CN109371499A - A kind of plant modified dacron fabric and preparation method thereof - Google Patents

A kind of plant modified dacron fabric and preparation method thereof Download PDF

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Publication number
CN109371499A
CN109371499A CN201811273783.5A CN201811273783A CN109371499A CN 109371499 A CN109371499 A CN 109371499A CN 201811273783 A CN201811273783 A CN 201811273783A CN 109371499 A CN109371499 A CN 109371499A
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Prior art keywords
modified dacron
parts
modifying agent
preparation
plant
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CN201811273783.5A
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Inventor
黄效谦
刘宇
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Zhongke Textile Research Institute (qingdao) Co Ltd
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Zhongke Textile Research Institute (qingdao) Co Ltd
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Priority to CN201811273783.5A priority Critical patent/CN109371499A/en
Publication of CN109371499A publication Critical patent/CN109371499A/en
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    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F8/00Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof
    • D01F8/04Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers
    • D01F8/14Conjugated, i.e. bi- or multicomponent, artificial filaments or the like; Manufacture thereof from synthetic polymers with at least one polyester as constituent
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/06Wet spinning methods
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/253Formation of filaments, threads, or the like with a non-circular cross section; Spinnerette packs therefor
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/09Addition of substances to the spinning solution or to the melt for making electroconductive or anti-static filaments
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • D01F1/103Agents inhibiting growth of microorganisms
    • DTEXTILES; PAPER
    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2331/00Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
    • D10B2331/04Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products polyesters, e.g. polyethylene terephthalate [PET]
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/06Load-responsive characteristics
    • D10B2401/063Load-responsive characteristics high strength
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/13Physical properties anti-allergenic or anti-bacterial
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2401/00Physical properties
    • D10B2401/16Physical properties antistatic; conductive

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Woven Fabrics (AREA)

Abstract

The present invention provides a kind of plant modified dacron fabric and preparation method thereof, and raw material includes polyester resin, acid fiber by polylactic, modifying agent, polyester resin, acid fiber by polylactic, modifying agent mass ratio be 80-100:24-27:4-4.8.Modifying agent is mixed with by plant extracts, glutathione, chitin, linseed oil according to 5:3:2:9;Plant extracts is the one or more of wormwood, peppermint, motherwort, honeysuckle.Modified dacron fabric of the present invention is suitable for fabric, lining, the shoes and hats etc. of outdoor dress ornament.

Description

A kind of plant modified dacron fabric and preparation method thereof
Technical field
The present invention relates to a kind of plant modified dacron fabrics and preparation method thereof, belong to textile technology field.
Background technique
Dacron intensity with higher and elastic recovery capability, strong durable, wash and wear.Terylene is to close fine fabric The best fabric of middle heat resistance has thermoplasticity, can manufacture accordion-pleated skirt, rivel is lasting.The light resistance of dacron is preferable, but compares Acrylic fibers are poor;Resistance to various chemicals are functional.Acid, alkali are all little to its extent of the destruction, while not being afraid of mould, are not afraid of and damage by worms.
Although polyester fabric sucting wet air permeability is bad, personal clothes are made, dress is uncomfortable.But it is used to make gym suit, account Paulin, outdoor mountain-climbing clothes, mountain-climbing packet, climbing boot etc. are still very favorite by consumer.
Most modified dacron technologies, which are all put forth effort on, in the prior art improves its comfort, enhances that it is soft, affine, ventilative, And the performances such as antibacterial, radiation protection.Such as copper ion modified terylene, silver ion modified dacron, silk gum modified dacron.
A kind of modified polyester fibre of prior art CN201710722020.3, comprising: polyester fiber ontology, silver fiber, bamboo Carbon fibe and protein fibre, wherein the polyester fiber ontology accounts for a kind of modified polyester fibre mass percent 35%-50%, the silver fiber accounts for a kind of 10%-16% of modified polyester fibre mass percent, the bamboo charcoal Fiber accounts for a kind of 20%-25% of modified polyester fibre mass percent, and the protein fibre accounts for described one kind The 20%-24% of modified polyester fibre mass percent.By the above-mentioned means, improve polyster fibre dyeing and hygroscopicity difference lack Point improves the flexibility of polyester fiber, and skin affinity, while also having radiation protection and antibacterial effect.
A kind of production technology of copper ion modified polyester staple fiber socks of prior art CN201810241886.7 is passed through Socks, margin to seam and setting process are knitted in the selection of raw material, complete the production technology of copper ion modified polyester staple fiber socks;Advantage Be: the present invention can assign the stronger gas permeability of socks, no by selecting copper ion modified polyester staple fiber in raw material Easy pilling, prolonged endurable, socks surfacing, smooth, antibacterial bacteriostatic.
A kind of silk gum modified dacron Rachael blanket of prior art CN201710952490.9, the silk gum modified dacron are drawn She Er woollen blanket is antistatic, the antibacterial dacron Rachael blanket that fiber surface is grafted with sericin, and preparation step includes that alkali subtracts Amount, elargol prepare and are modified.Polyester raschel blanket is modified using the fulmargin containing antistatic agent, obtains silk gum Modified dacron Rachael blanket has good antistatic, antibacterial and comfort property.
Rarely has pure plant modified dacron in the modified dacron fabric of the prior art, to further increase the resistance to of its face liber Photosensitiveness, mosquito repellent, insect prevention technical report.
Summary of the invention
The problem to be solved in the present invention is against the above deficiency, to provide a kind of plant modified dacron fabric and its preparation side Method, to realize following goal of the invention: making polyester fabric have preferable mosquito repellent, insect prevention performance, good light resistance is preferably suitable It closes it and is used for outdoor dress ornament, luggage, shoes and hats etc..
In order to solve the above technical problems, the technical solution adopted by the present invention is as follows:
A kind of plant modified dacron fabric, raw material include polyester resin, acid fiber by polylactic, modifying agent, polyester resin, polylactic acid Fiber, modifying agent mass ratio be 80-100:24-27:4-4.8;The modifying agent is by plant extracts, glutathione, chitin Matter, linseed oil are mixed with according to 5:3:2:9;The plant extracts is wormwood, peppermint, motherwort, honeysuckle It is one or more of.
A kind of plant modified dacron fabric, raw material further include following components: sodium alginate, lubricant, α-sorb Alcohol, oleic acid.
A kind of plant modified dacron fabric, raw material includes following components in parts by weight: 80-100 parts of polyester resin, 24-27 parts of acid fiber by polylactic, 4-4.8 parts of modifying agent, 14-17 parts of sodium alginate, 1-1.5 parts of lubricant, α -4-5 parts of sorbierite, 4-5 parts of oleic acid;
The polyester resin: fineness is 60 mesh, water content≤0.2%;
The acid fiber by polylactic: fibre number is 1.5 denier, fibre length 0.3-0.45mm;
The sodium alginate: fineness is 80 mesh, viscosity 200-300 mpa.s, moisture content 10-12%, calcium content 0.3%;
The lubricant: stearic acid vinyl ester and calcium stearate are mixed according to the mass ratio of 4:1;
The plant extracts: active principle content 96.5%, 100% logical sieves with 100 mesh sieve;
The glutathione: active principle content 98%, 100% passes through 200 meshes.
A kind of preparation method of plant modified dacron fabric, comprising the following steps:
Step 1: the preparation of modifying agent: plant extracts, glutathione, chitin, linseed oil are mixed according to 5:3:2:9, Open stirring, mixing speed 1000rpm, mixing time 1h;After stirring, mixed liquor is subjected to microwave treatment, the microwave Processing: power 250w, treatment temperature are 52 DEG C, and the processing time is 70s, and number of processes is 3 times, interval time 2min;Microwave After processing, mixed liquor is heated into 30min under the conditions of 85-89 DEG C, obtains modifying agent.
Step 2: the preparation of modified dacron master batch: polyester resin being heated to 298 DEG C, opens stirring, stirring rate is 1200rpm is added modifying agent, persistently stirs 2.5h;Then cooling is prepared into modified dacron master batch.
Step 3: the preparation of spinning solution: by modified dacron master batch and acid fiber by polylactic, sodium alginate, α-sorbierite, oleic acid Mixing, is heated to 310 DEG C, heating time 50min, stirring rate 200rpm;Lubricant is added in side stirring, side;It is melted Melt spinning solution.
Step 4: spinning
Spinning solution is imported in manifold, fiber is sprayed from the hole of spinneret, and the hole cross section of spinneret is equilateral triangle, Extrusion temperature is 257 DEG C, and subsequently into coagulating bath, coagulation bath temperature is 60-65 DEG C, the concentration of ethylene methacrylic pyridine in coagulating bath For 45-47%, internal circulating load 60-65kL/h;Obtain fibre bundle.
Step 5: drawing-off oils
It obtains fibre bundle and carries out 4 drawing-offs, draw ratio is respectively 1:1.08,1:1.21,1:1.15,1:1.05;After drawing-off, give Fibre bundle sprays finish, and it is compound that the finish is that polyethylene glycol laurate, tripalmitin are prepared with mass ratio 5:3 Finish.
Fibre bundle drying after oiling, is curled at cooling, and plant modified dacron is obtained.
Step 6: weaving
The plant modified dacron prepared using step 5 weaves fabric.
It will be put into after fabric in plasma treatment instrument, be passed through the argon gas that pressure is 32Pa and carry out plasma treatment, plasma The processing time 2 minutes.
Then determine drying and shaping, obtain plant modified dacron fabric.
The invention adopts the above technical scheme, compared with prior art, has the advantages that
(1) plant modified dacron fabric finished product of the present invention: there is apparent repelling effect, it is 90-93.5% that mosquito, which walks quickly and keeps away rate,;Water After washing 10 times, mosquito walks quickly and keeps away rate still up to 80-87%.
(2) when the addition number of modifying agent is in 3.5-4, degradation temperature is set as 55 DEG C, and intensity of illumination is set as 0.95W/m2, after irradiating 300h, strength retention is higher, especially when it is 4 that number, which is added, reach peak value, fabric fibre Strength retention is up to 85.6%.
(3) plant modified dacron fabric finished product of the present invention: there is apparent insect prevention performance, through testing, ant walks quickly and keeps away rate and reaches 95-97.2%;After washing 10 times, ant walks quickly and keeps away rate still up to 90-93%.
(4) plant modified dacron fabric finished product of the present invention: antistatic property is good, and continuous friction 500 times does not play electrostatic;It is suitable For garment material.
Polyester fabric is set to have preferable mosquito repellent, insect prevention performance, meanwhile, there is apparent wear-resisting, antistatic performance, especially Dress ornament, luggage, shoes and hats for being used suitable for outdoor sports, excursion, mountain climbing expedition etc. etc..
Specific embodiment
It should be appreciated that preferred embodiments described herein are only used to illustrate and explain the present invention, it is not used to limit this Invention.
A kind of plant modified dacron fabric of embodiment 1
Its raw material includes following components in parts by weight: 80 parts of polyester resin, 25 parts of acid fiber by polylactic, 4.4 parts of modifying agent, alginic acid 14 parts of sodium, 1 part of lubricant, 5 parts of α-sorbierite, 4.5 parts of oleic acid;
The polyester resin: fineness is 60 mesh, water content≤0.2%;
The acid fiber by polylactic: fibre number is 1.5 denier, fibre length 0.3-0.45mm;
The modifying agent is mixed with by plant extracts, glutathione, chitin, linseed oil according to 5:3:2:9.
The sodium alginate: fineness is 80 mesh, viscosity 200-300 mpa.s, moisture content 10-12%, calcium content 0.3%;
The lubricant: stearic acid vinyl ester and calcium stearate are mixed according to the mass ratio of 4:1;
The plant extracts 100% is logical to be sieved with 100 mesh sieve;The plant extracts is wormwood extract.
The glutathione: active principle content 98%, 100% passes through 200 meshes.
A kind of plant modified dacron fabric of embodiment 2
Identical with embodiment 1, only change following: the raw material of fabric includes following components in parts by weight: 90 parts of polyester resin, poly- cream 27 parts of sour fiber, 4 parts of modifying agent, 15 parts of sodium alginate, 1.4 parts of lubricant, 4 parts of α-sorbierite, 4 parts of oleic acid.
A kind of plant modified dacron fabric of embodiment 3
Identical with embodiment 1, only change following: the raw material of fabric includes following components in parts by weight: 100 parts of polyester resin gathers 24 parts of acid fiber, 4.8 parts of modifying agent, 17 parts of sodium alginate, 1.5 parts of lubricant, 4.5 parts of α-sorbierite, 5 parts of oleic acid.
A kind of preparation method of the plant modified dacron fabric of embodiment 4
According to the composition of raw materials of embodiment 1-3, follow the steps below:
Step 1: the preparation of modifying agent: plant extracts, glutathione, chitin, linseed oil are mixed according to 5:3:2:9, Open stirring, mixing speed 1000rpm, mixing time 1h;After stirring, mixed liquor is subjected to microwave treatment, the microwave Processing: power 250w, treatment temperature are 52 DEG C, and the processing time is 70s, and number of processes is 3 times, interval time 2min;Microwave After processing, mixed liquor is heated into 30min under the conditions of 85-89 DEG C, obtains modifying agent.
Step 2: the preparation of modified dacron master batch: polyester resin being heated to 298 DEG C, opens stirring, stirring rate is 1200rpm is added modifying agent, persistently stirs 2.5h;Then cooling is prepared into modified dacron master batch.
Step 3: the preparation of spinning solution: by modified dacron master batch and acid fiber by polylactic, sodium alginate, α-sorbierite, oleic acid Mixing, is heated to 310 DEG C, heating time 50min, stirring rate 200rpm;Lubricant is added in side stirring, side;It is melted Melt spinning solution.
Step 4: spinning
Spinning solution is imported in manifold, fiber is sprayed from the hole of spinneret, and the hole cross section of spinneret is equilateral triangle, Extrusion temperature is 257 DEG C, and subsequently into coagulating bath, coagulation bath temperature is 60-65 DEG C, the concentration of ethylene methacrylic pyridine in coagulating bath It is 46%, internal circulating load 60-65kL/h;Obtain fibre bundle.
Step 5: drawing-off oils
It obtains fibre bundle and carries out 4 drawing-offs, draw ratio is respectively 1:1.08,1:1.21,1:1.15,1:1.05;After drawing-off, give Fibre bundle sprays finish, and it is compound that the finish is that polyethylene glycol laurate, tripalmitin are prepared with mass ratio 5:3 Finish.
Fibre bundle drying after oiling, is curled at cooling, and plant modified dacron is obtained.
Step 6: weaving
The plant modified dacron prepared using step 5 weaves fabric.
It will be put into after fabric in plasma treatment instrument, be passed through the argon gas that pressure is 32Pa and carry out plasma treatment, plasma The processing time 2 minutes.
Then determine drying and shaping, obtain plant modified dacron fabric.
Comparative example 1
The raw material of fabric of use includes following weight parts component: identical with embodiment 1, only change following: the raw material of fabric includes Following components in parts by weight: 90 parts of polyester resin, 27 parts of acid fiber by polylactic, 4 parts of modifying agent, 15 parts of sodium alginate, lubricant 1.4 Part, 4 parts of α-sorbierite, 4 parts of oleic acid.
The modifying agent is mixed with by glutathione, chitin according to 3:2.
Preparation method: it is same as Example 4, only change following steps:
Step 1: the preparation of modifying agent: glutathione, chitin being mixed according to 3:2, open stirring, mixing speed is 1000rpm, mixing time 1h;Mixed liquor is heated into 30min under the conditions of 85-89 DEG C, obtains modifying agent.
Step 5: drawing-off oils
It obtains fibre bundle and carries out 4 drawing-offs, draw ratio is respectively 1:1.08,1:1.21,1:1.15,1:1.05;
It by fibre bundle drying, cooling, curls, obtains modified dacron.
Comparative example 2
The raw material of fabric of use includes following weight parts component: identical with embodiment 1, only change following: the raw material of fabric includes Following components in parts by weight: 90 parts of polyester resin, 27 parts of acid fiber by polylactic, 4 parts of modifying agent, 15 parts of sodium alginate, lubricant 1.4 Part, 4 parts of α-sorbierite, 4 parts of oleic acid.
The modifying agent is mixed with by plant extracts, linseed oil according to 5:9.
Preparation method: it is same as Example 4, only change following steps:
Step 1: the preparation of modifying agent: plant extracts, linseed oil being mixed according to 5:9, open stirring, mixing speed is 1000rpm, mixing time 1h;Mixed liquor is heated into 30min under the conditions of 85-89 DEG C, obtains modifying agent.
Step 5: drawing-off oils
It obtains fibre bundle and carries out 4 drawing-offs, draw ratio is respectively 1:1.08,1:1.21,1:1.15,1:1.05;
It by fibre bundle drying, cooling, curls, obtains modified dacron.
Through testing, the technical indicator testing result of embodiment 1-3 and comparative example 1-2 are shown in Table 1;
Table 1
The present invention tests the calculating to rate of walking quickly and keeping away using the meter in GB/T 28408-2012 protective clothes insect prevention standard What calculation method carried out.
Embodiment 5 is in order to further test modifying agent of the invention to the shadow of polyester fabric fiber prepared by the present invention It rings, is tested as follows:
Using the method for embodiment 2, only changes the number of the addition of modifying agent, test its influence to index of correlation of the present invention.
Test method:
Modified dacron fabric prepared by the present invention has good anti-aging property: the polyester fabric fibers of preparation is placed in always Change in testing machine, is uniformly dispersed, degradation temperature is set as 55 DEG C, and intensity of illumination is set as 0.95W/m2, after irradiating 300h, The strength retention for detecting its fiber, is specifically shown in Table 2;
Table 2
As can be seen from the above table, during the present invention prepares polyester fabric, illumination of the modifying agent of use to polyester fabric fiber Strength retention, mosquito and the rate of walking quickly and keeping away of ant have large effect, especially when the addition number of modifying agent is in 3.5-4 When, degradation temperature is set as 55 DEG C, and intensity of illumination is set as 0.95W/m2, after irradiating 300h, strength retention is higher, special It is not to reach peak value, conservation rate 85.6% when it is 4 that number, which is added,.
Unless specifically indicated, ratio of the present invention is mass ratio, and the percentage is mass percent.
Finally, it should be noted that the foregoing is only a preferred embodiment of the present invention, it is not intended to restrict the invention, Although the present invention is described in detail referring to the foregoing embodiments, for those skilled in the art, still may be used To modify the technical solutions described in the foregoing embodiments or equivalent replacement of some of the technical features. All within the spirits and principles of the present invention, any modification, equivalent replacement, improvement and so on should be included in of the invention Within protection scope.

Claims (9)

1. a kind of plant modified dacron fabric, it is characterised in that: raw material includes polyester resin, acid fiber by polylactic, modifying agent, terylene Resin, acid fiber by polylactic, modifying agent mass ratio be 80-100:24-27:4-4.8;The modifying agent is by plant extracts, paddy The sweet peptide of Guang, chitin, linseed oil are mixed with according to 5:3:2:9;The plant extracts is wormwood, peppermint, benefit mother Careless, honeysuckle one or more.
2. a kind of plant modified dacron fabric according to claim 1, it is characterised in that: its raw material further includes following groups Point: sodium alginate, lubricant, α-sorbierite, oleic acid.
3. a kind of plant modified dacron fabric according to claim 1, it is characterised in that: raw material includes following weight parts group Point: 80-100 parts of polyester resin, 24-27 parts of acid fiber by polylactic, 4-4.8 parts of modifying agent, 14-17 parts of sodium alginate, lubricant 1- 1.5 parts, α -4-5 parts of sorbierite, 4-5 parts of oleic acid.
4. a kind of plant modified dacron fabric according to claim 1, it is characterised in that:
The polyester resin: fineness is 60 mesh, water content≤0.2%;
The acid fiber by polylactic: fibre number is 1.5 denier, fibre length 0.3-0.45mm.
5. a kind of plant modified dacron fabric according to claim 1, it is characterised in that: the sodium alginate: fineness is 80 mesh, viscosity 200-300 mpa.s, moisture content 10-12%, calcium content 0.3%;
The lubricant: stearic acid vinyl ester and calcium stearate are mixed according to the mass ratio of 4:1.
6. a kind of preparation method of plant modified dacron fabric, it is characterised in that: the preparation step including modifying agent;
The preparation of the modifying agent: plant extracts, glutathione, chitin, linseed oil are mixed according to 5:3:2:9, opened Open stirring, mixing speed 1000rpm, mixing time 1h;After stirring, mixed liquor is subjected to microwave treatment, at the microwave Reason: power 250w, treatment temperature are 52 DEG C, and the processing time is 70s, and number of processes is 3 times, interval time 2min;At microwave After reason, mixed liquor is heated into 30min under the conditions of 85-89 DEG C, obtains modifying agent.
7. a kind of preparation method of plant modified dacron fabric according to claim 7, it is characterised in that: further include being modified Dacron master grain step;
The modified dacron master batch: being heated to 298 DEG C for polyester resin, opens stirring, and stirring rate 1200rpm is added Modifying agent persistently stirs 2.5h.
8. a kind of preparation method of plant modified dacron fabric according to claim 7, it is characterised in that: further include spinning The preparation step of liquid;
The preparation of the spinning solution: modified dacron master batch is mixed with acid fiber by polylactic, sodium alginate, α-sorbierite, oleic acid, It is heated to 310 DEG C, heating time 50min, stirring rate 200rpm.
9. a kind of preparation method of plant modified dacron fabric according to claim 7, it is characterised in that: further include spinning With drawing-off oiling step;
The spinning: fiber is 257 DEG C from spinneret extrusion temperature, and coagulation bath temperature is 60-65 DEG C, methyl second in coagulating bath The concentration of annulated pyridine is 45-47%, internal circulating load 60-65kL/h;
The drawing-off: pass through 4 drawing-offs, draw ratio is respectively 1:1.08,1:1.21,1:1.15,1:1.05;
Described oils: it is compound that the finish used is that polyethylene glycol laurate, tripalmitin are prepared with mass ratio 5:3 Finish.
CN201811273783.5A 2018-10-30 2018-10-30 A kind of plant modified dacron fabric and preparation method thereof Pending CN109371499A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
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CN110331461A (en) * 2019-06-10 2019-10-15 中科纺织研究院(青岛)有限公司 A kind of polyester fiber and preparation method thereof containing aloe extract
CN110592713A (en) * 2019-05-24 2019-12-20 苏州峰佳达化纤纺织有限公司 Preparation method of antibacterial polyacrylonitrile fiber
CN110735211A (en) * 2019-11-06 2020-01-31 青岛百草新材料股份有限公司 plant functional seat fabric and preparation method thereof
CN110901488A (en) * 2019-11-06 2020-03-24 青岛百草新材料股份有限公司 Plant automobile carpet and preparation method thereof
CN111172613A (en) * 2020-03-03 2020-05-19 百事基材料(青岛)股份有限公司 Terylene staple fiber containing mint extract and preparation method thereof
CN112442782A (en) * 2020-11-19 2021-03-05 绍兴市千岩里纺织品有限公司 Polylactic acid fiber fabric

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CN105671964A (en) * 2016-02-25 2016-06-15 苏州三和开泰花线织造有限公司 Preparation method of oiling agent for polyester spinning
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CN110592713A (en) * 2019-05-24 2019-12-20 苏州峰佳达化纤纺织有限公司 Preparation method of antibacterial polyacrylonitrile fiber
CN110331461A (en) * 2019-06-10 2019-10-15 中科纺织研究院(青岛)有限公司 A kind of polyester fiber and preparation method thereof containing aloe extract
CN110735211A (en) * 2019-11-06 2020-01-31 青岛百草新材料股份有限公司 plant functional seat fabric and preparation method thereof
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CN112442782A (en) * 2020-11-19 2021-03-05 绍兴市千岩里纺织品有限公司 Polylactic acid fiber fabric

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Application publication date: 20190222