CN109487369A - A kind of Khotan jade fiber and preparation method thereof - Google Patents
A kind of Khotan jade fiber and preparation method thereof Download PDFInfo
- Publication number
- CN109487369A CN109487369A CN201811555839.6A CN201811555839A CN109487369A CN 109487369 A CN109487369 A CN 109487369A CN 201811555839 A CN201811555839 A CN 201811555839A CN 109487369 A CN109487369 A CN 109487369A
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- Prior art keywords
- khotan jade
- preparation
- slurry
- khotan
- parts
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/14—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F8/00—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
- D01F8/04—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
- D01F8/08—Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyacrylonitrile as constituent
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a kind of preparation methods of Khotan jade fiber, this method is added fibre stuff using Khotan jade and the fiber with Khotan jade ingredient is made, since Khotan jade contains the microelement beneficial to human body, the fibre made of Khotan jade, its microelement can be absorbed by the body, activating cell tissue improves the functions such as immune of human body.Reliable product quality, it is Nantural non-toxic, without side-effects.Khotan jade particle is evenly distributed on inside corpus fibrosum and appearance, and fiber surface is bright, in Khotan jade ingredient have good health effect.
Description
Technical field
The present invention relates to fiber technology of preparing, a kind of Khotan jade fiber and preparation method thereof is particularly related to.
Background technique
With the continuous development of science and technology, the textile fiber for meeting people's difference needs emerges one after another, and is disappeared with meeting
The demand of the person of expense plays increasingly important role in people's daily life.With the continuous development of industry, the city of fiber
Field is also constantly expanding, but all effect is more single mostly for fiber, and manufactured fabric only has the function of blocking, and can not
So that people are when wearing with a preferable comfort level and excellent service performance.
Polyester fiber have many advantages, such as intensity is high, wearability is good, surface is smooth, can thermal finalization, physical and chemical performance stablize, it is wide
It is general to be applied to dress ornament field.But duration essential oil ongoing health care's function of polyester fiber is not developed, patent
Product disclosed in CN102134769A is the chemical fibre strip ontology a kind of containing multiple micropores, adheres to essential oil particle.It is this
Method attachment fastness is poor, and durability is poor, intolerant to washing.In order to improve health functions, Chinese medicine is largely added in Many researchers
Ingredient makes polyester fiber have a kind of flavour of a drug to volatilize, welding sense with fresh air, also gives people a kind of heavy feeling.
Khotan jade is not only the symbol of beauty, also has medical value.Khotan jade is the consummate of yin-yang gas, is had to human health
Magical effect, it is all on the books in the ancient medicines masterpiece such as Shennong's Herbal, Compendium of Material Medica.Khotan jade have except it is middle heat,
Moistening herat and lung grows hair, supports the five internal organs, peace soul, dredges the curative effects such as blood vessels, bright knowledge, there is the method for 106 kinds of Orally taken and externallies.Contain 10
Various trace elements, gold, silver, silicon, iron, selenium, magnesium, manganese etc., there is the benefits of lengthening one's life of eliminating disease and prolong life.Such as Zn-ef ficiency can activate pancreas islet
Element, adjust energetic supersession, safeguard immune function of human body, promote children's intelligence development, have the effects that anticancer, prevent it is abnormal, anti-aging.
Manganese element can damage free radical resisting caused by human body, participate in the synthesis of protein, vitamin, promote blood circulation, add
Fast metabolism, prevents senile dementia, osteoporosis, vascular sclerosis etc..Selenium element can be catalyzed nitrous oxide restore it is harmless
Alkyl compound, thus protect biomembrane from its evil, increase immune function of human body, improve body resistance against diseases reach anticancer,
The effect of anti-cancer.Khotan jade is a kind of substance that storage gas is most abundant, and by wearing jadeware ornaments, beneficial element can pass through skin
Skin, acupuncture point, into human body, so that Yin Yang balancing qi and blood, promotes the health of people.
Therefore, the fiber that there is an urgent need to a kind of by the way that Khotan jade ingredient is added solves problems.
Summary of the invention
Aiming at the shortcomings in the prior art, the technical problem to be solved in the present invention is that provide a kind of Khotan jade fiber and
Preparation method.
In order to solve the above technical problems, the present invention is realized by following scheme: a kind of preparation method of Khotan jade fiber,
Method includes the following steps:
A, the processing of raw material:
A1, Khotan jade block is taken；
A2, Khotan jade block is broken into particle by crushing device, broken Khotan jade particle passes through clear water formula cleaning device
Decontamination, the Khotan jade particle after decontamination are sent into grinding device and are ground, what the Khotan jade formation after grinding was mixed with water
Slurry；
Khotan jade slurry is put into reaction kettle, is stirred evenly, sulfuric acid or hydrochloric acid or nitric acid are added during stirring,
Sulfuric acid or hydrochloric acid or nitric acid react to form harmless ionic compound with the harmful substance in Khotan jade；
The obtained slurry of harmful substance will be removed, sodium hydroxid neutralisation treatment is added；
Slurry after neutralisation treatment carries out settlement treatment in subsider, the solution discharge on upper layer, remaining sediment after sedimentation
It moves to drying device to be dried, the substance after drying forms Khotan jade powder；
Khotan jade powder was subjected to magnetic treatment by conveyer belt；
B, take a2 treated Khotan jade powder and polyester fiber slurry, polyacrylonitrile pulp to be placed in by the ratio of 1:3:3
High-speed stirred dispersing apparatus is stirred after ethyl alcohol is added, while being dispersed with stirring equipment and being heated to 70 ~ 90 degree, is added sub-
Phosphate ester and binder stir 1 ~ 4 hour, at slurry form, stop stirring；
C, by step b, treated that slurry carries out drying and processing at a temperature of 70~120 DEG C, until ethyl alcohol all volatilizees, at this time
Mixture after solidification is wet shape solidfied material, and moisture accounting is 5%-10%；
D, the wet shape solidfied material in step c is subjected to solution beam processing 10min~60min with supersonic speed depth solution beam device, made
Corpus fibrosum produced is uniform-distribution with Khotan jade particle；
E, the formalin that corpus fibrosum immerses 35% carries out disinfection sterilization treatment；
F, step e treated corpus fibrosum heating, drying is handled, keeps formaldehyde volatilization clean；
G, Khotan jade fiber required for finally obtaining.
Further, the diameier of the Khotan jade powder is between 0.01 nanometer~100 nanometers.
Further, in step a2: the pH value of the neutralisation treatment is between 6.5-7.5.
Further, the quality of ethyl alcohol is the 5%- of Khotan jade powder and polyester fiber slurry, polyacrylonitrile pulp gross mass
10%。
Further, the binder is phenol-formaldehyde binders, one kind of epoxy adhesive or polyurethane adhesive.
Further, the invention also includes the preparation of polyester fiber slurry, preparation method is as follows:
1) mass fraction for, taking PET polyester is 70-90 parts, and the mass fraction of phthalic acid is 10-30 parts, the quality of ethylene glycol
Number is 10-30 parts, water quality number is 30-50 parts；
2), phthalic acid, ethylene glycol, PET polyester and water are mixed evenly, obtain polyester fiber slurry.
Further, the invention also includes the preparation of polyacrylonitrile pulp, preparation method is as follows:
1) 60-90 parts of polyacrylonitrile of high molecular polymer, are taken by mass parts, the spinning of acrylonitrile itaconic acid bipolymer is former
18-30 parts of liquid, 20-50 parts of dimethyl sulfoxide, 30-50 parts of water；
2), polyacrylonitrile, acrylonitrile itaconic acid bipolymer spinning solution, dimethyl sulfoxide and water are mixed evenly, and obtain
To polyacrylonitrile pulp.
Further, the viscosity of the acrylonitrile itaconic acid bipolymer spinning solution is 80Pas~96Pas.
Compared with the existing technology, the beneficial effects of the present invention are: fibre stuff, which is added, using Khotan jade in the present invention is made band
There is the fiber of Khotan jade ingredient, since Khotan jade contains the microelement beneficial to human body, the fibre made of Khotan jade,
Its microelement can be absorbed by the body, activating cell tissue, improve the functions such as immune of human body.Reliable product quality, natural nothing
It is malicious, without side-effects.Khotan jade particle is evenly distributed on inside corpus fibrosum and appearance, and fiber surface is bright, in Khotan jade at
Dividing has good health effect.
Detailed description of the invention
Fig. 1 is the functional block diagram of Khotan jade preparation method of the present invention.
Specific embodiment
Following will be combined with the drawings in the embodiments of the present invention, and technical solution in the embodiment of the present invention carries out clear, complete
Site preparation description, enables advantages and features of the invention to be easier to be readily appreciated by one skilled in the art, thus to protection of the invention
Range is more clearly defined.Obviously, embodiment described in the invention is only a part of the embodiment of the present invention,
Instead of all the embodiments.Based on the embodiments of the present invention, those of ordinary skill in the art are not making creative labor
Every other embodiment obtained under the premise of dynamic, shall fall within the protection scope of the present invention.
Please refer to attached drawing 1, a kind of preparation method of Khotan jade fiber of the invention, method includes the following steps:
A, the processing of raw material:
A1, Khotan jade block is taken；
A2, Khotan jade block is broken into particle by crushing device, broken Khotan jade particle passes through clear water formula cleaning device
Decontamination, the Khotan jade particle after decontamination are sent into grinding device and are ground, what the Khotan jade formation after grinding was mixed with water
Slurry；
Khotan jade slurry is put into reaction kettle, is stirred evenly, sulfuric acid or hydrochloric acid or nitric acid are added during stirring,
Sulfuric acid or hydrochloric acid or nitric acid react to form harmless ionic compound with the harmful substance in Khotan jade；
The obtained slurry of harmful substance will be removed, sodium hydroxid neutralisation treatment is added；
Slurry after neutralisation treatment carries out settlement treatment in subsider, the solution discharge on upper layer, remaining sediment after sedimentation
It moves to drying device to be dried, the substance after drying forms Khotan jade powder；
Khotan jade powder was subjected to magnetic treatment by conveyer belt；
B, take a2 treated Khotan jade powder and polyester fiber slurry, polyacrylonitrile pulp to be placed in by the ratio of 1:3:3
High-speed stirred dispersing apparatus is stirred after ethyl alcohol is added, while being dispersed with stirring equipment and being heated to 70 ~ 90 degree, is added sub-
Phosphate ester and binder stir 1 ~ 4 hour, at slurry form, stop stirring；
C, by step b, treated that slurry carries out drying and processing at a temperature of 70~120 DEG C, until ethyl alcohol all volatilizees, at this time
Mixture after solidification is wet shape solidfied material, and moisture accounting is 5%-10%；
D, the wet shape solidfied material in step c is subjected to solution beam processing 10min~60min with supersonic speed depth solution beam device, made
Corpus fibrosum produced is uniform-distribution with Khotan jade particle；
E, the formalin that corpus fibrosum immerses 35% carries out disinfection sterilization treatment；
F, step e treated corpus fibrosum heating, drying is handled, keeps formaldehyde volatilization clean；
G, Khotan jade fiber required for finally obtaining.
A kind of optimal technical scheme of the present embodiment: the diameier of the Khotan jade powder is received 0.01 nanometer~100
Between rice.
A kind of optimal technical scheme of the present embodiment: in step a2: the pH value of the neutralisation treatment 6.5-7.5 it
Between.
A kind of optimal technical scheme of the present embodiment: the quality of ethyl alcohol is Khotan jade powder and polyester fiber slurry, poly- third
The 5%-10% of alkene nitrile slurry gross mass.
A kind of optimal technical scheme of the present embodiment: the binder is phenol-formaldehyde binders, epoxy adhesive or poly-
One kind of urethane binder.
A kind of optimal technical scheme of the present embodiment: the preparation including polyester fiber slurry, preparation method are as follows:
1) mass fraction for, taking PET polyester is 70-90 parts, and the mass fraction of phthalic acid is 10-30 parts, the quality of ethylene glycol
Number is 10-30 parts, water quality number is 30-50 parts；
2), phthalic acid, ethylene glycol, PET polyester and water are mixed evenly, obtain polyester fiber slurry.
7. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that: including polyacrylonitrile
The preparation of slurry, preparation method are as follows:
1) 60-90 parts of polyacrylonitrile of high molecular polymer, are taken by mass parts, the spinning of acrylonitrile itaconic acid bipolymer is former
18-30 parts of liquid, 20-50 parts of dimethyl sulfoxide, 30-50 parts of water；
2), polyacrylonitrile, acrylonitrile itaconic acid bipolymer spinning solution, dimethyl sulfoxide and water are mixed evenly, and obtain
To polyacrylonitrile pulp.
A kind of optimal technical scheme of the present embodiment: the viscosity of the acrylonitrile itaconic acid bipolymer spinning solution
For 80Pas~96Pas.
The present invention is added fibre stuff using Khotan jade and the fiber with Khotan jade ingredient is made, since Khotan jade contains pair
The beneficial microelement of human body, the fibre made of Khotan jade, microelement can be absorbed by the body, activating cell group
It knits, improves the functions such as immune of human body.Reliable product quality, it is Nantural non-toxic, without side-effects.Khotan jade particle is evenly distributed on
Inside corpus fibrosum and appearance, fiber surface is bright, in Khotan jade ingredient have good health effect.Khotan jade contains more than 10
Kind microelement, gold, silver, silicon, iron, selenium, magnesium, manganese etc. have the benefits of lengthening one's life of eliminating disease and prolong life.Such as Zn-ef ficiency can activate pancreas islet
Element, adjust energetic supersession, safeguard immune function of human body, promote children's intelligence development, have the effects that anticancer, prevent it is abnormal, anti-aging.
Manganese element can damage free radical resisting caused by human body, participate in the synthesis of protein, vitamin, promote blood circulation, add
Fast metabolism, prevents senile dementia, osteoporosis, vascular sclerosis etc..Selenium element can be catalyzed nitrous oxide restore it is harmless
Alkyl compound, thus protect biomembrane from its evil, increase immune function of human body, improve body resistance against diseases reach anticancer,
The effect of anti-cancer.
The foregoing is merely the preferred embodiment of the present invention, are not intended to limit the scope of the invention, all benefits
The equivalent structure or equivalent flow shift made by description of the invention and accompanying drawing content is applied directly or indirectly in other phases
The technical field of pass, is included within the scope of the present invention.
Claims (8)
1. a kind of preparation method of Khotan jade fiber, which is characterized in that method includes the following steps:
A, the processing of raw material:
A1, Khotan jade block is taken；
A2, Khotan jade block is broken into particle by crushing device, broken Khotan jade particle passes through clear water formula cleaning device
Decontamination, the Khotan jade particle after decontamination are sent into grinding device and are ground, what the Khotan jade formation after grinding was mixed with water
Slurry；
Khotan jade slurry is put into reaction kettle, is stirred evenly, sulfuric acid or hydrochloric acid or nitric acid are added during stirring,
Sulfuric acid or hydrochloric acid or nitric acid react to form harmless ionic compound with the harmful substance in Khotan jade；
The obtained slurry of harmful substance will be removed, sodium hydroxid neutralisation treatment is added；
Slurry after neutralisation treatment carries out settlement treatment in subsider, the solution discharge on upper layer, remaining sediment after sedimentation
It moves to drying device to be dried, the substance after drying forms Khotan jade powder；
Khotan jade powder was subjected to magnetic treatment by conveyer belt；
B, take a2 treated Khotan jade powder and polyester fiber slurry, polyacrylonitrile pulp to be placed in by the ratio of 1:3:3
High-speed stirred dispersing apparatus is stirred after ethyl alcohol is added, while being dispersed with stirring equipment and being heated to 70 ~ 90 degree, is added sub-
Phosphate ester and binder stir 1 ~ 4 hour, at slurry form, stop stirring；
C, by step b, treated that slurry carries out drying and processing at a temperature of 70~120 DEG C, until ethyl alcohol all volatilizees, at this time
Mixture after solidification is wet shape solidfied material, and moisture accounting is 5%-10%；
D, the wet shape solidfied material in step c is subjected to solution beam processing 10min~60min with supersonic speed depth solution beam device, made
Corpus fibrosum produced is uniform-distribution with Khotan jade particle；
E, the formalin that corpus fibrosum immerses 35% carries out disinfection sterilization treatment；
F, step e treated corpus fibrosum heating, drying is handled, keeps formaldehyde volatilization clean；
G, Khotan jade fiber required for finally obtaining.
2. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that: the Khotan jade powder
Diameier is between 0.01 nanometer~100 nanometers.
3. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that step a2: at the neutralization
The pH value of reason is between 6.5-7.5.
4. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that: the quality of ethyl alcohol is and field
The 5%-10% of beautiful powder and polyester fiber slurry, polyacrylonitrile pulp gross mass.
5. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that: the binder is phenolic aldehyde
One kind of binder, epoxy adhesive or polyurethane adhesive.
6. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that: including polyester fiber slurry
Preparation, preparation method is as follows:
1) mass fraction for, taking PET polyester is 70-90 parts, and the mass fraction of phthalic acid is 10-30 parts, the quality of ethylene glycol
Number is 10-30 parts, water quality number is 30-50 parts；
2), phthalic acid, ethylene glycol, PET polyester and water are mixed evenly, obtain polyester fiber slurry.
7. a kind of preparation method of Khotan jade fiber according to claim 1, it is characterised in that: including polyacrylonitrile pulp
Preparation, preparation method is as follows:
1) 60-90 parts of polyacrylonitrile of high molecular polymer, are taken by mass parts, the spinning of acrylonitrile itaconic acid bipolymer is former
18-30 parts of liquid, 20-50 parts of dimethyl sulfoxide, 30-50 parts of water；
2), polyacrylonitrile, acrylonitrile itaconic acid bipolymer spinning solution, dimethyl sulfoxide and water are mixed evenly, and obtain
To polyacrylonitrile pulp.
8. a kind of preparation method of Khotan jade fiber according to claim 7, it is characterised in that: the acrylonitrile-clothing health
The viscosity of sour bipolymer spinning solution is 80Pas~96Pas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811555839.6A CN109487369A (en) | 2018-12-19 | 2018-12-19 | A kind of Khotan jade fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811555839.6A CN109487369A (en) | 2018-12-19 | 2018-12-19 | A kind of Khotan jade fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109487369A true CN109487369A (en) | 2019-03-19 |
Family
ID=65710928
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811555839.6A Pending CN109487369A (en) | 2018-12-19 | 2018-12-19 | A kind of Khotan jade fiber and preparation method thereof |
Country Status (1)
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Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6342970A (en) * | 1986-08-06 | 1988-02-24 | 健繊株式会社 | Production of fiber product |
| CN1146220A (en) * | 1994-04-19 | 1997-03-26 | 纳幕尔杜邦公司 | Improvements relating to making fiberballs |
| CN1345390A (en) * | 2000-01-26 | 2002-04-17 | 东丽株式会社 | Fiber structure having deodorizing or antibacterial property |
| CN101691275A (en) * | 2009-08-31 | 2010-04-07 | 河北工业大学 | Method for preparing nano mineral fiber |
| CN102912468A (en) * | 2012-08-20 | 2013-02-06 | 肖晖 | Hetian jade fibers and preparation method thereof |
| CN107130427A (en) * | 2017-05-18 | 2017-09-05 | 浙江宏都寝具有限公司 | A kind of negative-ion fiber and its manufacturing process |
| CN107604641A (en) * | 2017-09-01 | 2018-01-19 | 江苏鑫轮特种纤维科技发展有限公司 | A kind of preparation of anion Composite Double functional fibre and its application method |
-
2018
- 2018-12-19 CN CN201811555839.6A patent/CN109487369A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS6342970A (en) * | 1986-08-06 | 1988-02-24 | 健繊株式会社 | Production of fiber product |
| CN1146220A (en) * | 1994-04-19 | 1997-03-26 | 纳幕尔杜邦公司 | Improvements relating to making fiberballs |
| CN1345390A (en) * | 2000-01-26 | 2002-04-17 | 东丽株式会社 | Fiber structure having deodorizing or antibacterial property |
| CN101691275A (en) * | 2009-08-31 | 2010-04-07 | 河北工业大学 | Method for preparing nano mineral fiber |
| CN102912468A (en) * | 2012-08-20 | 2013-02-06 | 肖晖 | Hetian jade fibers and preparation method thereof |
| CN107130427A (en) * | 2017-05-18 | 2017-09-05 | 浙江宏都寝具有限公司 | A kind of negative-ion fiber and its manufacturing process |
| CN107604641A (en) * | 2017-09-01 | 2018-01-19 | 江苏鑫轮特种纤维科技发展有限公司 | A kind of preparation of anion Composite Double functional fibre and its application method |
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Application publication date: 20190319 |