CN109431871A - A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application - Google Patents
A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application Download PDFInfo
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- CN109431871A CN109431871A CN201811590727.4A CN201811590727A CN109431871A CN 109431871 A CN109431871 A CN 109431871A CN 201811590727 A CN201811590727 A CN 201811590727A CN 109431871 A CN109431871 A CN 109431871A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/732—Starch; Amylose; Amylopectin; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/738—Cyclodextrins
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application, preparation, the preparation of mixed solution B, the preparation of mixed solution C, the preparation of emulsifier solution D and pressure regulation and homogenizing step including mixture A.The present invention is directed to the limitation of menthol and borneol, and other cool taste products is selected to substitute.But other cool taste products, on the skin in use, can also face cool feeling looks into the phenomenon slow with cool feeling, then, for the problem that cool feeling is slow, we have started Study on compatibility, and so that the molecule of each monomer is dissolved into single molecule level as far as possible using homogeneous technology.Keep the unimolecule of each monomer more easily affine with skin using emulsifier simultaneously, ultimately forms product of the invention.When this product is used on the skin, not only cool feeling works quickly, and has prolonged refrigerant sense, even if washing off after smearing, cool feeling still can be continued for an extended period of time, this is that freshener product used in existing cool cream product is incomparable.
Description
Technical field
The present invention relates to a kind of preparation methods of long-acting refrigerant preparation for making an addition to the cool cream of external application, belong to flavors and fragrances processing
Technical field.
Background technique
Cool cream with cooling effect is a kind of common type in cosmetics, in addition to containing having drug effect to skin in cool cream
Ingredient outside, can also add some fresheners makes it feel more comfortable in use.Publication No. CN106692450A
Patent of invention disclose a kind of purple ice cold cream, be made of the raw material of following parts by weight: 110-140 parts of Asian puccoon, Radix Angelicae Sinensis 35-
40 parts, 35-40 parts of radix saposhnikoviae, 35-40 parts of radix rehmanniae recen, 35-40 parts of the root of Dahurain angelica, 35-40 parts of peppermint, 60-65 parts of camphor, cortex cinnamomi 35-40
Part, 35-40 parts of cloves, 1200-2400 parts of macadamia nut oil, 1200-2400 parts of sunflower oil, 50-150 parts of beeswax and borneol 2-10
Part.L-menthol and borneol are added in the patent application as freshener.Application No. is 201710140289.0, " one kind, which has, relaxes
Delay the beautiful millettia root cold cream of refrigerant function " patent application in use peppermint oil as freshener；Application No. is
Use peppermint and borneol as clear in the patent application of 201710460352.9 " a kind of to treat the bald external application cold cream of pillow for baby "
Cool dose.
L-menthol, peppermint oil used in conventional formulation and borneol have its limitation because they all have it is very strong
Volatility, and all there is very strong irritation taste, especially borneol very poor with other flavors and fragrances compatibilities can be shown
Apparent Chinese medicine taste, makes one not like.Simultaneously as their volatility feature, make its cool feeling duration on the skin
It is very short.Furthermore menthol and borneol are difficult to show its cool feeling in the environment of no water.Once and peppermint and borneol are in skin
When showing cool feeling on skin, a kind of feeling that cold air is bored into skin is had, it is very uncomfortable.
Summary of the invention
The purpose of the present invention is to provide a kind of preparation methods of long-acting refrigerant preparation for making an addition to the cool cream of external application.
In order to achieve the above objects and other related objects, present invention provide the technical scheme that one kind to make an addition to external application cool
The preparation method of the long-acting refrigerant preparation of cream, the preparation of preparation, mixed solution B including mixture A, the preparation of mixed solution C,
The preparation and pressure regulation of emulsifier solution D and homogenizing step；
The preparation of the mixture A includes: by coolant agent WS-23,0- of the l-menthol of 25-75 parts by weight, 0-75 parts by weight
After the coolant agent WS-5 mixing of coolant agent WS-3,0-75 parts by weight of 75 parts by weight, under the conditions of 40 ~ 50 DEG C, stirs evenly, obtain
To mixture A；
The preparation of the mixed solution B includes: by the coolant agent WS- without terpene peppermint oil and 30-70 parts by weight of 30-70 parts by weight
10 mixing, obtain mixed solution B after mixing evenly；
The preparation of the mixed solution C includes: by the peppermint glycerol acetonide of mixed solution B, 25-75 parts by weight of 25-75 parts by weight
Ketone mixing, obtains mixed solution C after mixing evenly；
The preparation of the emulsifier solution D includes: by the octene of the hydroxypropylβ-cyclodextrin of 8-17 parts by weight, 15-18 parts by weight
Base succinic acid starch ester, the propylene glycol of 45-50 parts by weight, ten polyglycereol monolaurates of 15-28 parts by weight are uniformly mixed,
Temperature is 40-50 DEG C, ultrasonic frequency 25-35KHz, power density 0.35-0.45w/cm2Under conditions of, 1-3h is handled,
Then 1-5h is kept the temperature under the conditions of 45-55 DEG C, obtains emulsifier solution D；
The pressure regulation and homogeneous include: by the mixed solution C of mixture A, 30-70 parts by weight of 30-70 parts by weight and 3-10 weight
The emulsifier solution D mixing for measuring part, is put into planetary mixer, under the conditions of 38-42 DEG C, stirs evenly completion allotment, so
Material after allotment uses to the pressure homogeneous of 30-40Mpa afterwards, circular treatment 3-5 times is to get to the length for making an addition to the cool cream of external application
Imitate refrigerant preparation.
Preferred technical solution are as follows: the coolant agent WS-23 is N, 2,3- trimethyl -2- butanamide；It is described cool
Taste agent WS-3 is N- ethyl -2- isopropyl -5- methyl-cyclohexyl alkane formamide；The coolant agent WS-5 is N- (carbethoxyl group first
Base)-to alkane -3- formamide.
Preferred technical solution are as follows: the coolant agent WS-10 is menthoxy propylene glycol.
Preferred technical solution are as follows: the main shaft speed of agitator of the planetary mixer is 80-120r/min, when stir process
Between be 15-25min.
Since above-mentioned technical proposal is used, the present invention has the advantage, that compared with prior art
In view of the shortcomings of the prior art, the present invention is directed to the limitation of menthol and borneol, and other cool taste products is selected to replace
Generation.But other cool taste products are on the skin in use, can also face cool feeling looks into the phenomenon slow with cool feeling, then, for
The slow problem of cool feeling, we have started Study on compatibility, and dissolve the molecule of each monomer as far as possible using homogeneous technology
At single molecule level.Keep the unimolecule of each monomer more easily affine with skin using emulsifier simultaneously, ultimately forms of the invention
Product.When this product is used on the skin, not only cool feeling works quickly, and has prolonged refrigerant sense, even if after smearing
It washes off, cool feeling still can continue for an extended period of time, this is that freshener product used in existing cool cream product is incomparable.
Specific embodiment
Embodiments of the present invention are illustrated by particular specific embodiment below, those skilled in the art can be by this implementation
Content disclosed by example is understood other advantages and efficacy of the present invention easily.
The purpose of term used herein, which is only that, illustrates particular embodiment, it is not intended to be limited to the present invention.It removes
Non- context is explicitly shown, otherwise singular " one " used herein, "one" also include plural form.
When illustrating preferred embodiment, it is potentially based on clear purpose and uses special term；However, this specification institute
Revealer is not intended to be limited in the selected special term；And it is to be understood that each particular element includes having
Identical function, all equivalence techniques for operating in a similar manner and reaching similar effects.
A kind of embodiment one: preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application
A kind of long-acting refrigerant preparation and preparation method thereof making an addition to the cool cream of external application, includes the following steps.
(1) mixture A is prepared
By the l-menthol of 50 parts by weight, the coolant agent WS-23 of 32 parts by weight, the coolant agent WS-3 of 33 parts by weight, 33 parts by weight
Coolant agent WS-5, mix, under the conditions of temperature 45 C, stir in proportion, obtain mixture A.
The coolant agent WS-23, i.e. n,2,3-trimethyl-2-isopropylbutanamide；Coolant agent WS-3, i.e. N- ethyl-
2- isopropyl -5- methyl-cyclohexyl alkane formamide；Coolant agent WS-5, i.e. N- (ethoxycarbonylmethyl group)-are to alkane -3- formamide.
(2) mixed solution B is prepared
By the coolant agent WS-10 without terpene Peppermint Oil 50 parts by weight of 50 parts by weight, mixes, stir in proportion, obtain
Mixed solution B.
The coolant agent WS-10, i.e. menthoxy propylene glycol.
(3) mixed solution C is prepared
It by the Frescolat MGA of the mixed liquid B of 50 parts by weight, 50 parts by weight, mixes, stirs in proportion, mixed
Close solution C.
(4) emulsifier solution D is prepared
By the hydroxypropylβ-cyclodextrin of 12.5 parts by weight, the starch octenyl succinate anhydride of 16.5 parts by weight, 47.5 parts by weight
Ten polyglycereol monolaurates of propylene glycol, 22 parts by weight, mix in proportion, in temperature 45 C, ultrasonic frequency 25-
35KHz, power density 0.4w/cm2Under the conditions of, 2h is handled, then 3h is kept the temperature under the conditions of 50 DEG C of temperature, obtains emulsifier solution
D。
(5) allotment and homogeneous
By 50 parts of mixture A, 50 parts of mixed solution Cs, 6 parts of emulsifier solution D, mixes in proportion, be put into the closed of controllable temperature
In formula planetary mixer, temperature control is 40 DEG C, and main shaft speed of agitator is 100r/min, stir process 20min, so that material is mixed
It closes uniformly, completes allotment.Material after allotment is high-pressure homogeneous using 5Mpa, and circular treatment 4 times is to get to can make an addition to external application
The long-acting refrigerant preparation of cool cream.
A kind of embodiment two: preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application
A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application, preparation, mixed solution B including mixture A
Preparation, the preparation of mixed solution C, the preparation of emulsifier solution D and pressure regulation and homogenizing step；
The preparation of the mixture A includes: by the l-menthol of 25 parts by weight, the coolant agent WS-3 of 1 parts by weight, 1 parts by weight
After coolant agent WS-5 mixing, under the conditions of 40 DEG C, stirs evenly, obtain mixture A；
The preparation of the mixed solution B includes: mixing without terpene peppermint oil and the coolant agent WS of 30 parts by weight by 30 parts by weight, is stirred
Mixed solution B is obtained after mixing uniformly；
The preparation of the mixed solution C includes: to mix the Frescolat MGA of the mixed solution B of 25 parts by weight, 25 parts by weight,
Mixed solution C is obtained after mixing evenly；
The preparation of the emulsifier solution D includes: by the octenyl succinic of the hydroxypropylβ-cyclodextrin of 8 parts by weight, 15 parts by weight
Acid-starch ester, the propylene glycol of 45 parts by weight, 15 parts by weight ten polyglycereol monolaurates be uniformly mixed, temperature be 40 DEG C,
Ultrasonic frequency is 25KHz, power density 0.35w/cm2Under conditions of, 1h is handled, then keeps the temperature 1h under the conditions of 45 DEG C,
Obtain emulsifier solution D；
The pressure regulation and homogeneous include: by the emulsification of the mixture A of 30 parts by weight, the mixed solution C of 30 parts by weight and 3 parts by weight
Agent solution D mixing, is put into planetary mixer, under the conditions of 38 DEG C, completion allotment is stirred evenly, then by the object after allotment
Material uses the pressure homogeneous of 30Mpa, and circular treatment 3 times is to get to the long-acting refrigerant preparation for making an addition to the cool cream of external application.
Preferred embodiment are as follows: the coolant agent WS-23 is N, 2,3- trimethyl -2- butanamide；It is described cool
Taste agent WS-3 is N- ethyl -2- isopropyl -5- methyl-cyclohexyl alkane formamide；The coolant agent WS-5 is N- (carbethoxyl group first
Base)-to alkane -3- formamide.
Preferred embodiment are as follows: the coolant agent WS-10 is menthoxy propylene glycol.
Preferred embodiment are as follows: the main shaft speed of agitator of the planetary mixer is 80r/min, and the stir process time is
15min。
A kind of embodiment three: preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application
A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application, preparation, mixed solution B including mixture A
Preparation, the preparation of mixed solution C, the preparation of emulsifier solution D and pressure regulation and homogenizing step；
The preparation of the mixture A includes: by the l-menthol of 75 parts by weight, the coolant agent WS-23 of 75 parts by weight, 75 parts by weight
Coolant agent WS-3,75 parts by weight coolant agent WS-5 mixing after, under the conditions of 50 DEG C, stir evenly, obtain mixture A；
The preparation of the mixed solution B includes: to mix the coolant agent WS-10 without terpene peppermint oil and 70 parts by weight of 70 parts by weight
It closes, obtains mixed solution B after mixing evenly；
The preparation of the mixed solution C includes: to mix the Frescolat MGA of the mixed solution B of 75 parts by weight, 75 parts by weight,
Mixed solution C is obtained after mixing evenly；
The preparation of the emulsifier solution D includes: by the octenyl succinic of the hydroxypropylβ-cyclodextrin of 17 parts by weight, 18 parts by weight
Acid-starch ester, the propylene glycol of 50 parts by weight, 28 parts by weight ten polyglycereol monolaurates be uniformly mixed, temperature be 50 DEG C,
Ultrasonic frequency is 35KHz, power density 0.45w/cm2Under conditions of, 3h is handled, then keeps the temperature 5h under the conditions of 55 DEG C,
Obtain emulsifier solution D；
The pressure regulation and homogeneous include: by the cream of the mixture A of 70 parts by weight, the mixed solution C of 70 parts by weight and 10 parts by weight
The mixing of agent solution D, is put into planetary mixer, under the conditions of 42 DEG C, stirs evenly completion allotment, then will be after allotment
Material uses the pressure homogeneous of 40Mpa, and circular treatment 5 times is to get to the long-acting refrigerant preparation for making an addition to the cool cream of external application.
Preferred embodiment are as follows: the coolant agent WS-23 is N, 2,3- trimethyl -2- butanamide；It is described cool
Taste agent WS-3 is N- ethyl -2- isopropyl -5- methyl-cyclohexyl alkane formamide；The coolant agent WS-5 is N- (carbethoxyl group first
Base)-to alkane -3- formamide.
Preferred embodiment are as follows: the coolant agent WS-10 is menthoxy propylene glycol.
Preferred embodiment are as follows: the main shaft speed of agitator of the planetary mixer is 120r/min, stir process time
For 25min.
As described above is only to be not intended to tool to explain the preferred embodiments of the invention to do any shape to the present invention
Limitation in formula should all wrap therefore all have any modification or change for making the related present invention under identical spirit
It includes in the scope that the invention is intended to protect.
Claims (4)
1. a kind of preparation method for the long-acting refrigerant preparation for making an addition to the cool cream of external application, it is characterised in that: the system including mixture A
Standby, mixed solution B preparation, the preparation of mixed solution C, the preparation of emulsifier solution D and pressure regulation and homogenizing step；
The preparation of the mixture A includes: by coolant agent WS-23,0- of the l-menthol of 25-75 parts by weight, 0-75 parts by weight
After the coolant agent WS-5 mixing of coolant agent WS-3,0-75 parts by weight of 75 parts by weight, under the conditions of 40 ~ 50 DEG C, stirs evenly, obtain
To mixture A；
The preparation of the mixed solution B includes: by the coolant agent WS- without terpene peppermint oil and 30-70 parts by weight of 30-70 parts by weight
10 mixing, obtain mixed solution B after mixing evenly；
The preparation of the mixed solution C includes: by the peppermint glycerol acetonide of mixed solution B, 25-75 parts by weight of 25-75 parts by weight
Ketone mixing, obtains mixed solution C after mixing evenly；
The preparation of the emulsifier solution D includes: by the octene of the hydroxypropylβ-cyclodextrin of 8-17 parts by weight, 15-18 parts by weight
Base succinic acid starch ester, the propylene glycol of 45-50 parts by weight, ten polyglycereol monolaurates of 15-28 parts by weight are uniformly mixed,
Temperature is 40-50 DEG C, ultrasonic frequency 25-35KHz, power density 0.35-0.45w/cm2Under conditions of, 1-3h is handled,
Then 1-5h is kept the temperature under the conditions of 45-55 DEG C, obtains emulsifier solution D；
The pressure regulation and homogeneous include: by the mixed solution C of mixture A, 30-70 parts by weight of 30-70 parts by weight and 3-10 weight
The emulsifier solution D mixing for measuring part, is put into planetary mixer, under the conditions of 38-42 DEG C, stirs evenly completion allotment, so
Material after allotment uses to the pressure homogeneous of 30-40Mpa afterwards, circular treatment 3-5 times is to get to the length for making an addition to the cool cream of external application
Imitate refrigerant preparation.
2. the preparation method of the long-acting refrigerant preparation according to claim 1 for making an addition to the cool cream of external application, it is characterised in that: institute
Stating coolant agent WS-23 is N, 2,3- trimethyl -2- butanamide；The coolant agent WS-3 is N- ethyl -2- isopropyl -5-
Methyl-cyclohexyl alkane formamide；The coolant agent WS-5 is N- (ethoxycarbonylmethyl group)-to alkane -3- formamide.
3. the preparation method of the long-acting refrigerant preparation according to claim 1 for making an addition to the cool cream of external application, it is characterised in that: institute
Stating coolant agent WS-10 is menthoxy propylene glycol.
4. the preparation method of the long-acting refrigerant preparation according to claim 1 for making an addition to the cool cream of external application, it is characterised in that: institute
The main shaft speed of agitator for stating planetary mixer is 80-120r/min, and the stir process time is 15-25min.
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| CN201811590727.4A CN109431871A (en) | 2018-12-25 | 2018-12-25 | A kind of preparation method for the long-acting refrigerant preparation making an addition to the cool cream of external application |
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| CN114681361A (en) * | 2022-04-02 | 2022-07-01 | 厦门金泰生物科技有限公司 | Ice-cold compound liquid and preparation method thereof |
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Application publication date: 20190308 |