CN109251594A - A kind of peasant's paint and preparation method thereof and application method - Google Patents
A kind of peasant's paint and preparation method thereof and application method Download PDFInfo
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D103/00—Coating compositions based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09D103/12—Amylose; Amylopectin; Degradation products thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/02—Processes; Apparatus
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K3/00—Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
- B27K3/16—Inorganic impregnating agents
- B27K3/18—Compounds of alkaline earth metals
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
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- B27K5/0085—Thermal treatments, i.e. involving chemical modification of wood at temperatures well over 100°C
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B27—WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
- B27K—PROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
- B27K9/00—Chemical or physical treatment of reed, straw, or similar material
- B27K9/002—Cane, bamboo
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B30/00—Preparation of starch, degraded or non-chemically modified starch, amylose, or amylopectin
- C08B30/20—Amylose or amylopectin
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- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
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- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
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Abstract
The present invention provides a kind of peasant's paint and preparation method thereof and application method, and in particular to painting material technical field.The present invention includes the raw material of following weight part ratio: 400-500 parts of water, 80-120 parts of water-saturated n-butanol, 25-35 parts of cassava, 25-35 parts of glutinous rice, 25-35 parts of building glue, 5-15 parts of lime paste powder, 5-15 parts of Chinese gall ash, 5-15 parts of fruit of a cubeb litsea tree charcoal, 125-165 parts of lemon juice, 1-3 parts of ethyl acetate and 0.5-1.5 parts of antioxidant 1010.Peasant picture paint color produced by the present invention is gorgeous, glossiness is high, anti-oxidant, fast light, environmentally friendly；Preparation method raw material availability provided by the invention is high, pigment is with high purity, and technological parameter is controllable, is easy to industrialization；The drawing works of drawing pigment of the present invention can be not easy it is infested, not perishable, be not easy to go mouldy.
Description
[technical field]
The present invention relates to painting material technical fields, and in particular to a kind of peasant's paint and preparation method thereof and user
Method.
[background technique]
Magnificent dazzling, gorgeous, different style national folk technique is people of all nationalities in long-term production, life
The art constantly created and accumulated in practice.It not only reflects the life style and thought of different times various nationalities
Consciousness, and be the specific and tangible witness of each historical progress of various nationalities.Wherein, the peasant picture of Guangxi Dong ethnic group
It is a wherein dazzling jewel, is a kind of phenomenon of Guangxi Minority social life, its basis is the society of this nationality
Living needs visually reflect religious ethics thought, philosophy of life, the aesthetic reason of ethnic group in the form of two-dimensional space
Think, national spirit, folkways, national memory, history expression, material life environmental aspect, there is hand down, communality, reality
With property and functionality.
Dong ancients gradually find out the various types of materials for making paint in permanent work, to keep paintings color
The vividness and persistence in pool, it is a large amount of to use the heavy metals minerals as main component such as many leaded, arsenic, mercury, make to paint
Works produce potential threat to people's health, and by directly contacting or sucking contact, these heavy metals easily enter circulation
System leads to hematologic disease and organ disease.
Currently, it is less for the linguistic term of peasant's paint, but Tangka's drawing pigment with Tibetan's characteristic occurs
Relevant Research Literature, upper and peasant's paint has similarity in material composition, Chinese patent Authorization Notice No. is
CN105038299B, it is entitled it is a kind of draw Tangka pigment production method patent document in, disclose it is a kind of using safflower,
The method that Asian puccoon, indigo plant leaf, gamboge make three kinds of Essential colour pigment of red, blue, yellow is improving mainly using plant as primary raw material
There is certain improvement in vegetable pigment color persistence, but does not make a search to the light fade of pigment, and also inevitably
The cinnabar containing mercuric sulphide ingredient is used, however it remains the risk of heavy metal poisoning.Although some researchs are not belonging to a small number of people
Race's painting field, but be also the wisdom crystallization of civil working people, in the improvement that can also use for reference peasant's paint, China is specially
Sharp Publication No. CN102618106A, it is entitled one kind several pieces pictures environmental-friendly pigment patent document in, propose a kind of use
Huang that safflower, cinnabar, Asian puccoon, Liaolan, azurite, folium isatidis, gamboge liquid, pine-soot ink various plants and mineral are mixed, blueness,
Red, black four kinds of Essential colour pigment, improves water-fast, fast light, colour fading performance；But every kind of raw material has itself intrinsic color, not
Identical to the greatest extent, a kind of color uses the preparation of various plants raw material in the invention, leads to colour contamination, not pure enough, so that pigment
Vividness is not high, color is dull.
Therefore, it to solve the problems, such as that the traditional farmers paint feature of environmental protection is low, color is dull, light fugitive, oxidizable, needs out
Send out peasant's paint a kind of.
[summary of the invention]
Goal of the invention of the invention is: for peasant's paint feature of environmental protection is low, color is dull, light fugitive, oxidizable
Problem provides a kind of peasant's paint, and peasant picture paint color of the invention is gorgeous, glossiness is high, anti-oxidant, fast light, environmentally friendly；
Preparation method raw material availability provided by the invention is high, pigment is with high purity, and technological parameter is controllable, is easy to industrialization；Agriculture of the present invention
People's paint draw works can be not easy it is infested, not perishable, be not easy to go mouldy.
To achieve the goals above, The technical solution adopted by the invention is as follows:
A kind of peasant's paint, the raw material including following weight part ratio: 400-500 parts of water, water-saturated n-butanol 80-120
Part, 25-35 parts of cassava, 25-35 parts of glutinous rice, 25-35 parts of building glue, 5-15 parts of lime paste powder, 5-15 parts of Chinese gall ash and mountain
Grey sub- charcoal 5-15 parts.
The scheme advanced optimized further includes the raw material of following weight part ratio: 125-165 parts of lemon juice, ethyl acetate 1-3
Part and antioxidant 1010 0.5-1.5 parts.
The scheme advanced optimized, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross 70-90
After mesh to get.
The scheme advanced optimized, the fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then powder
It is broken, cross 85-95 mesh to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 30-50 minutes, water is then added, is heated 8-16 minutes at 80-90 DEG C, keeps temperature-resistant, continuously adds water saturation
N-butanol is cooled to room temperature, then filters, after filtrate recycling design, be dried to do at 90-100 DEG C after stirring 3-6 minutes
Cream, then crushed, obtain starch mixture；
B. starch mixture is taken, Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder is added, is uniformly mixed, building is then added
Glue heats 20-30 minutes at 70-80 DEG C, is then cooled to room temperature, obtains black pigment.
The scheme advanced optimized, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 35-45 minutes, water is then added, is heated 14-20 minutes at 75-85 DEG C, keeps temperature-resistant, continuously adds water saturation
N-butanol is cooled to room temperature, then filters, after filtrate recycling design, be dried at 105-110 DEG C after stirring 5-10 minutes
Dry cream, then crushed, obtain starch mixture；
B. take antioxidant 1010, grind 6-10 minute, ethyl acetate is then added, continue to grind 6-10 minutes, then plus
Enter lemon juice, stir evenly, adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stir evenly, then at 65-75 DEG C
After being heated to reflux 50-70 minutes, then evaporation water to relative density is 1.18-1.23 at 65-75 DEG C, obtains charcoal ash mixing
Object；
C. it takes starch mixture and charcoal ash mixture, building glue is added, heat 30-40 minutes at 75-85 DEG C, then
It is cooled to room temperature, obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；The dustpan and plank pass through pretreatment, the preprocess method before drafting are as follows: use
Boiling water 15-25 minutes, taking-up was dried；The bamboo chip is before drafting by pretreatment, the preprocess method are as follows: use limewash
It impregnates 20-30 minutes, taking-up is dried.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:
1. the present invention prepares peasant's paint using pure plant raw material, wherein addition cassava and glutinous rice increase the viscous of pigment
Degree property, promote the fusion of various raw material colors, make paint color it is pure, it is bright-coloured, glossy, be not cracked；Add antioxidant 1010
And lemon juice, the stickiness and inoxidizability of pigment can be increased, be that pigment color is purer, glossiness is higher, protect raw material
Not fugitive color.Peasant picture paint color produced by the present invention is gorgeous, glossiness is high, anti-oxidant, fast light, environmentally friendly；The present invention provides
Preparation method raw material availability is high, pigment purity is high, technological parameter is controllable, is easy to industrialization；Drawing pigment of the present invention is drawn
Production product can be not easy it is infested, not perishable, be not easy to go mouldy.
2. the present invention isolates cassava, the strong viscosity amylopectin in glutinous rice using water-saturated n-butanol, face can be increased
The viscosity of material can make not break up between the melanin extracted in plant material and other raw material, preferably can mutually melt
It closes, forms pure color；Also pigment color fastness can be kept high, light shine, not fugitive color because of high-intensitive viscosity.It is conventional
The starch that water sedimentation method extracts is the mixture of amylopectin and amylose, when heating starch generates gelatinization, forms tool
Sticking viscous fluid, at this point, amylose forms mesh outside, amylopectin is wrapped in, mainly play viscous effect
Substance be amylose.However, the viscosity of amylopectin is much higher than amylose in fact, the starch that conventional method obtains is viscous
It spends limited, for the effect for preferably playing the strong viscosity of amylopectin, separating-purifying need to be carried out to amylopectin and amylose, this
Inventing first boiling makes the starch in cassava and glutinous rice expand, be gelatinized, reduction amylopectin and amylose winding degree, then plus
Enter water and water-saturated n-butanol carries out heating stirring, by the power of stirring and the fuel factor of solvent molecule, further by branch
Starch and amylose are peeled away, and the amylose of removing forms precipitating in water-saturated n-butanol and is removed, with regard to realizing
The separating-purifying of amylopectin, it is then that the amylopectin of purification is dry, it finally carries out primary heating again with unclassified stores and mixes,
Final pigment is obtained, during which starch is heated repeatedly, amylopectin can be made repeatedly reversible by hankering generating
Expansion and further winding, gelatinization, viscosity are enhanced, and can be reduced the generation of drawing surface cracking, the starch property after gelatinization
Also become transparent, the color of pigment itself will not be covered.
3. the present invention using be added lime paste, increase drawing pigment paintings carrier surface compactness, avoid pigment with
Paintings carrier is detached from and picture cracking occurs.The lemon juice of addition is under the antioxidation of antioxidant 1010, lemon therein
Acid forms chelate with calcium ion in lime paste, further stablizes the chemical composition of lime paste, keeps the compactness of pigment higher.Together
When, antioxidant 1010 is dispersed in pigment using polishing, the inoxidizability of pigment can be improved, pigment is made to be not easy to take off
Color.
4. the charcoal mixing that the present invention is fired using the ash and the fruit of a cubeb litsea tree of Chinese gall firing, can be made bright-colored, have light
The black pigment in pool.Fruit of a cubeb litsea tree charcoal has the gloss of carbon black, can scatter sunlight, makes black more beautiful.Chinese gall ash has fixation work
With making pigment not fugitive color, a variety of inorganic cations therein have electrostatic effect, can be effectively reduced in fruit of a cubeb litsea tree charcoal
Carbon black molecule cohesiveness, is uniformly distributed carbon black, reduces the light scattering effect of carbon black, enhances light absorption degree, improves the fruit of a cubeb litsea tree
The blackness of charcoal makes to reach optimum balance on gloss and blackness.
5. peasant's paint prepared by the present invention can draw paintings on dustpan, plank, bamboo chip, metope, wherein dustpan
With plank after boiling water dries pretreatment, extra moisture is eliminated, can prevent from deforming and is rotted, meanwhile, high temperature can
To dustpan and plank sterilization, deinsectization；Bamboo chip, can be with deinsectization after processing is dried in limewash immersion, and moisture is isolated, bamboo chip
It prevents from rotting.
[specific embodiment]
Below with reference to embodiment, the invention will be further described.
Embodiment 1
A kind of peasant's paint, the raw material including following weight part ratio: 400 parts of water, 80 parts of water-saturated n-butanol, cassava 25
Part, 25 parts of glutinous rice, 25 parts of building glue, 5 parts of lime paste powder, 5 parts and 5 parts of fruit of a cubeb litsea tree charcoal of Chinese gall ash.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 70 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 85 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 30 minutes, water is then added, is heated 8 minutes at 80 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It after mixing 3 minutes, is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 90 DEG C, then crushed, obtained
Starch mixture；
B. starch mixture is taken, Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder is added, is uniformly mixed, building is then added
Glue heats 20 minutes at 70 DEG C, is then cooled to room temperature, obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 15
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 20 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 2
A kind of peasant's paint, the raw material including following weight part ratio: 500 parts of water, 120 parts of water-saturated n-butanol, cassava
35 parts, 35 parts of glutinous rice, 35 parts of building glue, 15 parts of lime paste powder, 15 parts and 15 parts of fruit of a cubeb litsea tree charcoal of Chinese gall ash.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 90 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 95 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 50 minutes, water is then added, is heated 16 minutes at 90 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It after mixing 6 minutes, is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 100 DEG C, then crushed,
Obtain starch mixture；
B. starch mixture is taken, Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder is added, is uniformly mixed, building is then added
Glue heats 30 minutes at 80 DEG C, is then cooled to room temperature, obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 25
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 30 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 3
A kind of peasant's paint, the raw material including following weight part ratio: 450 parts of water, 100 parts of water-saturated n-butanol, cassava
30 parts, 30 parts of glutinous rice, 30 parts of building glue, 10 parts of lime paste powder, 10 parts and 10 parts of fruit of a cubeb litsea tree charcoal of Chinese gall ash.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 80 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 90 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 40 minutes, water is then added, is heated 12 minutes at 85 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It after mixing 4 minutes, is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 95 DEG C, then crushed, obtained
Starch mixture；
B. starch mixture is taken, Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder is added, is uniformly mixed, building is then added
Glue heats 25 minutes at 75 DEG C, is then cooled to room temperature, obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 20
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 25 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 4
A kind of peasant's paint, the raw material including following weight part ratio: 400 parts of water, 80 parts of water-saturated n-butanol, cassava 25
Part, 25 parts of glutinous rice, 25 parts of building glue, 5 parts of lime paste powder, Chinese gall grey 5 parts, 5 parts of fruit of a cubeb litsea tree charcoal, 125 parts of lemon juice, acetic acid
1 part and 0.5 part of antioxidant 1010 of ethyl ester.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 70 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 85 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 35 minutes, water is then added, is heated 14 minutes at 75 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It mixes after five minutes, is cooled to room temperature, then filter, after filtrate recycling design, dry cream is dried at 105 DEG C, then crushed,
Obtain starch mixture；
B. antioxidant 1010 is taken, grinds 6 minutes, ethyl acetate is then added, continues grinding 6 minutes, is subsequently added into lemon
Juice stirs evenly, and adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stirs evenly, be then heated to reflux 50 at 65 DEG C
After minute, then evaporation water to relative density is 1.18 at 65 DEG C, obtains charcoal ash mixture；
C. starch mixture and charcoal ash mixture are taken, building glue is added, heats 30 minutes, is then cooled at 75 DEG C
Room temperature obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 15
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 20 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 5
A kind of peasant's paint, the raw material including following weight part ratio: 500 parts of water, 120 parts of water-saturated n-butanol, cassava
35 parts, 35 parts of glutinous rice, 35 parts of building glue, 15 parts of lime paste powder, Chinese gall grey 15 parts, 15 parts of fruit of a cubeb litsea tree charcoal, lemon juice 165
Part, 3 parts of ethyl acetate and 1.5 parts of antioxidant 1010.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 90 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 95 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 45 minutes, water is then added, is heated 20 minutes at 85 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It mixes after ten minutes, is cooled to room temperature, then filter, after filtrate recycling design, dry cream is dried at 110 DEG C, then crushed,
Obtain starch mixture；
B. antioxidant 1010 is taken, grinds 10 minutes, ethyl acetate is then added, continues grinding 10 minutes, is subsequently added into lemon
Lemon juice, stirs evenly, and adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stirs evenly, be then heated to reflux at 75 DEG C
After 70 minutes, then evaporation water to relative density is 1.23 at 75 DEG C, obtains charcoal ash mixture；
C. starch mixture and charcoal ash mixture are taken, building glue is added, heats 40 minutes, is then cooled at 85 DEG C
Room temperature obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 25
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 30 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 6
A kind of peasant's paint, the raw material including following weight part ratio: 420 parts of water, 90 parts of water-saturated n-butanol, cassava 28
Part, 27 parts of glutinous rice, 27 parts of building glue, 8 parts of lime paste powder, Chinese gall grey 7 parts, 8 parts of fruit of a cubeb litsea tree charcoal, 135 parts of lemon juice, acetic acid
1.5 parts and 0.8 part of antioxidant 1010 of ethyl ester.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 75 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 87 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 37 minutes, water is then added, is heated 15 minutes at 77 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It after mixing 6 minutes, is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 106 DEG C, then crushed,
Obtain starch mixture；
B. antioxidant 1010 is taken, grinds 7 minutes, ethyl acetate is then added, continues grinding 7 minutes, is subsequently added into lemon
Juice stirs evenly, and adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stirs evenly, be then heated to reflux 55 at 68 DEG C
After minute, then evaporation water to relative density is 1.19 at 68 DEG C, obtains charcoal ash mixture；
C. starch mixture and charcoal ash mixture are taken, building glue is added, heats 38 minutes, is then cooled at 77 DEG C
Room temperature obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 18
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 27 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 7
A kind of peasant's paint, the raw material including following weight part ratio: 470 parts of water, 110 parts of water-saturated n-butanol, cassava
32 parts, 33 parts of glutinous rice, 33 parts of building glue, 12 parts of lime paste powder, Chinese gall grey 13 parts, 12 parts of fruit of a cubeb litsea tree charcoal, lemon juice 155
Part, 2.5 parts of ethyl acetate and 1.3 parts of antioxidant 1010.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 85 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 92 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 42 minutes, water is then added, is heated 19 minutes at 83 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It after mixing 9 minutes, is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 108 DEG C, then crushed,
Obtain starch mixture；
B. antioxidant 1010 is taken, grinds 9 minutes, ethyl acetate is then added, continues grinding 9 minutes, is subsequently added into lemon
Juice stirs evenly, and adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stirs evenly, be then heated to reflux 65 at 72 DEG C
After minute, then evaporation water to relative density is 1.22 at 72 DEG C, obtains charcoal ash mixture；
C. starch mixture and charcoal ash mixture are taken, building glue is added, heats 37 minutes, is then cooled at 83 DEG C
Room temperature obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 22
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 27 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 8
A kind of peasant's paint, the raw material including following weight part ratio: 450 parts of water, 100 parts of water-saturated n-butanol, cassava
30 parts, 30 parts of glutinous rice, 30 parts of building glue, 10 parts of lime paste powder, Chinese gall grey 10 parts, 10 parts of fruit of a cubeb litsea tree charcoal, lemon juice 145
Part, 2 parts of ethyl acetate and 1 part of antioxidant 1010.
Wherein, Chinese gall ash the preparation method comprises the following steps: take Chinese gall branch, incinerate, cross after 80 meshes to get；
Fruit of a cubeb litsea tree charcoal the preparation method comprises the following steps: take fruit of a cubeb litsea tree branch, char, then crush, cross 90 meshes to get.
The preparation method of above-mentioned peasant's paint, comprising the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof in pot
Boiling 40 minutes, water is then added, is heated 17 minutes at 80 DEG C, keeps temperature-resistant, continuously adds water-saturated n-butanol, stir
It after mixing 8 minutes, is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 107 DEG C, then crushed,
Obtain starch mixture；
B. antioxidant 1010 is taken, grinds 8 minutes, ethyl acetate is then added, continues grinding 8 minutes, is subsequently added into lemon
Juice stirs evenly, and adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stirs evenly, be then heated to reflux 60 at 70 DEG C
After minute, then evaporation water to relative density is 1.21 at 70 DEG C, obtains charcoal ash mixture；
C. starch mixture and charcoal ash mixture are taken, building glue is added, heats 35 minutes, is then cooled at 80 DEG C
Room temperature obtains black pigment.
The application method of above-mentioned peasant's paint, steps are as follows: pigment is plotted on dustpan, plank, bamboo chip or metope,
Then it dries, then sprays varnish；Dustpan and plank pass through pretreatment, preprocess method before drafting are as follows: use boiling water 20
Minute, taking-up is dried；Bamboo chip is before drafting by pretreatment, preprocess method are as follows: is impregnated 25 minutes with limewash, taking-up is dried in the air
It is dry.
Embodiment 9
In addition to being added without water-saturated n-butanol solution in step a, remaining method is the same as embodiment 5.
Embodiment 10
In addition to being added without Chinese gall ash in step a, remaining method is the same as embodiment 5.
Embodiment 11
In addition to the boiling step for omitting cassava and glutinous rice in step a, remaining method is the same as embodiment 5.
Embodiment 12
In addition to being added without lime paste powder in step b, remaining method is the same as embodiment 5.
Laboratory sample 13
In addition to ethyl acetate, antioxidant 1010 and lemon juice is not added in step b, remaining method is the same as embodiment 5.
Laboratory sample 14
In addition to not heating in step c, remaining method is the same as embodiment 5.
The comparison of 15 implementation result of embodiment
1. the preparation of laboratory sample
Peasant's paint is prepared by the method for embodiment 1-14, pigment obtained in each embodiment is respectively designated as testing
Sample 1-14.
2. evaluation method
2.1, using colour difference meter measurement experiment sample 1, the color difference (△ E) of the pigment of 3,4,6,8-14, measure pigment color
Take off change degree, to judge the light resistance and inoxidizability of pigment, △ E is bigger, indicate light resistance and inoxidizability it is poorer.
2.1.1 light shine measuring method: at room temperature, pigment is first painted to the consistent picture of thickness on bamboo chip, is put
It sets dark place to dry, then uses ultraviolet light bamboo chip, after irradiating a period of time, not carry out the pigment picture of illumination as blank,
Color difference between measurement experiment object and blank sample, obtaining color difference the results are shown in Table 1.
2.2.1 inoxidizability measuring method: at room temperature, pigment is first painted to the consistent picture of thickness on bamboo chip, is put
It sets dark place to dry, the bamboo chip then sprayed with 0.5% liquor potassic permanganate places one in the environment of relative humidity is 90%
After the section time, using the pigment picture of non-spray solution as blank, color difference between measurement experiment object and blank sample obtains color
Difference the results are shown in Table 1.
2.2 smear the pigment of laboratory sample 3,4,6,8,11,12,13 on bamboo chip into the consistent picture of thickness respectively,
It is placed in the climatic chamber that temperature is 40 DEG C, humidity is 90% and places a period of time, carry out the test that accelerates the failure, observe bamboo chip
The cracking degree of surface drawing pigment picture, the results are shown in Table 2.
3. evaluation result
1 color difference evaluation result of table
Table 2 accelerates the failure test result
4. experimental result
As seen from Table 1, laboratory sample 4,6,8 is best in quality, and light resistance, inoxidizability are most strong, laboratory sample 1,3,
13 quality is preferable, and the quality of laboratory sample 9,10,11,12,14 is worst；As seen from Table 2, laboratory sample 4,6,8 is complete
Degree is best, and the integrity degree of laboratory sample 1,3,13 is preferable, and the integrity degree of laboratory sample 11,12 is worst.
Ethyl acetate, antioxidant 1010 and lemon juice is not added during the preparation process in laboratory sample 1,3 and 13, so that
Pigment stickiness is inadequate, and light resistance and inoxidizability decline, and for drawing a picture, the probability for crack phenomenon occur also increases.
During the preparation process, the starch being added without in water-saturated n-butanol purification cassava and glutinous rice leads to face to laboratory sample 9
Material viscosity is not strong enough, so that light resistance and inoxidizability reduce obviously.
Laboratory sample 10 during the preparation process, is added without Chinese gall ash, makes that Yellow Pigment is poor, glossiness is not high, illumination
It is easy to fade with oxidation.
During the preparation process, the boiling step of cassava and glutinous rice is omitted in laboratory sample 11, and prepared by laboratory sample 12
In the process, it is added without gypsum, causes the adhesiveness of pigment to reduce, occurs breaking up and glossiness is not high, so that pigment pole
Being cracked and removing easily occur in fugitive color, drawing surface.
Laboratory sample 14 preparation process final step material mixing when without heating so that pigment viscosity not
Enough, illumination and oxidation are easily faded.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
Bright patent claim, it is all the present invention suggested by technical spirit under completed same changes or modifications change, should all belong to
In the covered the scope of the patents of the present invention.
Claims (7)
1. a kind of peasant's paint, which is characterized in that the raw material including following weight part ratio: 400-500 parts of water, the positive fourth of water saturation
80-120 parts of alcohol, 25-35 parts of cassava, 25-35 parts of glutinous rice, 25-35 parts of building glue, 5-15 parts of lime paste powder, Chinese gall ash 5-
15 parts and 5-15 parts of fruit of a cubeb litsea tree charcoal.
2. a kind of peasant's paint according to claim 1, which is characterized in that further include the raw material of following weight part ratio:
125-165 parts of lemon juice, 1-3 parts of ethyl acetate and 0.5-1.5 parts of antioxidant 1010.
3. a kind of peasant's paint according to claim 1 or 2, which is characterized in that the preparation method of the Chinese gall ash
Are as follows: take Chinese gall branch, incinerate, cross 70-90 mesh after to get.
4. a kind of peasant's paint according to claim 1 or 2, which is characterized in that the preparation method of the fruit of a cubeb litsea tree charcoal
Are as follows: take fruit of a cubeb litsea tree branch, char, then crush, cross 85-95 mesh to get.
5. a kind of preparation method of peasant's paint described in claim 1, which comprises the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof boiling in pot
30-50 minutes, water is then added, is heated 8-16 minutes at 80-90 DEG C, keeps temperature-resistant, continuously adds the positive fourth of water saturation
Alcohol is cooled to room temperature, then filters, after filtrate recycling design, dry cream is dried at 90-100 DEG C after stirring 3-6 minute, then
It is crushed, obtains starch mixture；
B. starch mixture is taken, Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder is added, is uniformly mixed, building glue is then added,
It is heated 20-30 minutes at 70-80 DEG C, is then cooled to room temperature, obtains black pigment.
6. a kind of preparation method of peasant's paint as claimed in claim 2, which comprises the following steps:
A. by weight, cassava is taken, peels, be sliced, dry, glutinous rice is then added, crushes, is then placed in water proof boiling in pot
35-45 minutes, water is then added, is heated 14-20 minutes at 75-85 DEG C, keeps temperature-resistant, continuously adds the positive fourth of water saturation
Alcohol is cooled to room temperature, then filters, after filtrate recycling design, be dried to dry cream at 105-110 DEG C after stirring 5-10 minute,
It is crushed again, obtains starch mixture；
B. antioxidant 1010 is taken, grinds 6-10 minutes, ethyl acetate is then added, continues grinding 6-10 minutes, is subsequently added into lemon
Lemon juice, stirs evenly, and adds Chinese gall ash, fruit of a cubeb litsea tree charcoal and lime paste powder, stirs evenly, then heat at 65-75 DEG C
After reflux 50-70 minutes, then evaporation water to relative density is 1.18-1.23 at 65-75 DEG C, obtains charcoal ash mixture；
C. starch mixture and charcoal ash mixture are taken, building glue is added, heats 30-40 minutes at 75-85 DEG C, then cools down
To room temperature, black pigment is obtained.
7. a kind of application method of peasant's paint of any of claims 1 or 2, which is characterized in that steps are as follows: pigment is drawn
Then system is dried, then spray varnish on dustpan, plank, bamboo chip or metope；The dustpan and plank are passed through before drafting
Cross pretreatment, the preprocess method are as follows: use boiling water 15-25 minutes, taking-up is dried；The bamboo chip is before drafting by pre- place
Reason, the preprocess method are as follows: impregnated 20-30 minutes with limewash, taking-up is dried.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111671872A (en) * | 2020-08-05 | 2020-09-18 | 姜金林 | Bone-knitting plaster powder |
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| CN102482510A (en) * | 2009-08-28 | 2012-05-30 | 科·汉森有限公司 | High strength carbo substances |
| CN104017436A (en) * | 2014-05-28 | 2014-09-03 | 南昌大学 | Children pigment composed of edible composition |
| CN104693865A (en) * | 2013-12-07 | 2015-06-10 | 招远鲁娃婴幼儿用品有限公司 | Pigment for writing and drawing on toy surface |
| CN106280685A (en) * | 2016-08-17 | 2017-01-04 | 湖北科亿华科技有限公司 | A kind of water-fast edible printing-ink and preparation method thereof |
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|---|---|---|---|---|
| CN102482510A (en) * | 2009-08-28 | 2012-05-30 | 科·汉森有限公司 | High strength carbo substances |
| CN104693865A (en) * | 2013-12-07 | 2015-06-10 | 招远鲁娃婴幼儿用品有限公司 | Pigment for writing and drawing on toy surface |
| CN104017436A (en) * | 2014-05-28 | 2014-09-03 | 南昌大学 | Children pigment composed of edible composition |
| CN106280685A (en) * | 2016-08-17 | 2017-01-04 | 湖北科亿华科技有限公司 | A kind of water-fast edible printing-ink and preparation method thereof |
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| CN111671872A (en) * | 2020-08-05 | 2020-09-18 | 姜金林 | Bone-knitting plaster powder |
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