CN109440472B - Preparation method of washable moisture-absorbing quick-drying finishing agent with soft hand feeling - Google Patents
Preparation method of washable moisture-absorbing quick-drying finishing agent with soft hand feeling Download PDFInfo
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- CN109440472B CN109440472B CN201811270416.XA CN201811270416A CN109440472B CN 109440472 B CN109440472 B CN 109440472B CN 201811270416 A CN201811270416 A CN 201811270416A CN 109440472 B CN109440472 B CN 109440472B
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/507—Polyesters
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Polyesters Or Polycarbonates (AREA)
- Woven Fabrics (AREA)
- Details Of Garments (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a preparation method of a washable moisture-absorbing quick-drying finishing agent with soft hand feeling, which adopts new raw materials DMT and PEG, and uses a catalyst and an antioxidant in a matching manner, thereby greatly reducing the product cost, saving great production cost for subsequent printing and dyeing manufacturers, and increasing the processing competitive advantage of the printing and dyeing manufacturers; the product of the invention can be cut into pieces by cold water, has little foam and high temperature resistance, can be used for bath together with terylene dyeing, meets the process requirements of energy conservation and emission reduction, and reduces the pressure of enterprises on environmental protection; the product has the washing resistance times of more than 30 times, completely solves the washing resistance problem of the common household sports fabric, and can achieve good hydrophilic and quick-drying functions after 30 times; the product of the invention has good fluffy and soft hand feeling, and the dosage of the softening agent in the later period can be reduced; the product of the invention does not contain silicon, conforms to the provisions of GOTS and ZDHC regulations and is environment-friendly.
Description
Technical Field
The invention relates to the technical field of textile chemicals, in particular to a preparation method of a washable moisture-absorbing quick-drying finishing agent with soft hand feeling.
Background
The modern society is along with the environment that economic rapid development brought, and food problem makes people's health receive certain infringement, and social survival competition also brings certain pressure to people's mind and body, and the sports body-building is very important, also is enjoyed by people. The body building can not only eliminate body pain, but also relieve psychological pressure. With the improvement of living standard, the requirement of people on the comfort of the sports fabric is continuously improved. The fabric of the sports wear is required to have good comfort, and once sweat streams down the back during activity, the garment is not stuck to the skin to generate cold and wet feeling, so that the moisture absorption and sweat releasing function is required. At present, the demand of the field of sports clothes on the fabric is very strong, and the number of moisture absorption and sweat releasing products is gradually increased. The sports fabric is mainly made of polyester fibers, the polyester fibers are one of the largest varieties of the current synthetic fibers, and the sports fabric is high in breaking strength and good in wear resistance, so that the sports fabric is popular among people. However, the polyester fiber is hydrophobic, the moisture absorption and sweat releasing performance of the polyester fiber is poor, the polyester fiber generates an electrostatic effect and is easy to stain, and the moisture absorption and sweat releasing finishing agent is produced at the same time.
Different products are available in the market, but the products have the defects of high cost, difficult material melting, large foam, poor compatibility, incapability of being used together with terylene dyeing, washability and the like.
Disclosure of Invention
In view of the above, the present invention provides a method for preparing a washable moisture-absorbing quick-drying finishing agent with soft hand feeling, which improves the effect, greatly reduces the cost, and has the characteristics of good washability and soft hand feeling.
In order to achieve the purpose, the invention adopts the following technical scheme:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 160 ℃ for 150-;
(2) adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent.
Preferably, the catalyst is chromium oxide.
Compared with the prior art, the invention has obvious advantages and beneficial effects, and specifically, the technical scheme includes that:
the product of the invention adopts new raw materials, greatly reduces the product cost, saves great production cost for subsequent printing and dyeing manufacturers, and increases the processing competitive advantage of the printing and dyeing manufacturers; the product of the invention can be cut into pieces by cold water, has little foam and high temperature resistance, can be used for bath together with terylene dyeing, meets the process requirements of energy conservation and emission reduction, and reduces the pressure of enterprises on environmental protection; the product has the washing resistance times of more than 30 times, completely solves the washing resistance problem of the common household sports fabric, and can achieve good hydrophilic and quick-drying functions after 30 times; the product of the invention has good fluffy and soft hand feeling, and the dosage of the softening agent in the later period can be reduced; the product of the invention does not contain silicon, conforms to the provisions of GOTS and ZDHC regulations and is environment-friendly
Detailed Description
The invention discloses a preparation method of a washable moisture-absorbing quick-drying finishing agent with soft hand feeling, which comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 160 ℃ for 150-; the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The invention is illustrated in more detail below in the following examples:
example 1:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 150 ℃, adding 80g of PEG and 0.003g of catalyst after the DMT is completely melted, continuously heating to 235 ℃, carrying out ester exchange reaction until the distilled amount of methanol is 96% of a theoretical value, and finishing the ester exchange reaction; the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The moisture absorption quick-drying finishing agent is prepared into a 10% solution, and the solution is treated by an immersion method: the dosage is 4% (o.w.f.), bath ratio: 1:10, 40 ℃ for 30min, pre-baking for 100 ℃ for 3min, and baking for 160 ℃ for 80 s.
The hydrophilicity of the moisture absorption quick-drying finishing agent is identified by the capillary effect of the finished polyester fabric, the capillary effect is large, the hydrophilicity of the finishing agent is good, the capillary effect is tested by referring to FZ/T01071-1999, the capillary effect reaches 22cm, the hydrophilicity is very good, the fabric is washed by referring to GB/T8629-. The moisture-absorbing quick-drying finishing agent has good hydrophilicity, can achieve the moisture-absorbing quick-drying effect, has lower cost than the prior art, and still has good moisture-absorbing and sweat-releasing effects after 30 times of washing resistance.
Example 2:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 155 ℃, adding 80g of PEG and 0.003g of catalyst after DMT is completely melted, continuing to heat to 230 ℃, and carrying out transesterification until the distilled amount of methanol is 95% of the theoretical value, wherein the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The moisture absorption quick-drying finishing agent is prepared into a 10% solution, and the solution is treated by an immersion method: the dosage is 4% (o.w.f.), bath ratio: 1:10, 40 ℃ for 30min, pre-baking for 100 ℃ for 3min, and baking for 160 ℃ for 80 s.
The hydrophilicity of the moisture absorption quick-drying finishing agent is identified by the capillary effect of the finished polyester fabric, the capillary effect is large, the hydrophilicity of the finishing agent is good, the capillary effect is tested by referring to FZ/T01071-1999, the capillary effect reaches 22cm, the hydrophilicity is very good, the fabric is washed by referring to GB/T8629-. The moisture absorption quick-drying finishing agent has good hydrophilicity, can achieve the moisture absorption quick-drying effect, has lower cost than the prior art, and still has good moisture absorption and sweat releasing effects after 35 times of washing resistance.
Example 3:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 158 ℃, adding 80g of PEG and 0.003g of catalyst after DMT is completely melted, continuing to heat to 238 ℃, and carrying out transesterification until the methanol distillation amount is 97% of a theoretical value, wherein the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The moisture absorption quick-drying finishing agent is prepared into a 10% solution, and the solution is treated by an immersion method: the dosage is 4% (o.w.f.), bath ratio: 1:10, 40 ℃ for 30min, pre-baking for 100 ℃ for 3min, and baking for 160 ℃ for 80 s.
The hydrophilicity of the moisture absorption quick-drying finishing agent is identified by the capillary effect of the finished polyester fabric, the capillary effect is large, the hydrophilicity of the finishing agent is good, the capillary effect is tested by referring to FZ/T01071-1999, the capillary effect reaches 22cm, the hydrophilicity is very good, the fabric is washed by referring to GB/T8629-. The moisture-absorbing quick-drying finishing agent has good hydrophilicity, can achieve the moisture-absorbing quick-drying effect, has lower cost than the prior art, and still has good moisture-absorbing and sweat-releasing effects after being washed for 32 times.
Example 4:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 160 ℃, adding 80g of PEG and 0.003g of catalyst after DMT is completely melted, continuing to heat to 236 ℃, and carrying out transesterification until the distilled amount of methanol is 98% of the theoretical value, wherein the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The moisture absorption quick-drying finishing agent is prepared into a 10% solution, and the solution is treated by an immersion method: the dosage is 4% (o.w.f.), bath ratio: 1:10, 40 ℃ for 30min, pre-baking for 100 ℃ for 3min, and baking for 160 ℃ for 80 s.
The hydrophilicity of the moisture absorption quick-drying finishing agent is identified by the capillary effect of the finished polyester fabric, the capillary effect is large, the hydrophilicity of the finishing agent is good, the capillary effect is tested by referring to FZ/T01071-1999, the capillary effect reaches 22cm, the hydrophilicity is very good, the fabric is washed by referring to GB/T8629-. The moisture absorption quick-drying finishing agent has good hydrophilicity, can achieve the moisture absorption quick-drying effect, has lower cost than the prior art, and still has good moisture absorption and sweat releasing effects after being washed for 33 times.
Example 5:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g DMT into a 250mL three-neck flask, heating to 153 ℃, adding 80g PEG and 0.003g catalyst after DMT is completely melted, continuing to heat to 240 ℃, and carrying out transesterification until the distilled amount of methanol is 96% of the theoretical value, wherein the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The moisture absorption quick-drying finishing agent is prepared into a 10% solution, and the solution is treated by an immersion method: the dosage is 4% (o.w.f.), bath ratio: 1:10, 40 ℃ for 30min, pre-baking for 100 ℃ for 3min, and baking for 160 ℃ for 80 s.
The hydrophilicity of the moisture absorption quick-drying finishing agent is identified by the capillary effect of the finished polyester fabric, the capillary effect is large, the hydrophilicity of the finishing agent is good, the capillary effect is tested by referring to FZ/T01071-1999, the capillary effect reaches 22cm, the hydrophilicity is very good, the fabric is washed by referring to GB/T8629-. The moisture-absorbing quick-drying finishing agent has good hydrophilicity, can achieve the moisture-absorbing quick-drying effect, has lower cost than the prior art, and still has good moisture-absorbing and sweat-releasing effects after being washed for 40 times.
Example 6:
a method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 154 ℃, adding 80g of PEG and 0.003g of catalyst after DMT is completely melted, continuously heating to 239 ℃, and carrying out transesterification until the distilled amount of methanol is 98% of the theoretical value, wherein the catalyst is chromium oxide.
(2) Adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent. The catalyst is chromium oxide.
The moisture absorption quick-drying finishing agent is prepared into a 10% solution, and the solution is treated by an immersion method: the dosage is 4% (o.w.f.), bath ratio: 1:10, 40 ℃ for 30min, pre-baking for 100 ℃ for 3min, and baking for 160 ℃ for 80 s.
The hydrophilicity of the moisture absorption quick-drying finishing agent is identified by the capillary effect of the finished polyester fabric, the capillary effect is large, the hydrophilicity of the finishing agent is good, the capillary effect is tested by referring to FZ/T01071-1999, the capillary effect reaches 22cm, the hydrophilicity is very good, the fabric is washed by referring to GB/T8629-. The moisture-absorbing quick-drying finishing agent has good hydrophilicity, can achieve the moisture-absorbing quick-drying effect, has lower cost than the prior art, and still has good moisture-absorbing and sweat-releasing effects after being washed for 36 times.
The design key points of the invention are as follows: the product of the invention adopts new raw materials, greatly reduces the product cost, saves great production cost for subsequent printing and dyeing manufacturers, and increases the processing competitive advantage of the printing and dyeing manufacturers; the product of the invention can be cut into pieces by cold water, has little foam and high temperature resistance, can be used for bath together with terylene dyeing, meets the process requirements of energy conservation and emission reduction, and reduces the pressure of enterprises on environmental protection; the product has the washing resistance times of more than 30 times, completely solves the washing resistance problem of the common household sports fabric, and can achieve good hydrophilic and quick-drying functions after 30 times; the product of the invention has good fluffy and soft hand feeling, and the dosage of the softening agent in the later period can be reduced; the product of the invention does not contain silicon, conforms to the provisions of GOTS and ZDHC regulations and is environment-friendly
The technical principle of the present invention is described above in connection with specific embodiments. The description is made for the purpose of illustrating the principles of the invention and should not be construed in any way as limiting the scope of the invention. Based on the explanations herein, those skilled in the art will be able to conceive of other embodiments of the present invention without inventive effort, which would fall within the scope of the present invention.
Claims (2)
1. A method for preparing washable moisture-absorbing quick-drying finishing agent with soft hand feeling is characterized in that: the method comprises the following steps:
(1) adding 15g of DMT into a 250mL three-neck flask, heating to 160 ℃ for 150-;
(2) adding 155g of PEG1500, TPP and 0.003g of catalyst, introducing nitrogen, heating to the polycondensation reaction temperature of 260 ℃, preserving the temperature for one hour, vacuumizing, maintaining the vacuum degree of 0.1MPa and the temperature of 260 ℃ for polycondensation reaction, cooling and discharging after 5 hours of reaction, cooling and drying, and crushing into blocks to obtain the moisture-absorbing quick-drying finishing agent.
2. A process for preparing a wash-durable, soft-touch, moisture-absorbent quick-dry finish according to claim 1, characterized in that: the catalyst is chromium oxide.
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Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105421117A (en) * | 2015-12-16 | 2016-03-23 | 张家港市德宝化工有限公司 | Application of moisture absorbing and sweat releasing finishing agent to polyester fiber materials |
CN107629201A (en) * | 2017-10-20 | 2018-01-26 | 宜昌中盈合成材料有限公司 | A kind of high water resistance type heavy water-soluble poly ester material and preparation method thereof |
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Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105421117A (en) * | 2015-12-16 | 2016-03-23 | 张家港市德宝化工有限公司 | Application of moisture absorbing and sweat releasing finishing agent to polyester fiber materials |
CN107629201A (en) * | 2017-10-20 | 2018-01-26 | 宜昌中盈合成材料有限公司 | A kind of high water resistance type heavy water-soluble poly ester material and preparation method thereof |
Non-Patent Citations (1)
Title |
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影响聚酯聚醚嵌段共聚型整理剂亲水性的因素;吴明华 等;《功能高分子学报》;20070331;第19-20卷(第1期);第64-67、73页 * |
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