CN109423242A - A kind of thiocarbamide/quick adhesive of amine condensation product - Google Patents

A kind of thiocarbamide/quick adhesive of amine condensation product Download PDF

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Publication number
CN109423242A
CN109423242A CN201710767368.4A CN201710767368A CN109423242A CN 109423242 A CN109423242 A CN 109423242A CN 201710767368 A CN201710767368 A CN 201710767368A CN 109423242 A CN109423242 A CN 109423242A
Authority
CN
China
Prior art keywords
thiocarbamide
condensation product
adhesive
tetraethylenepentamine
grams
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710767368.4A
Other languages
Chinese (zh)
Inventor
梁沛明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhongshan Zhi Zhi Enterprise Incubator Development Co Ltd
Original Assignee
Zhongshan Zhi Zhi Enterprise Incubator Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhongshan Zhi Zhi Enterprise Incubator Development Co Ltd filed Critical Zhongshan Zhi Zhi Enterprise Incubator Development Co Ltd
Priority to CN201710767368.4A priority Critical patent/CN109423242A/en
Publication of CN109423242A publication Critical patent/CN109423242A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G59/00Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
    • C08G59/18Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
    • C08G59/40Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the curing agents used
    • C08G59/50Amines
    • C08G59/504Amines containing an atom other than nitrogen belonging to the amine group, carbon and hydrogen
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/04Non-macromolecular additives inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/06Non-macromolecular additives organic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J163/00Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2227Oxides; Hydroxides of metals of aluminium

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Adhesives Or Adhesive Processes (AREA)
  • Epoxy Resins (AREA)

Abstract

The present invention relates to a kind of thiocarbamide/quick adhesive of amine condensation product, it include: epoxy resin 100, polysulfide rubber 20, tricresyl phosphate 10, alumina powder 50, thiocarbamide-tetraethylenepentamine condensation product 20, the preparation method of the adhesive: first by 3.8 grams of thiocarbamide, 28.4 grams of tetraethylenepentamine are reacted 1 hour at 160 DEG C in there-necked flask, obtain brownish red oily liquids, then prepare by above-mentioned formula rate.The beneficial effects of the present invention are: adhesive strength is high, good water-proof effect is environmentally protective.

Description

A kind of thiocarbamide/quick adhesive of amine condensation product
Technical field
The present invention relates to a kind of adhesive, specifically a kind of thiocarbamide/quick adhesive of amine condensation product belongs to coating class neck Domain.
Background technique
Adhesive is a kind of substance with fine bond properties.By adhesion strength and cohesive force by surface bonding company Connect the effect of object.China's adhesives industries are started in nineteen fifties, and it is high that the eighties form first production Tide.Last decade has the development advanced by leaps and bounds, and initially enters the new period of high speed development.The bonding of adhesive on the market at present Degree is all poor, and waterproof effect is also poor.
Summary of the invention
To overcome the shortcomings of the existing technology, the present invention provides a kind of thiocarbamide/quick adhesive of amine condensation product, it is strong to realize bonding Degree is high, good water-proof effect, environmentally protective purpose.
To solve prior art problem, the technical scheme adopted by the invention is that:
A kind of thiocarbamide/quick adhesive of amine condensation product, comprising: epoxy resin 100, polysulfide rubber 20, tricresyl phosphate 10, oxygen Change aluminium powder 50, thiocarbamide-tetraethylenepentamine condensation product 20.
The preparation method of the adhesive: first by 3.8 grams of thiocarbamide, 28.4 grams of tetraethylenepentamine anti-at 160 DEG C in there-necked flask It answers 1 hour, obtains brownish red oily liquids, then prepare by above-mentioned formula rate.
The beneficial effects of the present invention are: adhesive strength is high, good water-proof effect is environmentally protective.
Specific embodiment
In order to enable those skilled in the art more to understand technical solution of the present invention, below with reference to embodiment to the present invention It is further analyzed.
A kind of thiocarbamide/quick adhesive of amine condensation product, comprising: epoxy resin 100, polysulfide rubber 20, tricresyl phosphate 10, alumina powder 50, thiocarbamide-tetraethylenepentamine condensation product 20.
The preparation method of the adhesive: first by 3.8 grams of thiocarbamide, 28.4 grams of tetraethylenepentamine anti-at 160 DEG C in there-necked flask It answers 1 hour, obtains brownish red oily liquids, then prepare by above-mentioned formula rate.
Technical solution provided herein is described in detail above, embodiment used herein is to the application Principle and embodiment be expounded, the explanation of above embodiments be served only for help understand the present processes and its core Thought;At the same time, for those skilled in the art, according to the thought of the application, in specific embodiment and application range Upper there will be changes, in conclusion the contents of this specification should not be construed as limiting the present application.

Claims (1)

1. a kind of thiocarbamide/quick adhesive of amine condensation product, it is characterised in that: include: epoxy resin 100, polysulfide rubber 20, phosphoric acid Front three phenolic ester 10, alumina powder 50, thiocarbamide-tetraethylenepentamine condensation product 20;The preparation method of the adhesive: first by 3.8 grams of thiocarbamide, 28.4 grams of tetraethylenepentamine are reacted 1 hour at 160 DEG C in there-necked flask, obtain brownish red oily liquids, then press above-mentioned formula Ratio is prepared.
CN201710767368.4A 2017-08-31 2017-08-31 A kind of thiocarbamide/quick adhesive of amine condensation product Pending CN109423242A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710767368.4A CN109423242A (en) 2017-08-31 2017-08-31 A kind of thiocarbamide/quick adhesive of amine condensation product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710767368.4A CN109423242A (en) 2017-08-31 2017-08-31 A kind of thiocarbamide/quick adhesive of amine condensation product

Publications (1)

Publication Number Publication Date
CN109423242A true CN109423242A (en) 2019-03-05

Family

ID=65505088

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710767368.4A Pending CN109423242A (en) 2017-08-31 2017-08-31 A kind of thiocarbamide/quick adhesive of amine condensation product

Country Status (1)

Country Link
CN (1) CN109423242A (en)

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Legal Events

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PB01 Publication
PB01 Publication
WD01 Invention patent application deemed withdrawn after publication
WD01 Invention patent application deemed withdrawn after publication

Application publication date: 20190305