CN109330966A - A kind of whitening mask liquid and preparation method thereof - Google Patents
A kind of whitening mask liquid and preparation method thereof Download PDFInfo
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- CN109330966A CN109330966A CN201811337202.XA CN201811337202A CN109330966A CN 109330966 A CN109330966 A CN 109330966A CN 201811337202 A CN201811337202 A CN 201811337202A CN 109330966 A CN109330966 A CN 109330966A
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/673—Vitamin B group
- A61K8/675—Vitamin B3 or vitamin B3 active, e.g. nicotinamide, nicotinic acid, nicotinyl aldehyde
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/986—Milk; Derivatives thereof, e.g. butter
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Abstract
The invention proposes a kind of whitening mask liquid, are prepared from the following materials: 10-20 parts of niacinamide, 5-10 parts of tea polyphenols, 30-40 parts of ferulic acid, 20-40 parts of hyaluronic acid, 5-10 parts of arbutin, 5-15 parts of isoflavones, 20-30 parts of milk, 10-20 parts of pearl powder, 5-10 parts of butanediol, 5-10 parts of hydroquinone, 1-10 parts of glycerol, 5-15 parts of tea tree ethereal oil, 30-50 parts of Chinese medicine whitening extract, 1-3 parts of EDETATE SODIUM, 1-3 parts of carbomer, 1-5 parts of antioxidant, 5-10 parts of plants essential oil and 80-120 parts of deionized water.The present invention since source, inhibits tyrosinase to generate using a variety of whitening compositions, slows down or lower the formation of melanin, and natural whiting ingredient of arranging in pairs or groups, free radical resisting reduces the generation of melanin, while isolation ultraviolet；For the melanocyte formed, promote the cell detachment containing melanin by accelerating the renewal speed of Skin Cell.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of whitening mask liquid.
Background technique
It is well known that the color of skin depends on the content and distribution of melanin.The physiology course that melanin is formed is basic
Summarize are as follows: melanocyte generates melanin；Melanin granule is shifted by melanocyte dendritic processes to epithelial cells；
The melanin granule for being transferred to epithelial cells goes upward to cuticula with epidermal cell, and falls off and drain with cuticula.In black
In plain cell, the formation of melanin occurs in a certain specific cells device in melanocyte, which is referred to as melanocyte
Body, wherein the enzyme is a polyphenol oxidase containing tyrosinase (being sometimes referred to do copper tyrosinase because containing Cu2+ in the enzyme)
Enzyme belongs to redox enzymes, is one of essential enzyme in melanin forming process.The synthesis of melanin must there are three types of
Substance participates in: 1. tyrosine is the primary raw material for manufacturing melanin；2. tyrosinase is that tyrosine is changed into the main of melanin
Rate-limiting enzyme；3. tyrosine generates melanin under the action of tyrosinase, such effect is oxidation process, it is necessary in conjunction with oxygen
Melanin can be changed into.Useful tartaric acid whitening product on the market is made using the removing that the tartaric acid of high concentration carries out skin keratin
With, promote aging cutin layer to fall off, the renewal speed of acceleration horn cell and small part upper layer epidermal cell, however tartaric acid whitening
Cuticula is only peeled off by force with strong acid, achievees the effect that whitening, and effect is had no to the melanin of basal layer, therefore this is
Palliative method.With the improvement of living standards, consumer has higher requirement, especially Asia to whitening product
Beauty and skin care market, whitening are still consumer and pay close attention to the most.But skin care item market at present, the generally existing institute of whitening mask
Need effect constituent species various, raw material valuableness etc., portioned product whitening effect is bad, even there is also toxic side effects etc. to lack
It falls into.
Currently, also there is the report that Chinese herbal medicine is much used for whitening and skin-protecting, the China such as Publication No. 101797208A is special
Benefit application, for another example Chinese patent application of Publication No. 101744756A.These current reports, it is often multiple with constituent
Miscellaneous disadvantage, as Publication No. 101744756A Chinese patent application constituent up to as many as 20 kinds, other existing group
Closing object is also at least seven kinds or more.Specifically, firstly, the complicated component of Chinese medicine, many important ingredients are not yet understood fully completely
Chu, excessive Chinese medicine mixing, complex reaction can occur between each other, increase the uncertain risk of Chinese medicine, particularly with
In the drug or health care product that delay senescence and skin whitening uses, generally require to take for a long time, to increase side reaction even
The carcinogenic risk of pathogenic teratogenesis；Secondly, it is many kinds of, difficulty is also brought for the acquisition of production cost, raw material, particularly in
Medicine resource owes manufacturer abundant, increases its production cost, directly affects Business Economic Benefit.
For the deficiency of existing Skin whitening care cosmetics, exploitation is a safely and effectively, does not stimulate naturally, the day that pure plant is extracted
Right whitening mask will will receive liking for numerous female friends.
Summary of the invention
In order to solve the above technical problems, the present invention provides a kind of whitening mask liquid and preparation method thereof, and purpose exists
In, a kind of whitening mask liquid is provided, it is smart by being added to whitening composition arbutin, isoflavones, milk, pearl powder, tea tree
Oil and Chinese medicine whitening extract inhibit tyrosinase to generate, slow down or lower black using a variety of whitening compositions since source
The formation of element, natural whiting ingredient of arranging in pairs or groups, the inside reduce the activity of tyrosinase containing Macro and microelements, and free radical resisting subtracts
The generation of few melanin, while isolation ultraviolet；For the melanocyte formed, by the update for accelerating Skin Cell
Speed is to promote the cell detachment containing melanin.
The present invention provides a kind of whitening mask liquid, is prepared from the following materials: niacinamide, tea polyphenols, ferulic acid, transparent
Matter acid, arbutin, isoflavones, milk, pearl powder, butanediol, hydroquinone, glycerol, tea tree ethereal oil, Chinese medicine whitening are extracted
Object, EDETATE SODIUM, carbomer, antioxidant, plants essential oil and deionized water.
Improve, be prepared from the following materials as of the invention further: 10-20 parts of niacinamide, 5-10 parts of tea polyphenols,
30-40 parts of ferulic acid, 20-40 parts of hyaluronic acid, 5-10 parts of arbutin, 5-15 parts of isoflavones, 20-30 parts of milk, pearl
10-20 parts of powder, 5-10 parts of butanediol, 5-10 parts of hydroquinone, 1-10 parts of glycerol, 5-15 parts of tea tree ethereal oil, Chinese medicine whitening are extracted
30-50 parts of object, 1-3 parts of EDETATE SODIUM, 1-3 parts of carbomer, 1-5 parts of antioxidant, 5-10 parts of plants essential oil and deionized water 80-
120 parts.
Improve, be prepared from the following materials as of the invention further: 12-17 parts of niacinamide, 6-9 parts of tea polyphenols,
32-37 parts of ferulic acid, 25-35 parts of hyaluronic acid, 6-9 parts of arbutin, 7-12 parts of isoflavones, 22-27 parts of milk, pearl powder
12-17 parts, 6-8 parts of butanediol, 6-8 parts of hydroquinone, 2-8 parts of glycerol, 7-12 parts of tea tree ethereal oil, Chinese medicine whitening extract 35-
45 parts, 1-2 parts of EDETATE SODIUM, 1-2 parts of carbomer, 2-4 parts of antioxidant, 6-8 parts of plants essential oil and 90-110 parts of deionized water.
As further improvement of the invention, it is prepared from the following materials: 16 parts of niacinamide, 7 parts of tea polyphenols, ferulic acid
35 parts, 30 parts of hyaluronic acid, 8 parts of arbutin, 10 parts of isoflavones, 25 parts of milk, 14 parts of pearl powder, 7 parts of butanediol, to benzene
7 parts of diphenol, 10 parts of tea tree ethereal oil, 405 parts of Chinese medicine whitening extract, 1.5 parts of EDETATE SODIUM, 1.7 parts of carbomer, resists 5 parts of glycerol
3 parts of oxygen agent, 7 parts of plants essential oil and 100 parts of deionized water.
Improved as of the invention further, the Chinese medicine whitening extract the preparation method is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and drying is beaten
Powder obtains traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, microwave heating is stirred to 60 DEG C
It mixes after extracting 3-5h, filtering, filter residue repeats to extract 2 times, and merge extracting solution three times, ethyl alcohol is recovered under reduced pressure, obtained concentrate
Continue heating to be concentrated into density to be 1.2-1.6g/cm3, Chinese medicine whitening extract is made.
As further improvement of the invention, the microwave power is 400-700W.
As further improvement of the invention, the antioxidant is selected from potassium sorbate, sorbic acid, sodium lactate, superoxides
One or more of mutase, glutathione peroxidase, tea polyphenols, vitamin E, vitamin C and Co-Q10.
As further improvement of the invention, the plants essential oil is selected from lavender oil, lemon oil, bergamot oil, cloves
One or more of oil, peppermint oil, cinnamon oil, attar of rose, rosemary oil and thyme linaloe oil.
The present invention further protects a kind of preparation method of above-mentioned whitening mask liquid, is prepared according to the following steps:
(1) by niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract
Reactor is added, 1/5 deionized water is added, moderate-speed mixer obtains mixed liquor A to being uniformly mixed；
(2) antioxidant, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, mixed liquor A is added
In, 1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, milk and treasure is added after stirring 10min
Pearl powder, stirs evenly, and 1/5 deionized water is added after 30min, and after deionized water adds, high-speed stirred 20min is cold
But to room temperature, mixing speed is reduced to middling speed, plants essential oil is added and tea tree ethereal oil obtains whitening mask after mixing evenly
Liquid.
As further improvement of the invention, the moderate-speed mixer revolving speed is 300-500r/min, and high-speed stirred revolving speed is
500-700r/min。
The invention has the following beneficial effects:
1, the present invention is added to whitening composition arbutin, isoflavones, milk, pearl powder, tea tree ethereal oil and Chinese medicine beauty
White extract inhibits tyrosinase to generate, slows down or lower the formation of melanin using a variety of whitening compositions since source,
Collocation natural whiting ingredient, the inside reduce the activity of tyrosinase containing Macro and microelements, and free radical resisting reduces melanin
It generates, while isolation ultraviolet；For the melanocyte formed, by accelerating the renewal speed of Skin Cell to promote
Into the cell detachment containing melanin；
2, the present invention is added to moisturizing moisturizing ingredient niacinamide, ferulic acid and hyaluronic acid, facilitates deep skin reparation,
Cell elasticity and vigor are kept, treating for skin disease is facilitated；
3, raw material sources of the invention are wide, and whitening composition is pure natural not to stimulate, and are free of Pn, to skin fanout free region, effectively promote
It falls off into melanocyte, the vigor for cell of keeping fit, so that skin-whitening is only saturating.
Detailed description of the invention
Fig. 1 is the preparation technology figure of whitening mask liquid.
Specific embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, the embodiment described is the embodiment of part of representative of the invention, rather than whole embodiments, this field are general
Other all embodiments obtained belong to protection of the invention to logical technical staff without making creative work
Range.
Embodiment 1
Raw material forms (parts by weight): 10 parts of niacinamide, 5 parts of tea polyphenols, 30 parts of ferulic acid, 20 parts of hyaluronic acid, arbutin 5
Part, 5 parts of isoflavones, 20 parts of milk, 10 parts of pearl powder, 5 parts of butanediol, 5 parts of hydroquinone, 1 part of glycerol, tea tree ethereal oil 5
Part, 30 parts of Chinese medicine whitening extract, 1 part of EDETATE SODIUM, 1 part of carbomer, 1 part of potassium sorbate, 5 parts of thyme linaloe oil and deionized water
80 parts；
The Chinese medicine whitening extract the preparation method is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and drying is beaten
Powder obtains traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, microwave heating is micro- to 60 DEG C
Wave power is 400W, and after 3h is extracted in stirring, filtering, filter residue repeats to extract 2 times, merges extracting solution three times, ethyl alcohol is recovered under reduced pressure,
Obtained concentrate continues heating to be concentrated into density to be 1.2g/cm3, Chinese medicine whitening extract is made.
The preparation method of the whitening mask liquid, is prepared according to the following steps:
(1) by niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract
Reactor is added, 1/5 deionized water is added, for moderate-speed mixer to being uniformly mixed, speed of agitator 300r/min obtains mixed liquor
A；
(2) potassium sorbate, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, mixing is added
In liquid A, 1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, stir be added after 10min milk with
Pearl powder stirs evenly, and 1/5 deionized water is added after 30min, after deionized water adds, high-speed stirred 20min,
Speed of agitator is 500r/min, is cooled to room temperature, and mixing speed is reduced to middling speed, speed of agitator 300r/min is added hundred
In sesame oil and tea tree ethereal oil obtain whitening mask liquid after mixing evenly.
Embodiment 2
Raw material forms (parts by weight): 20 parts of niacinamide, 10 parts of tea polyphenols, 40 parts of ferulic acid, 40 parts of hyaluronic acid, arbutin
10 parts, 15 parts of isoflavones, 30 parts of milk, 20 parts of pearl powder, 10 parts of butanediol, 10 parts of hydroquinone, 10 parts of glycerol, tea tree
It 15 parts of essential oil, 50 parts of Chinese medicine whitening extract, 3 parts of EDETATE SODIUM, 3 parts of carbomer, 5 parts of vitamin C, 10 parts of rosemary oil and goes
120 parts of ionized water；
The Chinese medicine whitening extract the preparation method is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and drying is beaten
Powder obtains traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, microwave heating is micro- to 60 DEG C
Wave power is 700W, and after 5h is extracted in stirring, filtering, filter residue repeats to extract 2 times, merges extracting solution three times, ethyl alcohol is recovered under reduced pressure,
Obtained concentrate continues heating to be concentrated into density to be 1.6g/cm3, Chinese medicine whitening extract is made.
The preparation method of the whitening mask liquid, is prepared according to the following steps:
(1) by niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract
Reactor is added, 1/5 deionized water is added, for moderate-speed mixer to being uniformly mixed, speed of agitator 500r/min obtains mixed liquor
A；
(2) vitamin C, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, mixed liquor is added
In A, 1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, milk and treasure is added after stirring 10min
Pearl powder, stirs evenly, and 1/5 deionized water is added after 30min, after deionized water adds, high-speed stirred 20min is stirred
Mixing revolving speed is 700r/min, is cooled to room temperature, and mixing speed is reduced to middling speed, speed of agitator 500r/min is added fan and changes
Sesame oil and tea tree ethereal oil obtain whitening mask liquid after mixing evenly.
Embodiment 3
Raw material forms (parts by weight): 12 parts of niacinamide, 6 parts of tea polyphenols, 32 parts of ferulic acid, 25 parts of hyaluronic acid, arbutin 6
Part, 7 parts of isoflavones, 22 parts of milk, 12 parts of pearl powder, 6 parts of butanediol, 6 parts of hydroquinone, 2 parts of glycerol, tea tree ethereal oil 7
It part, 35 parts of Chinese medicine whitening extract, 1 part of EDETATE SODIUM, 1 part of carbomer, 2 parts of superoxide dismutase, 6 parts of lavender oil and goes
90 parts of ionized water；
The Chinese medicine whitening extract the preparation method is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and drying is beaten
Powder obtains traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, microwave heating is micro- to 60 DEG C
Wave power is 450W, and after 3.5h is extracted in stirring, filtering, filter residue repeats to extract 2 times, merges extracting solution three times, second is recovered under reduced pressure
Alcohol, obtained concentrate continue heating to be concentrated into density to be 1.3g/cm3, Chinese medicine whitening extract is made.
The preparation method of the whitening mask liquid, is prepared according to the following steps:
(1) by niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract
Reactor is added, 1/5 deionized water is added, for moderate-speed mixer to being uniformly mixed, speed of agitator 350r/min obtains mixed liquor
A；
(2) superoxide dismutase, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, are added
Enter in mixed liquor A, 1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, be added after stirring 10min
Milk and pearl powder, stir evenly, and 1/5 deionized water, after deionized water adds, high-speed stirred are added after 30min
20min, speed of agitator 550r/min, is cooled to room temperature, and mixing speed is reduced to middling speed, speed of agitator 350r/min,
Lavender oil is added and tea tree ethereal oil obtains whitening mask liquid after mixing evenly.
Embodiment 4
Raw material forms (parts by weight): 17 parts of niacinamide, 9 parts of tea polyphenols, 37 parts of ferulic acid, 35 parts of hyaluronic acid, arbutin 9
Part, 12 parts of isoflavones, 27 parts of milk, 17 parts of pearl powder, 8 parts of butanediol, 8 parts of hydroquinone, 8 parts of glycerol, tea tree ethereal oil
12 parts, 45 parts of Chinese medicine whitening extract, 2 parts of EDETATE SODIUM, 2 parts of carbomer, 4 parts of sodium lactate, 8 parts of bergamot oil and deionized water
110 parts；
The Chinese medicine whitening extract the preparation method is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and drying is beaten
Powder obtains traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, microwave heating is micro- to 60 DEG C
Wave power is 650W, and after 4.5h is extracted in stirring, filtering, filter residue repeats to extract 2 times, merges extracting solution three times, second is recovered under reduced pressure
Alcohol, obtained concentrate continue heating to be concentrated into density to be 1.5g/cm3, Chinese medicine whitening extract is made.
The preparation method of the whitening mask liquid, is prepared according to the following steps:
(1) by niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract
Reactor is added, 1/5 deionized water is added, for moderate-speed mixer to being uniformly mixed, speed of agitator 450r/min obtains mixed liquor
A；
(2) sodium lactate, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, mixed liquor A is added
In, 1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, milk and treasure is added after stirring 10min
Pearl powder, stirs evenly, and 1/5 deionized water is added after 30min, after deionized water adds, high-speed stirred 20min is stirred
Mixing revolving speed is 650r/min, is cooled to room temperature, and mixing speed is reduced to middling speed, fragrant lemon is added in speed of agitator 450r/min
Lemon oil and tea tree ethereal oil obtain whitening mask liquid after mixing evenly.
Embodiment 5
Raw material forms (parts by weight): 16 parts of niacinamide, 7 parts of tea polyphenols, 35 parts of ferulic acid, 30 parts of hyaluronic acid, arbutin 8
Part, 10 parts of isoflavones, 25 parts of milk, 14 parts of pearl powder, 7 parts of butanediol, 7 parts of hydroquinone, 5 parts of glycerol, tea tree ethereal oil
10 parts, 405 parts of Chinese medicine whitening extract, 1.5 parts of EDETATE SODIUM, 1.7 parts of carbomer, 3 parts of Co-Q10,7 parts of attar of rose and go from
100 parts of sub- water；
The Chinese medicine whitening extract the preparation method is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and drying is beaten
Powder obtains traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, microwave heating is micro- to 60 DEG C
Wave power is 550W, and after 3-5h is extracted in stirring, filtering, filter residue repeats to extract 2 times, merges extracting solution three times, second is recovered under reduced pressure
Alcohol, obtained concentrate continue heating to be concentrated into density to be 1.4g/cm3, Chinese medicine whitening extract is made.
The preparation method of the whitening mask liquid, is prepared according to the following steps:
(1) by niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract
Reactor is added, 1/5 deionized water is added, for moderate-speed mixer to being uniformly mixed, speed of agitator 400r/min obtains mixed liquor
A；
(2) Co-Q10, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, mixed liquor is added
In A, 1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, milk and treasure is added after stirring 10min
Pearl powder, stirs evenly, and 1/5 deionized water is added after 30min, after deionized water adds, high-speed stirred 20min is stirred
Mixing revolving speed is 600r/min, is cooled to room temperature, and mixing speed is reduced to middling speed, rose is added in speed of agitator 400r/min
Oil and tea tree ethereal oil obtain whitening mask liquid after mixing evenly.
1 patch test of test example
1. tested material: whitening mask liquid prepared by embodiment 5
2. negative control: deionized water
3. subject: totally 30 people, male 0 people, 30 people of female the age 25-48 years old, meet subject and volunteer inclusion criteria.
4. patch method: selecting qualified spot tester, with enclosed patch test method, about by tested material and negative control
0.020mL-0.025mL (semifluid) is dripped in spot tester, and external application special adhesive tape is pasted on subject back, removes after 24 hours
Tested material, observation dermoreaction in 0.5,24,48 hour after removing respectively, by skin in " cosmetics health specification " (version in 2007)
Reaction grade scale records its result.Test result is shown in Table 1:
1 human skin patch test result of table
Human skin patch test result is shown: 0 there is skin adverse reaction in 30 people；Illustrate whitening face of the invention
Film liquid uses safe.
The test of 2 whitening effect of test example
1. sample sets: whitening mask liquid prepared by embodiment 5
2. control group: commercially available whitening mask liquid
3. subject: totally 30 people, male 0 people, 30 people of female the age 30-59 years old, meet subject and volunteer inclusion criteria.
4. the principle of dermal melanin and ferroheme test:
Mexameter MX18 is the principle (RGB) based on spectral absorption, by measuring the illumination of specific wavelength in human body
Volume reflection after on skin determines the content of melanin and ferroheme in skin.The transmitter of instrument probe issues wavelength difference
It is radiated at skin surface for the light of tri- kinds of wavelength of 568nm, 660nm and 880nm, recipient measures the light of skin reflex.Due to hair
It is certain for penetrating the amount of light, therefore can measure the amount for the light being absorbed by the skin, and measures containing for dermal melanin and ferroheme
Amount.The measurement range of instrument is 0-999, and measurement numerical value is higher, illustrates that the content of melanin and ferroheme is higher in skin.
5. test method:
Before subject smears sample, first experiment position is cleaned, smears sample after drying.The left and right cheek of subject is successively
Cycle labeling: the area of 4 × 4cm size is as tested region and blank control region；Subject is daily sooner or later in Experimental Area
Twice using tested material, during experiment, subject cannot smear any other cosmetics in Test sites.Subject continuously makes
After tested material one week, two weeks, three weeks and four weeks, same time subject cleans position is smeared weekly, is used by tester
The content at position is smeared in Mexameter MX18 tester and the measurement of MicroSkin II Multi-functional skin mirror image analysis system.
Every is surveyed five times, is averaged.It the results are shown in Table 2.
Melanin reduced rate (%)=[the secondary melanin content (%)-for the first time melanin content (%)] ÷ melanin for the first time
Content (%) × 100%
Relative melanin reduced rate (the %)=secondary sample sets melanin reduced rate (the %)-secondary control group pigment reduced rate
(%)
2 each group tested material Comparative result table of table
As shown in Table 1, sample sets and control group are reduced using rear melanin content, and over time in incremental
Trend, and sample sets melanin content lowers rate and is substantially better than control group, after four weeks, relative melanin reduced rate reaches
7.4%, and after four weeks, average black cellulose content is 126%, it is seen that the whitening effect of sample sets is substantially better than control group, and beauty
White effect is lasting.
Human skin patch is carried out according to the above method using the obtained whitening mask liquid of embodiment 1-4 and whitening is imitated
Fruit test, obtains the test result similar with above-mentioned test result.
Those skilled in the art is not under conditions of departing from the spirit and scope of the present invention that claims determine, also
Various modifications can be carried out to the above content.Therefore the scope of the present invention is not limited in above explanation, but by
The range of claims determines.
Claims (10)
1. a kind of whitening mask liquid, which is characterized in that be prepared from the following materials: niacinamide, tea polyphenols, ferulic acid, transparent
Matter acid, arbutin, isoflavones, milk, pearl powder, butanediol, hydroquinone, glycerol, tea tree ethereal oil, Chinese medicine whitening are extracted
Object, EDETATE SODIUM, carbomer, antioxidant, plants essential oil and deionized water.
2. a kind of whitening mask liquid according to claim 1, which is characterized in that be prepared from the following materials: niacinamide 10-
20 parts, 5-10 parts of tea polyphenols, 30-40 parts of ferulic acid, 20-40 parts of hyaluronic acid, 5-10 parts of arbutin, isoflavones 5-15
Part, 20-30 parts of milk, 10-20 parts of pearl powder, 5-10 parts of butanediol, 5-10 parts of hydroquinone, 1-10 parts of glycerol, tea tree ethereal oil
5-15 parts, 30-50 parts of Chinese medicine whitening extract, 1-3 parts of EDETATE SODIUM, 1-3 parts of carbomer, 1-5 parts of antioxidant, plants essential oil 5-
10 parts and deionized water 80-120 parts.
3. a kind of whitening mask liquid according to claim 2, which is characterized in that be prepared from the following materials: niacinamide 12-
17 parts, 6-9 parts of tea polyphenols, 32-37 parts of ferulic acid, 25-35 parts of hyaluronic acid, 6-9 parts of arbutin, 7-12 parts of isoflavones,
22-27 parts of milk, 12-17 parts of pearl powder, 6-8 parts of butanediol, 6-8 parts of hydroquinone, 2-8 parts of glycerol, 7-12 parts of tea tree ethereal oil,
It 35-45 parts of Chinese medicine whitening extract, 1-2 parts of EDETATE SODIUM, 1-2 parts of carbomer, 2-4 parts of antioxidant, 6-8 parts of plants essential oil and goes
90-110 parts of ionized water.
4. a kind of whitening mask liquid according to claim 3, which is characterized in that be prepared from the following materials: niacinamide 16
Part, 7 parts of tea polyphenols, 35 parts of ferulic acid, 30 parts of hyaluronic acid, 8 parts of arbutin, 10 parts of isoflavones, 25 parts of milk, pearl powder
14 parts, 7 parts of butanediol, 7 parts of hydroquinone, 5 parts of glycerol, 10 parts of tea tree ethereal oil, 405 parts of Chinese medicine whitening extract, EDETATE SODIUM
1.5 parts, 1.7 parts of carbomer, 3 parts of antioxidant, 7 parts of plants essential oil and 100 parts of deionized water.
5. a kind of whitening mask liquid according to claim 1, which is characterized in that the preparation method of the Chinese medicine whitening extract
It is as follows:
(1) flower bud of lily magnolia, sea-buckthorn, datura flower, root of kirilow rhodiola, Radix Paeoniae Alba, the bletilla striata, chamomile, Bai Chihua are weighed in proportion, and powder is beaten in drying, is obtained
To traditional Chinese medicine powder；
(2) ethanol solution of traditional Chinese medicine powder and 75% is mixed by solid-to-liquid ratio 1:10, impregnates 10h, to 60 DEG C, stirring is mentioned for microwave heating
After taking 3-5h, filtering, filter residue repeats to extract 2 times, merges extracting solution three times, ethyl alcohol is recovered under reduced pressure, and obtained concentrate continues
It is 1.2-1.6g/cm that heating, which is concentrated into density,3, Chinese medicine whitening extract is made.
6. a kind of whitening mask liquid according to claim 5, which is characterized in that the microwave power is 400-700W.
7. a kind of whitening mask liquid according to claim 1, which is characterized in that the antioxidant is selected from potassium sorbate, sorb
In acid, sodium lactate, superoxide dismutase, glutathione peroxidase, tea polyphenols, vitamin E, vitamin C and Co-Q10
It is one or more of.
8. a kind of whitening mask liquid according to claim 1, which is characterized in that the plants essential oil is selected from lavender oil, lemon
One or more of lemon oil, bergamot oil, caryophyllus oil, peppermint oil, cinnamon oil, attar of rose, rosemary oil and thyme linaloe oil.
9. a kind of preparation method of whitening mask liquid according to claim 1, which is characterized in that be prepared according to the following steps:
(1) niacinamide, tea polyphenols, ferulic acid, hyaluronic acid, arbutin, isoflavones and Chinese medicine whitening extract are added
Reactor, is added 1/5 deionized water, and moderate-speed mixer obtains mixed liquor A to being uniformly mixed；
(2) antioxidant, butanediol, hydroquinone, glycerol, EDETATE SODIUM and carbomer are uniformly mixed, are added in mixed liquor A,
1/5 deionized water is added in former speed stirring, is warming up to 60 DEG C, continues to stir, milk and pearl is added after stirring 10min
Powder stirs evenly, and 1/5 deionized water is added after 30min, and after deionized water adds, high-speed stirred 20min is cooling
To room temperature, mixing speed is reduced to middling speed, plants essential oil is added and tea tree ethereal oil obtains whitening mask liquid after mixing evenly.
10. preparation method according to claim 9, which is characterized in that the moderate-speed mixer revolving speed is 300-500r/min, high
Fast speed of agitator is 500-700r/min.
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110859795A (en) * | 2019-12-27 | 2020-03-06 | 海南海润生物科技股份有限公司 | Freckle-removing and anti-aging composition, preparation method thereof and facial mask pearl powder |
| CN111643388A (en) * | 2020-07-17 | 2020-09-11 | 深圳市南科微木生物科技有限公司 | Skin care composition and skin care product containing same |
| CN112494408A (en) * | 2020-12-31 | 2021-03-16 | 淮阴工学院 | Whitening and inflammation diminishing mask liquid and preparation method thereof |
| CN113813208A (en) * | 2021-10-21 | 2021-12-21 | 百色百香文化科技产业有限公司 | Whitening mask liquid, mask and preparation method of mask liquid |
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2018
- 2018-11-12 CN CN201811337202.XA patent/CN109330966A/en active Pending
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110859795A (en) * | 2019-12-27 | 2020-03-06 | 海南海润生物科技股份有限公司 | Freckle-removing and anti-aging composition, preparation method thereof and facial mask pearl powder |
| CN111643388A (en) * | 2020-07-17 | 2020-09-11 | 深圳市南科微木生物科技有限公司 | Skin care composition and skin care product containing same |
| CN111643388B (en) * | 2020-07-17 | 2023-06-27 | 深圳市南科微木生物科技有限公司 | Skin care composition and skin care product containing same |
| CN112494408A (en) * | 2020-12-31 | 2021-03-16 | 淮阴工学院 | Whitening and inflammation diminishing mask liquid and preparation method thereof |
| CN112494408B (en) * | 2020-12-31 | 2022-03-22 | 淮阴工学院 | Whitening and inflammation diminishing mask liquid |
| CN114306188A (en) * | 2020-12-31 | 2022-04-12 | 淮阴工学院 | Preparation method of whitening and inflammation diminishing mask liquid |
| CN114306188B (en) * | 2020-12-31 | 2023-09-29 | 淮阴工学院 | Preparation method of whitening and anti-inflammatory mask liquid |
| CN113813208A (en) * | 2021-10-21 | 2021-12-21 | 百色百香文化科技产业有限公司 | Whitening mask liquid, mask and preparation method of mask liquid |
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