CN102912468A - Hetian jade fibers and preparation method thereof - Google Patents
Hetian jade fibers and preparation method thereof Download PDFInfo
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- CN102912468A CN102912468A CN2012102960641A CN201210296064A CN102912468A CN 102912468 A CN102912468 A CN 102912468A CN 2012102960641 A CN2012102960641 A CN 2012102960641A CN 201210296064 A CN201210296064 A CN 201210296064A CN 102912468 A CN102912468 A CN 102912468A
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- khotan jade
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Abstract
The invention discloses fibers prepared by Hetian jade as components and a preparation method of the fibers. The fibers are processed by polishing and refining the Hetian jade into Hetian jade fine powder, and mixing with silicate, mineral wool, inorganic acid, a bonding agent and water. The components are prepared in percentage by weight: 3% to 5% of Hetian jade, 5% to 15% of silicate, 30% to 60% of mineral wool, 1% to 10% of inorganic acid, and 5% to 10% bonding agent. The fibers prepared by the Hetian jade as the components containing trace elements, such as zinc, iron, copper, manganese, magnesium, cobalt, selenium, chromium, titanium, lithium, calcium, potassium and sodium. The trace elements of a diet prepared by the Hetian jade or/and a fiber product having direct contact with the skin can be absorbed by human bodies, thereby activating cell tissues and improving functions, such as human immune. A natural product is reliable in quality, and free from toxic and side effects. Particles of the Hetian jade are uniformly distributed in fiber bodies and outer surfaces, so that the fibers are like strings of unusual bright and smooth pearl necklaces.
Description
Technical field
The present invention relates to a kind of fibre, relating in particular to a kind of is fiber of producing of composition and preparation method thereof with Khotan jade.
Background technology
Fiber generally refers to thin and long material.Fiber has that elastic modelling quantity is large, and plastic deformation is little, and the intensity high has very high crystallizing power, and molecular weight is little, is generally several ten thousand.Fiber applications is extensive, can be made into fine rule, the end of a thread and the rope made of hemp, papermaking or can also be made into fibrage when knitting felt; Simultaneously also be commonly used to make unclassified stores, and jointly form composite with unclassified stores.
Fiber comprises natural fabric, chemical fibre, wherein natural fabric comprises string, animal fiber, mineral fibres, string, animal fiber can extract by the fiber extraction equipment, mineral fibres by binding agent under 180 ℃～250 ℃ temperature, be cured moulding, utilize the disposable production moulding of automatic production line.Chemical fibre comprises artificial fibre or regenerated fiber, synthetic fiber, inorfil, and artificial fibre is with the material that contains natural fabric or azelon, and other lose the fibrous raw material that textile process is worth, through the textile fabric of making after the chemical process.Regenerated fiber is the fiber of making behind the slurries height sublimate that natural high polymer is made, such as regenerated celulose fibre, azlon, regeneration starch fiber and regeneration synthetic fiber.The chemical composition of synthetic fiber is fully different with natural fabric, material such as oil, coal, natural gas, lime stone or the agricultural byproducts that itself do not contain cellulose or protein from some, fiber is made with the method for chemical synthesis and machining again by synthetic unit first.Inorfil is take natural inorganic thing or phasphorus-containing polymer fiber as raw material, through manually reeling off raw silk from cocoons or direct carbonization is made.Comprise glass fibre, metal fibre and carbon fiber.Through retrieval, all find to utilize product of the fibre that Khotan jade makes for composition and preparation method thereof at home and abroad.
Summary of the invention
The technical problem to be solved in the present invention has been to provide a kind of fiber that contains Khotan jade composition manufacturing production and preparation method thereof.
For solving the problems of the technologies described above, the present invention realizes by following scheme: a kind of Khotan jade fiber, be finish-ground to the Khotan jade fine powder by the Khotan jade polishing, and form with silicate, mineral wool, inorganic acid, binding agent, water formulated, its percentage by weight is:
Khotan jade 3%～5%, silicate 5%～15%, mineral wool 30%～60%, inorganic acid 1%～10%, binding agent 5%～10%.
Described Khotan jade fine powder comprises nano-powder, superfine powder, powder, and the nano-powder diameter is between 0.01 nanometer～100 nanometers, and the superfine powder diameter is between 100 nanometers～45 micron, and powder is between 45 microns～1 millimeter.
Described Khotan jade fine powder contains the trace elements such as zinc, iron, copper, manganese, magnesium, cobalt, selenium, chromium, titanium, lithium, calcium, potassium, sodium, meals made from Khotan jade or the fibre that directly contacts is arranged with skin, its trace element can be absorbed by the body, the activating cell tissue, the functions such as immunity of raising human body.
A kind of preparation method of Khotan jade fiber may further comprise the steps:
A, selected Khotan jade, Khotan jade is cleaned up, polish with refiner through fragmentation, and grinding becomes the Khotan jade fine powder, this Khotan jade fine powder comprises nano-powder, superfine powder, powder, the nano-powder diameter is between 0.01 nanometer～100 nanometers, and the superfine powder diameter is between 100 nanometers～45 micron, and powder is between 45 microns～1 millimeter;
B, pour the Khotan jade fine powder into the washing and filtering device, add entry and stir, filter simultaneously cleaning, and do dry the processing, the gained fine powder is the first component;
C, silicate, mineral wool, inorganic acid, binding agent are added water in mixer, fully mix 1～2 hour;
D, with the solution left standstill of c gained, treat that solution can see the sedimentation mixture to lower floor clearly, the upper strata clear solution is discharged, remaining sedimentation mixture carries out drying again, the gained mixture is second component;
E, second component is taken out, insert the high-speed stirred dispersing apparatus, and add ethanol, start the high-speed stirred dispersing apparatus, heat simultaneously to 70～90 ℃, keep constant temperature, add phosphoric acid fat, stirred 1～4 hour, the form slurry state stops to stir, and the gained slurry is the 3rd component;
F, the 3rd component is carried out vacuumize under 70～120 ℃ of temperature, all volatilize to ethanol, obtained component is the 4th component;
G, the first component is added in the 4th component, use supersonic speed degree of depth solution beam device to separate bundle and process 10min～60min, make in the corpus fibrosum of producing and be uniform-distribution with the Khotan jade particulate with appearance, fiber is just as a string pearl necklace one by one, unusual bright smooth, by demand, can distinguish preparing nano level Khotan jade fiber, ultra-fine Khotan jade fiber, common Khotan jade fiber.
Described silicate is one or more of asbestos, mica, talcum, kaolinite, montmorillonite, zeolite, elects montomorillonite as.
Described inorganic acid is commercial acid, is specially a kind of in hydrochloric acid, nitric acid or the sulfuric acid, is preferably sulfuric acid.
Described binding agent is a kind of of phenol-formaldehyde binders, epoxy adhesive or polyurethane adhesive, is preferably phenol-formaldehyde binders.
Described water, ethanol, phosphoric acid fat are supplies.
Advantage of the present invention is: adopting Khotan jade is the fiber that composition is made, contain the trace elements such as zinc, iron, copper, manganese, magnesium, cobalt, selenium, chromium, titanium, lithium, calcium, potassium, sodium, meals made from Khotan jade or the fibre that directly contacts is arranged with skin, its trace element can be absorbed by the body, the activating cell tissue, the functions such as immunity of raising human body.Reliable product quality, has no side effect at Nantural non-toxic.The Khotan jade particulate is evenly distributed in the corpus fibrosum and appearance, and fiber is just as a string pearl necklace one by one, and is unusual bright smooth.
The specific embodiment
A kind of Khotan jade fiber, be finish-ground to the Khotan jade fine powder by the Khotan jade polishing, form with silicate, mineral wool, inorganic acid, binding agent, water formulated, its percentage by weight is Khotan jade 3%～5%, silicate 5%～15%, mineral wool 30%～60%, inorganic acid 1%～10%, binding agent 5%～10%.
Embodiment 1, and manufacture of the present invention divides following steps:
A, selected Khotan jade 500g, Khotan jade is cleaned up, polish with refiner through fragmentation, and grinding becomes the Khotan jade fine powder, this Khotan jade fine powder comprises nano-powder, superfine powder, powder, the nano-powder diameter is between 0.01 nanometer～100 nanometers, and the superfine powder diameter is between 100 nanometers～45 micron, and powder is between 45 microns～1 millimeter;
B, pour the Khotan jade fine powder into the washing and filtering device, add entry and stir, filter simultaneously cleaning, and do dry the processing, the gained fine powder is the first component, and weight is 492g;
C, with montmorillonite 2 000g, mineral wool 5000g, commercial sulphuric acid 1000g, phenol-formaldehyde binders 1500g, add 10 kilograms of entry and in mixer, fully mix 1～2 hour;
D, with the solution left standstill of c gained, treat that solution can see the sedimentation mixture to lower floor clearly, the upper strata clear solution is discharged, remaining sedimentation mixture carries out drying again, the gained mixture is second component, its weight is 9868g;
E, second component mixture 9868g is taken out, insert the high-speed stirred dispersing apparatus, and add 2 kilograms of ethanol, start the high-speed stirred dispersing apparatus, heat simultaneously to 70～90 ℃, keep constant temperature, add 1 kilogram in auxiliary material phosphoric acid fat, stirred 1～4 hour, the form slurry state, stop to stir, the gained slurry is the 3rd component, and its weight is 10763g;
F, the 3rd component 10763g is carried out vacuumize under 70～120 ℃ of temperature, all volatilize to ethanol, obtained component is the 4th component, and its weight is 9824g;
G, the first component 492g is added in the 4th component 9824g, use supersonic speed degree of depth solution beam device to separate bundle and process 10min～60min, make in the corpus fibrosum produced and appearance is uniform-distribution with Khotan jade fine particulates in the first component, fiber is just as a string pearl necklace one by one, unusual bright smooth, by demand, can distinguish preparing nano level Khotan jade fiber, ultra-fine Khotan jade fiber, common Khotan jade fiber.
The fiber that utilizes Khotan jade to make for composition is not only applicable to prescription of the present invention, and is applicable to the prescription of other fibre.
The above only is preferred embodiment of the present invention; be not so limit claim of the present invention; every equivalent method or equivalent flow process conversion that utilizes specification of the present invention to do; or directly or indirectly be used in other relevant technical field, all in like manner be included in the scope of patent protection of the present invention.
Claims (9)
1. Khotan jade fiber is characterized in that: described Khotan jade fiber is finish-ground to the Khotan jade fine powder by the Khotan jade polishing, forms with silicate, mineral wool, inorganic acid, binding agent, water formulated, and its percentage by weight is:
Khotan jade 3%～5%, silicate 5%～15%, mineral wool 30%～60%, inorganic acid 1%～10%, binding agent 5%～10%.
2. according to a kind of Khotan jade fiber claimed in claim 1, it is characterized in that: described Khotan jade fine powder comprises nano-powder, superfine powder, powder, the nano-powder diameter is between 0.01 nanometer～100 nanometers, the superfine powder diameter is between 100 nanometers～45 micron, and powder is between 45 microns～1 millimeter.
3. according to claim 1 or 2 described a kind of Khotan jade fibers, it is characterized in that: described Khotan jade fine powder contains the trace elements such as zinc, iron, copper, manganese, magnesium, cobalt, selenium, chromium, titanium, lithium, calcium, potassium, sodium, meals made from Khotan jade or the fibre that directly contacts is arranged with skin, its trace element can be absorbed by the body, the activating cell tissue, the functions such as immunity of raising human body.
4. the preparation method of a Khotan jade fiber is characterized in that following steps:
A, selected Khotan jade clean up Khotan jade, polish with refiner through fragmentation, and grinding become the Khotan jade fine powder;
B, pour the Khotan jade fine powder into the washing and filtering device, add entry and stir, filter simultaneously cleaning, and do dry the processing, the gained fine powder is the first component;
C, silicate, mineral wool, inorganic acid, binding agent are added water in mixer, fully mix 1～2 hour;
D, with the solution left standstill of c gained, treat that solution can see the sedimentation mixture to lower floor clearly, the upper strata clear solution is discharged, remaining sedimentation mixture carries out drying again, the gained mixture is second component;
E, second component is taken out, insert the high-speed stirred dispersing apparatus, and add ethanol, start the high-speed stirred dispersing apparatus, heat simultaneously to 70～90 ℃, keep constant temperature, add phosphoric acid fat, stirred 1～4 hour, the form slurry state stops to stir, and the gained slurry is the 3rd component;
F, the 3rd component is carried out vacuumize under 70～120 ℃ of temperature, all volatilize to ethanol, obtained component is the 4th component;
G, the first component is added in the 4th component, use supersonic speed degree of depth solution beam device to separate bundle and process 10min～60min, make in the corpus fibrosum of producing and be uniform-distribution with the Khotan jade particulate with appearance, fiber is just as a string pearl necklace one by one, unusual bright smooth, by demand, can distinguish preparing nano level Khotan jade fiber, ultra-fine Khotan jade fiber, common Khotan jade fiber.
5. according to the preparation method of a kind of Khotan jade fiber claimed in claim 4, it is characterized in that: described Khotan jade fine powder comprises nano-powder, superfine powder, powder, the nano-powder diameter is between 0.01 nanometer～100 nanometers, the superfine powder diameter is between 100 nanometers～45 micron, and powder is between 45 microns～1 millimeter.
6. according to the preparation method of a kind of Khotan jade fiber claimed in claim 4, it is characterized in that: described silicate is one or more of asbestos, mica, talcum, kaolinite, montmorillonite, zeolite, is preferably montmorillonite.
7. according to the preparation method of a kind of Khotan jade fiber claimed in claim 4, it is characterized in that: described inorganic acid is commercial acid, is specially a kind of in hydrochloric acid, nitric acid or the sulfuric acid, is preferably sulfuric acid.
8. according to the preparation method of a kind of Khotan jade fiber claimed in claim 4, it is characterized in that: described binding agent is a kind of of phenol-formaldehyde binders, epoxy adhesive or polyurethane adhesive, is preferably phenol-formaldehyde binders.
9. according to the preparation method of a kind of Khotan jade fiber claimed in claim 4, it is characterized in that: described water, ethanol, phosphoric acid fat are supplies.
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012102960641A CN102912468A (en) | 2012-08-20 | 2012-08-20 | Hetian jade fibers and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN2012102960641A CN102912468A (en) | 2012-08-20 | 2012-08-20 | Hetian jade fibers and preparation method thereof |
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| CN102912468A true CN102912468A (en) | 2013-02-06 |
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| CN2012102960641A Pending CN102912468A (en) | 2012-08-20 | 2012-08-20 | Hetian jade fibers and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103320885A (en) * | 2013-06-03 | 2013-09-25 | 王美生 | Manufacturing method of multifunctional textile fiber containing Dushan jade |
| CN109280988A (en) * | 2018-09-20 | 2019-01-29 | 广东山石微量元素研究院（普通合伙） | A kind of polypropylene fiber of the micro mist containing Khotan jade and preparation method thereof |
| CN109487369A (en) * | 2018-12-19 | 2019-03-19 | 肖晖 | A kind of Khotan jade fiber and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN1156705A (en) * | 1996-04-18 | 1997-08-13 | 孙宏贺 | Multipurpose material with eight functions |
| CN101070626A (en) * | 2007-06-12 | 2007-11-14 | 江苏盛虹化纤有限公司 | Microelement biological jade fiber |
| CN101691275A (en) * | 2009-08-31 | 2010-04-07 | 河北工业大学 | Method for preparing nano mineral fiber |
| CN102534949A (en) * | 2012-03-12 | 2012-07-04 | 江苏丹毛纺织股份有限公司 | Elastic worsted fabric with contact coldness sense and preparation method thereof |
-
2012
- 2012-08-20 CN CN2012102960641A patent/CN102912468A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1156705A (en) * | 1996-04-18 | 1997-08-13 | 孙宏贺 | Multipurpose material with eight functions |
| CN101070626A (en) * | 2007-06-12 | 2007-11-14 | 江苏盛虹化纤有限公司 | Microelement biological jade fiber |
| CN101691275A (en) * | 2009-08-31 | 2010-04-07 | 河北工业大学 | Method for preparing nano mineral fiber |
| CN102534949A (en) * | 2012-03-12 | 2012-07-04 | 江苏丹毛纺织股份有限公司 | Elastic worsted fabric with contact coldness sense and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103320885A (en) * | 2013-06-03 | 2013-09-25 | 王美生 | Manufacturing method of multifunctional textile fiber containing Dushan jade |
| CN109280988A (en) * | 2018-09-20 | 2019-01-29 | 广东山石微量元素研究院（普通合伙） | A kind of polypropylene fiber of the micro mist containing Khotan jade and preparation method thereof |
| CN109487369A (en) * | 2018-12-19 | 2019-03-19 | 肖晖 | A kind of Khotan jade fiber and preparation method thereof |
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Application publication date: 20130206 |
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