CN109381380A - A method of foot bath solution is prepared using pickled vegetable fermentation liquor - Google Patents
A method of foot bath solution is prepared using pickled vegetable fermentation liquor Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
- A61P31/04—Antibacterial agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A61Q19/00—Preparations for care of the skin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
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- C11B9/00—Essential oils; Perfumes
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- C11B9/027—Recovery of volatiles by distillation or stripping
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Abstract
The invention belongs to field of health care products, specially a kind of foot bath solution containing industrial pickled vegetable fermentation liquor.Industrial pickled vegetable fermentation liquor is salt marsh treatment fluid, preparation step after processing are as follows: 1) precipitates coarse filtration: by fermenting-ripening, salinity is that the salted vegetable water of 10-15% is collected in adjusting sedimentation basin, after staticly settling, coarse filtration is carried out to its supernatant, it is thick to consider mesh diameter 0.15mm, the wide 0.25mm of mesh；2) decoloration and deodorizing process；3) the salt marsh treatment fluid for obtaining step 2 carries out physical and chemical and sanitary inspection, determines salinity, acidity and the pH value in treatment fluid；4) according to measurement result, the salinity of salt marsh treatment fluid is adjusted by being diluted with water, and adjusts pH value, it is final to keep pH in 4.2-5.0.Pickle fermentation salt water is directly recycled by the present invention, solves the problems, such as pickles scale wastewater treatment, since material is derived from natural plants, is had no toxic side effect, and is rich in minerals and nutriment, has promoting blood circulation, moisturizing and other effects.
Description
Technical field
The invention belongs to field of health care products, specially a kind of method for preparing foot bath solution using pickled vegetable fermentation liquor.
Background technique
With the sharp increase of the market demand, pickles industry size grows stronger day by day, and the by-product that processing pickles generate also is presented
It is doubled and redoubled.Salted vegetable fermentation is the Main By product of pickles processing, in salting process, in hyperosmosis and lactic acid bacteria
Under fermentation, vegetable juice is constantly oozed out, and the salt of addition is slowly dissolved, and various biochemical reactions during which occur, and is generated a large amount of
Salted vegetable fermentation.The pickles enterprise that 1 year vegetable for processing amount is 80,000 tons, the vegetable fermentation liquid 1.6~2.0 generated every year
Ten thousand tons, since salted vegetable fermentation carries out salt recycling, handling is relatively high, so using less, pickles industry at present
Mode to salted vegetable fermentation processing is mainly: entering Sewage Biological Treatment after fermentation liquid is diluted to 1% or so salinity
System is handled, and is discharged again after processing is up to standard, is not only increased enterprise's treatment pressure of sewage, and cause the wasting of resources.
To salted vegetable fermentation processing technique but without obtaining corresponding progress, the vegetables water dilution row to high salinity is remained in
It puts the stage, not only polluted surrounding enviroment, and cause the wasting of resources.
Foot is one of the place of collaterals of human convergence, and each organ of human body has specific echo area in foot, and foot is anti-
The precious legacy that massotherapy is Chinese medical is penetrated, there are more than 3000 years traditional histories, it is by stimulating each organ of human body to exist
Corresponding acupuncture point in biped generates neural reflex, activates the function of induction mechanism, have good auxiliary curative effect, while in heat
Environment in, human body stomata decontrol, it is preferable to absorption of nutrient ingredients.Therefore people like reaching when steeping foot using foot bath solution
The effects of sterilization, skin care, treatment tinea pedis, foot odour.Foot bath solution is many kinds of, for the effect of and have nothing in common with each other.Existing market
The preferable foot bath solution of finished product foot bath solution quality of upper purchase is mostly Chinese herbal medicine decoction, and complex process is expensive, and cheap
Foot bath solution be mostly that complicated chemical substance is used to deploy, for the people of certain skin quality sensitivities, then there may be side effects.Cause
This, it is necessary to develop a kind of more natural foot bath solution.
Summary of the invention
The purpose of the present invention is in view of the above technical problems, provide a kind of side that foot bath solution is prepared using pickled vegetable fermentation liquor
Method.For natural plants, the product being prepared has no toxic side effect the raw material that the present invention uses, and is rich in minerals and nutrients
Matter has promoting blood circulation, moisturizing and other effects, and due to the antibacterial substance rich in lactic acid bacteria metabolism, has to most of bacterium and fungi
There is inhibiting effect, has effects that treat tinea pedis, preparation method is also simple and easy.
To achieve the goals above, the specific technical proposal of the invention is:
A kind of foot bath solution containing pickled vegetable fermentation liquor, containing industrial pickled vegetable fermentation liquor treated liquid in the foot bath solution,
That is salt marsh treatment fluid, wherein the preparation step of the salt marsh treatment fluid are as follows:
1) precipitate coarse filtration: by fermenting-ripening, salinity is that the salted vegetable water (industrial pickled vegetable fermentation liquor) of 10-15% is collected in
Sedimentation basin is adjusted, after staticly settling, coarse filtration is carried out to its supernatant, it is thick to consider mesh diameter 0.15mm, the wide 0.25mm of mesh, to remove
Remove bulky grain suspended impurity and remaining vegetable leaf；
2) decoloration and deodorizing process: addition chitosan in the vegetable fermentation liquid obtained is slightly considered to step 1) and is flocculated, is taken
Its supernatant, then add active carbon and carry out deodorization, obtain salt marsh treatment fluid；
3) the salt marsh treatment fluid for obtaining step 2) carries out physical and chemical and sanitary inspection, determines salinity, the acidity in treatment fluid
And pH value；
4) according to measurement result in step 3), the salinity of salt marsh treatment fluid is adjusted by being diluted with water, finally keeps salinity
For 5%-8%, the sodium hydroxide solution for adding 1mol/L adjusts pH value to obtain the final product, final to keep pH in 4.2-5.0.
Preferably, the additive amount of chitosan is the thick 0.008%-0.02 ‰ for considering and obtaining quality of fermentation broth, flocculation sedimentation
Time is 60-180min.
Preferably, the additive amount of active carbon is the thick 2%-5% for considering and obtaining quality of fermentation broth.
Preferably, the light transmittance > 80% of vegetable fermentation liquid, color is bright, without visually see particle, without fermentative smell.
Ingredient A and ingredient B, in terms of mass percentage, salt marsh treatment fluid can also be contained in above-described foot bath solution
For 85%-90%, ingredient A9%-14%, ingredient B0.5%-1%, the sum of gross mass percentage composition is 100%.
Ingredient A's the preparation method comprises the following steps: with water Fresh leaf of aloe rinsed clean, wipes crust off with disinfection blade, will be saturating
Bright aloe gel takes out, and is crushed after mixing with the water ratio of 1:1 in mass ratio with high speed disintegrator to obtain the final product.
B's the preparation method comprises the following steps: fresh fingered citron will be scraped off skin with knife be cut into strip to the ingredient, using water vapour
The way of distillation extracts the volatile oil in fingered citron, the obtained ingredient B for giving out fragrant.Vapor distillation method is extracted as routine techniques.
The positive effect of the present invention is embodied in:
(1), directly pickle fermentation salt water is recycled in the application of this hair, solves pickles scale wastewater treatment
The problem of.
(2), this method is by the amino acid being rich in vegetable fermentation liquid, organic acid, various Esters, minerals, various
Vitamin and up to 15% salt content are applied well, in addition, foot bath solution is prepared using this method, simple process,
Material is derived from natural plants, has no toxic side effect, and is rich in minerals and nutriment, and vegetable fermentation liquid is applied after treatment
In the preparation of foot bath solution, the problem of pickles enterprise wastewater discharges, but also the foot bath solution natural nutrition object prepared not only can solve
Matter is abundant, has skin care, removal and other effects.
(3), the antibacterial substance containing lactic acid bacteria metabolism in foot bath solution, it is inhibited to most of bacterium and fungi,
Have effects that treat tinea pedis.
Detailed description of the invention:
Fig. 1 is the process flow chart of foot bath solution preparation in the present invention.
Fig. 2 is use and unused foot bath solution, the skin friction power change curve different with the time.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, right With reference to embodiment
The present invention is described in further detail, but the range that this should not be interpreted as to the above-mentioned theme of the present invention is only limitted to following implementations
Example.Without departing from the idea case in the present invention described above, it according to ordinary skill knowledge and customary means, makes various
Replacement and change, should all be included within the scope of the invention.
In present specification, unless otherwise specified, expression wt%, proportionate relationship is mass ratio to %, and part also all indicates
Parts by weight；Used raw material, it is outer unless otherwise specified, it is commercial product.
Embodiment 1:
A kind of foot bath solution containing pickled vegetable fermentation liquor, the foot bath solution are that industrial pickled vegetable fermentation liquor is obtained through processing.Wherein, locate
Reason method is as follows:
(1) by fermenting-ripening, salted vegetable water that salinity is 10-15% (i.e. industry generates the pickled vegetable fermentation liquor after pickles)
It is collected in adjusting sedimentation basin, after staticly settling, coarse filtration is carried out to its supernatant, thick to consider mesh diameter 0.15mm, mesh is wide
0.25mm, to remove bulky grain suspended impurity and remaining vegetable leaf.
(2) vegetable fermentation liquid that step (1) coarse filtration obtains is decolourized, deodorizing process, i.e., is added into fermentation liquid
The chitosan of 0.01 ‰ (in terms of the quality of the vegetable fermentation liquid obtained by coarse filtration) flocculates, and flocculation sedimentation 100min takes thereon
Clear liquid, then 3% active carbon (in terms of the quality of the vegetable fermentation liquid obtained by coarse filtration) progress deodorization is added, obtain salt marsh treatment fluid.
The light transmittance of the salt marsh treatment fluid answers > 80%, and it is bright to reach color, without visually see particle, without fermentative smell.
(3) step (2) salt marsh treatment fluid obtained is subjected to every physical and chemical inspection, determines salinity in treatment fluid, acid
Degree and pH value.
(4) according to measurement result in step (3), the salinity of vegetable fermentation liquid is adjusted by being diluted with water, finally keeps salt
Degree is 6%, then by adding 1mol/L sodium hydroxide solution to adjust pH value, and final holding pH is 4.5.It stirs and evenly mixs, makes after allotment
It is standby to become salt marsh treatment fluid, the alternatively referred to as initial liquid of lavipeditum.
(5) the initial liquid of lavipeditum prepared by step (4) is packed into (it is recommended that every bag of 3000g), using irradiation after pack
Sterilization treatment is prepared into foot bath solution.
Embodiment 2:
A kind of foot bath solution containing industrial pickled vegetable fermentation liquor, containing handling the liquid after industrial pickled vegetable fermentation liquor in the foot bath solution
Body (i.e. salt marsh treatment fluid), ingredient A and ingredient B.In terms of mass percentage, salt marsh treatment fluid 85%, ingredient A14%, ingredient
B1%.It is specific the preparation method is as follows:
(1) by fermenting-ripening, salinity is that the salted vegetable water of 10-15% is collected in adjusting sedimentation basin, right after staticly settling
Its supernatant carries out coarse filtration, thick to consider mesh diameter 0.15mm, the wide 0.25mm of mesh, to remove bulky grain suspended impurity and remaining
Vegetable leaf.
(2) step (1) vegetable fermentation liquid that slightly worry obtains is decolourized, deodorizing process, is added into fermentation liquid
The chitosan of 0.02 ‰ (in terms of the quality of the vegetable fermentation liquid obtained by coarse filtration) flocculates, and flocculation sedimentation 100min takes thereon
Clear liquid, then add 5% active carbon (in terms of the quality of the vegetable fermentation liquid obtained by coarse filtration) progress deodorization.The fermented vegetable
The light transmittance of liquid answers > 80%, reaches that color is bright, without visually see particle, the salt marsh treatment fluid without fermentative smell.
(3) step (2) salt marsh treatment fluid obtained is subjected to every physical and chemical inspection, determines salinity in treatment fluid, acid
Degree and pH value.
(4) according to measurement result in step (3), the salinity of vegetable fermentation liquid is adjusted by being diluted with water, finally keeps salt
Degree is 8%, then by adding 1mol/L sodium hydroxide solution to adjust pH value, and final holding pH is 5.0.It stirs and evenly mixs, makes after allotment
It is standby to become salt marsh treatment fluid.
(5) preparation of ingredient A: with water Fresh leaf of aloe rinsed clean, crust is wiped off with disinfection blade, by transparent aloe
Gel takes out, and is crushed after mixing with the water ratio of 1:1 in mass ratio with high speed disintegrator up to ingredient A.
(6) preparation of ingredient B: skin will be scraped off by fresh fingered citron with knife and be cut into strip, using steam distillation
Extract the volatile oil in fingered citron, the obtained ingredient B for giving out fragrant.Vapor distillation method is extracted as routine techniques.
(7) salt marsh treatment fluid prepared by step (4), ingredient A and ingredient B are mixed in proportion, is then filled
Bag (it is recommended that every bag of 3000g) is handled using irradiation sterilization after pack, is prepared into foot bath solution.It is made in embodiment 1 and embodiment 2
Standby obtained foot bath solution meets physical and chemical and sanitary index:
The salinity and mild acidity of finished product foot bath solution, heavy metal substance content is qualified, no detection pesticide residue, microorganism
Clump count also complies with national standard, therefore is safe and applicable.
Content of mineral substances in finished product foot bath solution
Note: a unit is kj/100g；B unit is mg/100g；C unit is μ g/100g.
10 products of random inspection from the foot bath solution being prepared in embodiment 2, and the minerals detected contained by it contain
Amount, concrete outcome see the table below:
As seen from table, foot bath solution mineral rich content, wherein potassium and calcium content are most.Potassium is adjustable intracellular suitable
The acid-base balance of suitable osmotic pressure and body fluid participates in the metabolism of endocellular sugar and protein, it is seen that foot bath solution of the present invention, which has, lives
The effect of blood, moisturizing.
Experiment 1: foot bath solution bacteriostasis efficacy verifying
It first draws 5.0mL foot bath solution (being prepared using the method in embodiment 2) to be put into sterilized test tube, then inhales
Taking 0.1mL test bacteria liquid, (concentration is transferred to 1 × 104-9×104cfu·mL-1) be added in foot lotion sample liquid, it mixes rapidly.
And timing immediately, after effect to 30min, test organisms and sample mixed liquor 1mL are drawn, the sterilized phosphate of 5.0mL is added to
In buffer (PBS) test tube, mix well.Place 10min after, draw each 1mL of mixed liquor, be seeded in respectively 2 it is sterilized
In plane ware, with 15mL, 40 DEG C of culture medium is poured into, and rotational plane ware mixes well it, is overturn after agar solidification flat
Face ware.Foot bath solution sample liquid is replaced with PBS, by above step repetitive operation, as control sample.If test organisms is coliform
When group, Pseudomonas aeruginosa or staphylococcus aureus, culture dish is placed in 37 DEG C of insulating box and cultivates 16-18h；If test organisms is
When microsporum canis, Microsporum gypseum, alpha fungus, acrothesium floccosum or Trichophyton rubrum, culture dish is placed in
7d is cultivated in 26 DEG C of insulating box.Then the counting of viable bacteria bacterium colony is done.According to formula, bacteriostasis rate=(control sample average colony
Number-test specimen average colony number)/control sample average colony number × 100%, calculate bacteriostasis rate.Experiment is repeated 3 times, and asks it
Average value.Experimental result such as following table,
| Strain | Bacteriostasis rate |
| Microsporum canis | 99 |
| Microsporum gypseum | 97 |
| Acrothesium floccosum | 95 |
| Trichophyton rubrum | 97 |
| Alpha fungus | 99 |
| Escherichia coli | 99 |
| Pseudomonas aeruginosa | 99 |
| Staphylococcus aureus | 97 |
As seen from the above table, the foot bath solution being prepared using this programme all there is obvious inhibition to make the common flora of tinea pedis
With having effects that except tinea pedis.
Experiment 2: foot bath solution skin-care effect verifying
Select 20-50 people using foot bath solution (being prepared according to the method in embodiment 2) at random, respectively the 1st week, the 2nd
Given the test agent region and blank control region skin are measured using the measurement of skin friction force tester when week, the 3rd week, the 4th week
Friction force value.Numerical value is smaller to illustrate that skin surface frictional force is smaller, and skin is more smooth, and concrete outcome is shown in Fig. 2.
As shown in Figure 2, it compared with blank control group, is reduced using the skin friction power of foot bath solution crowd, illustrates the present invention
Foot bath solution improves skin smoothness, has effects that certain moisturizing.
Example described above is only the preferred embodiment of this patent, but the protection scope of this patent is not limited thereto.
It should be pointed out that for those skilled in the art, under the premise of not departing from this patent principle, specially according to this
The technical solution and its inventional idea of benefit, can also make several improvements and modifications, these improvements and modifications also should be regarded as this specially
Within the protection scope of benefit.
Claims (7)
1. a kind of foot bath solution containing pickled vegetable fermentation liquor, it is characterised in that after being handled in the foot bath solution containing industrial pickled vegetable fermentation liquor
Liquid, i.e. salt marsh treatment fluid, the preparation step of the salt marsh treatment fluid are as follows:
1) precipitate coarse filtration: by fermenting-ripening, salinity is that the salted vegetable water of 10-15% is collected in adjusting sedimentation basin, is staticly settled
Afterwards, coarse filtration is carried out to its supernatant, it is thick to consider mesh diameter 0.15mm, the wide 0.25mm of mesh, with remove bulky grain suspended impurity and
Remaining vegetable leaf；
2) decoloration and deodorizing process: addition chitosan in the vegetable fermentation liquid of acquisition is slightly considered to step 1) and is flocculated, is taken thereon
Clear liquid, then add active carbon and carry out deodorization, obtain salt marsh treatment fluid；
3) the salt marsh treatment fluid for obtaining step 2 carries out physical and chemical and sanitary inspection, determines salinity, acidity and the pH in treatment fluid
Value；
4) according to measurement result in step 3), the salinity of salt marsh treatment fluid is adjusted by being diluted with water, it is final to keep salinity for 5%-
8%, the sodium hydroxide solution for adding 1mol/L adjusts pH value, final to keep pH in 4.2-5.0.
2. foot bath solution as described in claim 1, it is characterised in that: the additive amount of chitosan is that thick worry obtains quality of fermentation broth
0.008%-0.02 ‰, flocculation sedimentation time are 60-180min.
3. foot bath solution as described in claim 1, it is characterised in that: the additive amount of active carbon is that thick worry obtains quality of fermentation broth
2%-5%。
4. foot bath solution as described in claim 1, it is characterised in that: the light transmittance > 80% of vegetable fermentation liquid, color is bright, nothing
Naked eyes are shown in particle, without fermentative smell.
5. the foot bath solution as described in any one of claim 1-4 claim, it is characterised in that: also contain in the foot bath solution
Ingredient A and ingredient B, in terms of mass percentage, salt marsh treatment fluid be 85%-90%, ingredient A9%-14%, ingredient B0.5%-1%, always
The sum of mass percentage is 100%.
6. foot bath solution as claimed in claim 5, it is characterised in that ingredient A's the preparation method comprises the following steps: with water Fresh leaf of aloe
Rinsed clean wipes crust off with disinfection blade, and transparent aloe gel is taken out, with water after the ratio of 1:1 mixes in mass ratio
It is crushed with high speed disintegrator to obtain the final product.
7. foot bath solution as claimed in claim 5, it is characterised in that ingredient B's the preparation method comprises the following steps: fresh fingered citron is used
Skin will be scraped off and be cut into strip by knife, extract the volatile oil in fingered citron using steam distillation, what is obtained gives out fragrant
Ingredient B.
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