CN109307677A - Water base bleeding agent and preparation method thereof, aqueous-based ceramic flaw detection agent and preparation method thereof - Google Patents
Water base bleeding agent and preparation method thereof, aqueous-based ceramic flaw detection agent and preparation method thereof Download PDFInfo
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- CN109307677A CN109307677A CN201710625244.2A CN201710625244A CN109307677A CN 109307677 A CN109307677 A CN 109307677A CN 201710625244 A CN201710625244 A CN 201710625244A CN 109307677 A CN109307677 A CN 109307677A
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- 239000000919 ceramic Substances 0.000 title claims abstract description 122
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 title claims abstract description 95
- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 91
- 230000000740 bleeding effect Effects 0.000 title claims abstract description 57
- 238000001514 detection method Methods 0.000 title claims abstract description 57
- 238000002360 preparation method Methods 0.000 title claims abstract description 22
- 239000012216 imaging agent Substances 0.000 claims abstract description 60
- 239000000975 dye Substances 0.000 claims abstract description 40
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims abstract description 31
- 230000000149 penetrating effect Effects 0.000 claims abstract description 29
- 239000002904 solvent Substances 0.000 claims abstract description 29
- 239000004094 surface-active agent Substances 0.000 claims abstract description 26
- 238000012545 processing Methods 0.000 claims abstract description 22
- 238000003384 imaging method Methods 0.000 claims abstract description 21
- IQFVPQOLBLOTPF-HKXUKFGYSA-L congo red Chemical compound [Na+].[Na+].C1=CC=CC2=C(N)C(/N=N/C3=CC=C(C=C3)C3=CC=C(C=C3)/N=N/C3=C(C4=CC=CC=C4C(=C3)S([O-])(=O)=O)N)=CC(S([O-])(=O)=O)=C21 IQFVPQOLBLOTPF-HKXUKFGYSA-L 0.000 claims abstract description 17
- 235000012730 carminic acid Nutrition 0.000 claims abstract description 15
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 14
- -1 ethoxy compound Chemical class 0.000 claims abstract description 8
- 235000011187 glycerol Nutrition 0.000 claims abstract description 7
- SBASXUCJHJRPEV-UHFFFAOYSA-N 2-(2-methoxyethoxy)ethanol Chemical compound COCCOCCO SBASXUCJHJRPEV-UHFFFAOYSA-N 0.000 claims abstract description 6
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 claims abstract description 6
- 235000019387 fatty acid methyl ester Nutrition 0.000 claims abstract description 5
- 239000000203 mixture Substances 0.000 claims description 25
- 239000003463 adsorbent Substances 0.000 claims description 22
- 239000003822 epoxy resin Substances 0.000 claims description 16
- 229920000647 polyepoxide Polymers 0.000 claims description 16
- 150000001408 amides Chemical class 0.000 claims description 13
- 230000003213 activating effect Effects 0.000 claims description 3
- 230000008595 infiltration Effects 0.000 abstract description 22
- 238000001764 infiltration Methods 0.000 abstract description 22
- 230000035945 sensitivity Effects 0.000 abstract description 16
- 230000000694 effects Effects 0.000 abstract description 12
- 238000004040 coloring Methods 0.000 abstract description 7
- 231100000252 nontoxic Toxicity 0.000 abstract description 5
- 230000003000 nontoxic effect Effects 0.000 abstract description 5
- 239000002994 raw material Substances 0.000 abstract description 3
- 238000003756 stirring Methods 0.000 description 38
- 239000000047 product Substances 0.000 description 28
- 238000005507 spraying Methods 0.000 description 19
- CPLXHLVBOLITMK-UHFFFAOYSA-N Magnesium oxide Chemical compound [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 18
- 239000007921 spray Substances 0.000 description 16
- 239000013527 degreasing agent Substances 0.000 description 15
- 238000001035 drying Methods 0.000 description 14
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 13
- 229940037003 alum Drugs 0.000 description 13
- 238000005303 weighing Methods 0.000 description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 11
- 238000000034 method Methods 0.000 description 10
- 239000000395 magnesium oxide Substances 0.000 description 9
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 9
- 238000005406 washing Methods 0.000 description 9
- 239000003595 mist Substances 0.000 description 8
- 238000000967 suction filtration Methods 0.000 description 8
- 241000220317 Rosa Species 0.000 description 7
- 239000000853 adhesive Substances 0.000 description 7
- 230000001070 adhesive effect Effects 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 238000004506 ultrasonic cleaning Methods 0.000 description 7
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
- 239000000377 silicon dioxide Substances 0.000 description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- MCMNRKCIXSYSNV-UHFFFAOYSA-N Zirconium dioxide Chemical compound O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 description 4
- 238000007689 inspection Methods 0.000 description 4
- 230000007794 irritation Effects 0.000 description 4
- 231100000419 toxicity Toxicity 0.000 description 4
- 230000001988 toxicity Effects 0.000 description 4
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 3
- 238000004140 cleaning Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- 235000017858 Laurus nobilis Nutrition 0.000 description 2
- 235000005212 Terminalia tomentosa Nutrition 0.000 description 2
- 244000125380 Terminalia tomentosa Species 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 235000014113 dietary fatty acids Nutrition 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 230000002708 enhancing effect Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000194 fatty acid Substances 0.000 description 2
- 229930195729 fatty acid Natural products 0.000 description 2
- 150000004665 fatty acids Chemical class 0.000 description 2
- 231100001261 hazardous Toxicity 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- 229940051841 polyoxyethylene ether Drugs 0.000 description 2
- 229920000056 polyoxyethylene ether Polymers 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000001044 red dye Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004408 titanium dioxide Substances 0.000 description 2
- 231100000331 toxic Toxicity 0.000 description 2
- 230000002588 toxic effect Effects 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 241000721047 Danaus plexippus Species 0.000 description 1
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical compound COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 1
- 241000790917 Dioxys <bee> Species 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 229910003978 SiClx Inorganic materials 0.000 description 1
- 229920000180 alkyd Polymers 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 1
- 239000012964 benzotriazole Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000003599 detergent Substances 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- LRMHFDNWKCSEQU-UHFFFAOYSA-N ethoxyethane;phenol Chemical compound CCOCC.OC1=CC=CC=C1 LRMHFDNWKCSEQU-UHFFFAOYSA-N 0.000 description 1
- 210000000887 face Anatomy 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 230000001795 light effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 238000009738 saturating Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/84—Systems specially adapted for particular applications
- G01N21/88—Investigating the presence of flaws or contamination
- G01N21/91—Investigating the presence of flaws or contamination using penetration of dyes, e.g. fluorescent ink
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Investigating Materials By The Use Of Optical Means Adapted For Particular Applications (AREA)
Abstract
The present invention relates to a kind of water base bleeding agents and preparation method thereof, aqueous-based ceramic flaw detection agent and preparation method thereof.A kind of water base bleeding agent includes: 3.5 parts~8.5 parts of dyestuff according to the mass fraction；50.0 parts~65.0 parts of penetrating solvent；5.0 parts~20.0 parts of surfactant；And 11.5 parts~41.5 parts of water；Dyestuff includes: 2.0 parts~4.0 parts carmine according to the mass fraction；1.0 parts~3.0 parts of Aniline Red；And Congo red 0.5 part~1.5 parts；Penetrating solvent is selected from least one of diethylene glycol ether, glycerine and diethylene glycol monomethyl ether；Surfactant is selected from least one of fatty acid methyl ester ethoxy compound and ethoxylated dodecyl alcohol.Above-mentioned water base bleeding agent and aqueous-based ceramic flaw detection agent are used to carry out ceramics infiltration processing, then are handled ceramics with imaging agent so that the cracks of ceramics are identified.Above-mentioned dye colour is deep, has preferable coloring effect, so that imaging results more preferably, further increase the sensitivity of detection；And the raw material used are nontoxic, pollution-free, non-volatile and nonflammable.
Description
Technical field
The present invention relates to the penetrant inspection detection technique fields of ceramics, more particularly to water base bleeding agent and its preparation side
Method, aqueous-based ceramic flaw detection agent and preparation method thereof.
Background technique
Zirconia ceramics due to it is high, small to microwave signal and microwave signal and micro sensing effect of signals with dielectric constant,
The advantages that such as beautiful general texture of appearance, hardness height, high-wearing feature, it is therefore widely used in structural ceramics field.With city
The development of field demand is largely used as appearance ornamental pieces material in the consumer electronics products such as smart phone, smartwatch, but
Since ceramics have the shortcomings that frangible, and structure is complicated for consumer electronics product, more at thin-walled, after sintering product in grinding plus
Micro-crack is easy to appear in work, the detection referring now to micro-crack be all by manually being identified, it is anti-after especially ceramic polished
Light effect is obvious, cannot intuitively show bad, increases the difficulty of artificial detection, easily carries out step process under bad inflow
Processing, finds not in time, cost is caused to waste.Have flaw detection agent at present for technical field of nondestructive inspection, however existing infiltration
There are still the problems being more toxic and flaw detection sensitivity is not high for saturating agent and flaw detection agent.
Summary of the invention
Based on this, it is necessary to which for current bleeding agent and flaw detection agent, there are still be more toxic and flaw detection sensitivity is not high asks
Topic provides a kind of water base bleeding agent and preparation method thereof, aqueous-based ceramic flaw detection agent and preparation method thereof.
A kind of water base bleeding agent, according to the mass fraction, comprising:
Wherein, the dyestuff is according to the mass fraction, comprising:
It is 2.0 parts~4.0 parts carmine；
1.0 parts~3.0 parts of Aniline Red；And
Congo red 0.5 part~1.5 parts；
Wherein, the penetrating solvent is selected from least one of diethylene glycol ether, glycerine and diethylene glycol monomethyl ether；Institute
It states surfactant and is selected from least one of fatty acid methyl ester ethoxy compound and ethoxylated dodecyl alcohol.
The preparation method of above-mentioned water base bleeding agent, comprising the following steps:
The penetrating solvent and the dyestuff are uniformly mixed and obtain mixture；And
The surfactant is added into the mixture and the water is uniformly mixed.
In a wherein embodiment, described be uniformly mixed the penetrating solvent and the dyestuff obtains mixture
The time of mixed processing is 1h~2h in step.
It is described that the surfactant and water mixing are added into the mixture in a wherein embodiment
The time of mixed processing is 0.5h~1h in uniform step.
A kind of aqueous-based ceramic flaw detection agent, above-mentioned water base bleeding agent and imaging agent.
In a wherein embodiment, the imaging agent is according to the mass fraction, comprising:
In a wherein embodiment, the adsorbent is according to the mass fraction, comprising:
The preparation method of above-mentioned aqueous-based ceramic flaw detection agent, comprising the following steps:
The penetrating solvent and the dyestuff are uniformly mixed and obtain mixture；
The surfactant is added into the mixture and the water is uniformly mixed and obtains water base bleeding agent；And
Prepare the imaging agent.
In a wherein embodiment, described the step of preparing the imaging agent, is specifically included:
Adsorbent, fatty diglycollic amide and epoxy resin are uniformly mixed and obtain blend；And
Into blend, addition water, which is uniformly mixed, obtains the imaging agent.
Above-mentioned water base bleeding agent and aqueous-based ceramic flaw detection agent are used to carry out infiltration processing to ceramics, then with imaging agent to ceramics
It is handled so that the cracks of ceramics are identified.Congo red cooperate using carmine, Aniline Red and according to a certain ratio
It is deep to dye colour, there is preferable coloring effect, so that imaging results more preferably, further increase the sensitivity of detection；
And the raw material used are nontoxic, pollution-free, non-volatile and nonflammable.
Detailed description of the invention
Fig. 1 is the flow chart of the preparation method of the aqueous-based ceramic flaw detection agent of an embodiment；
Fig. 2 is the flow chart of the ceramic method for detection fault detection of an embodiment.
Specific embodiment
Below in conjunction with specific embodiment and attached drawing to water base bleeding agent and preparation method thereof, aqueous-based ceramic flaw detection agent and
Preparation method is described in further detail.
The aqueous-based ceramic flaw detection agent of one embodiment includes water base bleeding agent and imaging agent.
In a wherein embodiment, aqueous-based ceramic flaw detection agent is mainly used for the nondestructive inspection detection of zirconia ceramics.
Certainly, in other embodiments, aqueous-based ceramic flaw detection agent can be also used for the nondestructive inspection detection of other ceramics.
In a wherein embodiment, water base bleeding agent includes: according to the mass fraction
In a wherein embodiment, dyestuff is according to the mass fraction, comprising:
It is 2.0 parts~4.0 parts carmine；
1.0 parts~3.0 parts of Aniline Red；And
Congo red 0.5 part~1.5 parts.
It is deep that dye colour is obtained using carmine, Aniline Red and Congo red cooperation according to a certain ratio, have compared with
Good coloring effect, so that the sensitivity of carrying out flaw detection improves, and above-mentioned material is nontoxic, has preferable safety.
In a wherein embodiment, penetrating solvent is in diethylene glycol ether, glycerine and diethylene glycol monomethyl ether
At least one.Above-mentioned penetrating solvent all has preferable water solubility, so that water base bleeding agent has preferable wetability, and easily
In cleaned, prevent bleeding agent from remaining on ceramic product and ceramic product is damaged.And above-mentioned penetrating solvent is with lower
Molecular weight, compared to high molecular polymer have better thermal stability.
In a wherein embodiment, surfactant is selected from fatty acid methyl ester ethoxy compound (PMEE) and laurel
At least one of alcohol polyoxyethylene ether.Most surfactant such as polyoxyethylene alkylphenol base ether all has toxicity, right
The eyes and skin of human body have a biggish irritation, and above-mentioned surfactant have compared to other surfaces activating agent it is lower
Irritation, more safety and environmental protection.
Above-mentioned water base bleeding agent obtains dyestuff using carmine, Aniline Red and Congo red cooperation according to a certain ratio, and
It is subject to penetrating solvent, surfactant and water, above-mentioned material all has that toxicity is lower, environment is non-hazardous, non-volatile, nonflammable
Feature, and coloring effect is good, can effectively improve detection sensitivity.Meanwhile above-mentioned water base bleeding agent has preferable water solubility, easily
In being cleaned.
In a wherein embodiment, imaging agent is according to the mass fraction, comprising:
In a wherein embodiment, adsorbent is according to the mass fraction, comprising:
It is added that alum is primarily due to carmine, Aniline Red and the dyestuffs such as Congo red dye when in use in imaging agent
Ability is limited, inadequate in the adhesive force of ceramic surface, and the metallic salts such as iron, aluminium can be used as carmine mordant, enhancing
Dyestuff so that imaging results are more preferably, therefore are added alum in imaging agent and imaging effect can be improved in the adhesive force of ceramic surface
Fruit further increases the sensitivity of detection.
In a wherein embodiment, the partial size of silica is 40nm~100nm.
In a wherein embodiment, the partial size of magnesia is 40nm~100nm.
In a wherein embodiment, the partial size of titanium oxide is 40nm~100nm.
In a wherein embodiment, epoxy resin in E-42 type epoxy resin, E-44 type epoxy resin extremely
Few one kind.
Alum is added in above-mentioned imaging agent, dyestuff can be improved in the adhesive force of ceramic surface, so that imaging results are more preferably,
Further increase the sensitivity of detection；And fatty diglycollic amide has preferable water-soluble, stability and stronger infiltration
The advantages of detergency, so that imaging agent water can clean up, it is more adaptable；And the material of above-mentioned imaging agent is to environment
It is pollution-free and non-volatile, nonflammable, environment and human body will not be damaged, the bulk strong applicability used.
The flaw detection agent of above-mentioned aqueous-based ceramic includes water base bleeding agent and imaging agent, first using above-mentioned water base bleeding agent to ceramics into
Row infiltration processing, then ceramics are handled with imaging agent so that the cracks of ceramics are identified.Above-mentioned aqueous-based ceramic flaw detection agent
It is deep that dye colour is obtained using carmine, Aniline Red and Congo red cooperation according to a certain ratio, there is preferable colouring
Effect, then alum is added in imaging agent, dyestuff can be improved in the adhesive force of ceramic surface, so that imaging results are more preferably, into
One step improves the sensitivity of detection；And the raw material used are nontoxic, pollution-free, non-volatile and nonflammable.
Referring to Fig. 1, the preparation method of above-mentioned aqueous-based ceramic flaw detection agent, comprising the following steps:
S110, water base bleeding agent is prepared.
In a wherein embodiment, the step of preparing water base bleeding agent, is specifically included:
S111, penetrating solvent is uniformly mixed to obtain mixture with dyestuff.
In a wherein embodiment, penetrating solvent is uniformly mixed with dyestuff in blender.
In a wherein embodiment, the rate of stirring is 20rad/min~60rad/min；The time of stirring is 1h
~2h.
S112, into mixture, addition surfactant and water are uniformly mixed.
In a wherein embodiment, surfactant is added into mixture in blender and water is uniformly mixed.
In a wherein embodiment, the rate of stirring is 20rad/min~60rad/min；The time of stirring is
0.5h~1h.
S113, suction filtration processing is carried out to mixture.
In a wherein embodiment, strainer when suction filtration is 200 mesh or more.
S120, imaging agent is prepared.
In a wherein embodiment, the step of preparing imaging agent, is specifically included:
S121, by adsorbent, fatty diglycollic amide and epoxy resin be uniformly mixed obtain blend.
In a wherein embodiment, adsorbent, fatty diglycollic amide and epoxy resin are mixed in blender
It closes and uniformly obtains blend.
In a wherein embodiment, the rate of stirring is 20rad/min~60rad/min；The time of stirring is 1h
~2h.
S122, into blend, addition water is uniformly mixed.
In a wherein embodiment, water is added into blend in blender and is uniformly mixed.
In a wherein embodiment, the rate of stirring is 20rad/min~60rad/min；The time of stirring is
0.5h~1h.
The preparation method of above-mentioned aqueous-based ceramic flaw detection agent is simple, is easy to realize industrial production.
Referring to Fig. 2, a kind of ceramics method for detection fault detection, includes the following steps:
S210, ceramics are started the cleaning processing.
In a wherein embodiment, the step of starting the cleaning processing to ceramics, includes:
S211, cerdip is ultrasonically treated in degreaser.
In a wherein embodiment, ceramic product is put on rack for cleaning, the detection faces of product are unified upward.
Preferably, ceramics are completely immersed in degreaser.
In a wherein embodiment, degreaser is neutral degreaser agent.Preferably, degreaser is selected from Shijiazhuang Xiu Erte
It is limited that Hong Kongnization work is won in the GDT-664 of cleaning agent Co., Ltd, the JH-1212D of Changzhou monarch and Science and Technology Co., Ltd. or Suzhou
The agent for carbon hydrogen detergent of company.
In a wherein embodiment, the solvent of degreaser is water, and the mass concentration of degreaser is 5%~10%.
In a wherein embodiment, power when being ultrasonically treated is 4KW~6KW.
In a wherein embodiment, the time being ultrasonically treated is 10min~20min.
The greasy dirt and particle of surface of ceramic products can be effectively removed by the way that cerdip to be ultrasonically treated in degreaser
Object guarantees surface of ceramic products without greasy dirt, powder particle, and above-mentioned substance can all influence the effect of bleeding agent and imaging agent, greasy dirt
The surface of ceramics can be attached to and cause bleeding agent that can not permeate, and powder particle can make bleeding agent and imaging agent be unevenly distributed
Uniform residual, but also detection effect is deteriorated.
S212, ceramics are washed.
In a wherein embodiment, ceramics are washed by the way of spray.
In a wherein embodiment, the time of washing is 3min~7min.
S213, ceramics are dried.
In a wherein embodiment, withering temperature is 140 DEG C~160 DEG C, withering
Time is 10min~30min.
S220, infiltration processing is carried out to ceramics.
In a wherein embodiment, the step of infiltration is handled is carried out to ceramics and is specifically included:
S221, cerdip is permeated in water base bleeding agent.
In a wherein embodiment, water base bleeding agent is stirred so that water base bleeding agent helical form stream
It is dynamic.
In a wherein embodiment, the revolving speed of stir process is 20rad/min~60rad/min.
In a wherein embodiment, time that cerdip is permeated in water base bleeding agent be 5min~
20min。
In a wherein embodiment, water base bleeding agent includes: according to the mass fraction
In a wherein embodiment, dyestuff is according to the mass fraction, comprising:
It is 2.0 parts~4.0 parts carmine；
1.0 parts~3.0 parts of Aniline Red；And
Congo red 0.5 part~1.5 parts.
It is deep that dye colour is obtained using carmine, Aniline Red and Congo red cooperation according to a certain ratio, have compared with
Good coloring effect, so that the sensitivity of carrying out flaw detection improves, and above-mentioned material is nontoxic, has preferable safety.
In a wherein embodiment, penetrating solvent is in diethylene glycol ether, glycerine and diethylene glycol monomethyl ether
At least one.Above-mentioned penetrating solvent all has preferable water solubility, so that water base bleeding agent has preferable wetability, and easily
In cleaned, prevent bleeding agent from remaining on ceramic product and ceramic product is damaged.And above-mentioned penetrating solvent is with lower
Molecular weight, compared to high molecular polymer have better thermal stability.
In a wherein embodiment, surfactant is selected from fatty acid methyl ester ethoxy compound (PMEE) and laurel
At least one of alcohol polyoxyethylene ether.Most surfactant such as polyoxyethylene alkylphenol base ether all has toxicity, right
The eyes and skin of human body have a biggish irritation, and above-mentioned surfactant have compared to other surfaces activating agent it is lower
Irritation, more safety and environmental protection.
Above-mentioned water base bleeding agent obtains dyestuff using carmine, Aniline Red and Congo red cooperation according to a certain ratio, and
It is subject to penetrating solvent, surfactant and water, above-mentioned material all has that toxicity is lower, environment is non-hazardous, non-volatile, nonflammable
Feature, and coloring effect is good, can effectively improve detection sensitivity.Meanwhile above-mentioned water base bleeding agent has preferable water solubility, easily
In being cleaned.
S222, ceramics are washed.
In a wherein embodiment, ceramics are washed by the way of spray.
In a wherein embodiment, the time of washing is 3min~7min.
S223, ceramics are dried.
In a wherein embodiment, withering temperature is 50 DEG C~60 DEG C, when withering
Between be 10min~20min.
230, imaging processing is carried out to ceramics.
In a wherein embodiment, imaging agent is subjected to imaging processing to ceramics by the way of spraying.
In a wherein embodiment, mist of the ceramics in imaging agent is spraying the time be 2min~5min.
In a wherein embodiment, ceramics rotation in imaging agent is spraying is carried out, so that ceramics are uniformly in contact with aobvious
As agent.And imaging agent is subjected to processing to ceramics by the way of spraying and can control the thickness of imaging liquid, moreover, relative to leaching
Mode not can greatly save the dosage of imaging agent by the way of spraying, while imaging agent being made uniformly to remain in product
Surface, imaging results consistency are strong.
In a wherein embodiment, imaging agent is according to the mass fraction, comprising:
In a wherein embodiment, adsorbent is according to the mass fraction, comprising:
It is added that alum is primarily due to carmine, Aniline Red and the dyestuffs such as Congo red dye when in use in imaging agent
Ability is limited, inadequate in the adhesive force of ceramic surface, and the metallic salts such as iron, aluminium can be used as carmine mordant, enhancing
Dyestuff so that imaging results are more preferably, therefore are added alum in imaging agent and imaging effect can be improved in the adhesive force of ceramic surface
Fruit further increases the sensitivity of detection.
In a wherein embodiment, the partial size of silica is 40nm~100nm.
In a wherein embodiment, the partial size of magnesia is 40nm~100nm.
In a wherein embodiment, the partial size of titanium oxide is 40nm~100nm.
In a wherein embodiment, epoxy resin in E-42 type epoxy resin, E-44 type epoxy resin extremely
Few one kind.
Alum is added in above-mentioned imaging agent, dyestuff can be improved in the adhesive force of ceramic surface, so that imaging results are more preferably,
Further increase the sensitivity of detection；And fatty diglycollic amide has preferable water-soluble, stability and stronger infiltration
The advantages of detergency, so that imaging agent water can clean up, it is more adaptable；And the material of above-mentioned imaging agent is to environment
It is pollution-free and non-volatile, nonflammable, environment and human body will not be damaged, the bulk strong applicability used.
S240, ceramics are identified and are classified.
In a wherein embodiment, ceramic product is placed in automatic image detection device using manipulator, it is right
Ceramic product is identified and is classified, and the detection of product is completed.
Above-mentioned ceramics method for detection fault detection, is used cooperatively, no pollution to the environment and not using water base bleeding agent and imaging agent
It volatilizees, is nonflammable, environment and human body will not be damaged, the bulk strong applicability used, and above-mentioned ceramic carrying out flaw detection
Method identifiability is strong, the high sensitivity of detection.
It should be noted that step S210 and step S240 also can be omitted in above-mentioned ceramics method for detection fault detection.
Here is the explanation of specific embodiment, and following embodiment is unless otherwise specified, then inevitably miscellaneous without containing removing
The component pointed out is not known in other other than matter.
Embodiment 1
The dyestuff for weighing penetrating solvent diethylene glycol ether 50Kg and 3.5Kg is placed in blender, in stirring rate 50rad/
1h is stirred under the revolving speed of min to being uniformly mixed, wherein dyestuff includes the rigid of the famille rose of 2Kg, the Aniline Red of 1Kg and 0.5Kg
Arnotto；The surfactant ethoxylated dodecyl alcohol of 5Kg and the water of 41.5Kg is added into blender again, continues in stirring speed
0.5h is stirred under the revolving speed of rate 50rad/min；Product is all passed through to suction filtration again to handle to obtain water base bleeding agent, wherein strainer is
200 mesh filter screens.
The epoxy resin for weighing the adsorbent of 8Kg, the fatty diglycollic amide of 40Kg and 15Kg is placed in blender,
1h is stirred under the revolving speed of stirring rate 50rad/min to being uniformly mixed, wherein adsorbent includes the titanium dioxide of the alum of 5Kg, 1Kg
The titanium oxide of silicon, the magnesia of 1Kg and 1Kg；In the water that 37Kg is added into blender, continue continuing in stirring rate
0.5h is stirred under the revolving speed of 50rad/min obtains imaging agent.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
10min, then ceramics are washed by the way of spray, the time of washing is 3min, in 140 DEG C of drying process 10min；
Again cerdip is subjected to infiltration 5min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 3min, in 50 DEG C of drying process 10min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 2min；Ceramic product is identified.
Embodiment 2
The dyestuff for weighing penetrating solvent 60Kg and 4.5Kg is placed in blender, under the revolving speed of stirring rate 50rad/min
Stir 1h to be uniformly mixed, wherein penetrating solvent includes the diethylene glycol ether of 30Kg and the glycerine of 30Kg, and dyestuff includes 3Kg
Famille rose, 1Kg Aniline Red and 0.5Kg it is Congo red；Again into blender be added 5Kg surfactant FMEE and
The water of 30.5Kg, continuation stir 1h under the revolving speed of stirring rate 50rad/min；Product is all passed through to suction filtration again to handle to obtain
Water base bleeding agent, wherein strainer is 200 mesh filter screens.
The epoxy resin for weighing the adsorbent of 10.5Kg, the fatty diglycollic amide of 45Kg and 20Kg is placed in blender
In, 1h is stirred under the revolving speed of stirring rate 50rad/min to being uniformly mixed, wherein adsorbent includes the alum of 7.5Kg, 1Kg
Silica, the magnesia of 1Kg and the titanium oxide of 1Kg；In the water that 24.5Kg is added into blender, continue continuing stirring
It mixes stirring 1h under the revolving speed of rate 50rad/min and obtains imaging agent.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
15min, then ceramics are washed by the way of spray, the time of washing is 5min, in 150 DEG C of drying process 15min；
Again cerdip is subjected to infiltration 20min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 3min, in 50 DEG C of drying process 15min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 2min；Ceramic product is identified.
Embodiment 3
The dyestuff for weighing penetrating solvent 65Kg and 8Kg is placed in blender, is stirred under the revolving speed of stirring rate 60rad/min
Mix 1h to be uniformly mixed, wherein penetrating solvent includes the diethylene glycol of the glycerine of 19Kg, the diethylene glycol ether of 27Kg and 19Kg
Monomethyl ether, dyestuff include the Congo red of the famille rose of 4Kg, the Aniline Red of 3Kg and 1Kg；It is added 15Kg's into blender again
The water of surfactant and 12Kg, wherein surfactant includes the fatty diglycollic amide of the FMEE and 10Kg of 5Kg, is continued
0.5h is stirred under the revolving speed of stirring rate 60rad/min；Product is all passed through to suction filtration again to handle to obtain water base bleeding agent,
Middle strainer is 200 mesh filter screens.
The epoxy resin for weighing the adsorbent of 12Kg, the fatty diglycollic amide of 55Kg and 25Kg is placed in blender,
1h is stirred under the revolving speed of stirring rate 60rad/min to being uniformly mixed, wherein adsorbent includes the alum of 7.5Kg, 1.5Kg
The titanium oxide of silica, the magnesia of 2Kg and 1Kg；In the water that 8Kg is added into blender, continue continuing in stirring speed
0.5h is stirred under the revolving speed of rate 60rad/min obtains imaging agent.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
15min, then ceramics are washed by the way of spray, the time of washing is 5min, in 150 DEG C of drying process 15min；
Again cerdip is subjected to infiltration 7min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 7min, in 50 DEG C of drying process 15min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 3min；Ceramic product is identified.
Embodiment 4
The dyestuff for weighing penetrating solvent diethylene glycol ether 65Kg and 8.5Kg is placed in blender, in stirring rate 40rad/
1h is stirred under the revolving speed of min to being uniformly mixed, wherein dyestuff includes the rigid of the famille rose of 4Kg, the Aniline Red of 3Kg and 1.5Kg
Arnotto；The surfactant ethoxylated dodecyl alcohol of 20Kg and the water of 6.5Kg is added into blender again, continues in stirring speed
0.5h is stirred under the revolving speed of rate 40rad/min；Product is all passed through to suction filtration again to handle to obtain water base bleeding agent, wherein strainer is
200 mesh filter screens.
The epoxy resin for weighing the adsorbent of 17Kg, the fatty diglycollic amide of 55Kg and 25Kg is placed in blender,
Under the revolving speed of stirring rate 40rad/min stir 1h to be uniformly mixed, wherein adsorbent include the alum of 10Kg, 2Kg two
The titanium oxide of silica, the magnesia of 3Kg and 2Kg；In the water that 3Kg is added into blender, continue continuing in stirring rate
0.5h is stirred under the revolving speed of 40rad/min obtains imaging agent.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
15min, then ceramics are washed by the way of spray, the time of washing is 7min, in 160 DEG C of drying process 10min；
Again cerdip is subjected to infiltration 20min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 7min, in 60 DEG C of drying process 10min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 2min；Ceramic product is identified.
Embodiment 5
The dyestuff for weighing penetrating solvent diethylene glycol monomethyl ether 65Kg and 3.5Kg is placed in blender, in stirring rate
Under the revolving speed of 50rad/min stir 1h to be uniformly mixed, wherein dyestuff include the famille rose of 2Kg, 1Kg Aniline Red and
0.5Kg's is Congo red；The water of the surfactant FMEE and 26.5Kg of 5Kg is added into blender again, continues in stirring rate
0.5h is stirred under the revolving speed of 50rad/min；Product is all passed through to suction filtration again to handle to obtain water base bleeding agent, wherein strainer is
200 mesh filter screens.
The epoxy resin for weighing the adsorbent of 8Kg, the fatty diglycollic amide of 55Kg and 15Kg is placed in blender,
1h is stirred under the revolving speed of stirring rate 50rad/min to being uniformly mixed, wherein adsorbent includes the titanium dioxide of the alum of 5Kg, 1Kg
The titanium oxide of silicon, the magnesia of 1Kg and 1Kg；In the water that 22Kg is added into blender, continue continuing in stirring rate
0.5h is stirred under the revolving speed of 50rad/min obtains imaging agent.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
10min, then ceramics are washed by the way of spray, the time of washing is 3min, in 140 DEG C of drying process 10min；
Again cerdip is subjected to infiltration 5min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 3min, in 50 DEG C of drying process 10min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 2min；Ceramic product is identified.
Embodiment 6
The dyestuff for weighing penetrating solvent diethylene glycol ether 60Kg and 5.5Kg is placed in blender, in stirring rate 50rad/
1h is stirred under the revolving speed of min to being uniformly mixed, wherein dyestuff includes the rigid of the famille rose of 2Kg, the Aniline Red of 2Kg and 0.5Kg
Arnotto；The surfactant ethoxylated dodecyl alcohol of 5Kg and the water of 30.5Kg is added into blender again, continues in stirring speed
0.5h is stirred under the revolving speed of rate 50rad/min；Product is all passed through to suction filtration again to handle to obtain water base bleeding agent, wherein strainer is
200 mesh filter screens.
The epoxy resin for weighing the adsorbent of 13Kg, the fatty diglycollic amide of 50Kg and 20Kg is placed in blender,
1h is stirred under the revolving speed of stirring rate 50rad/min to being uniformly mixed, wherein adsorbent includes the dioxy of the alum of 8Kg, 2Kg
The titanium oxide of SiClx, the magnesia of 2Kg and 1Kg；In the water that 17Kg is added into blender, continue continuing in stirring rate
0.5h is stirred under the revolving speed of 50rad/min obtains imaging agent.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
10min, then ceramics are washed by the way of spray, the time of washing is 3min, in 140 DEG C of drying process 10min；
Again cerdip is subjected to infiltration 5min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 3min, in 50 DEG C of drying process 10min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 5min；Ceramic product is identified.
Embodiment 7
Weigh fatty acid triglycolyl amine, the 0.05Kg of the polyalcohol ethylene oxide adduct of 25Kg, the dyestuff of 6Kg, 7Kg
Benzotriazole, the polyoxyethylene alkylphenol base ether of 0.8Kg and the water of 61.15Kg be uniformly mixed and obtain penetrating fluid, wherein dyestuff packet
Include the Congo red of the rose-red of 2Kg, the famille rose of 2Kg and 2Kg.
Weigh the water soluble alkyd resin of 8Kg, the adsorbent of 6Kg, the fatty acid triglycolyl amine of 1.2Kg, 0.9Kg it is poly-
The water of ethylene oxide alkyl phenol ether through reaction and 83.9Kg are uniformly mixed and obtain imaging agent, and wherein adsorbent includes the magnesia of 3Kg, 1Kg
Titanium oxide and 2Kg white carbon black.
Ceramics are cleaned by ultrasonic using degreaser, wherein the power being ultrasonically treated is 6KW, the time of ultrasonic cleaning is
10min, then ceramics are washed by the way of spray, the time of washing is 3min, in 140 DEG C of drying process 10min；
Again cerdip is subjected to infiltration 5min in above-mentioned water base bleeding agent, then ceramics is washed by the way of spray, water
The time washed is 3min, in 50 DEG C of drying process 10min；Above-mentioned imaging agent is handled by infiltration by the way of spraying
Ceramics carry out imaging processing, mist of the ceramics in imaging agent is spraying the time be 5min；Ceramic product is identified.
The recall rate and sensitivity of the water base bleeding agent of Examples 1 to 7, imaging agent and ceramic method for detection fault detection are carried out
Assessment, is tested using 30um test block, and the results are shown in Table 1, and wherein recall rate and sensitivity are according to state marked as GB/T
18851.2-2005 method test.
Table 1
Each technical characteristic of embodiment described above can be combined arbitrarily, for simplicity of description, not to above-mentioned reality
It applies all possible combination of each technical characteristic in example to be all described, as long as however, the combination of these technical characteristics is not deposited
In contradiction, all should be considered as described in this specification.
The embodiments described above only express several embodiments of the present invention, and the description thereof is more specific and detailed, but simultaneously
It cannot therefore be construed as limiting the scope of the patent.It should be pointed out that coming for those of ordinary skill in the art
It says, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to protection of the invention
Range.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (9)
1. a kind of water base bleeding agent, which is characterized in that according to the mass fraction, comprising:
Wherein, the dyestuff is according to the mass fraction, comprising:
It is 2.0 parts~4.0 parts carmine；
1.0 parts~3.0 parts of Aniline Red；And
Congo red 0.5 part~1.5 parts；
Wherein, the penetrating solvent is selected from least one of diethylene glycol ether, glycerine and diethylene glycol monomethyl ether；The table
Face activating agent is selected from least one of fatty acid methyl ester ethoxy compound and ethoxylated dodecyl alcohol.
2. the preparation method of water base bleeding agent as described in claim 1, which comprises the following steps:
The penetrating solvent and the dyestuff are uniformly mixed and obtain mixture；And
The surfactant is added into the mixture and the water is uniformly mixed.
3. the preparation method of water base bleeding agent according to claim 2, which is characterized in that it is described by the penetrating solvent and
The time that the dyestuff is uniformly mixed mixed processing in the step of obtaining mixture is 1h~2h.
4. the preparation method of water base bleeding agent according to claim 2, which is characterized in that described to add into the mixture
The time for entering mixed processing in the step that the surfactant and the water are uniformly mixed is 0.5h~1h.
The agent 5. a kind of aqueous-based ceramic is detected a flaw, which is characterized in that including water base bleeding agent as described in claim 1 and imaging agent.
The agent 6. aqueous-based ceramic according to claim 5 is detected a flaw, which is characterized in that the imaging agent according to the mass fraction, wraps
It includes:
The agent 7. aqueous-based ceramic according to claim 6 is detected a flaw, which is characterized in that the adsorbent according to the mass fraction, wraps
It includes:
8. such as the preparation method of the described in any item aqueous-based ceramic flaw detection agent of claim 5~7, which is characterized in that including following
Step:
The penetrating solvent and the dyestuff are uniformly mixed and obtain mixture；
The surfactant is added into the mixture and the water is uniformly mixed and obtains water base bleeding agent；And
Prepare the imaging agent.
9. the preparation method of aqueous-based ceramic flaw detection agent according to claim 8, which is characterized in that described to prepare the imaging
The step of agent, specifically includes:
Adsorbent, fatty diglycollic amide and epoxy resin are uniformly mixed and obtain blend；And
Into blend, addition water, which is uniformly mixed, obtains the imaging agent.
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