CN109439438A - A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill - Google Patents

A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill Download PDF

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Publication number
CN109439438A
CN109439438A CN201811563896.9A CN201811563896A CN109439438A CN 109439438 A CN109439438 A CN 109439438A CN 201811563896 A CN201811563896 A CN 201811563896A CN 109439438 A CN109439438 A CN 109439438A
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CN
China
Prior art keywords
cocoa
cigarette
dripping pill
essence
flavor essence
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201811563896.9A
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Chinese (zh)
Inventor
赵国豪
刘剑峰
王娜
马舒翼
赵同林
潘婷婷
彭建
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Priority to CN201811563896.9A priority Critical patent/CN109439438A/en
Publication of CN109439438A publication Critical patent/CN109439438A/en
Withdrawn legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/28Treatment of tobacco products or tobacco substitutes by chemical substances
    • A24B15/30Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
    • A24B15/302Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/02Recovery or refining of essential oils from raw materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Toxicology (AREA)
  • General Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Fats And Perfumes (AREA)

Abstract

A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill provided by the invention.The cocoa flavor essence be by 94.0~97.5% cocoa extract, 0.5~1.0% isodihydrolavandulal and 2.0~5.0% ethyl laurate.The cocoa extract is using cocoa power as raw material, the Glycerin, mixed triester with caprylic acid capric acid of 8~10 times of its weight is added, in 120~150 DEG C of condition heat reflux 2h~2.5h of oil bath temperature, row centrifuging and taking supernatant is obtained using 0.2~0.8 micron of membrane filtration after being then ultrasonically treated 30~60min.Cocoa flavor essence provided by the invention has preferable technique suitability, improves the production efficiency of cocoa flavor cigarette dripping pill and yield rate, reduces its production cost;It is easy in cigarette application, enriches cigarette flavor, assigns cigarette characteristic flavor on basis.

Description

A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill
Technical field
The present invention relates to technical field of cigarette flavors, in particular to a kind of cocoa flavor essence for cigarette dripping pill And its application.
Background technique
As cigarette consumption demand is gradually from type, enjoying type is met to novel sex reversal, the demand to cigarette is by past list One sucks hobby, gradually forms a variety of demands such as healthy, safe and environment-friendly, consumer not only focuses on the comfort of cigarette smoking With pleasant sexual experience, and with the raising of cigarette consumption structure, consumer is in terms of the novelty of cigarette, specificity, otherness Demand further enhance.
Compared with traditional cigarette flavoring technology, cigarette is to inhale not by burning in abundant cigarette with the essence that dripping pill adds It is small on the influence of cigarette entirety comfortable taste while food taste, imparting cigarette characteristic flavor on basis, it can also be achieved in smoking property of cigarette mistake What fragrance discharged in journey is artificial controllable.Meanwhile cigarette improves the experience of consumer from more sense organ dimensions such as tactile, the sense of hearing with dripping pill Sense.Cigarette is in the gesture of accelerated development with application of the dripping pill flavoring in cigarette in recent years, becomes and pulls cigarette quality, sales volume and structure The bright spot of promotion.
In the prior art, cigarette is common due to more or less having the flavor deployments such as alcohol, propylene glycol and water with dripping pill essence Solvent, technique suitability is relatively low, causes that cigarette dripping pill production efficiency is relatively low, yield rate is relatively low, production cost is universal higher etc. Problem more or less constrains the further application and development of cigarette dripping pill.Therefore, it is necessary to from improve cigarette dripping pill essence technique Suitability is started with, and the new technology of cigarette dripping pill flavor deployment is developed.
Summary of the invention
The cocoa flavor essence and its preparation method and application that it is an object of that present invention to provide a kind of for cigarette dripping pill, should Flavor of raw material not spirituosity, propylene glycol and water equal solvent, while abundant smoking property of cigarette taste, assigning cigarette characteristic flavor on basis, With preferable technique suitability, improves the production efficiency of cocoa flavor cigarette dripping pill and yield rate, reduce its production cost.
The present invention is achieved through the following technical solutions: a kind of cocoa flavor essence for cigarette dripping pill, Be characterized in that the cocoa flavor essence is by the material composition of following mass percent: 94.0~97.5% can extract Object, 0.5~1.0% isodihydrolavandulal, 2.0~5.0% ethyl laurate;The gross mass percentage of above-mentioned substance is 100%;Its Described in cocoa extract be the Glycerin, mixed triester with caprylic acid capric acid of 8~10 times of its weight to be added, in oil bath temperature using cocoa power as raw material 120~150 DEG C of condition heat flow back 2h~2.5h, are then 150~250W/L in ultrasonic power by it, and supersonic frequency is 20~ The condition of 25kHz handles row 20~30min of centrifugal treating after 30~60min, and supernatant is taken to use 0.2~0.8 micron of filter membrane Filtering, is clarified, transparent filtrate is cocoa extract.
The present invention preferably technical solution: the cocoa flavor essence is by the material composition of following mass percent: 95.0~96.0% cocoa extract, 0.8~1.0% isodihydrolavandulal, 3.0~4.2% ethyl laurate.
A kind of preparation method of cocoa flavor essence for cigarette dripping pill provided by the invention, it is characterised in that specific step It is rapid as follows:
(1) cocoa power is taken, 8~10 times of Glycerin, mixed triester with caprylic acid capric acid is added by its weight, then in oil bath temperature 120~150 DEG C condition heat flows back 2h~2.5h;
(2) by after hot reflow treatment in step (1) material be ultrasonically treated 30~60min, ultrasonic power be 150~ 250W/L, supersonic frequency are 20~25kHz;
(3) take supernatant using 0.2~0.8 micron after the material after ultrasonic treatment in step (2) being carried out centrifugal treating Membrane filtration, clarified, transparent filtrate is cocoa extract;
(4) prepare raw material according to the formula of following mass percent: 94.0~97.5% cocoa extract, 0.5~ 1.0% isodihydrolavandulal, 2.0~5.0% ethyl laurate;And the raw material components of above-mentioned mass fraction are uniformly mixed stirring 1 It~3 hours, is then allowed to stand after 24~48 hours and obtains cocoa flavor essence.
The present invention preferably technical solution: 500~2000rpm of revolving speed of centrifugal treating, centrifugal treating in the step (3) 20~30min of time.
A kind of application of cocoa flavor essence for cigarette dripping pill provided by the invention, it is characterised in that: by it is above-mentioned can Can flavor essence be added in the essence tank of pill dripping machine, regulate essence pump discharge, then with the drop that is placed in pill dripping machine rubber cement tank It is 3~10mg that weight, which is made, according to the preparation process of dripping pill in ball lapping and the curing agent being placed in Sheng ball device, and crushing is strong Degree is 0.3kPa~2.0kPa, and diameter is the cigarette dripping pill of 2~5mm;During cigarette filter wire-beam forming, by the cigarette of preparation It is applied in filter rod with dripping pill positioning, and cigarette is made.
The cocoa power is commercially available common natural pure cocoa power, and Glycerin, mixed triester with caprylic acid capric acid, isodihydrolavandulal, ethyl laurate are commercially available Conventional food additive.
Cocoa flavor essence in the present invention selects cocoa extract as cocoa flavor main body and basis, assigns cocoa wind Natural cocoa is fragrant with mellow for taste essence;It selects isodihydrolavandulal to modify, increases the intensity of cocoa flavor;Select ethyl laurate Make further to increase the mellow and full sense of cocoa flavor with conjunction and coordination.The cocoa flavor essence assigns the cocoa wind that cigarette is coordinated Taste feature enriches cigarette flavor, while promoting the smooth sense and pleasant feeling of flue gas.
The present invention is compared with prior art: more or less having wine for the flavor essence of cigarette dripping pill in the prior art The flavor deployments common solvents such as essence, propylene glycol and water, and the alcohol, propylene glycol and water equal size in flavor essence directly affect drop The molding of ball dripping, the more low then dripping pill dripping molding effect of alcohol, propylene glycol and water equal size in flavor essence is better, yield rate It is higher.Body material used in cocoa flavor essence in the present invention is the cocoa extract that Glycerin, mixed triester with caprylic acid capric acid directly extracts, Not spirituosity, propylene glycol and water, not spirituosity, propylene glycol and the water, and institute such as other related component isodihydrolavandulals and ethyl laurate The not additional alcohol of cocoa flavor essence, propylene glycol and water equal solvent are stated, therefore, the cocoa flavor essence is in cigarette dripping pill dripping Technique suitability is good in forming process, easily package pelletization, and cracky, production are not stablized, and dripping yield rate improves 20~30%, has Effect reduces cigarette dripping pill production cost.
A kind of cocoa flavor essence for cigarette dripping pill provided by the invention has preferable technique suitability, improves The production efficiency and yield rate of cocoa flavor cigarette dripping pill reduce its production cost;It is easy in cigarette application, enriches volume Cigarette perfume gas assigns cigarette characteristic flavor on basis.Therefore, the present invention has very strong practicability and application value.
Specific embodiment
Explanation is further explained to the present invention below with reference to embodiment.
Cocoa extract employed in following embodiments, prepares as follows:
(1) cocoa power of constant weight is weighed, 8 times of amount (weight ratio) Glycerin, mixed triester with caprylic acid capric acid (ODO) are added by weight, 120 DEG C of condition heat reflux 2.5h of oil bath temperature;
(2) material in step (1) is subjected to ultrasonic treatment 30min, ultrasonic power 150W/L, supersonic frequency 20kHz;
(3) material after ultrasonic treatment in step (2) is subjected to centrifugal treating, revolving speed 1000rpm, 20min take supernatant Liquid.The membrane filtration that supernatant is used to 0.2 micron, is clarified, transparent filtrate is cocoa extract.
A kind of cocoa flavor essence for cigarette dripping pill that embodiment 1 provides, specifically by following mass percent Material composition: 94.0% cocoa extract, 1.0% isodihydrolavandulal, 5.0% ethyl laurate.The original of above-mentioned mass fraction Expect that component is uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains cocoa flavor essence A.
The cocoa flavor essence A drop that will be prepared in embodiment 1 according to existing cigarette with dripping pill preparation process using pill dripping machine Cigarette dripping pill is made, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and makes It is cocoa flavor dripping pill cigarette at cigarette.
A kind of cocoa flavor essence for cigarette dripping pill that embodiment 2 provides, specifically by following mass percent Material composition: 95.0% cocoa extract, 0.8% isodihydrolavandulal, 4.2% ethyl laurate.The original of above-mentioned mass fraction Expect that component is uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains cocoa flavor essence B.
The cocoa flavor essence B drop that will be prepared in embodiment 2 according to existing cigarette with dripping pill preparation process using pill dripping machine Cigarette dripping pill is made, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and makes It is cocoa flavor dripping pill cigarette at cigarette.
A kind of cocoa flavor essence for cigarette dripping pill that embodiment 3 provides, specifically by following mass percent Material composition: 97.0% cocoa extract, 0.6% isodihydrolavandulal, 2.4% ethyl laurate.The original of above-mentioned mass fraction Expect that component is uniformly mixed stirring 2 hours, is then allowed to stand after 48 hours and obtains cocoa flavor essence C.
The cocoa flavor essence C drop that will be prepared in embodiment 3 according to existing cigarette with dripping pill preparation process using pill dripping machine Cigarette dripping pill is made, by existing filter stick production technology, positioning applies cigarette dripping pill during cigarette filter rod wire-beam forming, and makes It is cocoa flavor dripping pill cigarette at cigarette.
Comparative test 1: applicant is using being currently used in dripping pill cocoa flavor essence according to technique identical with embodiment Cigarette dripping pill is prepared, and is existed for cocoa flavor essence A, B, C and existing cocoa flavor essence of the preparation in three embodiments Knitting technology adaptive data when preparing dripping pill is detected, and the results are shown in Table 1:
Table 1 is the cocoa flavor essence prepared in three embodiments and the test of existing flavor essence knitting technology suitability As a result
Carry out the cocoa flavor essence of the method preparation in the application as can be seen from Table 1 during preparing dripping pill, thereon Machine technique suitability is more preferable.
Comparative test 2: it to cocoa flavor dripping pill cigarette prepared by the embodiment of the present invention 1~3, is commented by 7 professional sense organs Valence personnel's reference examples blank cigarette sample (same position adds blank dripping pill) compares suction evaluation.Analyses Methods for Sensory Evaluation Results is shown in Table 2.
2 three kinds of cocoa flavor dripping pill cigarette sample Analyses Methods for Sensory Evaluation Results of table
It is special to show that the cocoa flavor essence in the present invention assigns the cocoa Flavor that cigarette is coordinated by smoking result in table 2 Sign, enriches cigarette flavor, while improving the smooth sense and pleasant feeling of flue gas.
Present inventor carries out physical index detection, detection for the cocoa extract prepared in above-described embodiment Concrete outcome is as follows:
By the above results as can be seen that cocoa extract items physical index prepared by the present invention meets tobacco aromaticss Index.
Present inventor carries out physical index detection for the above-mentioned cocoa flavor essence for cigarette dripping pill, specifically As a result as follows:
Project Detected value
Appearance Clarify glassy yellow oily liquids
Fragrance Mellow, mellow and full and natural cocoa is fragrant
Relative density (20/20 DEG C) 0.9435
Refraction index (20 DEG C) 1.4540
Miscible degree (25 DEG C) It can be miscible with the ODO of arbitrary volume
Lead content (mg/kg) ≤5.0
Arsenic content (mg/kg) ≤1.0
Above-mentioned physical index meets the index of flavouring essence for tobacco.

Claims (5)

1. a kind of cocoa flavor essence for cigarette dripping pill, it is characterised in that the cocoa flavor essence is by following quality hundred Divide the material composition of ratio: 94.0~97.5% cocoa extract, 0.5~1.0% isodihydrolavandulal, 2.0~5.0% lauric acid Ethyl ester;
Wherein the cocoa extract is the Glycerin, mixed triester with caprylic acid capric acid of 8~10 times of its weight to be added, in oil bath using cocoa power as raw material Then it is 150~250W/L, supersonic frequency 20 in ultrasonic power by 120~150 DEG C of condition heat reflux 2h~2.5h of temperature The condition of~25kHz handles row 20~30min of centrifugal treating after 30~60min, and supernatant is taken to use 0.2~0.8 micron of filter Film filtering, is clarified, transparent filtrate is cocoa extract.
2. a kind of cocoa flavor essence for cigarette dripping pill according to claim 1, it is characterised in that the cocoa wind Taste essence is by the material composition of following mass percent: 95.0~96.0% cocoa extract, 0.8~1.0% cocoa Aldehyde, 3.0~4.2% ethyl laurate.
3. the preparation method described in a kind of claim 1 for the cocoa flavor essence of cigarette dripping pill, it is characterised in that tool Steps are as follows for body:
(1) cocoa power is taken, 8~10 times of Glycerin, mixed triester with caprylic acid capric acid is added by its weight, then in 120~150 DEG C of items of oil bath temperature Part heat reflux 2h~2.5h;
(2) material after hot reflow treatment in step (1) is ultrasonically treated 30~60min, ultrasonic power is 150~250W/ L, supersonic frequency are 20~25kHz;
(3) filter that supernatant will be taken to use 0.2~0.8 micron after the material progress centrifugal treating after ultrasonic treatment in step (2) Film filtering, is clarified, transparent filtrate is cocoa extract;
(4) prepare raw material according to the formula of following mass percent: 94.0~97.5% cocoa extract, 0.5~1.0% Isodihydrolavandulal, 2.0~5.0% ethyl laurate;And the raw material components of above-mentioned mass fraction are uniformly mixed stirring 1~3 hour, It is then allowed to stand after 24~48 hours and obtains cocoa flavor essence.
4. a kind of preparation method of cocoa flavor essence for cigarette dripping pill according to claim 3, it is characterised in that: 500~2000rpm of revolving speed of centrifugal treating, 20~30min of centrifugal treating time in the step (3).
5. the application described in a kind of claims 1 or 2 for the cocoa flavor essence of cigarette dripping pill, it is characterised in that: will Above-mentioned cocoa flavor essence is added in the essence tank of pill dripping machine, regulates essence pump discharge, then be placed in pill dripping machine rubber cement tank In dripping pill lapping and be placed in contain ball device in curing agent according to the preparation process of dripping pill be made weight be 3~10mg, Crushing strength is 0.3kPa~2.0kPa, and diameter is the cigarette dripping pill of 2~5mm;During cigarette filter wire-beam forming, it will make Standby cigarette dripping pill positioning is applied in filter rod, and cigarette is made.
CN201811563896.9A 2018-12-20 2018-12-20 A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill Withdrawn CN109439438A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201811563896.9A CN109439438A (en) 2018-12-20 2018-12-20 A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201811563896.9A CN109439438A (en) 2018-12-20 2018-12-20 A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill

Publications (1)

Publication Number Publication Date
CN109439438A true CN109439438A (en) 2019-03-08

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CN201811563896.9A Withdrawn CN109439438A (en) 2018-12-20 2018-12-20 A kind of cocoa flavor essence and its preparation method and application for cigarette dripping pill

Country Status (1)

Country Link
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Application publication date: 20190308