CN109251614A - A kind of aqueous road paint marking and preparation method thereof - Google Patents
A kind of aqueous road paint marking and preparation method thereof Download PDFInfo
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- CN109251614A CN109251614A CN201810971793.XA CN201810971793A CN109251614A CN 109251614 A CN109251614 A CN 109251614A CN 201810971793 A CN201810971793 A CN 201810971793A CN 109251614 A CN109251614 A CN 109251614A
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- paint marking
- road paint
- aqueous road
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Road Signs Or Road Markings (AREA)
- Road Repair (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention discloses a kind of aqueous road paint marking, it is characterised in that: by weight percentage, including following components: polyester acrylic acid composite emulsion 15-20%, bead 25-28%, titanium dioxide 15-20%, talcum powder 12-15%, anti-settling agent 1-2%, antifreezing agent 0.5-1%, dispersing agent 0.5-0.8%, wetting agent 0.1-0.2%, defoaming agent 0.3-0.5%, pH adjusting agent 0.2-0.3%, preservative 0.2-0.6%, thickener 0.2-0.5%, water 20-25%.Aqueous road paint marking of the present invention has excellent wear-resistant and water resistance, while having extensive adhesive force, while the glass microballoon of its high refractive index reaches apparent reflecting signal function, is suitable for the pavement strips such as pitch or cement concrete.
Description
Technical field
The present invention relates to technical field of coatings, more particularly to a kind of aqueous road paint marking and preparation method thereof.
Background technique
Currently, China's paint marking coating is using C5 Petropols and Abietyl modified resin as the heat molten type of base-material and with poly- third
Alkene acid ester resin is based on the room temperature solvent type of base-material.With the development of the times, scientific and technological progress, such coating type is by single
Room temperature solvent type develop into room temperature solvent type, thermal solvent type, heat molten type and environment-friendly type coating.
Heat reflow paint there are speed of applications it is slow, execution conditions are poor, difficulty of relocating the disadvantages of, solvent based coating contains largely
Volatile organic matter (VOC) in paint film drying process, very big pollution and harm is caused to ambient enviroment, does not meet environmental protection
Requirement.And the solvent free of epoxy flooring coating mainly replaces non-activated thinner come real using reactive reactive diluent
Existing, non-activated thinner cannot be reacted with epoxy resin and curing agent, and sheerly physics is mixed into process in formula for it；Dosage
There is detrimental effect almost without influence, but to the chemical resistance of film to film physical property when few；Dosage can drop when big
Low film physical property, especially because non-activated thinner evolution volatilization, can cause under the increase of film shrinkage and bonding force
Drop.Reactive diluent viscosity itself is low, containing epoxy group, can be reacted into the microstructure of film with amine hardener, if with
Amount is suitable, can reduce viscosity of the coating and meet job requirements, ensure that the mechanical property and chemical resistance of film.However, nothing
Reactive diluent in solvent epoxy coating still has volatilization smell toxic, with irritating in coating material production and work progress,
Injury will cause to human body, in coating production process many times these all it is ignored fall.
Currently used paint marking product is not environmentally in the market, solid content is low and contains volatile solvent, coating when construction
Thicker, the 3-4 that needs to cross improves construction cost and manual labor all over that could form, and the paint marking color formed is not fresh
Gorgeous, profile pattern, glossiness are bad.Moreover, existing paint marking product, general to pass through addition such as lead, mercury, cadmium, arsenic and six
The poisonous and hazardous metallic element such as valence chromium can seriously endanger production in this way, apply to reduce cost, embody its color and performance
The personal safety of worker person.Therefore, the standard for how improving the performance of product, reducing coating number, reaching indoor and outdoor environmental protection
Become the necessary condition of product development.
Summary of the invention
The object of the present invention is to provide a kind of aqueous road paint markings and preparation method thereof, are deposited with solving the above-mentioned prior art
The problem of, make aqueous road paint marking that there is excellent wear-resistant and water resistance, while there is extensive adhesive force, at the same its
The glass microballoon of high refractive index reaches apparent reflecting signal function, is suitable for the pavement strips such as pitch or cement concrete.
To achieve the above object, the present invention provides following schemes:
The present invention provides a kind of aqueous road paint marking, it is characterised in that: by weight percentage, including following components:
Polyester acrylic acid composite emulsion 15-20%, bead 25-28%, titanium dioxide 15-20%, talcum powder 12-15%, anti-settling agent 1-
2%, antifreezing agent 0.5-1%, dispersing agent 0.5-0.8%, wetting agent 0.1-0.2%, defoaming agent 0.3-0.5%, pH adjusting agent
0.2-0.3%, preservative 0.2-0.6%, thickener 0.2-0.5%, water 20-25%.
Preferably, the titanium dioxide is rutile type titanium white, and content of titanium dioxide is greater than 95%, and whiteness is greater than 94%.
Preferably, the talcum powder is white silicate mineral, and partial size is 800-1250 mesh, and whiteness is greater than 90%.
Preferably, the anti-settling agent is aqueous polyamide anti-settling agent, and the antifreezing agent is propylene glycol.
Preferably, the dispersing agent is Sodium Polyacrylate dipersant, admittedly contain 40%.
Preferably, the wetting agent is fatty alcohol alkoxy compound, and the defoaming agent is organic silicon.
Preferably, the pH adjusting agent is 2-amino-2-methyl-1-propanol.
Preferably, the preservative is isothiazolinone preservative, and the thickener is non-ionic polyurethane association type
Thickener.
Preferably, the partial size of the bead is 100-200 mesh.
The present invention also provides a kind of preparation methods of aqueous road paint marking, it is characterised in that: the following steps are included:
(1) precise above-mentioned raw material proportioning the water of precise is added in scuffing of cylinder bore or big tank, in low speed 400-
In the state of 600r/min, it is successively slowly added to dispersing agent, wetting agent, defoaming agent, anti-settling agent stirs 1- after the completion of addition
2min；
(2) in the state of improving revolving speed to high speed 1000-1200r/min, after high speed dispersion 20-30min, revolving speed is reduced extremely
In the state of 400-600r/min, titanium dioxide, talcum powder are sequentially added, then improves revolving speed to 1000-1200r/min, high speed
Dispersion 30 minutes, until fineness≤55 μm；
(3) reduce revolving speed to low speed (400-600r/min) state under, be added polyester acrylic acid composite emulsion, bead,
After stirring 2-3min, thickener is added in antifreezing agent, pH adjusting agent, preservative, and being adjusted to viscosity is 85-95KU (25 DEG C), at a slow speed
(400-600r/min) is stirred 15 minutes, and aqueous road paint marking is made.
The invention discloses following technical effects:
(1) the polyester acrylic acid composite emulsion that the present invention selects, polyester is shell, and acrylic acid is core, has had both polyester and third
The advantages that hardness and durability of olefin(e) acid, and there is extensive adhesive force, excellent wear-resistant and water resistance, minimum film formation temperature
It is 0 DEG C, glass transition temperature is 45 DEG C, admittedly containing 50 ± 2%, does not need addition coalescing agent, the characteristic of quick-drying keeps paint film quick
Do not glue tire, nonflammable, safe operation.
(2) bead selected of the present invention is that demifacet is aluminized reflective glass beads, and refractive index is 1.9 or more, due to micro-
The high refraction action of pearl and optically focused on the special reflecting layer of microballon focus, reflecting layer by 88% light by transparent microballon again
Again it is reflected near light source, very bright reflected light can be seen at light source, keeps driver bad at night or the visual field
In the case of clearly see travel route.
(3) present invention is that environmental type product is equipped with good face and fills out using environmental protection, quick-dry type core-shell emulsion as base-material
Material, specific function auxiliary agent, deionized water etc. are refined with unique formula through modern crafts, by the glass for adding high refractive index
Glass pearl achievees the effect that reflective, warning, is suitable for the pavement strips such as pitch or cement concrete, and then be used for urban road, height
Fast highway, high-grade highway, airfield runway, parking lot graticule.
Specific embodiment
It is clearly and completely described below in conjunction with the technical solution in the embodiment of the present invention, it is clear that described reality
Applying example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is general
Logical technical staff every other embodiment obtained without making creative work belongs to what the present invention protected
Range.
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, With reference to embodiment
The present invention is described in further detail.
The preparation of 1 aqueous road paint marking of embodiment
(1) raw material proportioning
Prepare the raw material proportioning of aqueous road paint marking are as follows: by weight percentage, polyester acrylic acid composite emulsion 20%,
Bead 26%, titanium dioxide 16%, talcum powder 15%, anti-settling agent 1%, antifreezing agent 0.5%, dispersing agent 0.5%, wetting agent
0.1%, defoaming agent 0.3%, pH adjusting agent 0.2%, preservative 0.2%, thickener 0.2%, water 20%.
Wherein, titanium dioxide is rutile type titanium white, and content of titanium dioxide is greater than 95%, and whiteness is greater than 94%；Talcum powder
For white silicate mineral, partial size is 800-1250 mesh, and whiteness is greater than 90%；Anti-settling agent is aqueous polyamide anti-settling agent；It is antifreeze
Agent is propylene glycol；Dispersing agent is Sodium Polyacrylate dipersant, admittedly contain 40%；Wetting agent is fatty alcohol alkoxy compound；Defoaming
Agent is organic silicon, selects 5400 that this moral of hamming is modest；PH adjusting agent is 2-amino-2-methyl-1-propanol；Preservative is different thiophene
Oxazoline ketone preservative selects the MBS or RS of Sol；Thickener is nonionic polyurethane Associative thickener；The grain of bead
Diameter is 100-200 mesh.
(2) preparation of aqueous road paint marking
Step a, the water of precise is added in scuffing of cylinder bore or big tank raw material proportioning described in precise step (1),
In the state of low speed 400-600r/min, it is successively slowly added to dispersing agent, wetting agent, defoaming agent, anti-settling agent stirs after the completion of addition
Mix 1-2min；
Step b, it in the state of improving revolving speed to high speed 1000-1200r/min, after high speed dispersion 20-30min, reduces and turns
In the state of speed to 400-600r/min, titanium dioxide, talcum powder are sequentially added, then raising revolving speed to 1000-1200r/min,
High speed dispersion 30 minutes, until fineness≤55 μm；
Step c, it reduces under revolving speed to low speed (400-600r/min) state, polyester acrylic acid composite emulsion, glass is added
After stirring 2-3min, thickener is added in pearl, antifreezing agent, pH adjusting agent, preservative, and being adjusted to viscosity is 85-95KU (25 DEG C),
400-600r/min is stirred 15 minutes at a slow speed, and aqueous road paint marking is made.
The preparation of 2 aqueous road paint marking of embodiment
(1) raw material proportioning
Prepare the raw material proportioning of aqueous road paint marking are as follows: by weight percentage, polyester acrylic acid composite emulsion 18%,
Bead 27%, titanium dioxide 17%, talcum powder 13%, anti-settling agent 1.5%, antifreezing agent 0.6%, dispersing agent 0.6%, wetting agent
0.1%, defoaming agent 0.4%, pH adjusting agent 0.2%, preservative 0.3%, thickener 0.3%, water 21%.
Wherein, titanium dioxide is rutile type titanium white, and content of titanium dioxide is greater than 95%, and whiteness is greater than 94%；Talcum powder
For white silicate mineral, partial size is 800-1250 mesh, and whiteness is greater than 90%；Anti-settling agent is aqueous polyamide anti-settling agent；It is antifreeze
Agent is propylene glycol；Dispersing agent is Sodium Polyacrylate dipersant, admittedly contain 40%；Wetting agent is fatty alcohol alkoxy compound；Defoaming
Agent is organic silicon, selects 5400 that this moral of hamming is modest；PH adjusting agent is 2-amino-2-methyl-1-propanol；Preservative is different thiophene
Oxazoline ketone preservative selects the MBS or RS of Sol；Thickener is nonionic polyurethane Associative thickener；The grain of bead
Diameter is 100-200 mesh.
(2) preparation of aqueous road paint marking
Step a, the water of precise is added in scuffing of cylinder bore or big tank raw material proportioning described in precise step (1),
In the state of low speed 400-600r/min, it is successively slowly added to dispersing agent, wetting agent, defoaming agent, anti-settling agent stirs after the completion of addition
Mix 1-2min；
Step b, it in the state of improving revolving speed to high speed 1000-1200r/min, after high speed dispersion 20-30min, reduces and turns
In the state of speed to 400-600r/min, titanium dioxide, talcum powder are sequentially added, then raising revolving speed to 1000-1200r/min,
High speed dispersion 30 minutes, until fineness≤55 μm；
Step c, it reduces under revolving speed to low speed (400-600r/min) state, polyester acrylic acid composite emulsion, glass is added
After stirring 2-3min, thickener is added in pearl, antifreezing agent, pH adjusting agent, preservative, and being adjusted to viscosity is 85-95KU (25 DEG C),
(400-600r/min) is stirred 15 minutes at a slow speed, and aqueous road paint marking is made.
The preparation of 3 aqueous road paint marking of embodiment
(1) raw material proportioning
Prepare the raw material proportioning of aqueous road paint marking are as follows: by weight percentage, polyester acrylic acid composite emulsion 15%,
Bead 28%, titanium dioxide 18%, talcum powder 12%, anti-settling agent 1.4%, antifreezing agent 1%, dispersing agent 0.8%, wetting agent
0.2%, defoaming agent 0.5%, pH adjusting agent 0.3%, preservative 0.4%, thickener 0.4%, water 22%.
Wherein, titanium dioxide is rutile type titanium white, and content of titanium dioxide is greater than 95%, and whiteness is greater than 94%；Talcum powder
For white silicate mineral, partial size is 800-1250 mesh, and whiteness is greater than 90%；Anti-settling agent is aqueous polyamide anti-settling agent；It is antifreeze
Agent is propylene glycol；Dispersing agent is Sodium Polyacrylate dipersant, admittedly contain 40%；Wetting agent is fatty alcohol alkoxy compound；Defoaming
Agent is organic silicon, selects 5400 that this moral of hamming is modest；PH adjusting agent is 2-amino-2-methyl-1-propanol；Preservative is different thiophene
Oxazoline ketone preservative selects the MBS or RS of Sol；Thickener is nonionic polyurethane Associative thickener；The grain of bead
Diameter is 100-200 mesh.
(2) preparation of aqueous road paint marking
Step a, the water of precise is added in scuffing of cylinder bore or big tank raw material proportioning described in precise step (1),
In the state of low speed 400-600r/min, it is successively slowly added to dispersing agent, wetting agent, defoaming agent, anti-settling agent stirs after the completion of addition
Mix 1-2min；
Step b, it in the state of improving revolving speed to high speed 1000-1200r/min, after high speed dispersion 20-30min, reduces and turns
In the state of speed to 400-600r/min, titanium dioxide, talcum powder are sequentially added, then raising revolving speed to 1000-1200r/min,
High speed dispersion 30 minutes, until fineness≤55 μm；
Step c, it reduces under revolving speed to low speed (400-600r/min) state, polyester acrylic acid composite emulsion, glass is added
After stirring 2-3min, thickener is added in pearl, antifreezing agent, pH adjusting agent, preservative, and being adjusted to viscosity is 85-95KU (25 DEG C),
(400-600r/min) is stirred 15 minutes at a slow speed, and aqueous road paint marking is made.
Embodiment 4
Aqueous road paint marking prepared by embodiment 1-3 according to JT/T280-2004 " pavement marking paint ",
GB18582-2008 " limits of harmful substances in indoor decorating and refurnishing materials interior wall coating ", GB/T16311-2005 " road traffic
Graticule quality requirement and detection method " this 3 standards carry out functional detections, and testing result see the table below shown in 1.The results show that
Aqueous road paint marking prepared by embodiment 1-3 has excellent wear-resistant and water resistance, while having extensive adhesive force,
The glass microballoon of its high refractive index reaches apparent reflecting signal function simultaneously, and VOC and heavy metal etc. are in the model being not detected
It in enclosing, will not be affected human health in construction application, be suitable for the pavement strips such as pitch or cement concrete, in turn
For urban road, highway, high-grade highway, airfield runway, parking lot graticule.
Table 1
Embodiment described above is only that preferred embodiment of the invention is described, and is not carried out to the scope of the present invention
It limits, without departing from the spirit of the design of the present invention, those of ordinary skill in the art make technical solution of the present invention
Various changes and improvements, should all fall into claims of the present invention determine protection scope in.
Claims (10)
1. a kind of aqueous road paint marking, it is characterised in that: by weight percentage, including following components: the compound propylene of polyester
Yogurt liquid 15-20%, bead 25-28%, titanium dioxide 15-20%, talcum powder 12-15%, anti-settling agent 1-2%, antifreezing agent
0.5-1%, dispersing agent 0.5-0.8%, wetting agent 0.1-0.2%, defoaming agent 0.3-0.5%, pH adjusting agent 0.2-0.3% prevent
Rotten agent 0.2-0.6%, thickener 0.2-0.5%, water 20-25%.
2. aqueous road paint marking according to claim 1, it is characterised in that: the titanium dioxide is rutile titanium dioxide
Powder, content of titanium dioxide are greater than 95%, and whiteness is greater than 94%.
3. aqueous road paint marking according to claim 1, it is characterised in that: the talcum powder is white silicate mine
Object, partial size are 800-1250 mesh, and whiteness is greater than 90%.
4. aqueous road paint marking according to claim 1, it is characterised in that: the anti-settling agent is that aqueous polyamide is anti-settling
Agent, the antifreezing agent are propylene glycol.
5. aqueous road paint marking according to claim 1, it is characterised in that: the dispersing agent is Sodium Polyacrylate salinity
Powder, admittedly contain 40%.
6. aqueous road paint marking according to claim 1, it is characterised in that: the wetting agent is fatty alcohol alkoxylates
Object, the defoaming agent are organic silicon.
7. aqueous road paint marking according to claim 1, it is characterised in that: the pH adjusting agent is 2- amino -2- first
Base -1- propyl alcohol.
8. aqueous road paint marking according to claim 1, it is characterised in that: the preservative is anti-for isothiazolinone
Rotten agent, the thickener are nonionic polyurethane Associative thickener.
9. aqueous road paint marking according to claim 1, it is characterised in that: the partial size of the bead is 100-200
Mesh.
10. a kind of preparation method of aqueous road paint marking as described in any one of claims 1 to 9, it is characterised in that: including
Following steps:
(1) precise raw material proportioning described in claim 1 the water of precise is added in scuffing of cylinder bore or big tank, in low speed
In the state of 400-600r/min, it is successively slowly added to dispersing agent, wetting agent, defoaming agent, anti-settling agent stirs 1- after the completion of addition
2min；
(2) in the state of improving revolving speed to high speed 1000-1200r/min, after high speed dispersion 20-30min, revolving speed is reduced to 400-
In the state of 600r/min, titanium dioxide, talcum powder are sequentially added, then improves revolving speed to 1000-1200r/min, high speed dispersion
30 minutes, until fineness≤55 μm；
(3) reduce revolving speed to low speed 400-600r/min state under, be added polyester acrylic acid composite emulsion, bead, antifreezing agent,
After stirring 2-3min, thickener is added in pH adjusting agent, preservative, and it is 85-95KU that viscosity is adjusted under 25 DEG C of environment, at a slow speed
400-600r/min is stirred 15 minutes, and aqueous road paint marking is made.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201810971793.XA CN109251614A (en) | 2018-08-24 | 2018-08-24 | A kind of aqueous road paint marking and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810971793.XA CN109251614A (en) | 2018-08-24 | 2018-08-24 | A kind of aqueous road paint marking and preparation method thereof |
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| CN109251614A true CN109251614A (en) | 2019-01-22 |
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| CN109651898A (en) * | 2019-01-24 | 2019-04-19 | 苏州拓博琳新材料科技有限公司 | A kind of aqueous self-luminous gage mark coating and preparation method thereof |
| EP3778787A1 (en) * | 2019-08-12 | 2021-02-17 | M. Swarovski Gesellschaft m.b.H. | Paint composition |
| CN113621303A (en) * | 2021-09-09 | 2021-11-09 | 十堰恐龙化工有限公司 | Quick-drying and wear-resistant normal-temperature cold-sprayed thick-paste road marking paint and preparation method thereof |
| CN114907731A (en) * | 2022-04-14 | 2022-08-16 | 湖南优冠体育材料有限公司 | Preparation method and device of special marking paint for plastic track |
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| CN113621303A (en) * | 2021-09-09 | 2021-11-09 | 十堰恐龙化工有限公司 | Quick-drying and wear-resistant normal-temperature cold-sprayed thick-paste road marking paint and preparation method thereof |
| CN114907731A (en) * | 2022-04-14 | 2022-08-16 | 湖南优冠体育材料有限公司 | Preparation method and device of special marking paint for plastic track |
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Application publication date: 20190122 |