CN109464311A - A kind of whitening antiallergic anti-aging compound recipe essential oil and preparation method thereof - Google Patents
A kind of whitening antiallergic anti-aging compound recipe essential oil and preparation method thereof Download PDFInfo
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Abstract
Whitening antiallergic anti-aging compound recipe essential oil disclosed by the invention is for the first time using pine tree essence oil and toothed oak tree essential oil as the raw material of compound essential oil, it is aided with tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil and Peppermint essential oil, the functionality of essential oil can be enhanced by scientifically matching preparation, there is preferable whitening, antiallergic sense, crease-resistant function.Pine tree essence oil and toothed oak tree essential oil of the present invention carries out Microwave Extraction, ultrasonic vibration extraction and microwave abstracting, not only the effective component in pine tree can dramatically be extracted, and effective component and the effective component of other raw material essential oils can cooperate, and therapeutic effect is made to reach best.
Description
Technical field
The invention belongs to medicines and health protection fields, and in particular, to a kind of whitening antiallergic anti-aging compound recipe essential oil and its preparation
Method.
Background technique
Essential oil is in the flower from plant, leaf, stem, root or fruit, passes through steam distillation, extrusion, cold-maceration or molten
Agent extraction method refines the volatile flavor of extraction.Oil has lipophilicity, it is easy to be dissolved in grease, because of the molecule of essential oil
Chain is usually shorter, this permeates them easily in skin, and enters body by capillary abundant under subcutaneous fat
It is interior.Essential oil is made of the molecule of some very littles, these high volatile substances, can enter body by nasal membrane tissue resorption,
Message is directly sent to brain, by the limbic system of brain, adjusts the physiological function of mood and body.So in aromatotherapy
In, essential oil can strengthen the function of physiology and psychology.Each plants essential oil has a chemical structure to determine its fragrance, color
Color, mobility and it and system operation mode, but also each plants essential oil respectively has a set of special function speciality.
Essential oil skin care can enter blood readily through Cutaneous permeation due to the features such as molecule of essential oil is small, easy infiltration
Circulation, plays the role of conditioning to skin, thus the effect of reaching skin care.Cosmetics are prepared using essential oil, are not necessarily to essence,
Using safer.Different essential oils are applied in combination, and can learn from other's strong points to offset one's weaknesses, and play bigger effect.
Summary of the invention
The present invention provides a kind of whitening antiallergic anti-aging compound recipe essential oil.The present invention locates pine tree and toothed oak tree by ultrasonic wave in advance
Reason, be concentrated by evaporation, carbon dioxide supercritical extraction and shunt microwave abstracting and etc. be prepared, this compound essential oil effective component
Content is higher, can effectively enhance the nutrition of skin, and whitening, anti-inflammatory, antiallergy, anti-aging effects are good, generates Small side effects.
The present invention is achieved by the following technical solutions:
Disclosed whitening antiallergic anti-aging compound recipe essential oil, including following weight proportion: 10~25 parts of pine tree essence oil, toothed oak tree essence
20~25 parts of oil, 10~12 parts of tea tree ethereal oil, 5~10 parts of violet essential, 3~5 parts of olibanum essential oil, palmarosa essential oil 5~8
Part, 3~6 parts and 2~5 parts of Peppermint essential oil of fragrant citrus essential oil.
The preparation method of above-mentioned whitening antiallergic anti-aging compound recipe essential oil, comprising the following steps:
S1. the processing of pine extract or toothed oak tree extract: pine branch or mongolian oak bark are crushed respectively, use petroleum ether degreasing
After be added to the water, soaking, Microwave Extraction and sonic oscillation extract, and fibrous residue is obtained by filtration；Filtrate is decolourized, is concentrated, and obtains
Pine extract or toothed oak tree extract take intermediate clarified solution, as filtrate one or filtrate two after stratification；
S2. the extraction of effective component: the filtrate one of step S1 and filtrate two are evaporated concentration respectively, obtaining has medicine
Imitate ingredient solution one and solution two；
S3. the way of distillation is used, tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint are distilled respectively, prepare phase
The crude essential oil answered；
S4. the crude essential oil of the tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint is subjected to carbon dioxide respectively
Supercritical extract obtains the higher second level essential oil of purity；
S5. the effective component root Ju of the second level essential oil and step S2 is needed to carry out to draw section fractionation microwave extraction respectively
It takes, respectively obtains tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil, Peppermint essential oil, pine tree essence oil
With toothed oak tree essential oil；
S6. at 30~50 DEG C, tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus are sequentially added
Essential oil and Peppermint essential oil stir evenly, and add pine tree essence oil and toothed oak tree essential oil, stir evenly, and it is multiple both to have obtained whitening antiallergic anti-aging
Square essential oil.
Further, the ratio between ml of the grams of the pine tree and water is 1:12~18, the grams and water of the toothed oak tree
The ratio between ml be 1:10~15.
Further, the condition of Microwave Extraction described in step S1 are as follows: 650W~850W Microwave Extraction 5min~10min；
The condition that the sonic oscillation extracts are as follows: 60W~80W sonic oscillation extracts 20~30min.
Further, 20~40MPa of extracting pressure of the carbon dioxide supercritical extraction, 40~80 DEG C of temperature, CO2Stream
Measure 2~5L/h, 120~150min of extraction time.
Further, microwave abstracting is shunted described in step S5 specifically:, will by mixing speed control in 60~80r/min
Material is heated to 80~100 DEG C in distillation still, uses frequency for 5~10min of microwave treatment of 50~90MHZ.
Pine tree essence oil is used as main material by the present invention, can extend the effect of vitamin C in human body, activation vitamin C and
The effect of vitamin E, inhibits nucleic acid damaging caused by lipoprotein oxidation and hydroxy radical, and human activin is grown up hormonal point
It secretes, improve immune response and protects nerve cell from the salt as glutamic acid, destruction caused by rouge or its anionic form, it can
With immunity degradation and haemocyte the metabolic function decline occurred in anti-aging process, and they are restored to normal water
It is flat.
Embedded amine groups acid, organic acid, alcohols, phenols, ketone and amine, methylamine, dimethyl amine, pyrrole in toothed oak tree essential oil
The nitrogenous bases such as pyridine class, etc. component Multiple components.It can provide skin immune function controlling, adjust moisture, soda acid, equilibrium oil
Rouge has the antiallergic ability for improving sensitive, prevents the generation of wrinkle.Activate the peroxidating of Skin Cell hepatocuprein
The activity of object dispels the free radical of Skin Cell surplus, effective delay skin aging.Enhance the toxin expelling of lymphatic system, detoxify function
Can, effectively block infringement of the extraneous harmful substance to skin.Resisting skin allergy ability is improved, and to internal harmful substance and aging
Cell disintegration excretion.It prevents the collagen in excessive bivalent metal ion and skin from crosslinking effect, maintains enough
Collagenous fibres and elastomer make skin slip, fine and smooth high resilience.
Tea tree ethereal oil: bactericidal antiphlogistic, convergence pore effect are extremely strong, are suitable for oiliness and acne-prone skin.Violet essential: with
Smoothing wrinkle is helped, for middle aged skin, effect is particularly splendid.Palmarosa essential oil: being suitble to bellding water shortage skin, acne type skin, puts down
Weigh sebum secretion, re-forms the natural water-retaining film of skin surface, plays excellent moistening effect；Peppermint essential oil: it can adjust
Manage the skin of unclean obstruction, refrigerant feeling can shrink capilary, releive and itch, inflammation and burn, can also soft skin,
For removing blackhead and oily skin also great effect.Olibanum essential oil: removing crow's feet, treats venular rupture, goes red
The trace of blood.
The present invention is creatively obtained using pine tree as the raw material of essential oil by the special extraction to pine branch and mongolian oak bark
To the pine tree essence oil and toothed oak tree essential oil of drug effect very high concentrations, it is aided with tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essence
Oil, fragrant citrus essential oil and Peppermint essential oil, can enhance the functionality of essential oil by scientifically matching, not the simple superposition of effect, have
There are preferable whitening, antiallergic sense, crease-resistant function.
Compared with prior art, the present invention provides whitening antiallergic anti-aging compound recipe essential oil and preparation method thereof with following excellent
Gesture:
Whitening antiallergic anti-aging compound recipe essential oil of the present invention for the first time using pine tree essence oil and toothed oak tree essential oil as the raw material of compound essential oil,
It is aided with tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil and Peppermint essential oil, by scientifically matching
Preparation can enhance the functionality of essential oil, have the preferable crease-resistant function of whitening antiallergic.
Pine tree essence oil and toothed oak tree essential oil of the present invention carries out Microwave Extraction, ultrasonic vibration extraction and microwave abstracting, can not only incite somebody to action
Effective component in pine tree is dramatically extracted, and effective component and the effective component of other raw material essential oils can phase interworkings
It closes, therapeutic effect is made to reach best.
The preparation method of whitening antiallergic anti-aging compound recipe essential oil of the present invention, technical process is simple, during the reaction will not
Any harmful substance is generated to environment, it is easy to operate, and low energy consumption, pollution is few.
Specific embodiment
The present invention is further illustrated combined with specific embodiments below.Unless stated otherwise, it is used in the embodiment of the present invention
Raw material and method are the raw material of this field regular market purchase and conventional use of method, used equipment are that this field is routinely set
It is standby.
Whitening antiallergic anti-aging compound recipe essential oil provided by the invention, including following weight proportion: 10~25 parts of pine tree essence oil,
20~25 parts of toothed oak tree essential oil, 10~12 parts of tea tree ethereal oil, 5~10 parts of violet essential, 3~5 parts of olibanum essential oil, palmarosa essential oil
5~8 parts, 3~6 parts and 2~5 parts of Peppermint essential oil of fragrant citrus essential oil.
Embodiment 1
Whitening antiallergic anti-aging compound recipe essential oil provided in this embodiment, by table 1 raw material and weight be made.Tool
Steps are as follows for gymnastics work:
S1. the processing of pine extract or toothed oak tree extract: pine branch or mongolian oak bark are crushed respectively, use petroleum ether degreasing
After be added to the water, the ratio between ml of the grams of pine tree and water is 1:18, and the grams of toothed oak tree and the ratio between ml of water are 1:10；
Soaking, Microwave Extraction and sonic oscillation extract, and fibrous residue is obtained by filtration；Filtrate is decolourized, is concentrated, obtain pine extract or
Toothed oak tree extract takes intermediate clarified solution, as filtrate one or filtrate two after stratification；The condition of Microwave Extraction are as follows: 850W is micro-
Wave extracts 5min；The condition that sonic oscillation extracts are as follows: 80W sonic oscillation extracts 30min.
S2. the extraction of effective component: the filtrate one of step S1 and filtrate two are evaporated concentration respectively, obtaining has medicine
Imitate ingredient solution one and solution two；
S3. the way of distillation is used, tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint are distilled respectively, prepare phase
The crude essential oil answered；
S4. the crude essential oil of tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint is subjected to CO 2 supercritical respectively
Extraction, obtains the higher second level essential oil of purity；
S5. the effective component solution root Ju of second level essential oil and step S2 is needed to carry out to draw section fractionation microwave abstracting respectively,
Respectively obtain tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil, Peppermint essential oil, pine tree essence oil and
Toothed oak tree essential oil；Shunt microwave abstracting specifically: mixing speed is controlled in 60r/min, material in distillation still is heated to
80 DEG C, use frequency for the microwave treatment 5min of 90MHZ.
S6. at 30~50 DEG C, tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus are sequentially added
Essential oil and Peppermint essential oil stir evenly, and add pine tree essence oil and toothed oak tree essential oil, stir evenly, and it is multiple both to have obtained whitening antiallergic anti-aging
Square essential oil.
Embodiment 2
Whitening antiallergic anti-aging compound recipe essential oil provided in this embodiment, by table 1 raw material and weight be made.Tool
Steps are as follows for gymnastics work:
S1. the processing of pine extract or toothed oak tree extract: pine branch or mongolian oak bark are crushed respectively, use petroleum ether degreasing
After be added to the water, the ratio between ml of the grams of pine tree and water is 1:12, and the grams of toothed oak tree and the ratio between ml of water are 1:15.
Soaking, Microwave Extraction and sonic oscillation extract, and fibrous residue is obtained by filtration；Filtrate is decolourized, is concentrated, obtain pine extract or
Toothed oak tree extract takes intermediate clarified solution, as filtrate one or filtrate two after stratification；The condition of Microwave Extraction are as follows: 650W is micro-
Wave extracts 10min；The condition that sonic oscillation extracts are as follows: 60W sonic oscillation extracts 20min.
S2. the extraction of effective component: the filtrate one of step S1 and filtrate two are evaporated concentration respectively, obtaining has medicine
Imitate ingredient solution one and solution two；
S3. the way of distillation is used, tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint are distilled respectively, prepare phase
The crude essential oil answered；
S4. the crude essential oil of the tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint is subjected to carbon dioxide respectively
Supercritical extract obtains the higher second level essential oil of purity；
S5. the effective component root Ju of the second level essential oil and step S2 is needed to carry out to draw section fractionation microwave extraction respectively
It takes, respectively obtains tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil, Peppermint essential oil, pine tree essence oil
With toothed oak tree essential oil；Shunt microwave abstracting specifically: control mixing speed in 60r/min, by material heat temperature raising in distillation still
To 100 DEG C, use frequency for the microwave treatment 8min of 50MHZ.
S6. at 30~50 DEG C, tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus are sequentially added
Essential oil and Peppermint essential oil stir evenly, and add pine tree essence oil and toothed oak tree essential oil, stir evenly, and it is multiple both to have obtained whitening antiallergic anti-aging
Square essential oil.
Embodiment 3
Whitening antiallergic anti-aging compound recipe essential oil provided in this embodiment, by table 1 raw material and weight be made.Tool
Steps are as follows for gymnastics work:
S1. the processing of pine extract or toothed oak tree extract: pine branch or mongolian oak bark are crushed respectively, use petroleum ether degreasing
After be added to the water, the ratio between ml of the grams of pine tree and water is 1:16, and the grams of toothed oak tree and the ratio between ml of water are 1:15.
Soaking, Microwave Extraction and sonic oscillation extract, and fibrous residue is obtained by filtration；Filtrate is decolourized, is concentrated, obtain pine extract or
Toothed oak tree extract takes intermediate clarified solution, as filtrate one or filtrate two after stratification；The condition of Microwave Extraction are as follows: 700W is micro-
Wave extracts 10min；The condition that sonic oscillation extracts are as follows: 70W sonic oscillation extracts 20min.
S2. the extraction of effective component: the filtrate one of step S1 and filtrate two are evaporated concentration respectively, obtaining has medicine
Imitate ingredient solution one and solution two；
S3. the way of distillation is used, tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint are distilled respectively, prepare phase
The crude essential oil answered；
S4. the crude essential oil of the tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint is subjected to carbon dioxide respectively
Supercritical extract obtains the higher second level essential oil of purity；
The effective component root Ju of the second level essential oil and step S2 is needed to carry out to draw section fractionation microwave abstracting respectively by S5,
Respectively obtain tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil, Peppermint essential oil, pine tree essence oil and
Toothed oak tree essential oil；Shunt microwave abstracting specifically: mixing speed is controlled in 80r/min, material in distillation still is heated to
100 DEG C, use frequency for the microwave treatment 10min of 50MHZ.
S6. at 30~50 DEG C, tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus are sequentially added
Essential oil and Peppermint essential oil stir evenly, and add pine tree essence oil and toothed oak tree essential oil, stir evenly, and it is multiple both to have obtained whitening antiallergic anti-aging
Square essential oil.
Comparative example 1
This comparative example provides a kind of whitening antiallergic anti-aging compound recipe essential oil, by table 1 raw material and weight be made.
Concrete operation step is same as Example 1.
Comparative example 2
This comparative example provides a kind of whitening antiallergic anti-aging compound recipe essential oil, by table 1 raw material and weight be made.
Concrete operation step is same as Example 1.
Comparative example 3
This comparative example provides a kind of whitening antiallergic anti-aging compound recipe essential oil, by table 1 raw material and weight be made.
Pine tree essence oil and toothed oak tree essential oil are not added in its raw material, concrete operation step is substantially the same manner as Example 1, and removal is mentioned about pine tree
The step of taking and preparing.
Comparative example 4
This comparative example provides a kind of whitening antiallergic anti-aging compound recipe essential oil, by table 1 raw material and weight be made.
Preparation method difference from Example 1 is, without original step S1 and step S2, i.e., using the way of distillation to pine branch and
Mongolian oak bark is distilled, carbon dioxide supercritical extraction and fractionation microwave abstracting, remaining preparation method are same as Example 1.
Table 1
The effect of compound essential oil of above embodiments prevents skin aging is had shown that by following research:
Take SPF grades of female KM kind mouse, 3 the monthly age 20,12 the monthly age 80.By the mouse at 80 12 monthly ages with
Machine is divided into 4 groups: respectively Normal group, A group, B group and C group, and every group 20.Separately by the female KM at 20 3 monthly ages
Kind mouse is as young group of control, weight 25-27g.Mouse presses group sub-cage rearing.Under identical natural conditions,
Conventional feeding is drunk water, and starts to be tested after adaptive feeding.Skin is asked with what shaver sloughed two omoplate of back of mice before experiment
Hair 2cm × 4cm, A-C group on skin is applied with the compound essential oil prepared in Examples 1 to 3 outside respectively, and Normal group and youth are right
It is applied outside according to group with deionized water, preservative film protects 2h.It smears once daily, smears 0.5g every time, it is continuous to smear 50 days.It has tested
Mouse is put to death after, it is measured and tests HYP, SOD, MDA and LF value at skin.
The preparation of 10% Skin Homogenate and the measurement of SOD, MDA, LF:
Skin histology block about 0.5g after taking back to lose hair or feathers, pre-cooled 0.9% sodium chloride solution rinsing, remove subcutaneous fat and
Other connective tissues, filter paper are wiped dry, and weighed quality, tissue block pours into homogenate tube after shredding, and 9 times of quality of the tissue block are added
0.9% sodium chloride solution is pre-chilled, 10% tissue homogenate (carrying out in ice water) is made with interior cut type tissue refiner, then repeatedly
Freeze thawing 3 times, keep it completely broken, cellular content dissociates in the liquid phase completely.SOD activity, MDA content, skin in Skin Homogenate
The index parameters such as skin LF build up bio-engineering corporation's kit specification method referring to Nanjing and are measured.
The measurement result of mouse skin SOD, MDA, LF are shown: under Normal group SOD activity is significant compared with young control group
Drop, and the content of MDA, LF dramatically increase.
The compound essential oil of Examples 1 to 3 preparation can significantly raised natural aging mice skin SOD activity, make its MDA,
The content of LF is decreased obviously.This experimental result confirms that compound essential oil of the invention has significant function of anti-skin aging.
The measurement of HYP and collagen:
By back of mice skin depilatory and after removing connective tissue, acetone: ether: 1: 1 (V/V) degreasing, 80 DEG C of drying, essence
It is close to weigh 50mg, add 6mol/L hydrochloric acid solution 2mL to mix, hydrolyzes 36h in 80 DEG C of baking ovens；Take hydrolyzate 0.4mL with 6mol/L's
Sodium hydroxide solution adjusts its pH value between 6-7, and water is added to be settled to 10.0mL；It takes hydrolyzate 0.2mL to enter test tube, sequentially adds
Buffer 1mL, ammonia amine T lmL, perchloric acid 1mL, color developing agent 1mL are mixed, 60 DEG C of water-bath 15min, 550nm wavelength 1cm optical path ratios
Color, blank zeroing, while preparing standard curve pipe.The mass fraction of collagen is in sample with HYP mass in collagen point
Number is calculated for 13%.
The measurement result of mouse skin HYP and collagen content shows, in the mouse skin of A-C group the content of HYP compared with
Normal group is significantly improved, and difference has extremely significant property.This illustrates that compound essential oil of the invention can promote skin collagen
Synthesis, so that skin is tended to rejuvenation.
Compound essential oil obtained by 1~embodiment of embodiment 3 is subjected to volunteer's test.Test method: each experimental group and
Control group is 50 women (20-50 years old)；Test zone: inner forearm and face area；It uses: twice daily, persistently making
With 4 weeks；Test item: whitening, the mitigation of acne scar, humidity of skin, skin smoothness.The commercially available pox-eliminating whitening essential oil of control group,
Concrete outcome such as the following table 2.
Table 2
From the results shown in Table 2, the whitening antiallergic anti-aging compound recipe essential oil effect of the present embodiment is apparently higher than comparison
Example group and control group, wherein thering are 49 people's situations to be clearly better in 50 volunteers using after 4 weeks.
Detailed process equipment and processing step of the invention that the present invention is explained by the above embodiments, those skilled in the art
Member is not it should be appreciated that the present invention is limited by above-described embodiment, and the above embodiments and description only describe the present invention
Principle, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, this is to this field
It is it will be apparent that these changes and improvements all fall within the protetion scope of the claimed invention for technical staff.
Claims (6)
1. a kind of whitening antiallergic anti-aging compound recipe essential oil, which is characterized in that including following weight proportion: pine tree essence oil 10~25
Part, 20~25 parts of toothed oak tree essential oil, 10~12 parts of tea tree ethereal oil, 5~10 parts of violet essential, 3~5 parts of olibanum essential oil, palmarosa
5~8 parts of essential oil, 3~6 parts and 2~5 parts of Peppermint essential oil of fragrant citrus essential oil.
2. a kind of preparation method of whitening antiallergic anti-aging compound recipe essential oil according to claim 1, which is characterized in that including with
Lower step:
S1. the processing of pine extract or toothed oak tree extract: respectively crushing pine branch or mongolian oak bark, is added with after petroleum ether degreasing
Enter in water, soaking, Microwave Extraction and sonic oscillation extract, and fibrous residue is obtained by filtration；Filtrate is decolourized, is concentrated, and pine tree is obtained
Extract or toothed oak tree extract take intermediate clarified solution, as filtrate one or filtrate two after stratification；
S2. the extraction of effective component: being evaporated concentration for the filtrate one of step S1 and filtrate two respectively, obtain have drug effect at
Divide solution one and solution two；
S3. the way of distillation is used, respectively distills tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint, is prepared corresponding
Crude essential oil；
S4., the crude essential oil of the tea tree, rose, olibanum, palmarosa, fragrant citrus and peppermint carries out to carbon dioxide is super to be faced respectively
Boundary's extraction, obtains the higher second level essential oil of purity；
S5. the effective component root Ju of the second level essential oil and step S2 is needed to carry out to draw section fractionation microwave abstracting respectively, point
Tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil, Peppermint essential oil, pine tree essence oil and toothed oak are not obtained
Set essential oil；
S6. at 30~50 DEG C, tea tree ethereal oil, violet essential, olibanum essential oil, palmarosa essential oil, fragrant citrus essential oil are sequentially added
It is stirred evenly with Peppermint essential oil, adds pine tree essence oil and toothed oak tree essential oil, stir evenly, both obtained whitening antiallergic anti-aging compound recipe essence
Oil.
3. the preparation method of whitening antiallergic anti-aging compound recipe essential oil according to claim 2, which is characterized in that the pine tree
The ratio between ml of grams and water is 1:12~18, and the grams of the toothed oak tree and the ratio between ml of water are 1:10~15.
4. the preparation method of whitening antiallergic anti-aging compound recipe essential oil according to claim 2, which is characterized in that described in step S1
Microwave Extraction condition are as follows: 650W~850W Microwave Extraction 5min~10min；The condition that the sonic oscillation extracts are as follows:
60W~80W sonic oscillation extracts 20~30min.
5. the preparation method of whitening antiallergic anti-aging compound recipe essential oil according to claim 2, which is characterized in that the titanium dioxide
20~40MPa of extracting pressure of carbon supercritical extract, 40~80 DEG C of temperature, CO22~5L/h of flow, extraction time 120~
150min。
6. the preparation method of whitening antiallergic anti-aging compound recipe essential oil according to claim 2, which is characterized in that described in step S5
Shunt microwave abstracting specifically: by mixing speed control in 60~80r/min, material in distillation still is heated to 80~
100 DEG C, use frequency for 5~10min of microwave treatment of 50~90MHZ.
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| CN112481033A (en) * | 2020-11-17 | 2021-03-12 | 阜阳师范大学 | Extraction method of cedrela sinensis essential oil |
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| CN112481033A (en) * | 2020-11-17 | 2021-03-12 | 阜阳师范大学 | Extraction method of cedrela sinensis essential oil |
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