CN106280685A - A kind of water-fast edible printing-ink and preparation method thereof - Google Patents

A kind of water-fast edible printing-ink and preparation method thereof Download PDF

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Publication number
CN106280685A
CN106280685A CN201610675237.9A CN201610675237A CN106280685A CN 106280685 A CN106280685 A CN 106280685A CN 201610675237 A CN201610675237 A CN 201610675237A CN 106280685 A CN106280685 A CN 106280685A
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CN
China
Prior art keywords
ink
water
color lake
aluminum color
propylene glycol
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Pending
Application number
CN201610675237.9A
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Chinese (zh)
Inventor
黄耀华
明星
熊吉
周湘汉
刘萍
鲍荣艳
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Hubei Keyihua Technology Co Ltd
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Hubei Keyihua Technology Co Ltd
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Publication date
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Priority to CN201610675237.9A priority Critical patent/CN106280685A/en
Publication of CN106280685A publication Critical patent/CN106280685A/en
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/08—Printing inks based on natural resins
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00—Inks
    • C09D11/02—Printing inks
    • C09D11/03—Printing inks characterised by features other than the chemical nature of the binder

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

The invention discloses a kind of water-fast edible printing-ink and preparation method thereof, belong to printing-ink technology frontier.One disclosed by the invention is water-fast edible printing-ink and preparation method thereof, by mass percentage, described ink comprises: Lac 20 40%, ethanol 5 10%, n-butyl alcohol 15 30%, propylene glycol 10 25%, food coloring 0 30%, auxiliary agent 0.05 3%, ammonia 2 5%, purified water 0 5%.The raw material that ink of the present invention is used all meets food additive or the pharmaceutic adjuvant of CFDA license.Ink of the present invention has the printing performance of silk-screen ink, pad-transfer printing ink etc., and can reach state food safety criterion and pharmaceutic adjuvant standard, can print numerous food, medicine and packaging material thereof, have good resistance to water.

Description

A kind of water-fast edible printing-ink and preparation method thereof
Technical field
The invention belongs to printing-ink technical field, relate to a kind of edible ink and preparation method thereof, particularly to one Plant water-fast edible ink and preparation method thereof.
Background technology
In recent years, food safety and the personalization of food, and the popularization of businessman's brand is all the problem that everybody pays close attention to. The so-called environmental protection ink that present stage a lot of surface decoration effect all uses, this kind of ink overwhelming majority is all industry ink, The producer producing such ink does not all have food production licence, and such ink more or less all employ food safety country mark Raw material beyond standard.And the most edible ink major part is all ink-jet aspect, such edible jet ink ink needs Special printer and edible film, the shelf-life is short, stores inconvenience (needing low temperature storage), expensive, and yield mental retardation is held Loading is single, is not suitable for promoting the use of.
Therefore, for current current condition, need one really can meet national food safety standard and country is medicinal Adjuvant standard, resistance to aqueous ink easy to use, cheap, flexible and changeable, widely applicable.The present invention can provide this technology Scheme, a kind of water-fast edible printing-ink and preparation method thereof.
Summary of the invention
The technical problem to be solved is to provide one really can meet national food safety standard and state Family's pharmaceutic adjuvant standard, long shelf-life, it is convenient to store, cheap, easy to use, flexible and changeable, and widely applicable silk-screen moves Print spraying ink.The material that this ink can directly print has fresh purification fruit, cookies, chocolate, egg, confection, edible Facilitating material, tablet etc. by thin film, paper wrapper, papery, printing is firmly, water-fast acidproof.For realizing the purpose of the present invention, Adopt the following technical scheme that:
1. a water-fast edible printing-ink, its component and mass percentage content are: Lac 20-40%, ethanol 5-10%, N-butyl alcohol 15-30%, propylene glycol 10-25%, food coloring 0-30%, auxiliary agent 0.05-3%, ammonia 2-5%, purified water 0-5%.
2. the Lac described in, n-butyl alcohol, propylene glycol, ammonia, purified water are food grade or pharmaceutical grade, all meet food Safe national standard and country's pharmaceutic adjuvant standard.
3. the food coloring described in is: erythrosine and aluminum color lake, indigo and aluminum color lake, light blue and aluminum color lake, lemon Lemon Huang and aluminum color lake, sunset yellow and aluminum color lake thereof, amaranth and aluminum color lake thereof, the reddest and aluminum color lake, carmine and aluminum thereof Color lake, lure the one in red and aluminum color lake, titanium dioxide, iron oxide black, iron oxide red, plant white carbon black or kind more than.
4. the auxiliary agent described in is: span 20, sorbester p18, sorbester p17, soil temperature 20, soil temperature 60, POLYSORBATE 80, poly dimethyl silicon In oxygen alkane and emulsion, silicon dioxide, sodium aluminosilicate, calcium silicates, polyglyceryl fatty acid ester, the Dry Flo PC one Kind or more than one mixture.
5. the preparation method of ink described in comprises the steps:
Step one: Lac, ethanol, n-butyl alcohol, ammonia being thrown in container by proportioning, within the temperature range of 30 ~ 40 DEG C, rotating speed is Stir 1-2 hour under conditions of 600-800rpm so that it is after mix homogeneously, stand 24 hours；
Step 2: propylene glycol, food coloring, auxiliary agent, purified water are put into the mixed liquid in step one by proportioning, at 30 ~ 40 DEG C In temperature range, rotating speed is to stir 0.5-1 hour under conditions of 600-800rpm so that it is mix homogeneously；
Step 3: use three-roll grinder that mixed liquid scattered in step 2 is ground 2 times；
Step 4: after grinding, by proportioning, propylene glycol is supplied sum, within the temperature range of 30-40 DEG C, rotating speed is 600- Stir 0.5-1 hour under conditions of 800rpm so that it is mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
Detailed description of the invention
The present invention is illustrated further by following unrestriced embodiment, but is not used to limit the scope of the present invention, Percentage ratio in ink formulations is weight ratio.
Embodiment 1
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 20
2 Ethanol 5
3 N-butyl alcohol 25
4 Ammonia 5
5 Propylene glycol 10
6 Titanium dioxide 30
7 Silicon dioxide 1.5
8 Sorbester p17 0.5
9 Purified water 3
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-9 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 Time；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, make Its mix homogeneously, i.e. obtains a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 1.
Table 1
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 2
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 20
2 Ethanol 5
3 N-butyl alcohol 25
4 Ammonia 5
5 Propylene glycol 10
6 Iron oxide black 28
7 Sodium aluminosilicate 1.5
8 Tween 80 0.5
9 Purified water 5
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-9 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 Time；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, make Its mix homogeneously, i.e. obtains a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 2.
Table 2
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 3
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 40
2 Ethanol 10
3 N-butyl alcohol 20
4 Ammonia 10
5 Propylene glycol 15
6 Polyglyceryl fatty acid ester 1.5
7 Polydimethylsiloxane 1.5
8 Purified water 2
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-8 is mixed in proportion in the mixed liquid of 1-3 stirring and within 0.5 hour, makes its mix homogeneously, temperature control less than 40 DEG C, then stir Mix 0.5 hour so that it is mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 3.
Table 3
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 4
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 35
2 Ethanol 8
3 N-butyl alcohol 20
4 Ammonia 5
5 Propylene glycol 15
6 Erythrosine aluminum lake 10
7 Calcium silicates 1.5
8 Polydimethylsiloxane 0.5
9 Purified water 5
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-9 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 Time；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, make Its mix homogeneously, i.e. obtains a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 4.
Table 4
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 5
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 35
2 Ethanol 10
3 N-butyl alcohol 18
4 Ammonia 5
5 Propylene glycol 15
6 Brilliant blue aluminum lake 5
7 Indigo aluminum color lake 5
8 The Dry Flo PC 1.5
9 Span 20 0.5
10 Purified water 5
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-10 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 times；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, Make its mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 5.
Table 5
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 6
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 35
2 Ethanol 8
3 N-butyl alcohol 20
4 Ammonia 10
5 Propylene glycol 10
6 Tartrazine aluminum lake 5
7 Sunset yellow aluminum lake 5
8 Silicon dioxide 1.5
9 Tween 80 0.5
10 Purified water 5
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-10 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 times；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, Make its mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 6.
Table 6
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 7
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 35
2 Ethanol 5
3 N-butyl alcohol 23
4 Ammonia 5
5 Propylene glycol 15
6 Amaranth aluminum lake 5
7 New red aluminum lake 5
8 Silicon dioxide 1.5
9 Polydimethylsiloxane 0.5
10 Purified water 5
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-10 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 times；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, Make its mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 7.
Table 7
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Embodiment 8
The each component proportion of ink is as follows:
Sequence Material name Mass percent %
1 Lac 35
2 Ethanol 8
3 N-butyl alcohol 20
4 Ammonia 5
5 Propylene glycol 15
6 Ponceau 4R aluminum lake 5
7 Fancy red aluminum lake 5
8 Silicon dioxide 1.5
9 Polydimethylsiloxane 0.5
10 Purified water 5
The blender stirring using rotating speed to be 600rpm after being mixed in proportion by 1-4, temperature control less than 40 DEG C, quiet after stirring 2 hours Put 24 hours, 5-10 is mixed in proportion in the mixed liquid of 1-4 stirring and within 0.5 hour, makes its mix homogeneously be placed in three-roller grinding 2 times；Supply propylene glycol to the blender stirring using rotating speed to be 600rpm after total amount, temperature control less than 40 DEG C, stir 0.5 hour, Make its mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
Gained ink is printed by stencil printing apparatus and bat printing equipment or after spraying by natural drying film forming, through surveying After examination, its performance is as shown in table 8.
Table 8
Note: adhesion test method is finger friction, does not falls off as excellent for 30 times back and forth, comes off for difference.
Example 1-8 is attained by inventing the requirement reached required for this ink.

Claims (5)

1. a water-fast edible printing-ink, it is characterised in that its component and mass percentage content be: Lac 20-40%, Ethanol 5-10%, n-butyl alcohol 15-30%, propylene glycol 10-25%, food coloring 0-30%, auxiliary agent 0.05-3%, ammonia 2-5%, purified water 0-5%。
Ink the most according to claim 1, it is characterised in that described Lac, ethanol, n-butyl alcohol, propylene glycol, ammonia, Purified water is food stage or pharmaceutical grade.
Ink the most according to claim 1, it is characterised in that described food coloring is: erythrosine and aluminum color lake, indigo Indigo plant and aluminum color lake, light blue and aluminum color lake thereof, lemon yellow and aluminum color lake thereof, sunset yellow and aluminum color lake thereof, amaranth and aluminum color thereof Form sediment, the reddest and aluminum color lake, carmine and aluminum color lake thereof, lure red and aluminum color lake, titanium dioxide, iron oxide black, ferrum oxide One or more in red, plant white carbon black.
Ink the most according to claim 1, it is characterised in that described auxiliary agent is: span 20, sorbester p18, sorbester p17, soil Temperature 20, soil temperature 60, POLYSORBATE 80, polydimethylsiloxane and emulsion thereof, silicon dioxide, sodium aluminosilicate, calcium silicates, polyglycereol fat One or more in acid esters, the Dry Flo PC.
5. the preparation method of ink described in any one in Claims 1-4, it is characterised in that comprise the steps:
Step one: Lac, ethanol, n-butyl alcohol, ammonia are put in container by proportioning, within the temperature range of 30 ~ 40 DEG C, rotating speed For stirring 1-2 hour under conditions of 600-800rpm so that it is stand 24 hours after mix homogeneously；
Step 2: propylene glycol, food coloring, auxiliary agent, purified water are put into the mixed liquid in step one by proportioning, at 30 ~ 40 DEG C In temperature range, rotating speed is to stir 0.5-1 hour under conditions of 600-800rpm so that it is mix homogeneously；
Step 3: use three-roll grinder that mixed liquid scattered in step 2 is ground 2 times；
Step 4: again by proportioning, propylene glycol is supplied sum after grinding, within the temperature range of 30-40 DEG C, rotating speed is 600- Stir 0.5-1 hour under conditions of 800rpm so that it is mix homogeneously, i.e. obtain a kind of water-fast edible printing-ink.
CN201610675237.9A 2016-08-17 2016-08-17 A kind of water-fast edible printing-ink and preparation method thereof Pending CN106280685A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109251594A (en) * 2018-09-21 2019-01-22 三江县连城兴农业科技有限公司 A kind of peasant's paint and preparation method thereof and application method
CN110194906A (en) * 2019-06-17 2019-09-03 广州素旺生物科技有限公司 A kind of food grade shellac mixed liquor and preparation method thereof
US20210259275A1 (en) * 2018-06-28 2021-08-26 Mars, Incorporated Improved edible ink formulations including calcium carbonate
CN115521660A (en) * 2021-06-24 2022-12-27 芝浦机械电子装置株式会社 Ink, method for producing printed tablet using same, and tablet printing apparatus

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002249696A (en) * 2000-12-18 2002-09-06 Toyo Ink Mfg Co Ltd Printing inf for biodegradable plastic film
CN102101953A (en) * 2009-12-21 2011-06-22 上海延安药业有限公司 Edible ink and preparation method thereof
CN102485814A (en) * 2010-12-01 2012-06-06 上海全金康馨油墨科技有限公司 Medicinal printing ink and preparation method thereof
CN104046126A (en) * 2014-06-19 2014-09-17 杭州电子科技大学 Edible ink for screen printing and preparation method thereof
CN104487094A (en) * 2012-07-20 2015-04-01 大塚制药株式会社 Tablet having dry-ink film on surface thereof, and ink for inkjet printer

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002249696A (en) * 2000-12-18 2002-09-06 Toyo Ink Mfg Co Ltd Printing inf for biodegradable plastic film
CN102101953A (en) * 2009-12-21 2011-06-22 上海延安药业有限公司 Edible ink and preparation method thereof
CN102485814A (en) * 2010-12-01 2012-06-06 上海全金康馨油墨科技有限公司 Medicinal printing ink and preparation method thereof
CN104487094A (en) * 2012-07-20 2015-04-01 大塚制药株式会社 Tablet having dry-ink film on surface thereof, and ink for inkjet printer
CN104046126A (en) * 2014-06-19 2014-09-17 杭州电子科技大学 Edible ink for screen printing and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20210259275A1 (en) * 2018-06-28 2021-08-26 Mars, Incorporated Improved edible ink formulations including calcium carbonate
CN109251594A (en) * 2018-09-21 2019-01-22 三江县连城兴农业科技有限公司 A kind of peasant's paint and preparation method thereof and application method
CN110194906A (en) * 2019-06-17 2019-09-03 广州素旺生物科技有限公司 A kind of food grade shellac mixed liquor and preparation method thereof
CN115521660A (en) * 2021-06-24 2022-12-27 芝浦机械电子装置株式会社 Ink, method for producing printed tablet using same, and tablet printing apparatus
CN115521660B (en) * 2021-06-24 2024-02-27 芝浦机械电子装置株式会社 Ink, method for producing printed tablet using same, and tablet printing apparatus

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