CN114657574A - Preparation technology of efficient environment-friendly oil removal agent - Google Patents

Preparation technology of efficient environment-friendly oil removal agent Download PDF

Info

Publication number
CN114657574A
CN114657574A CN202210407419.3A CN202210407419A CN114657574A CN 114657574 A CN114657574 A CN 114657574A CN 202210407419 A CN202210407419 A CN 202210407419A CN 114657574 A CN114657574 A CN 114657574A
Authority
CN
China
Prior art keywords
parts
mixture
oil removing
removing agent
acid solution
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202210407419.3A
Other languages
Chinese (zh)
Inventor
陈振宇
何泽亮
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Xiamen Hecheng Huamei Technology Co ltd
Original Assignee
Xiamen Hecheng Huamei Technology Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Xiamen Hecheng Huamei Technology Co ltd filed Critical Xiamen Hecheng Huamei Technology Co ltd
Priority to CN202210407419.3A priority Critical patent/CN114657574A/en
Publication of CN114657574A publication Critical patent/CN114657574A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23GCLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G1/00Cleaning or pickling metallic material with solutions or molten salts
    • C23G1/24Cleaning or pickling metallic material with solutions or molten salts with neutral solutions

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention relates to the technical field of preparation of oil removal agents, in particular to a preparation process technology of an efficient environment-friendly oil removal agent, which comprises the following components in parts by weight: 30-60 parts of fatty alcohol-polyoxyethylene ether, 18-24 parts of pine oil, 16-40 parts of xylose powder, 10-15 parts of lignin, 40-80 parts of amino acid solution, 5 parts of swelling agent, 8 parts of plasticizer, 12 parts of thickener, 36 parts of dimethyl silicone oil and 100 parts of sterile water.

Description

Preparation technology of efficient environment-friendly oil removal agent
Technical Field
The invention relates to the technical field of preparation of oil removal agents, in particular to a preparation process technology of an efficient environment-friendly oil removal agent.
Background
When machining a metal workpiece, the surface of the metal product is often stained with oil. These oils mainly originate from oils introduced by mechanical or die-casting processes and from oils smeared during protective pre-treatments of the surfaces of metal products. These contaminants include engine oils, rust preventive oils, cutting oils, abrasive pastes, and the like. Such oil stains seriously affect the operation of the subsequent process and the quality of the product. The existing degreasing agent cannot completely remove oil stains on the surface of a metal product, and the degreasing agent contains more toxic substances and can cause harm to human bodies and the environment.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a preparation process technology of an efficient environment-friendly oil removing agent.
In order to achieve the purpose, the invention adopts the following technical scheme:
the preparation process technology of the high-efficiency environment-friendly oil removing agent comprises the following components in parts by weight: 30-60 parts of fatty alcohol-polyoxyethylene ether, 18-24 parts of pine oil, 16-40 parts of xylose powder, 10-15 parts of lignin, 40-80 parts of amino acid solution, 5 parts of swelling agent, 8 parts of plasticizer, 12 parts of thickener, 36 parts of dimethyl silicone oil and 100 parts of sterile water.
Preferably, the preparation method of the oil removing agent comprises the following steps:
s1, taking fatty alcohol-polyoxyethylene ether, terpineol oil, xylose powder, lignin and dimethyl silicone oil, stirring and mixing, and fully mixing the mixed material with an amino acid solution according to the mass ratio of 1:3 to obtain a mixture A;
s2, adding a swelling agent into the mixture A, and then putting the mixture A into an oven to dry for 2 hours at a constant temperature to obtain a mixture B;
s3, adding acid liquor into the mixture B, and adjusting the pH value to be 6-7 to obtain a mixture C;
s4, putting the mixture C into a reaction kettle, adding a plasticizer and sterile water, controlling the reaction temperature of the reaction kettle to be 55-70 ℃, and fully reacting for two hours to obtain a mixture D;
s5, adding a thickening agent into the mixture D to finally prepare the oil removing agent with the viscosity of 60-72 mPa & S.
Preferably, the fatty alcohol-polyoxyethylene ether comprises one or more of lauryl alcohol-polyoxyethylene ether and stearyl alcohol-polyoxyethylene ether.
Preferably, the swelling agent is an acidic swelling agent, and the swelling agent is one or more of potassium alum, ammonium alum and calcium hydrogen phosphate.
Preferably, the thickener is an inorganic thickener, and the thickener is one or more of methylcellulose, carboxymethylcellulose, hydroxyethylcellulose and hydroxypropylmethylcellulose.
Preferably, the dimethicone is one or more of polydimethylsiloxane, cyclomethicone, aminosiloxane, polymethylphenylsiloxane and polyether polysiloxane copolymer.
Preferably, the acid solution added to the reactant B is a weak acid solution, and the acid solution is citric acid or boric acid.
The invention has the beneficial effects that: through the degreaser that this scheme provided, solved the degreaser and can't thoroughly get rid of the greasy dirt, and the toxic component that contains in the degreaser can influence the health, causes the problem of environmental pollution etc. the efficiency piece is got rid of to the greasy dirt of metal surface rapidly to the proposition of this degreaser, and stubborn greasy dirt can not cause the injury to the human body yet, can not influence the environment yet, has extensive application market.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments.
Example 1
The preparation process technology of the high-efficiency environment-friendly oil removing agent comprises the following components in parts by weight: 30 parts of fatty alcohol-polyoxyethylene ether, 18 parts of pinitol oil, 20 parts of xylose powder, 10 parts of lignin, 40 parts of amino acid solution, 5 parts of swelling agent, 8 parts of plasticizer, 12 parts of thickening agent, 36 parts of dimethyl silicone oil and 100 parts of sterile water.
The preparation method of the oil removing agent comprises the following steps:
s1, taking fatty alcohol-polyoxyethylene ether, pinitol oil, xylose powder, lignin and polydimethylsiloxane, stirring and mixing, and fully mixing the mixed material with an amino acid solution according to the mass ratio of 1:3 to obtain a mixture A;
s2, adding potassium alum into the mixture A, putting the mixture A into an oven, and drying the mixture A for 2 hours at a constant temperature to obtain a mixture B;
s3, adding a citric acid solution into the mixture B, and adjusting the PH to be 6-7 to obtain a mixture C;
s4, putting the mixture C into a reaction kettle, adding a plasticizer and sterile water, controlling the reaction temperature of the reaction kettle to be 55-70 ℃, and fully reacting for two hours to obtain a mixture D;
s5, adding methyl cellulose into the mixture D to finally prepare the oil removing agent with viscosity of 60-72 mPa & S.
Example 2
The preparation process technology of the high-efficiency environment-friendly oil removing agent comprises the following components in parts by weight: 45 parts of fatty alcohol-polyoxyethylene ether, 20 parts of terpineol oil, 30 parts of xylose powder, 12 parts of lignin, 60 parts of amino acid solution, 5 parts of swelling agent, 8 parts of plasticizer, 12 parts of thickening agent, 36 parts of dimethyl silicone oil and 100 parts of sterile water.
The preparation method of the oil removing agent comprises the following steps:
s1, taking fatty alcohol-polyoxyethylene ether, pinitol oil, xylose powder, lignin and polydimethylsiloxane, stirring and mixing, and fully mixing the mixed material with an amino acid solution according to the mass ratio of 1:3 to obtain a mixture A;
s2, adding potassium alum into the mixture A, putting the mixture A into an oven, and drying the mixture A for 2 hours at a constant temperature to obtain a mixture B;
s3, adding a citric acid solution into the mixture B, and adjusting the PH to be 6-7 to obtain a mixture C;
s4, putting the mixture C into a reaction kettle, adding a plasticizer and sterile water, controlling the reaction temperature of the reaction kettle to be 55-70 ℃, and fully reacting for two hours to obtain a mixture D;
s5, adding methyl cellulose into the mixture D to finally prepare the oil removing agent with viscosity of 60-72 mPa & S.
Example 3
The preparation process technology of the high-efficiency environment-friendly oil removing agent comprises the following components in parts by weight: 60 parts of fatty alcohol-polyoxyethylene ether, 24 parts of pinitol oil, 40 parts of xylose powder, 15 parts of lignin, 80 parts of amino acid solution, 5 parts of swelling agent, 8 parts of plasticizer, 12 parts of thickening agent, 36 parts of dimethyl silicone oil and 100 parts of sterile water.
The preparation method of the oil removing agent comprises the following steps:
s1, taking fatty alcohol-polyoxyethylene ether, pinitol oil, xylose powder, lignin and polydimethylsiloxane, stirring and mixing, and fully mixing the mixed material with an amino acid solution according to the mass ratio of 1:3 to obtain a mixture A;
s2, adding potassium alum into the mixture A, putting the mixture A into an oven, and drying the mixture A for 2 hours at a constant temperature to obtain a mixture B;
s3, adding a boric acid solution into the mixture B, and adjusting the pH value to be 6-7 to obtain a mixture C;
s4, putting the mixture C into a reaction kettle, adding a plasticizer and sterile water, controlling the reaction temperature of the reaction kettle to be 55-70 ℃, and fully reacting for two hours to obtain a mixture D;
s5, adding methyl cellulose into the mixture D to finally prepare the oil removing agent with viscosity of 60-72 mPa & S.
The degreasing agents produced in the manufacturing processes of examples 1 to 3 were each subjected to a degreasing rate measurement according to JB/T4323.2-1999 Water-based Metal cleaner Standard; no. 45 steel is selected as the metal base material, and the specific test results are as follows:
example 1: the oil removal rate is 98.2%;
example 2: the oil removal rate is 99.1%;
example 3: the oil removal rate is 99.5%.
By combining the test components and the test data, the conclusion can be drawn that the oil removal agent prepared by using the raw materials provided by the application can meet the technical requirement of oil removal rate, the oil removal rate is obviously improved, and the raw materials do not contain hazardous substances, so that the harm to a human body can be reduced, and the pollution degree to the environment can also be reduced.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.

Claims (7)

1. The preparation technology of the high-efficiency environment-friendly oil removing agent is characterized by comprising the following components in parts by weight: 30-60 parts of fatty alcohol-polyoxyethylene ether, 18-24 parts of terpineol oil, 16-40 parts of xylose powder, 10-15 parts of lignin, 40-80 parts of amino acid solution, 5 parts of swelling agent, 8 parts of plasticizer, 12 parts of thickening agent, 36 parts of dimethyl silicone oil and 100 parts of sterile water.
2. The preparation process technology of the high-efficiency environment-friendly oil removing agent according to claim 1, characterized in that the preparation method of the oil removing agent comprises the following steps:
s1, taking fatty alcohol-polyoxyethylene ether, terpineol oil, xylose powder, lignin and dimethyl silicone oil, stirring and mixing, and fully mixing the mixed material with an amino acid solution according to the mass ratio of 1:3 to obtain a mixture A;
s2, adding a swelling agent into the mixture A, and then putting the mixture A into an oven to dry for 2 hours at a constant temperature to obtain a mixture B;
s3, adding acid liquor into the mixture B, and adjusting the pH value to be 6-7 to obtain a mixture C;
s4, putting the mixture C into a reaction kettle, adding a plasticizer and sterile water, controlling the reaction temperature of the reaction kettle to be 55-70 ℃, and fully reacting for two hours to obtain a mixture D;
s5, adding a thickening agent into the mixture D to finally prepare the oil removing agent with the viscosity of 60-72 mPa & S.
3. The preparation process technology of the efficient environment-friendly oil removing agent according to claim 1, characterized in that the fatty alcohol polyoxyethylene ether comprises one or more of lauryl alcohol polyoxyethylene ether and stearyl alcohol polyoxyethylene ether.
4. The preparation process technology of the high-efficiency environment-friendly oil removing agent according to claim 1, characterized in that the swelling agent is an acidic swelling agent, and the swelling agent is one or more of potassium alum, ammonium alum and calcium hydrogen phosphate.
5. The preparation process technology of the high-efficiency environment-friendly oil removing agent according to claim 1, characterized in that the thickener is an inorganic thickener, and is one or more of methylcellulose, carboxymethylcellulose, hydroxyethyl cellulose and hydroxypropyl methylcellulose.
6. The preparation process technology of the high-efficiency environment-friendly oil removing agent according to claim 1, characterized in that the dimethyl silicone oil is one or more of polydimethylsiloxane, cyclomethicone, aminosiloxane, polymethylphenylsiloxane and polyether polysiloxane copolymer.
7. The preparation process technology of the high-efficiency environment-friendly oil removing agent as claimed in claim 2, characterized in that the acid solution added in the reactant B is a weak acid solution, and the acid solution is citric acid or boric acid.
CN202210407419.3A 2022-04-19 2022-04-19 Preparation technology of efficient environment-friendly oil removal agent Pending CN114657574A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210407419.3A CN114657574A (en) 2022-04-19 2022-04-19 Preparation technology of efficient environment-friendly oil removal agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210407419.3A CN114657574A (en) 2022-04-19 2022-04-19 Preparation technology of efficient environment-friendly oil removal agent

Publications (1)

Publication Number Publication Date
CN114657574A true CN114657574A (en) 2022-06-24

Family

ID=82034450

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202210407419.3A Pending CN114657574A (en) 2022-04-19 2022-04-19 Preparation technology of efficient environment-friendly oil removal agent

Country Status (1)

Country Link
CN (1) CN114657574A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115536213A (en) * 2022-09-27 2022-12-30 广州思伊特环保科技有限公司 Oily wastewater treatment method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115536213A (en) * 2022-09-27 2022-12-30 广州思伊特环保科技有限公司 Oily wastewater treatment method

Similar Documents

Publication Publication Date Title
CN101113524B (en) Cleaning antirust agent and preparation method thereof
CN105297038A (en) Non-phosphorous water-based degreasing agent used in non-phosphorous coating pretreatment
CN114657574A (en) Preparation technology of efficient environment-friendly oil removal agent
CN107502892B (en) Alkaline chemical milling and polishing method for aluminum alloy
CN107513719A (en) A kind of metal cleaner for adding functional modification graphene and preparation method thereof
CN110067001A (en) A kind of metal cleaner and preparation method thereof
CN101012411A (en) Aluminum and aluminum alloy cleaning agent and using method thereof
CN109136964A (en) A kind of anti-rust cleaning agent and its application in hardware
CN110158107A (en) A kind of Wax removal water and its preparation process for medal polish part
CN109056028A (en) A kind of aluminium and aluminium alloy anode oxide aftertreatment fluid and preparation method thereof
CN111286418A (en) Plane grinding cleaning agent and preparation method thereof
CN106675875B (en) A kind of ceramics paraffin removal cleaning agent and preparation method thereof
CN107828546B (en) Environment-friendly passenger car engine cleaning agent and preparation process thereof
CN106894030B (en) Metal conditioner
CN104818492A (en) Aluminum alloy aqueous environment-friendly cleaning agent and preparation method of same
CN108754507A (en) A kind of ultrasonic cleaning agent and preparation method and application method
CN102400163A (en) Cleaning agent for stainless steel hot-rolled member and preparation method thereof
CN107474994A (en) Water-based air throttle cleaning agent and preparation method thereof
CN106637164A (en) Chelating phytic acid antirust enhanced water-based metal cleaner
CN106590967A (en) Rubber tire cleaning agent and preparation method and using method thereof
WO2017008219A1 (en) Wax removal agent
CN111321418B (en) Efficient heavy oil stain cleaning agent, preparation method thereof and heavy oil stain cleaning method
CN110882996A (en) Surface cleaning process for precision part
MY119363A (en) Anti-corrosive draining agent and rinsing process
CN108531300B (en) Scrubbing-free vehicle cleaning liquid and preparation method and application thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination