CN109439437A - A kind of coriander flavor essence and its preparation method and application for cigarette dripping pill - Google Patents
A kind of coriander flavor essence and its preparation method and application for cigarette dripping pill Download PDFInfo
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- CN109439437A CN109439437A CN201811563889.9A CN201811563889A CN109439437A CN 109439437 A CN109439437 A CN 109439437A CN 201811563889 A CN201811563889 A CN 201811563889A CN 109439437 A CN109439437 A CN 109439437A
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- China
- Prior art keywords
- coriander
- cigarette
- dripping pill
- flavor essence
- essence
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 90
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 72
- 235000019634 flavors Nutrition 0.000 title claims abstract description 72
- 239000006187 pill Substances 0.000 title claims abstract description 68
- 241000208308 Coriandrum Species 0.000 title claims abstract description 65
- 235000002787 Coriandrum sativum Nutrition 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims abstract description 22
- 229940029991 coriander extract Drugs 0.000 claims abstract description 21
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000000034 method Methods 0.000 claims abstract description 13
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims abstract description 12
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims abstract description 11
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims abstract description 11
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229930007744 linalool Natural products 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 239000001359 coriandrum sativum l. oleoresin Substances 0.000 claims abstract description 9
- NXMUXTAGFPJGTQ-UHFFFAOYSA-N decanoic acid;octanoic acid Chemical compound CCCCCCCC(O)=O.CCCCCCCCCC(O)=O NXMUXTAGFPJGTQ-UHFFFAOYSA-N 0.000 claims abstract description 7
- 235000011187 glycerol Nutrition 0.000 claims abstract description 7
- 150000005691 triesters Chemical class 0.000 claims abstract description 7
- 238000010992 reflux Methods 0.000 claims abstract description 6
- 239000006228 supernatant Substances 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims description 12
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 239000000203 mixture Substances 0.000 claims description 7
- 239000002245 particle Substances 0.000 claims description 6
- 238000009210 therapy by ultrasound Methods 0.000 claims description 6
- 239000000706 filtrate Substances 0.000 claims description 5
- 238000005374 membrane filtration Methods 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- -1 geranyl Ester Chemical class 0.000 claims description 3
- 239000004568 cement Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 241000723346 Cinnamomum camphora Species 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 abstract description 13
- 239000007788 liquid Substances 0.000 abstract description 2
- 238000001914 filtration Methods 0.000 abstract 1
- 238000002156 mixing Methods 0.000 abstract 1
- 239000000686 essence Substances 0.000 description 45
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 21
- 238000005516 engineering process Methods 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 239000002304 perfume Substances 0.000 description 4
- 230000000391 smoking effect Effects 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 238000011156 evaluation Methods 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000009940 knitting Methods 0.000 description 2
- 230000001953 sensory effect Effects 0.000 description 2
- 210000000697 sensory organ Anatomy 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- HIGQPQRQIQDZMP-FLIBITNWSA-N Acetic acid geraniol ester Natural products CC(C)=CCC\C(C)=C/COC(C)=O HIGQPQRQIQDZMP-FLIBITNWSA-N 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 240000005373 Panax quinquefolius Species 0.000 description 1
- 230000003044 adaptive effect Effects 0.000 description 1
- 229910052785 arsenic Inorganic materials 0.000 description 1
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- ODCCQUXDUXHSBP-UHFFFAOYSA-N decanoic acid;propane-1,2,3-triol Chemical compound OCC(O)CO.CCCCCCCCCC(O)=O ODCCQUXDUXHSBP-UHFFFAOYSA-N 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 235000011194 food seasoning agent Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 238000005453 pelletization Methods 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000008771 sex reversal Effects 0.000 description 1
- 230000001568 sexual effect Effects 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Botany (AREA)
- Agronomy & Crop Science (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a kind of coriander flavor essence and its preparation method and application for cigarette dripping pill.The coriander flavor essence be by 92.0~96.0% coriander extract, 2.0~3.0% linalool and 2.0~5.0% geranyl acetate stand 24~48h after mixing after obtain；The coriander extract is that after crushing using coriander seed as raw material, 6~8 times of Glycerin, mixed triester with caprylic acid capric acid is added by its weight ratio, heat reflux 1h~1.5h under conditions of 120~150 DEG C of oil bath temperature；Then it is being ultrasonically treated 10~30min, rear centrifuging and taking supernatant liquid filtering obtains.Coriander flavor essence in the present invention has preferable technique suitability, improves the production efficiency of coriander flavor cigarette dripping pill and yield rate, reduces its production cost；It is easy in cigarette application, enriches cigarette flavor, assigns cigarette characteristic flavor on basis.
Description
Technical field
The present invention relates to technical field of cigarette flavors, in particular to a kind of coriander flavor essence for cigarette dripping pill
And its application.
Background technique
As cigarette consumption demand is gradually from type, enjoying type is met to novel sex reversal, the demand to cigarette is by past list
One sucks hobby, gradually forms a variety of demands such as healthy, safe and environment-friendly, consumer not only focuses on the comfort of cigarette smoking
With pleasant sexual experience, and with the raising of cigarette consumption structure, consumer is in terms of the novelty of cigarette, specificity, otherness
Demand further enhance.
Compared with traditional cigarette flavoring technology, cigarette is to inhale not by burning in abundant cigarette with the essence that dripping pill adds
It is small on the influence of cigarette entirety comfortable taste while food taste, imparting cigarette characteristic flavor on basis, it can also be achieved in smoking property of cigarette mistake
What fragrance discharged in journey is artificial controllable.Meanwhile cigarette improves the experience of consumer from more sense organ dimensions such as tactile, the sense of hearing with dripping pill
Sense.Cigarette is in the gesture of accelerated development with application of the dripping pill flavoring in cigarette in recent years, becomes and pulls cigarette quality, sales volume and structure
The bright spot of promotion.
In the prior art, cigarette is common due to more or less having the flavor deployments such as alcohol, propylene glycol and water with dripping pill essence
Solvent, technique suitability is relatively low, causes that cigarette dripping pill production efficiency is relatively low, yield rate is relatively low, production cost is universal higher etc.
Problem more or less constrains the further application and development of cigarette dripping pill.Therefore, it is necessary to from improve cigarette dripping pill essence technique
Suitability is started with, and the new technology of cigarette dripping pill flavor deployment is developed.
Summary of the invention
The coriander flavor essence and its preparation method and application that it is an object of that present invention to provide a kind of for cigarette dripping pill, institute
Essence not spirituosity, propylene glycol and water equal solvent are stated, while abundant smoking property of cigarette taste, assigning cigarette characteristic flavor on basis, tool
There is preferable technique suitability, improve the production efficiency of coriander flavor cigarette dripping pill and yield rate, reduces its production cost.
The present invention is achieved through the following technical solutions: a kind of coriander flavor essence for cigarette dripping pill,
It is characterized in that the coriander flavor essence is by with the material composition of mass percent: 92.0~96.0% coriander extract,
2.0~3.0% linalool, 2.0~5.0% geranyl acetate；The gross mass percentage of above-mentioned substance is 100%；
Wherein, the coriander extract is that coriander seed is crushed the coriander particle for 40~80 mesh using coriander seed as raw material,
By weight 6~8 times of Glycerin, mixed triester with caprylic acid capric acid of addition, hot reflux 1h~1.5h under the conditions of 120~150 DEG C of oil bath temperature；Then exist
Ultrasonic power is 150~250W/L, and supersonic frequency is ultrasonically treated 10~30min under conditions of being 20~25kHz, later at centrifugation
20~30min is managed, takes supernatant to use 0.2~0.8 micron of membrane filtration, is clarified, transparent filtrate is that coriander mentions
Take object.
The present invention preferably technical solution: the coriander flavor essence is by with the material composition of mass percent: 93.0
~95.0% coriander extract, 2.2~2.5% linalool, 2.5~4.8% geranyl acetate.
The present invention provides a kind of preparation method of coriander flavor essence for cigarette dripping pill, it is characterised in that specific steps
It is as follows:
(1) coriander seed is crushed into the coriander particle for 40~80 mesh, by weight the pungent capric acid glycerol that 6~8 times of amounts are added
Ester, heat reflux 1h~1.5h under conditions of 120~150 DEG C of oil bath temperature；
(2) material of hot reflow treatment in step (1) being subjected to 10~30min of ultrasonic treatment, ultrasonic power is 150~
250W/L, supersonic frequency are 20~25kHz；
(3) material after ultrasonic treatment in step (2) is subjected to centrifugal treating, 500~2000rpm of revolving speed handles the time
For 20~30min, takes supernatant to use 0.2~0.8 micron of membrane filtration, clarified, transparent filtrate is that coriander mentions
Take object；
(4) according to following mass percent formula preparation raw material: 92.0~96.0% coriander extract, 2.0~3.0%
Linalool, 2.0~5.0% geranyl acetate；The raw material components of above-mentioned mass fraction are uniformly mixed stirring 1~3 hour,
It is then allowed to stand after 24~48 hours and obtains coriander flavor essence.
The present invention provides a kind of application of coriander flavor essence for cigarette dripping pill, it is characterised in that: by above-mentioned coriander
Flavor essence is added in the essence tank of pill dripping machine, regulates essence pump discharge, then with the dripping pill that is placed in pill dripping machine rubber cement tank
It is 3~10mg that weight, which is made, according to the preparation process of existing cigarette dripping pill in lapping and the curing agent being placed in Sheng ball device,
Crushing strength is 0.3kPa~2.0kPa, and diameter is the cigarette dripping pill of 2~5mm；During cigarette filter wire-beam forming, it will make
Standby cigarette dripping pill positioning is applied in filter rod, and cigarette is made.
Heretofore described coriander seed is commercially available conventional food seasoning, Glycerin, mixed triester with caprylic acid capric acid, linalool, geranyl acetate
For commercially available conventional food additive.
Coriander flavor essence in the present invention selects coriander extract as coriander flavor main body and basis, assigns coriander wind
The pungent perfume (or spice) of taste essence natural coriander with mild；It selects linalool to modify, increases the freshness of coriander flavor；Select acetic acid
Geraniol ester is made further to increase the mellow and full sense of coriander flavor with conjunction and coordination.The coriander flavor essence assigns what cigarette was coordinated
The pungent Flavor feature of coriander enriches cigarette flavor, while promoting the smooth sense and pleasant feeling of flue gas.
Compared with prior art, the flavor essence for being used for cigarette dripping pill in the prior art more or less has alcohol, third
The flavor deployments common solvent such as two alcohol and waters, and the alcohol, propylene glycol and water equal size in flavor essence directly affect dripping pill drop
Type is made, the more low then dripping pill dripping molding effect of the alcohol, propylene glycol and water equal size in flavor essence is better, yield rate more
It is high.Body material used in coriander flavor essence in the present invention is the coriander extract that Glycerin, mixed triester with caprylic acid capric acid directly extracts, no
Spirituosity, propylene glycol and water, not spirituosity, propylene glycol and the water such as other related component linalools and geranyl acetate, and it is described
The not additional alcohol of coriander flavor essence, propylene glycol and water equal solvent, therefore, the coriander flavor essence are made in cigarette dripping pill drop
Technique suitability is good during type, easily package pelletization, and cracky, production are not stablized, and dripping yield rate improves 10~15%, effectively
Reduce cigarette dripping pill production cost.
A kind of coriander flavor essence for cigarette dripping pill provided by the invention has preferable technique suitability, improves
The production efficiency and yield rate of coriander flavor cigarette dripping pill reduce its production cost；It is easy in cigarette application, enriches volume
Cigarette perfume gas assigns cigarette characteristic flavor on basis.Therefore, the present invention has very strong practicability and application value.
Specific embodiment
Explanation is further explained to the present invention below with reference to embodiment.
Coriander extract employed in following embodiments, prepares as follows:
(1) coriander seed is crushed into the particle for 40~60 mesh, weighs the coriander particle of constant weight, by weight addition 8
(weight ratio) Glycerin, mixed triester with caprylic acid capric acid (ODO) is measured again, oil bath heat reflux 1.5h at 150 DEG C；
(2) material in step (1) is subjected to ultrasonic treatment 30min, ultrasonic power 250W/L, supersonic frequency 25kHz；
(3) material after ultrasonic treatment in step (2) is subjected to centrifugal treating, revolving speed 1000rpm, 20min take supernatant
Using 0.2 micron of membrane filtration, clarified, transparent filtrate is coriander extract.
A kind of coriander flavor essence for cigarette dripping pill that embodiment 1 provides, is by the substance of following mass percent
Composition: 92.0% coriander extract, 3.0% linalool, 5.0% geranyl acetate.The raw material group of above-mentioned mass fraction
Divide and be uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains coriander flavor essence A.
The coriander flavor essence dripping that will be prepared in embodiment 1 according to existing cigarette with dripping pill preparation process using pill dripping machine
At cigarette dripping pill, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and is made
Cigarette is coriander flavor dripping pill cigarette.
A kind of coriander flavor essence for cigarette dripping pill that embodiment 2 provides, is by the substance of following mass percent
Composition: 94.2% coriander extract, 2.3% linalool, 3.5% geranyl acetate.The raw material group of above-mentioned mass fraction
Divide and be uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains coriander flavor essence B.
The coriander flavor essence dripping that will be prepared in embodiment 2 according to existing cigarette with dripping pill preparation process using pill dripping machine
At cigarette dripping pill, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and is made
Cigarette is coriander flavor dripping pill cigarette.
A kind of coriander flavor essence for cigarette dripping pill that embodiment 3 provides, is by the substance of following mass percent
Composition: 96.0% coriander extract, 2.0% linalool, 2.0% geranyl acetate.The raw material group of above-mentioned mass fraction
Divide and be uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains coriander flavor essence C.
The coriander flavor essence dripping that will be prepared in embodiment 3 according to existing cigarette with dripping pill preparation process using pill dripping machine
At cigarette dripping pill, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and is made
Cigarette is coriander flavor dripping pill cigarette.
Comparative test 1: applicant is using being currently used in dripping pill cortex cinnamomi flavor essence according to technique identical with embodiment
Cigarette dripping pill is prepared, and is existed for cortex cinnamomi flavor essence A, B, C and existing cortex cinnamomi flavor essence of the preparation in three embodiments
Knitting technology adaptive data when preparing dripping pill is detected, and the results are shown in Table 1:
Table 1 is the coriander flavor essence prepared in three embodiments and the test of existing flavor essence knitting technology suitability
As a result
Carry out the coriander flavor essence of the method preparation in the application as can be seen from Table 1 during preparing dripping pill, thereon
Machine technique suitability is more preferable.
Comparative test 2: it to coriander flavor dripping pill cigarette prepared by the embodiment of the present invention 1~3, is commented by 7 professional sense organs
Valence personnel's reference examples blank cigarette sample (same position adds blank dripping pill) compares suction evaluation.Analyses Methods for Sensory Evaluation Results is shown in
Table 2.
2 three kinds of coriander flavor dripping pill cigarette sample Analyses Methods for Sensory Evaluation Results of table
Show that the coriander flavor essence in the present invention assigns the pungent fragrant breeze for the coriander that cigarette is coordinated by smoking result in table 2
Taste feature enriches cigarette flavor, while improving the smooth sense and pleasant feeling of flue gas.
Present inventor detects for the coriander extract prepared in embodiment through physical index, and concrete outcome is such as
Under:
By the above results it can be seen that the coriander extract items physical index prepared in the present invention meets cigarette perfume
The index of material.
Coriander flavor essence for cigarette dripping pill of the present inventor for the preparation in above three embodiments
It is detected through physical index, concrete outcome is as follows:
| Project | Detected value |
| Appearance | Clarify glassy yellow oily liquids |
| Fragrance | The pungent perfume (or spice) of mellow, warm and natural coriander |
| Relative density (20/20 DEG C) | 0.9433 |
| Refraction index (20 DEG C) | 1.4536 |
| Miscible degree (25 DEG C) | It can be miscible with the ODO of arbitrary volume |
| Lead content (mg/kg) | ≤5.0 |
| Arsenic content (mg/kg) | ≤1.0 |
By testing result it can be seen that the coriander flavor essence items physics for cigarette dripping pill prepared in the present invention
Index meets the index of flavouring essence for tobacco.
Claims (4)
1. a kind of coriander flavor essence for cigarette dripping pill, it is characterised in that the coriander flavor essence is by with quality percentage
The material composition of ratio: 92.0~96.0% coriander extract, 2.0~3.0% linalool, 2.0~5.0% geranyl
Ester；
Wherein, the coriander extract is coriander seed to be crushed the coriander particle for 40~80 mesh, by it using coriander seed as raw material
6~8 times of Glycerin, mixed triester with caprylic acid capric acid is added in weight, heat reflux 1h~1.5h under conditions of 120~150 DEG C of oil bath temperature；Then
It is 150~250W/L in ultrasonic power, supersonic frequency is ultrasonically treated 10~30min under conditions of being 20~25kHz, is centrifuged later
20~30min is handled, takes supernatant to use 0.2~0.8 micron of membrane filtration, is clarified, transparent filtrate is coriander
Extract.
2. a kind of coriander flavor essence for cigarette dripping pill according to claim 1, it is characterised in that it is fragrant to state coriander flavor
Essence is by with the material composition of mass percent: 93.0~95.0% coriander extract, 2.2~2.5% linalool, 2.5
~4.8% geranyl acetate.
3. the preparation method described in a kind of claim 1 for the coriander flavor essence of cigarette dripping pill, it is characterised in that tool
Steps are as follows for body:
(1) coriander seed is crushed into the coriander particle for 40~80 mesh, the Glycerin, mixed triester with caprylic acid capric acid of 6~8 times of amounts is added by weight,
Heat reflux 1h~1.5h under conditions of 120~150 DEG C of oil bath temperature；
(2) material of hot reflow treatment in step (1) is subjected to 10~30min of ultrasonic treatment, ultrasonic power is 150~250W/
L, supersonic frequency are 20~25kHz；
(3) material after ultrasonic treatment in step (2) is subjected to centrifugal treating, 500~2000rpm of revolving speed, the processing time is 20
~30min takes supernatant to use 0.2~0.8 micron of membrane filtration, is clarified, transparent filtrate is coriander extract；
(4) prepare raw material: 92.0~96.0% coriander extract, 2.0~3.0% virtue according to following mass percent formula
Camphor tree alcohol, 2.0~5.0% geranyl acetate；The raw material components of above-mentioned mass fraction are uniformly mixed stirring 1~3 hour, then
Coriander flavor essence is obtained after standing 24~48 hours.
4. the application described in a kind of claims 1 or 2 for the coriander flavor essence of cigarette dripping pill, it is characterised in that: will
Above-mentioned coriander flavor essence is added in the essence tank of pill dripping machine, regulates essence pump discharge, then be placed in pill dripping machine rubber cement tank
In dripping pill lapping and be placed in contain ball device in curing agent according to the preparation process of existing cigarette dripping pill be made weight be 3
~10mg, crushing strength are 0.3kPa~2.0kPa, and diameter is the cigarette dripping pill of 2~5mm；In cigarette filter wire-beam forming process
In, the cigarette dripping pill positioning of preparation is applied in filter rod, and cigarette is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811563889.9A CN109439437A (en) | 2018-12-20 | 2018-12-20 | A kind of coriander flavor essence and its preparation method and application for cigarette dripping pill |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811563889.9A CN109439437A (en) | 2018-12-20 | 2018-12-20 | A kind of coriander flavor essence and its preparation method and application for cigarette dripping pill |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109439437A true CN109439437A (en) | 2019-03-08 |
Family
ID=65560176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811563889.9A Withdrawn CN109439437A (en) | 2018-12-20 | 2018-12-20 | A kind of coriander flavor essence and its preparation method and application for cigarette dripping pill |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109439437A (en) |
-
2018
- 2018-12-20 CN CN201811563889.9A patent/CN109439437A/en not_active Withdrawn
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