CN106675875B - A kind of ceramics paraffin removal cleaning agent and preparation method thereof - Google Patents
A kind of ceramics paraffin removal cleaning agent and preparation method thereof Download PDFInfo
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Abstract
The first object of the present invention is to provide a kind of ceramics paraffin removal cleaning agent, and raw material includes following components: potassium oleate, sodium cumene sulfonate, triethanolamine, glycerol, diethanol amine, ethylene glycol ethyl ether and deionized water.Ceramics of the invention are easy to get with each component in paraffin removal cleaning agent formula, and the cost being entirely formulated is low；The present invention, as surfactant and solubilizer, in conjunction with paraffin removal possessed by potassium oleate, has good cleaning effect for the wax of various compositions using sodium cumene sulfonate；Entire formula constitutes emulsion type cleaning agent, environmentally friendly, pollution-free.The second object of the present invention is to provide the preparation method that a kind of above-mentioned ceramics use paraffin removal cleaning agent, and processing step is simplified, and technological parameter is easy to control, and is suitble to industrialized production.
Description
Technical field
The present invention relates to ceramic processing technique fields, particularly, are related to a kind of ceramics paraffin removal cleaning agent and its preparation side
Method.
Background technique
When ceramic product is in process processed by shot blasting its surface, because product can not using clamp tool to its into
Row positioning need to be fixed product using sticky wax mode, and ceramic surface remains waxy substance after polishing treatment, therefore, need
The remaining wax of surface of ceramic products is removed, to achieve the purpose that clean surface.
Cleaning agent in the prior art is as follows:
Application No. is 201310728732.8 patent applications to disclose a kind of Environmental Safety scale removal wax removing agent, which removes
Cerate is formed according to weight percent: glycerol 10-20%, urea 1-2%, coconut acid diethanolamide 10-15%, ethanol amine
2.5-3%, hydrogen peroxide 10-20%, hydrochloric acid 5-10%, sodium metasilicate 2-9% and deionized water.This formula has scale removal brighter
Aobvious effect, and be not to paraffin removal effect it is particularly evident, to ceramics paraffin removal effect it is more unobvious.
Application No. is 201210395298.1 patent applications to disclose a kind of paraffin removal cleaning method, comprising the following steps:
(1) using the cleaning agent being made of following weight percent composition: 7.6-10.3% octyl phenol polyoxyethylene ether, 3.5-6.7%
Salicylic acid, 1.5-5.2% acetamide, 2.6-7.8%2- hydroxyphosphonoacetic acid, 4.1-8.3% sodium metasilicate, the Portugal 3.7-5.8%
Grape sodium saccharate, 5.1-9.2% ethyl alcohol, 1.3-4.0% isopropanol, 5.5-9.8% trichloro ethylene, surplus are deionized water；(2) first
The cloth of cleaning is immersed in cleaning agent, then wipes body surface with the cloth, until the removal of body surface wax is clean.The present invention
Paraffin removal method is not suitable for ceramic product, is easy to generate damage to product.
Application No. is 99115440.1 patent applications to disclose a kind of Wax removal water, the weight percent of constituent content
It is: coconut oil diethanol amide phosphate 18-25%, coconut oil diethanol amide 5-12%, fatty alcohol polyoxyethylene ether 1-
3%, nonylphenol polyoxyethylene ether 1-3%, thermally coupled distillation columns 1-5%, monoethanolamine 3-5%, water 56-63%
Composition.It is suitble to the polishing paraffin removal of metal product, is not suitable for ceramic product.
In conclusion paraffin removal formula in the prior art is not suitable for ceramic product, therefore, in industry be badly in need of it is a kind of at
This is low, paraffin removal effect is good and is suitable for the paraffin removal cleaning agent of ceramic product.
Summary of the invention
The first object of the present invention is to provide a kind of ceramics use at low cost, paraffin removal effect is good and suitable for ceramic product
Paraffin removal cleaning agent, specific technical solution are as follows:
A kind of ceramics paraffin removal cleaning agent, raw material includes following components in terms of mass fraction:
10.5-11.5 parts of triethanolamine of 0.4-0.8 parts of sodium cumene sulfonate of 12-13 parts of potassium oleate
4.0-4.5 parts of ethylene glycol ethyl ether of 1.0-1.5 parts of diethanol amine of 2.5-3.5 parts of glycerol
65-68 parts of deionized water.
Preferred in above technical scheme, raw material includes following components in terms of mass fraction:
12 parts of potassium oleate, 10.5 parts of triethanolamine of 0.4 part of sodium cumene sulfonate
2.5 parts of glycerol, 4.0 parts of ethylene glycol ethyl ether of 1.0 parts of diethanol amine
67 parts of deionized water.
Preferred in above technical scheme, raw material includes following components in terms of mass fraction:
12.5 parts of potassium oleate, 11 parts of triethanolamine of 0.6 part of sodium cumene sulfonate
3 parts of glycerol, 4.2 parts of ethylene glycol ethyl ether of 1.2 parts of diethanol amine
67 parts of deionized water.
Preferred in above technical scheme, raw material includes following components in terms of mass fraction:
13 parts of potassium oleate, 11.5 parts of triethanolamine of 0.8 part of sodium cumene sulfonate
3.5 parts of glycerol, 4.5 parts of ethylene glycol ethyl ether of 1.5 parts of diethanol amine
68 parts of deionized water.
Using ceramics of the invention paraffin removal cleaning agent, have the advantages that ceramics of the invention are cleaned with paraffin removal
Agent includes potassium oleate, sodium cumene sulfonate, triethanolamine, glycerol, diethanol amine, ethylene glycol ethyl ether and deionized water, is matched
Each component is easy to get in side, and the cost being entirely formulated is low.The present invention use sodium cumene sulfonate, have the effect that a,
As anionic surfactant, lotion is formed with water, there is excellent solvability, cleaning effect to rosin, organic compound
It is good；B, it is used as solubilizer, itself has excellent emulsification and dispersion performance, and stability is strong in acid and alkaline medium；Oil
Sour potassium has very strong paraffin removal, and in the hydrophobic grouping of oleic acid acid molecule, active biggish double bond, dissolubility is good, for
The greasy dirt of various compositions, wax all have good cleaning performance；Entire formula constitutes emulsion type cleaning agent, environmentally friendly,
It is pollution-free.
The second object of the present invention is to provide a kind of preparation method of above-mentioned ceramics paraffin removal cleaning agent, includes following step
It is rapid:
Deionized water first is weighed in designed ratio and is added into blender, turn on agitator；It successively will be corresponding
Six kinds of potassium oleate of ratio, sodium cumene sulfonate, triethanolamine, diethanol amine, ethylene glycol ethyl ether and glycerol substance difference
It feeds, the charging process is comprising being added raw material and stirring evenly two steps.
It is preferred in above technical scheme, it is described stir evenly during: stirring rate is 2000 rpms, stirring temperature
Degree is 22 degrees Celsius -27 degrees Celsius.
Preparation method processing step of the present invention is simplified, and technological parameter is easy to control, and is suitble to industrialized production.
Other than objects, features and advantages described above, there are also other objects, features and advantages by the present invention.
Below with reference to specific embodiment, the present invention is described in further detail.
Specific embodiment
Technical solution of the present invention is described in detail with reference to embodiments, but the present invention can be according to claim
It limits and the multitude of different ways of covering is implemented.
Embodiment 1:
A kind of ceramics paraffin removal cleaning agent, includes following components:
12 kilograms of potassium oleate, 10.5 kilograms of triethanolamine of 0.4 kilogram of sodium cumene sulfonate
2.5 kilograms of glycerol, 4.0 kilograms of ethylene glycol ethyl ether of 1.0 kilograms of diethanol amine
67 kilograms of deionized water.
The above-mentioned ceramics preparation method of paraffin removal cleaning agent comprising the steps of:
Step 1: first weighed deionized water is added in blender, turn on agitator；
Step 2: weighed potassium oleate is added in blender and is stirred uniformly, the first mixture is obtained；
Step 3: it will be stirred in the first mixture in weighed sodium cumene sulfonate addition blender
It is even, obtain the second mixture；
Step 4: it will be stirred uniformly, obtain in the second mixture in weighed triethanolamine addition blender
Third mixture；
Step 5: it will be stirred uniformly, obtain in the third mixture in weighed diethanol amine addition blender
4th mixture；
Step 6: it will be stirred uniformly, obtain in the 4th mixture in weighed ethylene glycol ethyl ether addition blender
To the 5th mixture；
Step 7: it will be stirred uniformly in the 5th mixture in weighed glycerol addition blender, obtain this hair
Bright ceramics paraffin removal cleaning agent, is labeled as MK1.
Above-mentioned steps two are into step 7, and the stirring rate of blender is set in 2000 rpms, whipping temp setting
At 25 degrees Celsius.
Embodiment 2:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
12.5 kilograms of potassium oleate, 11 kilograms of triethanolamine of 0.6 kilogram of sodium cumene sulfonate
3 kilograms of glycerol, 4.2 kilograms of ethylene glycol ethyl ether of 1.2 kilograms of diethanol amine
67 kilograms of deionized water.
The ceramics that the present embodiment is obtained are labeled as MK2 with paraffin removal cleaning agent.
Embodiment 3:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
13 kilograms of potassium oleate, 11.5 kilograms of triethanolamine of 0.8 kilogram of sodium cumene sulfonate
3.5 kilograms of glycerol, 4.5 kilograms of ethylene glycol ethyl ether of 1.5 kilograms of diethanol amine
68 kilograms of deionized water.
The ceramics that the present embodiment is obtained are labeled as MK3 with paraffin removal cleaning agent.
Comparative example 1:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
13 kilograms of potassium oleate, 4.5 kilograms of ethylene glycol ethyl ether of 11.5 kilograms of triethanolamine
3.5 kilograms of glycerol, 68 kilograms of deionized water of 1.5 kilograms of diethanol amine.
The above-mentioned ceramics preparation method of paraffin removal cleaning agent comprising the steps of:
Step 1: first weighed deionized water is added in blender, turn on agitator；
Step 2: weighed potassium oleate is added in blender and is stirred uniformly, the first mixture is obtained；
Step 3: it will be stirred uniformly, obtain in the first mixture in weighed triethanolamine addition blender
The second ' mixture；
Step 4: it will be stirred uniformly, obtain in the second ' mixture in weighed diethanol amine addition blender
Third ' mixture；
Step 5: it will be stirred uniformly, obtain in the third ' mixture in weighed ethylene glycol ethyl ether addition blender
To the 4th ' mixture；
Step 6: it will be stirred uniformly in the 4th ' mixture in weighed glycerol addition blender, it is right to obtain this
Than the ceramics paraffin removal cleaning agent of embodiment, it is labeled as DMK1.
Above-mentioned steps two are into step 7, and the stirring rate of blender is set in 2000 rpms, whipping temp setting
At 25 degrees Celsius.
Comparative example 2:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
13 kilograms of potassium oleate, 11.5 kilograms of triethanolamine of 0.05 kilogram of sodium cumene sulfonate
3.5 kilograms of glycerol, 4.5 kilograms of ethylene glycol ethyl ether of 1.5 kilograms of diethanol amine
68 kilograms of deionized water.
The ceramics that the present embodiment is obtained are labeled as DMK2 with paraffin removal cleaning agent.
Comparative example 3:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
13 kilograms of potassium oleate, 11.5 kilograms of triethanolamine of 0.2 kilogram of sodium cumene sulfonate
3.5 kilograms of glycerol, 4.5 kilograms of ethylene glycol ethyl ether of 1.5 kilograms of diethanol amine
68 kilograms of deionized water.
The ceramics that the present embodiment is obtained are labeled as DMK3 with paraffin removal cleaning agent.
Comparative example 4:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
13 kilograms of potassium oleate, 11.5 kilograms of triethanolamine of 1.0 kilograms of sodium cumene sulfonate
3.5 kilograms of glycerol, 4.5 kilograms of ethylene glycol ethyl ether of 1.5 kilograms of diethanol amine
68 kilograms of deionized water.
The ceramics that the present embodiment is obtained are labeled as DMK4 with paraffin removal cleaning agent.
Comparative example 5:
Difference from Example 1 is: ceramics include following components with paraffin removal cleaning agent:
13 kilograms of potassium oleate, 11.5 kilograms of triethanolamine of 1.2 kilograms of sodium cumene sulfonate
3.5 kilograms of glycerol, 4.5 kilograms of ethylene glycol ethyl ether of 1.5 kilograms of diethanol amine
68 kilograms of deionized water.
The ceramics that the present embodiment is obtained are labeled as DMK5 with paraffin removal cleaning agent.
Using following methods to embodiment 1, embodiment 2, embodiment 3 and comparative example 1-5 it is resulting totally eight kinds it is clear
Lotion is tested, and see Table 1 for details for effect.
Test method: same a batch ceramic product to be processed (yellow wax after surface adhesion solidification) is divided into according to 10 every group
8 groups；A certain amount of eight kinds of paraffin removal cleaning agents are measured respectively, are added in rinse bath, are increased temperature to 75 ± 5 DEG C, are opened ultrasonic wave,
Ultrasonic wave current strength is set as 2.5 amperes, and ultrasonic frequency is set as 28 kHz, and scavenging period is set as 180 seconds.
1 embodiment 1 of table, embodiment 2, the test result of embodiment 3 and comparative example 1-5 products obtained therefrom
As known from Table 1, when not adding sodium cumene sulfonate (comparative example 1) with addition sodium cumene sulfonate
(embodiment 1-3) compares, and the dosage for adding the paraffin removal cleaning agent of sodium cumene sulfonate significantly reduces, and paraffin removal effect has
It significantly improves；When sodium cumene sulfonate dosage very few (comparative example 2 and comparative example 3), the use of paraffin removal cleaning agent
It measures or bigger, but the wax of surface of ceramic products can be completely removed；When sodium cumene sulfonate dosage is excessive, (comparison is implemented
Example 4 and comparative example 5) when, the dosage of paraffin removal cleaning agent is not reduced significantly, and paraffin removal effect is basically unchanged.Therefore, it adopts
With the ceramics paraffin removal cleaning agent of inventive formulation, dosage is appropriate under the premise of guaranteeing paraffin removal effect, practical.
The foregoing is only a preferred embodiment of the present invention, is not intended to restrict the invention, for the skill of this field
For art personnel, the invention may be variously modified and varied.All within the spirits and principles of the present invention, made any to repair
Change, equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (6)
1. a kind of ceramics paraffin removal cleaning agent, it is characterised in that: raw material includes following components in terms of mass fraction:
2. ceramics paraffin removal cleaning agent according to claim 1, it is characterised in that: raw material includes following in terms of mass fraction
Component:
3. ceramics paraffin removal cleaning agent according to claim 1, it is characterised in that: raw material includes following in terms of mass fraction
Component:
4. ceramics paraffin removal cleaning agent according to claim 1, it is characterised in that: raw material includes following in terms of mass fraction
Component:
5. a kind of preparation method of the ceramics paraffin removal cleaning agent as described in claim 1-4 any one, it is characterised in that: packet
Containing following steps:
Deionized water first is weighed in designed ratio and is added into blender, turn on agitator；Successively by corresponding proportion
Potassium oleate, sodium cumene sulfonate, triethanolamine, six kinds of diethanol amine, ethylene glycol ethyl ether and glycerol substances carry out respectively
Charging, the charging process is comprising being added raw material and stirring evenly two steps.
6. the preparation method that ceramics according to claim 5 use paraffin removal cleaning agent, it is characterised in that: described to stir evenly
Cheng Zhong: stirring rate is 2000 rpms, and whipping temp is 22 degrees Celsius -27 degrees Celsius.
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| CN201510753831.0A CN106675875B (en) | 2015-11-06 | 2015-11-06 | A kind of ceramics paraffin removal cleaning agent and preparation method thereof |
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| CN106675875B true CN106675875B (en) | 2019-01-22 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107326372B (en) * | 2017-06-17 | 2019-12-03 | 苏州元联科技创业园管理有限公司 | A kind of preparation method of wax removing agent |
| EP3781373A4 (en) * | 2018-04-20 | 2022-03-16 | PostProcess Technologies Inc. | Finishing mediums and finishing suspensions |
| CN114574291B (en) * | 2022-03-02 | 2023-06-23 | 南充三环电子有限公司 | Wax removing composition, preparation method and application thereof |
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| CN1193341A (en) * | 1995-06-27 | 1998-09-16 | 普罗格特-甘布尔公司 | Cleaning/sanitizing methods, compositions, and/or articles for fabric |
| JPH11199896A (en) * | 1998-01-14 | 1999-07-27 | Asahi Chem Ind Co Ltd | Detergent without requiring water rinse |
| CN102010806A (en) * | 2010-11-11 | 2011-04-13 | 彭美东 | Rapid wax removing agent |
| CN102051271A (en) * | 2011-01-24 | 2011-05-11 | 北京洛娃日化有限公司 | Dewaxing agent |
| WO2012040561A1 (en) * | 2010-09-24 | 2012-03-29 | Invista Technologies S.A R.L. | Composition for surface treatment and process |
| CN103966034A (en) * | 2014-05-26 | 2014-08-06 | 深圳市荣强科技有限公司 | Surfactant for paraffin removal water and preparation method thereof |
| CN104745333A (en) * | 2013-12-25 | 2015-07-01 | 吴旭 | Environmental-protection safe descaling wax removing agent |
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2015
- 2015-11-06 CN CN201510753831.0A patent/CN106675875B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1193341A (en) * | 1995-06-27 | 1998-09-16 | 普罗格特-甘布尔公司 | Cleaning/sanitizing methods, compositions, and/or articles for fabric |
| JPH11199896A (en) * | 1998-01-14 | 1999-07-27 | Asahi Chem Ind Co Ltd | Detergent without requiring water rinse |
| WO2012040561A1 (en) * | 2010-09-24 | 2012-03-29 | Invista Technologies S.A R.L. | Composition for surface treatment and process |
| CN102010806A (en) * | 2010-11-11 | 2011-04-13 | 彭美东 | Rapid wax removing agent |
| CN102051271A (en) * | 2011-01-24 | 2011-05-11 | 北京洛娃日化有限公司 | Dewaxing agent |
| CN104745333A (en) * | 2013-12-25 | 2015-07-01 | 吴旭 | Environmental-protection safe descaling wax removing agent |
| CN103966034A (en) * | 2014-05-26 | 2014-08-06 | 深圳市荣强科技有限公司 | Surfactant for paraffin removal water and preparation method thereof |
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