.
Specific embodiment
Application scheme is further described by embodiment as follows:
A kind of salubrious three-phase Emulsified sunscreen cosmetic comprising: 5% to 15% grease, 0.5% to 1% table
Face activating agent, 10% to 20% polyalcohol, 10% to 20% sun-screening agent, 0.1% to 1% thickener, surplus is water.
Guarantee the dissolution of sun-screening agent while in order to maintain salubrious skin sense again, the selection skin sense of above-mentioned grease it is more frivolous and
It is combined with the preferable grease of sun-screening agent compatibility, specially carbonic acid dioctyl ester, the poly- trimethyl silicane of diphenyl silicon phenyl
Oxygen alkane, isohexadecane, C12-15 alcohol benzoic ether, isononyl isononanoate, caprylic/capric triglyceride, Parleam are worked as
One of, two or more.
In order to guarantee that interior Water-In-Oil is mutually stable and not cause sticky feeling, the surfactant selects HLB 3 to 5
Between polyethers silicone oil emulsification agent, specially lauryl PEG-9 Polydimethylsiloxyethyl Dimethicone, cetyl
PEG/PPG-10/1 dimethyl silicone polymer, PEG-10 Polydimethylsiloxane, one in PEG-9 dimethyl silicone polymer
It plants, two or more.
In order to enhance the stability of this product at low temperature, the freezing point of inner aqueous phase is reduced, the polyalcohol includes double third
Glycol, glycerol, isoprene, propylene glycol, 1,3-PD, sorbierite one of work as, two or more.
In order to reach excellent sun-screening function, the sun-screening agent includes physical sunscreen agent and chemical sun, the physics
Sun-screening agent includes titanium dioxide, and the chemical sun includes the own ester of diethylamino oxybenzene formylbenzoate, Octocrilene, butyl
Methoxy dibenzoylmethane, ethylhexyl methoxy cinnamate, one in double-ethylhexylphenol methylamino benzene piperazine
It plants, two or more.
More salubrious when in order to smear this product, the thickener includes Sodium Polyacrylate, carbomer, acrylic acid (ester)
Class/C10-30 alkylol acrylamide acid esters cross-linked polymer one of works as the mixture of ingredient or Multiple components, such thickener is not
Resistance to ion is demulsified fast when being in contact with the ion on skin, can generate and clearly feel apparent skin sense.
The preparation method of above-mentioned salubrious three-phase Emulsified sunscreen cosmetic, it includes:
Step 1, it in a reservoir disperses the surfactant of selected dosage and sun-screening agent in grease, and is heated to 80-
It 85 DEG C, is uniformly mixed to it within insulated and stirred 10 to 15 minutes, is stirred for being cooled to 40-42 DEG C, keep the temperature spare；
Step 2, the polyalcohol of selected dosage, thickener are dispersed in water by another extracting container, are heated to 80-90 DEG C, heat preservation
It is uniformly mixed to it within stirring 20 to 30 minutes, is stirred for being cooled to 40-42 DEG C, keep the temperature spare；
Step 3, to the aqueous mixture high-speed stirred prepared in step 2, then the oil mixture prepared in step 1 delayed
Slow filtering is pumped into aqueous mixture, and subsequent homogeneous 5 minutes scrapes uneven Material, is stirred for homogeneous 8 minutes, is cooled to 30-
35 DEG C discharge after the assay was approved.
The benchmark test of product of the present invention
The sun-proof chemicals that each test example is prepared using conventional method, with regard to sun-proof result, salubrious sense and stability this tripartite
Face is compared research.It should be noted that in following tests example, containing grease, surfactant, polyalcohol, sun-screening agent,
Thickener and water, and show that W/O/W three-phase emulsifies structure, the reality as this product under 25 DEG C of micro- sem observations
The test example number for applying the sunscreen composition of example is the first to seven group of test example.
Firstly, being illustrated to the evaluation method used in each test example.
First, sun-proof result
Product of the present invention is evaluated to the protection effect of ultraviolet light, is applied on PMMA plate and spreads the anti-of a certain amount of each test example
Composition is shone, absorption spectrum is measured later, thus evaluates ultraviolet protection effect.Show each sunscreen composition in wavelength in table
The value of the absorbance of 310nm and 360nm.Value is bigger, and ultraviolet protection effect is more excellent.
Second, it is salubrious to feel
Actual service test by 10 specialized review persons to each test example.Evaluation method is the subjective feeling of syndic,
Specific standards are: 1) salubrious: 6 or more syndics are clearly felt that salubrious sense；2) appropriate: 3 or more, less than 6 syndics
It is obvious to feel salubrious sense；3) lack: less than 3 syndics obviously experience salubrious sense.
Third, stability
Observe whether tested test agent will appear demulsifying phenomenon under cryogenic, specific standards are: 1) it is excellent: sample-
It saves 3 months, is restored to after room temperature without demulsifying phenomenon at 18 DEG C；2) good: sample saves 1 month at -18 DEG C, is restored to room temperature
Afterwards without demulsifying phenomenon；3) poor: sample saves 1 month at -18 DEG C, has demulsifying phenomenon after being restored to room temperature
According to the sunscreen composition for the proportion composition preparation test example recorded in following table 1, with regard to above-mentioned evaluation the first to three
Point carries out evaluation test.
First, second, third and fourth group of result is compared it is found that the collocation of different greases, emulsifier, thickener will lead to salubrious sense
On difference；First, five group of result is compared it is found that adding suitable polyalcohol, the stabilization of product under cryogenic can be enhanced
Property；First, six, seven group of result is compared it is found that different sun-screening agents is arranged in pairs or groups, obtained sun-proof result is different, and will affect production
The salubrious sense of product.
The comparison of 1 embodiment performance evaluation of table
It is that above-mentioned preferred embodiment should be regarded as application scheme embodiment for example, all with application scheme thunder
Same, approximate or technology deduction, replacement, improvement for making based on this etc., are regarded as the protection scope of this patent.
Claims (10)
1. a kind of salubrious three-phase Emulsified sunscreen cosmetic, which is characterized in that component include: 5% to 15% grease,
0.5% to 1% surfactant, 10% to 20% polyalcohol, 10% to 20% sun-screening agent, 0.1% to 1% thickening
Agent, surplus are water.
2. salubrious three-phase Emulsified sunscreen cosmetic according to claim 1, it is characterised in that: the grease includes carbon
Dioctyl phthalate, the poly- trimethicone of diphenyl silicon phenyl, isohexadecane, C12-15 alcohol benzoic ether, isononanoic acid
Different nonyl ester, caprylic/capric triglyceride, Parleam one of work as, two or more.
3. salubrious three-phase Emulsified sunscreen cosmetic according to claim 1, it is characterised in that: the surfactant
Select polyethers silicone oil emulsification agent of the HLB between 3 to 5.
4. salubrious three-phase Emulsified sunscreen cosmetic according to claim 3, it is characterised in that: the surfactant
Including lauryl PEG-9 Polydimethylsiloxyethyl Dimethicone, cetyl PEG/PPG-10/1 polydimethylsiloxanes
Alkane, PEG-10 Polydimethylsiloxane, PEG-9 dimethyl silicone polymer one of work as, two or more.
5. salubrious three-phase Emulsified sunscreen cosmetic according to claim 1, it is characterised in that: the polyalcohol includes
Dipropylene glycol, glycerol, isoprene, propylene glycol, 1,3- propylene glycol, sorbierite one of work as, two or more.
6. salubrious three-phase Emulsified sunscreen cosmetic according to claim 1, it is characterised in that: the sun-screening agent includes
Physical sunscreen agent and chemical sun, the physical sunscreen agent include titanium dioxide, and the chemical sun includes diethylamino hydroxyl
Benzoyl hexyl-benzoate, Octocrilene, butylmethoxydibenzoylmethane, ethylhexyl methoxy cinnamate, it is double-
Ethylhexylphenol methylamino benzene piperazine one of works as, two or more.
7. salubrious three-phase Emulsified sunscreen cosmetic according to claim 1-6, it is characterised in that: the increasing
Thick dose includes one in Sodium Polyacrylate, carbomer, acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross-linked polymer
It plants, two or more.
8. a kind of preparation method of salubrious three-phase Emulsified sunscreen cosmetic, characterized by comprising:
Step 1, it in a reservoir disperses the surfactant of selected dosage and sun-screening agent in grease, and is heated to 80-85 DEG C,
Insulated and stirred is uniformly mixed to it, is stirred for being cooled to 40-42 DEG C, be kept the temperature spare；
Step 2, the polyalcohol of selected dosage, thickener are dispersed in water by another extracting container, are heated to 80-90 DEG C, insulated and stirred
It is uniformly mixed to it, is stirred for being cooled to 40-42 DEG C, keep the temperature spare；
Step 3, to the aqueous mixture high-speed stirred prepared in step 2, then by the slow mistake of the oil mixture prepared in step 1
Filter is pumped into aqueous mixture, subsequent homogeneous several minutes, is scraped uneven Material, is stirred for homogeneous several minutes, is cooled to
It discharges after 30-35 DEG C.
9. the preparation method of salubrious three-phase Emulsified sunscreen cosmetic according to claim 8, it is characterised in that: described
The insulated and stirred time in step 1 is 10 to 15 minutes, and the insulated and stirred time in step 2 is 20 to 30 minutes.
10. the preparation method of salubrious three-phase Emulsified sunscreen cosmetic according to claim 8, it is characterised in that: institute
State in step 3 homogeneous operation when it is 5-10 minutes a length of.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811516549.0A CN109498474A (en) | 2018-12-12 | 2018-12-12 | A kind of salubrious three-phase Emulsified sunscreen cosmetic and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811516549.0A CN109498474A (en) | 2018-12-12 | 2018-12-12 | A kind of salubrious three-phase Emulsified sunscreen cosmetic and preparation method thereof |
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| CN201811516549.0A Pending CN109498474A (en) | 2018-12-12 | 2018-12-12 | A kind of salubrious three-phase Emulsified sunscreen cosmetic and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109908004A (en) * | 2019-04-23 | 2019-06-21 | 广东芭薇生物科技股份有限公司 | A kind of multiple emulsion sunscreen cosmetic and preparation method thereof |
| CN113876597A (en) * | 2021-11-02 | 2022-01-04 | 广州科妙生物科技有限公司 | Skin-moistening and moisturizing cream and preparation method thereof |
| CN114010544A (en) * | 2021-11-22 | 2022-02-08 | 南希生物科技(绍兴)有限公司 | Smearing type facial mask and preparation method thereof |
| CN114762660A (en) * | 2021-01-12 | 2022-07-19 | 新生活化妆品科技(上海)有限公司 | Cosmetic composition and cosmetic |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106821793A (en) * | 2016-12-28 | 2017-06-13 | 广州环亚化妆品科技有限公司 | A kind of gentle efficient multiple corpus mamillare suncream and preparation method thereof |
| CN107157782A (en) * | 2017-06-20 | 2017-09-15 | 广东盛美化妆品有限公司 | A kind of W/O/W CC frosts and preparation method thereof |
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2018
- 2018-12-12 CN CN201811516549.0A patent/CN109498474A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106821793A (en) * | 2016-12-28 | 2017-06-13 | 广州环亚化妆品科技有限公司 | A kind of gentle efficient multiple corpus mamillare suncream and preparation method thereof |
| CN107157782A (en) * | 2017-06-20 | 2017-09-15 | 广东盛美化妆品有限公司 | A kind of W/O/W CC frosts and preparation method thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109908004A (en) * | 2019-04-23 | 2019-06-21 | 广东芭薇生物科技股份有限公司 | A kind of multiple emulsion sunscreen cosmetic and preparation method thereof |
| CN109908004B (en) * | 2019-04-23 | 2021-11-16 | 广东芭薇生物科技股份有限公司 | Multiple emulsion sunscreen cosmetic and preparation method thereof |
| CN114762660A (en) * | 2021-01-12 | 2022-07-19 | 新生活化妆品科技(上海)有限公司 | Cosmetic composition and cosmetic |
| CN113876597A (en) * | 2021-11-02 | 2022-01-04 | 广州科妙生物科技有限公司 | Skin-moistening and moisturizing cream and preparation method thereof |
| CN113876597B (en) * | 2021-11-02 | 2024-01-26 | 广州科妙生物科技有限公司 | Moisturizing cream and preparation method thereof |
| CN114010544A (en) * | 2021-11-22 | 2022-02-08 | 南希生物科技(绍兴)有限公司 | Smearing type facial mask and preparation method thereof |
| CN114010544B (en) * | 2021-11-22 | 2024-02-09 | 浙江优肯包装有限公司 | Smearing type mask and preparation method thereof |
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