CN109276485A - A kind of acne-removing sheet and preparation method thereof - Google Patents
A kind of acne-removing sheet and preparation method thereof Download PDFInfo
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- CN109276485A CN109276485A CN201811129090.9A CN201811129090A CN109276485A CN 109276485 A CN109276485 A CN 109276485A CN 201811129090 A CN201811129090 A CN 201811129090A CN 109276485 A CN109276485 A CN 109276485A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0208—Tissues; Wipes; Patches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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Abstract
The invention discloses a kind of acne-removing sheets and preparation method thereof, belong to cosmetic technical field, acne-removing sheet is made of cured content on patch and patch, content is grouped as by the group of following mass percentage: Fermentation in Pichia Pastoris lysis object filtrate 5%~90%, glycerol 5%~90%, parahydroxyacet-ophenone 0.5%~1%, 1,2 hexylene glycols 0.5%~1% and hydroxy ethyl fiber 0~1%, surplus are water.The effect of formula and preparation method of acne-removing sheet of the present invention complement each other, can significantly improve anti-acne.
Description
Technical field
The invention belongs to cosmetic technical fields more particularly to a kind of acne-removing sheet and preparation method thereof.
Background technique
Acne-removing sheet is a kind of research staff's patch newly developed, and main advantage is safely and effectively and to facilitate local use.
The patch shape of acne-removing sheet is different, very attraction consumer's sight.Traditional acne-removing sheet is mainly with Chinese medicine composite parts, anti-corrosion
Fungicide is main component, wherein a part of acne-removing sheet is using patch material as Research Emphasis, which can prevent to infect.
However, existing acne-removing sheet is in terms of acne-removing up for further improving.Therefore, it is necessary to design a kind of new
The acne-removing sheet of type, the effect of to improve anti-acne.
Summary of the invention
Present invention aims to overcome that the shortcomings of the prior art, and a kind of acne-removing sheet is provided and preparation method thereof, it should
The effect of formula and preparation method of acne-removing sheet complement each other, can significantly improve anti-acne.
To achieve the above object, the technical scheme adopted by the invention is as follows: a kind of acne-removing sheet, by solidifying on patch and patch
Content composition, the content is grouped as by the group of following mass percentage: Fermentation in Pichia Pastoris lysis object
Filtrate 5%~90%, glycerol 5%~90%, parahydroxyacet-ophenone 0.5%~1%, 1,2 hexylene glycols 0.5%~1% and hydroxyl second
Base fiber 0~1%, surplus are water.
Fermentation in Pichia Pastoris lysis object filtrate is mentioned after being fermented under given conditions using pichia pastoris yeast
The lysis object filtrate taken, with powerful Antimicrobial ability, such as Propiobacterium；It can also promote wound healing, prevent scar
Trace promotes hyaluronic acid synthesis and repairs skin barrier and improve immunity.Currently, Fermentation in Pichia Pastoris lysis object is filtered
Liquid is only used for whitening in cosmetics.Glycerol is that colourless, odorless, sweet and appearance is in clear and bright thick liquid, can moisturizing, antioxygen
Change, promote alcoholization.Parahydroxyacet-ophenone is one of cosmetics new food preservative, with good anti-corrosion effect and high safety
Property, but itself preservative catalogue is not limited the use of " cosmetics safety technical specification " 2015 editions, very by consumer and factory
The preference of family.1,2- hexylene glycol is one of cosmetics new food preservative, with good anti-corrosion effect and high security,
But itself does not limit the use of preservative catalogue " cosmetics safety technical specification " 2015 editions, very by consumer and manufacturer
Preference.Hydroxyethyl cellulose (HEC) is a kind of white or faint yellow, tasteless and nontoxic threadiness or pulverulent solids, can
It is prepared by the etherified reaction of alkali cellulose and ethylene oxide (or chlorethanol), HEC has good thickening, suspends, divides
It dissipates, emulsification, bonding, film forming, the protection characteristics such as moisture and protecting colloid.
The content of acne-removing sheet of the present invention by Fermentation in Pichia Pastoris lysis object filtrate, glycerol, parahydroxyacet-ophenone,
1,2 oneself two and hydroxy ethyl fiber (or be not present hydroxy ethyl fiber) composition, have been surprisingly found that Fermentation in Pichia Pastoris lysis object
Filtrate can promote wound healing, prevention scar and reparation skin barrier and improve immunity, the fermentation material understood with consumer
With whitening and other effects difference, it is very suitable to acne-removing sheet；In addition, when the acne-removing sheet of production can facilitate local use and increase stop
Between well to play effect.
As an improvement of the above technical solution, the content is grouped as by the group of following mass percentage: Pasteur
Pichia pastoris fermentation lysis object filtrate 10%, glycerol 5%, parahydroxyacet-ophenone 0.5%, 1,2 hexylene glycols 0.5% and ethoxy are fine
Dimension 0.1%, surplus is water.
As an improvement of the above technical solution, the content is grouped as by the group of following mass percentage: Pasteur
Pichia pastoris fermentation lysis object filtrate 15%, glycerol 10%, parahydroxyacet-ophenone 1%, 1,2 hexylene glycols 1% and hydroxy ethyl fiber
0, surplus is water.
As an improvement of the above technical solution, the content is grouped as by the group of following mass percentage: Pasteur
Pichia pastoris fermentation lysis object filtrate 20%, glycerol 20%, parahydroxyacet-ophenone 1%, 1,2 hexylene glycols 1% and hydroxy ethyl fiber
0.5%, surplus is water.
The present invention is defined the inclusion content of acne-removing sheet, finds above-mentioned 3 kinds of acne-removing sheet anti-acne function allotted
Effect is more preferable.
In addition, the present invention also provides the preparation methods of the acne-removing sheet comprising following steps:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, is stirred
It mixes and is warming up to 80~85 DEG C, and keep the temperature 30 minutes；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate is added, is stirred
200 mesh screens are crossed after mixing uniformly, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content after sterilizing
Solidify on patch after sterilization, then successively sealing, coding and packaging.
The beneficial effects of the present invention are: the present invention to provide a kind of acne-removing sheet and preparation method thereof, acne-removing sheet of the present invention
Content by Fermentation in Pichia Pastoris lysis object filtrate, glycerol, parahydroxyacet-ophenone, 1,2 oneself two and hydroxy ethyl fiber group
At having been surprisingly found that Fermentation in Pichia Pastoris lysis object filtrate can promote wound healing, prevention scar and repair skin barrier
And improve immunity；In the preparation process of acne-removing sheet, the sequence and temperature that considered critical material is added are controlled, it is ensured that Pasteur
Pichia pastoris fermentation lysis object filtrate active constituent is active, and mixes well various components.
Specific embodiment
Purposes, technical schemes and advantages in order to better illustrate the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
Embodiment 1
The present embodiment provides a kind of acne-removing sheet, acne-removing sheet is made of cured content on patch and patch, content by
The group of following mass percentage is grouped as: Fermentation in Pichia Pastoris lysis object filtrate 10%, glycerol 5%, para hydroxybenzene
0.5%, 1,2 hexylene glycol 0.5% of ethyl ketone and hydroxy ethyl fiber 0.1%, surplus are water.
In addition, the preparation method of above-mentioned acne-removing sheet the following steps are included:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, is stirred
It mixes and is warming up to 80~85 DEG C, and keep the temperature 30 minutes；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate is added, is stirred
200 mesh screens are crossed after mixing uniformly, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content after sterilizing
Solidify on patch after sterilization, then successively sealing, coding and packaging.
Embodiment 2
The present embodiment provides a kind of acne-removing sheet, acne-removing sheet is made of cured content on patch and patch, content by
The group of following mass percentage is grouped as: Fermentation in Pichia Pastoris lysis object filtrate 15%, glycerol 10%, para hydroxybenzene
1%, 1,2 hexylene glycol 1% of ethyl ketone and hydroxy ethyl fiber 0, surplus are water.
In addition, the preparation method of above-mentioned acne-removing sheet the following steps are included:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, is stirred
It mixes and is warming up to 80~85 DEG C, and keep the temperature 30 minutes；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate is added, is stirred
200 mesh screens are crossed after mixing uniformly, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content after sterilizing
Solidify on patch after sterilization, then successively sealing, coding and packaging.
Embodiment 3
The present embodiment provides a kind of acne-removing sheet, acne-removing sheet is made of cured content on patch and patch, content by
The group of following mass percentage is grouped as: Fermentation in Pichia Pastoris lysis object filtrate 20%, glycerol 20%, para hydroxybenzene
1%, 1,2 hexylene glycol 1% of ethyl ketone and hydroxy ethyl fiber 0.5%, surplus are water.
In addition, the preparation method of above-mentioned acne-removing sheet the following steps are included:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, is stirred
It mixes and is warming up to 80~85 DEG C, and keep the temperature 30 minutes；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate is added, is stirred
200 mesh screens are crossed after mixing uniformly, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content after sterilizing
Solidify on patch after sterilization, then successively sealing, coding and packaging.
Embodiment 4
The present embodiment provides a kind of acne-removing sheet, acne-removing sheet is made of cured content on patch and patch, content by
The group of following mass percentage is grouped as: Fermentation in Pichia Pastoris lysis object filtrate 5%, glycerol 90%, para hydroxybenzene
0.7%, 1,2 hexylene glycol 0.8% of ethyl ketone and hydroxy ethyl fiber 1%, surplus are water.
In addition, the preparation method of above-mentioned acne-removing sheet the following steps are included:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, is stirred
It mixes and is warming up to 80~85 DEG C, and keep the temperature 30 minutes；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate is added, is stirred
200 mesh screens are crossed after mixing uniformly, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content after sterilizing
Solidify on patch after sterilization, then successively sealing, coding and packaging.
Embodiment 5
The present embodiment provides a kind of acne-removing sheet, acne-removing sheet is made of cured content on patch and patch, content by
The group of following mass percentage is grouped as: Fermentation in Pichia Pastoris lysis object filtrate 90%, glycerol 6%, para hydroxybenzene
0.5%, 1,2 hexylene glycol 0.5% of ethyl ketone and hydroxy ethyl fiber 0.5%, surplus are water.
In addition, the preparation method of above-mentioned acne-removing sheet the following steps are included:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, is stirred
It mixes and is warming up to 80~85 DEG C, and keep the temperature 30 minutes；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate is added, is stirred
200 mesh screens are crossed after mixing uniformly, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content after sterilizing
Solidify on patch after sterilization, then successively sealing, coding and packaging.
Comparative example 1
This comparative example provides a kind of acne-removing sheet, is with the distinctive points of 1 acne-removing sheet of embodiment: Bath is free of in content
Moral Pichia pastoris fermentation lysis object filtrate.
Comparative example 2
This comparative example provides a kind of acne-removing sheet, is with the distinctive points of 2 acne-removing sheet of embodiment: Bath is free of in content
Moral Pichia pastoris fermentation lysis object filtrate.
Comparative example 3
This comparative example provides a kind of acne-removing sheet, is with the distinctive points of 3 acne-removing sheet of embodiment: Bath is free of in content
Moral Pichia pastoris fermentation lysis object filtrate.
Effect example 1
Bacteriostatic experiment is carried out to Fermentation in Pichia Pastoris lysis object filtrate of the invention, strain is acne propionic acid bar
Bacterium, the results are shown in Table 1.
Table 1
As shown in table 1, the Fermentation in Pichia Pastoris lysis object filtrate being added in acne-removing sheet of the present invention has good
Bacteriostasis efficacy can inhibit bacterial growth in acne.
Effect example 2
Using the acne-removing sheet of Examples 1 to 3 as research object；60 subjects are chosen, men and women is fifty-fifty, and skin is normal；Point
It is 3 groups, each 10 people of every group of men and women.Acne-removing sheet is covered on subject's arm and is not easy touching place, 24 hours removing acne-removing sheets divide
Not Qu Chu after observation dermoreaction in 0.5,12,24,48 hour, be classified according to skin in " cosmetics safety technical specification " 2015 editions
Its result of standard recording.
Human skin patch experimental result is shown: each group subject pastes the acne-removing sheet of Examples 1 to 3,0.5,12,
24, do not occur skin adverse reaction after 48 hours, it is safe to illustrate that acne-removing sheet of the present invention uses.
Effect example 3
Using the acne-removing sheet of Examples 1 to 3 and comparative example 1~3 as research object；120 subjects are chosen, men and women is fifty-fifty,
Age is 20~40, and face has apparent acne and small pox, and no skin disease allergies meet subject and volunteer inclusion criteria.It surveys
Method for testing: selection has acne region, in clean affected part, respectively pastes 1 acne-removing sheet sooner or later daily, tries out 2 weeks；Subject is trying
Kept for good daily life system time and eating habit with period；The feedback of subject is counted after 2 weeks；The results are shown in Table 2.
Table 2
As shown in table 2, acne-removing sheet of the present invention can well anti-acne, repair skin and repair acne print, i.e., improvement red swelling of the skin,
The vigorous and smooth skin of fat secretion.
Only list the effect example of 1~3 acne-removing sheet of the embodiment of the present invention above, other embodiments of the invention acne-removing sheet can also be with
Obtain similar anti-acne effect.If the content of acne-removing sheet is grouped as by the group of following mass percentage: pichia pastoris yeast
Ferment lysis object filtrate 5%~90%, glycerol 5%~90%, parahydroxyacet-ophenone 0.5%~1%, 1,2 hexylene glycols 0.5%~
1% and hydroxy ethyl fiber 0~1%, surplus be water；Then acne-removing sheet can anti-acne reparation well.
Finally, it should be noted that above embodiments protect the present invention to illustrate technical solution of the present invention
The limitation of range, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should be managed
Solution, can modify to technical solution of the present invention or replace on an equal basis, without departing from technical solution of the present invention essence and
Range.
Claims (5)
1. a kind of acne-removing sheet is made of, which is characterized in that the content is by following matter cured content on patch and patch
The group of amount percentage composition is grouped as: Fermentation in Pichia Pastoris lysis object filtrate 5%~90%, glycerol 5%~90%, to hydroxyl
0.5%~1%, 1,2 hexylene glycol 0.5%~1% of benzoylformaldoxime and hydroxy ethyl fiber 0~1%, surplus are water.
2. acne-removing sheet as described in claim 1, which is characterized in that the content is grouped by the group of following mass percentage
At: Fermentation in Pichia Pastoris lysis object filtrate 10%, glycerol 5%, parahydroxyacet-ophenone 0.5%, 1,2 hexylene glycols 0.5%
With hydroxy ethyl fiber 0.1%, surplus is water.
3. acne-removing sheet as described in claim 1, which is characterized in that the content is grouped by the group of following mass percentage
At: Fermentation in Pichia Pastoris lysis object filtrate 15%, glycerol 10%, parahydroxyacet-ophenone 1%, 1,2 hexylene glycols 1% and hydroxyl
Ethyl cellulose 0, surplus are water.
4. acne-removing sheet as described in claim 1, which is characterized in that the content is grouped by the group of following mass percentage
At: Fermentation in Pichia Pastoris lysis object filtrate 20%, glycerol 20%, parahydroxyacet-ophenone 1%, 1,2 hexylene glycols 1% and hydroxyl
Ethyl cellulose 0.5%, surplus are water.
5. such as the preparation method of the described in any item acne-removing sheets of Claims 1 to 4, which comprises the following steps:
S1 water) is added into reaction kettle, glycerol, hydroxyethyl cellulose and parahydroxyacet-ophenone are sequentially added under homogeneous, stirring rises
Temperature keeps the temperature 30 minutes to 80~85 DEG C；
S2 after) stirring is cooled to 35 DEG C, 1,2- hexylene glycol, Fermentation in Pichia Pastoris lysis object filtrate are added, stirring is equal
200 mesh screens are crossed after even, are discharged up to content；
S3) select suitable patch, patch and content are fitted into aluminum foil bag sterilize it is spare；By the content solidification after sterilizing
On patch after sterilization, then successively sealing, coding and packaging.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811129090.9A CN109276485B (en) | 2018-09-26 | 2018-09-26 | Acne removing patch and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811129090.9A CN109276485B (en) | 2018-09-26 | 2018-09-26 | Acne removing patch and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN109276485A true CN109276485A (en) | 2019-01-29 |
| CN109276485B CN109276485B (en) | 2021-07-20 |
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| CN201811129090.9A Active CN109276485B (en) | 2018-09-26 | 2018-09-26 | Acne removing patch and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110123682A (en) * | 2019-04-03 | 2019-08-16 | 广州市拉凯尔干细胞研究所 | A kind of personal care articles preparation method with inhibition propionibacterium acnes |
| CN111920719A (en) * | 2020-08-28 | 2020-11-13 | 陈绍胜 | Composition for improving acne marks and scars and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176562A (en) * | 2016-07-22 | 2016-12-07 | 律璇 | A kind of antimicrobial form facial film with whitening skin and preserving moisture effect |
| CN106667854A (en) * | 2017-03-02 | 2017-05-17 | 刘金凤 | Hydrating and whitening mask capable of accelerating damaged skin regeneration |
-
2018
- 2018-09-26 CN CN201811129090.9A patent/CN109276485B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106176562A (en) * | 2016-07-22 | 2016-12-07 | 律璇 | A kind of antimicrobial form facial film with whitening skin and preserving moisture effect |
| CN106667854A (en) * | 2017-03-02 | 2017-05-17 | 刘金凤 | Hydrating and whitening mask capable of accelerating damaged skin regeneration |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110123682A (en) * | 2019-04-03 | 2019-08-16 | 广州市拉凯尔干细胞研究所 | A kind of personal care articles preparation method with inhibition propionibacterium acnes |
| CN111920719A (en) * | 2020-08-28 | 2020-11-13 | 陈绍胜 | Composition for improving acne marks and scars and preparation method thereof |
| CN111920719B (en) * | 2020-08-28 | 2021-09-07 | 广州市万千粉丝化妆品有限公司 | Composition for improving acne marks and scars and preparation method thereof |
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| CN109276485B (en) | 2021-07-20 |
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