CN109232126A - A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine - Google Patents
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine Download PDFInfo
- Publication number
- CN109232126A CN109232126A CN201811016994.0A CN201811016994A CN109232126A CN 109232126 A CN109232126 A CN 109232126A CN 201811016994 A CN201811016994 A CN 201811016994A CN 109232126 A CN109232126 A CN 109232126A
- Authority
- CN
- China
- Prior art keywords
- chinese herbal
- parts
- herbal medicine
- preparation
- training algae
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05C—NITROGENOUS FERTILISERS
- C05C11/00—Other nitrogenous fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The preparation method for training algae fertilizer containing Chinese herbal medicine that the invention discloses a kind of, its step are as follows: after taking Chinese herbal medicine to crush, water is added to carry out Microwave Extraction, after filtering, then organic solvent is added into filtrate and is precipitated and is filtered, filtrate is then gone to be concentrated, up to Chinese herbal and crude drugs preparations, after sodium humate, potassium fulvate, bamboo vinegar, microelement and attapulgite mixing is added into Chinese herbal and crude drugs preparations again, it is granulated simultaneously dry to get training algae fertilizer；Contain ethyl alcohol, usnic acid sodium and sodium butyrate in the Chinese herbal medicine precipitating organic solvent.A kind of preparation method of training algae fertilizer containing Chinese herbal medicine provided by the invention has the advantages that production energy consumption is low, grain forming is fast, raw material availability is high, high production efficiency；Made training algae fertilizer finished granule rate is high, and stability is good, can reach optimization algae phase, the purpose of quick rich water water purification.
Description
Technical field
The present invention relates to aquaculture fields, more particularly, to a kind of preparation method of training algae fertilizer containing Chinese herbal medicine.
Technical background
As China's aquaculture rapidly develops, specific gravity of the aquaculture in aquaculture is continued to increase, since market needs
The continuous expansion asked, the cultivation density at aquaculture family are also continuously increased.Cultivation density increases, and accelerates water quality aging, water quality
Deteriorate the period.First is that the pollution of breeding water body environment: disorderly being arranged due to abusing disinfectant of cleaning up the pond, insecticide, high-order pond bottom
The reasons such as dirty, coastal waters red tide plankton pollution, in recent years some water quality of the seawater that aquaculture pond is included in or the earth's surface well water of extraction
Physical and chemical index such as beneficial microbe, algae, the hardness basicity of water body, heavy metal index etc. are increasingly not suitable with the growth of algae,
Beneficial algae is difficult to be multiplied into population advantage, causes rich water difficult.Second is that old soil pool bottom of pond aging acidification: by nearly more than ten years
Exploitation cultivation, the acidification of soil pool bottom of pond is serious mostly, and bed mud viscosity is big, acid big, hardened, bed mud nutrient and water energy and substance
Exchange stagnation cause algae to be difficult to constant absorption to arrive balanced nutrient, causing algae, mutually shakiness, water colour are easily fallen clearly, the long moss of bottom of pond,
Mudcake reverse side etc..Third is that the good and bad jumbled together for rich water product in the market, without specific industry production and standard is used, also without clear
Product promotion use thinking；Part of the manufacturer produces not through everfermentation, miscellaneous bacteria, harmful bacteria are more, oxygen consumption is big organic fertilizer or nutrition
Single compound fertilizer is to cause algae phase bacterium mutually unbalance to shrimp agricultural fertilizer water, and beneficial algae is difficult to train into the original of dominant population for a certain area
Cause.
Dissolved oxygen is the most important index of cultivating pool, and dissolved oxygen is high, and the conversion ratio of bait can improve, and can save aquaculture cost；
Dissolved oxygen is high, and the harmful substance (such as hydrogen sulfide, nitrite) in water body can be with rapid conversion；Dissolved oxygen is high, aquatic livestock vigor
By force, it is not easy sick, the degenerate cllipticity of shrimp crab can be promoted.Under normal circumstances in pond 70% or more oxygen sources in the light of algae
Cooperation is used.In the breeding process, increase pond dissolved oxygen, mainly by cultivating pond algae phase.
The growth and breeding of algae needs to absorb various nutrients, and the culture solution of unicellular alga must have these nutrition
Element, and all should comply in nutritional ingredient and quantity the needs of algae, various algae to nutrition need it is many altogether
It is same, so the culture formula of algae, can apply to the culture of a variety of algae, only better conform to the battalion that culture type needs
It supports, is likely to obtain comparatively ideal effect.
Chinese herbal medicine has record as fertilizer additive very early on Chinese history, and China is vast in territory, Chinese herbal medicine money
Source is abundant, and easy kind is easily received, and using simplicity, resource is wide, at low cost.Drug residue free, nuisanceless in animal body, Chinese herbal medicine is
Natural materials maintain the naturality and bioactivity of various composition, and ingredient is easily absorbed and used, unabsorbable also
It is smoothly discharged in vitro, is decomposed in vitro by bacterium etc., water environment will not be polluted.Chinese herbal medicine toxic side effect is small or nothing, and animal body is not
It develops drug resistance, after Preparation process appropriate, toxicity can be reduced or be disappeared toxic Chinese herbal medicine；Pass through prescription compatibility, benefit
With the interaction between Chinese medicine, the effect of it is prevented and cured diseases is improved, weakens or avoid toxic side effect.
In recent years, Chinese herbal medicine is since its is at low cost, easy to process, aobvious without drug resistance and medicament residue, Small side effects, effect
The advantages that writing, is resourceful is more concerned by people.Due in the aquaculture of various chemical synthetic drugs and hormone
The health of the mankind is influenced again using so that aquatic livestock produces drug resistance, and in the intracorporal residual of aquatic livestock, and Chinese herbal medicine
Additive does not have the drawbacks of chemical synthetic drug then, while having the double action of trophism and Drug concurrently, therefore Chinese herbal medicine adds
Agent is added to have become the additive of new generation of substitution chemical synthetic drug and hormone.
Summary of the invention
That the purpose of the present invention is to provide a kind of production energy consumptions is low, grain forming is fast, raw material availability is high, high production efficiency
The training algae fertilizer containing Chinese herbal medicine preparation method, made training algae fertilizer finished granule rate height, stability is good, can reach and optimizes algae
The purpose of phase, quick rich water.
The present invention in background technique aiming at the problem that mentioning, the technical solution taken are as follows:
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, fertilizer are made
Grain, wherein precipitating specific steps are as follows: the organic solvent of 3~4 times of amounts is added into the Chinese herbal medicine extract, stirs evenly and stands 4
After~5h, filtering, then take filtrate to heat and recycle organic solvent, gained concentrate is Chinese herbal and crude drugs preparations.Organic solvent is added
It is and to retain the effective component of drug to remove the impurity in extracting solution, effective component is made to turn to be dissolved in organic solvent, and it is miscellaneous
Mucilaginous substance, matter of trampling in matter such as Microwave Extraction medical fluid, pigment, inorganic salts water-solubility impurity are then precipitated, to reach in flocculent deposit
To purification finished product, the purpose of finished dosage form quality is improved.
Preferably, organic solvent contains ethyl alcohol, usnic acid sodium and sodium butyrate, weight ratio is 11~15:1~1.5:1,
Usnic acid sodium and sodium butyrate in above-mentioned organic solvent can reduce the surface tension between organic solvent and the Chinese herbal medicine extract, body
The reduction of surface energy in system, so that penetration power of the organic solvent in extracting solution becomes strong, and then many contaminant particles is bound up on
It is formed together a floc sedimentation, and constantly increases and becomes larger, accelerates the sinking speed of impurity, improves production efficiency, while pine
Covalently complexing is formed in trailing plants acid sodium and sodium butyrate meeting and extracting solution between the hydroxyl of polysaccharide, increases the affinity of polysaccharide and ethyl alcohol
Without being removed, its package loss in precipitating is reduced, so that Chinese materia medica preparation finished product stability is high, raw material availability is increased
Add.
Preferably, Chinese herbal medicine batching step are as follows: take 4~7 parts of rheum officinale, 5~6 parts of scutellaria, Schisandra chinensis 6~9 by weight
Part, 3~5 parts of Cortex Phellodendri, 4~5 parts of Herba Andrographitis, 6~8 parts of Chinese gall, 5~7 parts of granatum, 6~9 parts of honeysuckle, dandelion 3~7
Part, 9~12 parts of the tuber of stemona, 8~13 parts of kuh-seng, 10~13 parts of fructus lycii, each herbal raw material is crushed, and crosses 40~50 meshes
Afterwards, it is spare to obtain traditional Chinese medicine powder.Chinese herbal medicine by crushing can destroy the structure of plant cell, increase drug specific surface area, make water
Increase with the contact area of Chinese herbal medicine, accelerate the leaching of effective component in medicinal material, improves bioavilability.
Preferably, Microwave Extraction step are as follows: the water of 6~8 times of amounts is added into traditional Chinese medicine powder, after impregnating 20~30min,
400~700W of power, under conditions of 100~110 DEG C of temperature, then 35~55min of Microwave Extraction is filtered, filtrate is medium-height grass
Medicament extracting solution.It is a certain or a variety of in orientation acquisition and concentration Chinese herbal medicine by extracting separation process using Chinese herbal medicine as raw material
It is more to have generally included alkaloid, organic acid, flavonoids, polyol class, terpenoid, steroids and volatile oil etc. for effective component
Kind of active material has broad-spectrum sterilization bacteriostatic activity, and drug is first flooded profit, and enters cell interior by cell wall, and each
Kind drug ingedient contact, is allowed to dissolve, and when carrying out Microwave Extraction, internal large quantity of moisture is more to microwave energy absorption, thus thin
Portion intracellular generates thermal stress, leads to cell rupture, enhances extraction process, obtains the effective active composition in Chinese herbal medicine sufficiently
It extracts, improves the utilization rate and yield rate of Chinese herbal medicine.
Preferably, granulation of fertilizer step are as follows: into Chinese herbal and crude drugs preparations be added sodium humate, potassium fulvate, bamboo vinegar and
Microelement adds attapulgite mixing, is then sent in pelletizer and is granulated after mixing evenly, fertilizer size controlling
It is fertile up to training algae after dry in 2~3mm.
Further preferably, parts by weight raw materials used in granulation of fertilizer step are as follows: 20~25 parts of Chinese herbal and crude drugs preparations, humic
11~14 parts of sour sodium, 10~15 parts of potassium fulvate, 6~8 parts of bamboo vinegar, 5~7 parts of microelement, 24~29 parts of attapulgite.This
Invent made training algae fertilizer scientific matching, enhance fertilizer efficiency to natural environmental-protective, include in the made preparation of the Chinese herbal medicine contained alkaloid,
The various actives substances such as organic acid, flavonoids, polyol class, terpenoid, steroids and volatile oil, active material in ion,
The state of chelating tells on after quickly being absorbed by phytoplankton, can not only promote the benign growths for cultivating algae in water system,
Achieve the purpose that optimize algae phase, quick rich water, promotes cultivation system productivity, can also prevent and control algae disease, effectively
It reduces in breeding water body that microbial metabolism generates the rate of ammonia nitrogen in organic matter accumulation and water, regulating water quality can be purified, improved
The breeding environment of algae.
Further preferably, microelement is made of borax and Chelating state calcium, magnesium, manganese, copper, zinc, and weight ratio is 2~2.5:
1.5~2.5:1~2:1:1:1, above-mentioned Chelating state calcium, magnesium, manganese, copper, zinc be respectively calcium glycine, magnesium glycinate, Mn-Gly,
The chelate molecule charge that basic copper chloride, basic zinc chloride, amino acid and microelement are formed tends to be neutral, can make micro
The solubility of element improves, and absorptivity increases, and improves bioavailability, and can avoid microelement and formed not with other substances
Molten or indissoluble metallic compound, and cannot be absorbed and utilized by algae, it can promote the benign growths of algae.
Compared with the prior art, the advantages of the present invention are as follows:
1) in training algae fertilizer produced by the present invention the Chinese herbal and crude drugs preparations that contain to various common causatives, including bacterium, fungi,
Virus, protozoon, conveyor screw etc. have killing and inhibiting effect, while having induced resistance effect, can play in breeding water body
The effect of preventing and curing diseases, and be used for a long time and do not develop drug resistance, it is free from environmental pollution, it is significant using safe effect；
2) effective component of Chinese herbal and crude drugs preparations is extracted using pure plant in training algae fertilizer produced by the present invention, each component
It is the common medicine in Chinese medicine prescription, it is highly safe to water body, aquatic livestock, human body without harmful components, it is not present after application
Environmental suitability problem, is not also influenced by environmental conditions, thus in breeding water body it is quick, effect is good, and in strong light
It puts in poison to imitate with high and low temperature and stablize persistently；
3) in training algae fertilizer preparation process produced by the present invention, Chinese herbal medicine has carried out organic solvent after Microwave Extraction
Precipitation operation further enhances the stability of effective active composition in Chinese herbal medicine so that the raw material availability of Chinese herbal medicine and at
Product rate increased, and improve production efficiency, reduce material loss rate and production cost；
4) training algae fertilizer particle internal density produced by the present invention is big, stability is high, and grain forming is fast in production, yield rate
Height has been significantly compression the volume of fertilizer, has both saved storage space, is also convenient for transporting, and reduces transportation cost, and can be fast instant
Solution, active material tell on after quickly being absorbed in the state of ion, chelating by phytoplankton, accelerate algal grown breeding, reach
The effect increased production to rich water；
5) method of present invention preparation training algae fertilizer is simple and effective, and strong operability, high production efficiency, repeatability is high, equipment
It is required that simple, easy to implement, practicability is high.
Specific embodiment
The present invention program is described further below by embodiment:
Embodiment 1:
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, fertilizer are made
Grain, wherein precipitating specific steps are as follows: the organic solvent of 3 times of amounts is added into the Chinese herbal medicine extract, after stirring evenly and standing 4h,
Filtering, then take filtrate to heat and recycle organic solvent, gained concentrate is Chinese herbal and crude drugs preparations.It is to remove that organic solvent, which is added,
The impurity in extracting solution is removed, and retains the effective component of drug, effective component is made to turn to be dissolved in organic solvent, and impurity such as microwave
The water-solubility impurities such as mucilaginous substance, matter of trampling on, pigment, the inorganic salts in medical fluid are extracted, then is precipitated in flocculent deposit, is refined into reaching
Product improve the purpose of finished dosage form quality.
Organic solvent is ethyl alcohol, usnic acid sodium and sodium butyrate, weight ratio 11:1:1, the sunglo in above-mentioned organic solvent
Sour sodium and sodium butyrate can reduce the surface tension between organic solvent and the Chinese herbal medicine extract, and the reduction of surface energy, makes in system
It obtains penetration power of the organic solvent in extracting solution and becomes strong, and then many contaminant particles are bound up to form a floc sedimentation, and
Continuous increase becomes larger, and accelerates the sinking speed of impurity, improves production efficiency, at the same usnic acid sodium and sodium butyrate can with mention
Take in liquid and to form covalently complexing between the hydroxyl of polysaccharide, increase the affinity of polysaccharide and ethyl alcohol without being removed, reduce its
Package loss in precipitating, so that Chinese materia medica preparation finished product stability is high, raw material availability be increased.
Chinese herbal medicine batching step are as follows: take 4 parts of rheum officinale, 5 parts of scutellaria, 6 parts of Schisandra chinensis, 3 parts of Cortex Phellodendri, Herba Andrographitis 4 by weight
Part, 6 parts of Chinese gall, 5 parts of granatum, 6 parts of honeysuckle, 3 parts of dandelion, 9 parts of the tuber of stemona, 8 parts of kuh-seng, 10 parts of fructus lycii, by each medium-height grass
Medicine raw material is crushed, and after crossing 40 meshes, it is spare to obtain traditional Chinese medicine powder.Chinese herbal medicine by crushing can destroy the knot of plant cell
Structure increases drug specific surface area, increases the contact area of water and Chinese herbal medicine, accelerates the leaching of effective component in medicinal material, improves
Bioavilability.
Microwave Extraction step are as follows: the water of 6 times of amounts is added into traditional Chinese medicine powder, after impregnating 20min, in power 400W, temperature 100
Under conditions of DEG C, then Microwave Extraction 35min is filtered, filtrate is the Chinese herbal medicine extract.Using Chinese herbal medicine as raw material, by mentioning
Take separation process, orientation obtain and concentration Chinese herbal medicine in a certain kind or plurality of active ingredients, generally included alkaloid, organic
The various actives substances such as acid, flavonoids, polyol class, terpenoid, steroids and volatile oil have the antibacterial work of broad-spectrum sterilization
Property, drug is first flooded profit, and enters cell interior by cell wall, contacts with various drug ingedients, is allowed to dissolve, and carries out micro-
When wave extracts, internal large quantity of moisture is more to microwave energy absorption, thus portion generates thermal stress in the cell, leads to cell rupture,
Enhance extraction process, extract the effective active composition in Chinese herbal medicine sufficiently, improve Chinese herbal medicine utilization rate and at
Product rate.
Granulation of fertilizer step are as follows: sodium humate, potassium fulvate, bamboo vinegar and microelement are added into Chinese herbal and crude drugs preparations,
After mixing evenly, attapulgite mixing is added, is then sent in pelletizer and is granulated, fertilizer size controlling is in 2mm, drying
Afterwards up to training algae fertilizer.
Raw materials used parts by weight are as follows in granulation of fertilizer step: 20 parts of Chinese herbal and crude drugs preparations, 11 parts of sodium humate, fulvic acid
10 parts of potassium, 6 parts of bamboo vinegar, 5 parts of microelement, 25 parts of attapulgite, made training algae fertilizer scientific matching, natural environmental-protective ground enhanced fertilizer
It imitates, includes alkaloid, organic acid, flavonoids, polyol class, terpenoid, steroids in the made preparation of the Chinese herbal medicine contained
It with the various actives substance such as volatile oil, can not only promote the benign growths for cultivating algae in water system, reach optimization algae phase, quickly
The purpose of rich water promotes cultivation system productivity, can also prevent and control algae disease, be effectively reduced organic in breeding water body
Microbial metabolism generates the rate of ammonia nitrogen, the breeding environment that can be purified regulating water quality, improve algae in object accumulation and water.
Microelement is made of borax and Chelating state calcium, magnesium, manganese, copper, zinc, weight ratio 2:1.5:1:1:1:1, above-mentioned
Chelating state calcium, magnesium, manganese, copper, zinc are respectively calcium glycine, magnesium glycinate, Mn-Gly, basic copper chloride, basic zinc chloride, ammonia
The chelate molecule charge that base acid and microelement are formed tends to be neutral, the solubility of microelement can be made to improve, absorptivity
Increase, improve bioavailability, and can avoid microelement and form insoluble or indissoluble metallic compound with other substances, and
It cannot be absorbed and utilized by algae, can promote the benign growths of algae.
Embodiment 2:
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, fertilizer are made
Grain, the specific steps are as follows:
1) 5 parts of rheum officinale, 5 parts of scutellaria, 7 parts of Schisandra chinensis, 4 parts of Cortex Phellodendri, 4 parts of Herba Andrographitis, 7 parts of Chinese gall, stone are taken by weight
Each herbal raw material is carried out powder by 6 parts of pomegranate skin, 7 parts of honeysuckle, 5 parts of dandelion, 10 parts of the tuber of stemona, 10 parts of kuh-seng, 11 parts of fructus lycii
It is broken, after crossing 40 meshes, it is spare to obtain traditional Chinese medicine powder；
2) water of 8 times of amounts is added into traditional Chinese medicine powder, it is micro- under conditions of power 600W, 100 DEG C of temperature after impregnating 25min
Wave extracts 45min, then filters, filtrate is the Chinese herbal medicine extract；
3) organic solvent of 3 times of amounts is added into the Chinese herbal medicine extract, after stirring evenly and standing 5h, filtering, then take filter
Liquid heats and recycles organic solvent, and gained concentrate is Chinese herbal and crude drugs preparations, and above-mentioned organic solvent is ethyl alcohol, usnic acid sodium and fourth
Sour sodium, weight ratio 14:1.5:1；
4) sodium humate, potassium fulvate, bamboo vinegar and microelement are added into Chinese herbal and crude drugs preparations, after mixing evenly, then
Attapulgite is added to mix, is then sent in pelletizer and is granulated, fertilizer size controlling trains algae fertilizer after dry in 2mm to obtain the final product.
Raw materials used parts by weight are as follows in step 4): 22 parts of Chinese herbal and crude drugs preparations, 12 parts of sodium humate, potassium fulvate 12
Part, 7 parts of bamboo vinegar, 6 parts of microelement, 27 parts of attapulgite, wherein microelement by borax and Chelating state calcium, magnesium, manganese, copper,
Zinc composition, weight ratio 2:2:2:1:1:1, above-mentioned Chelating state calcium, magnesium, manganese, copper, zinc be respectively calcium glycine, magnesium glycinate,
Mn-Gly, basic copper chloride, basic zinc chloride.
Embodiment 3:
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, fertilizer are made
Grain, the specific steps are as follows:
1) 6 parts of rheum officinale, 6 parts of scutellaria, 8 parts of Schisandra chinensis, 5 parts of Cortex Phellodendri, 5 parts of Herba Andrographitis, 8 parts of Chinese gall, stone are taken by weight
Each herbal raw material is carried out powder by 7 parts of pomegranate skin, 9 parts of honeysuckle, 6 parts of dandelion, 11 parts of the tuber of stemona, 13 parts of kuh-seng, 12 parts of fructus lycii
It is broken, after crossing 50 meshes, it is spare to obtain traditional Chinese medicine powder；
2) water of 7 times of amounts is added into traditional Chinese medicine powder, it is micro- under conditions of power 500W, 110 DEG C of temperature after impregnating 30min
Wave extracts 50min, then filters, filtrate is the Chinese herbal medicine extract；
3) organic solvent of 4 times of amounts is added into the Chinese herbal medicine extract, after stirring evenly and standing 4.5h, filtering, then take
Organic solvent is heated and recycled to filtrate, and gained concentrate is Chinese herbal and crude drugs preparations, above-mentioned organic solvent be ethyl alcohol, usnic acid sodium and
Sodium butyrate, weight ratio 13:1:1；
4) sodium humate, potassium fulvate, bamboo vinegar and microelement are added into Chinese herbal and crude drugs preparations, after mixing evenly, then
Attapulgite is added to mix, is then sent in pelletizer and is granulated, fertilizer size controlling trains algae fertilizer after dry in 3mm to obtain the final product.
Raw materials used parts by weight are as follows in step 4): 25 parts of Chinese herbal and crude drugs preparations, 13 parts of sodium humate, potassium fulvate 14
Part, 8 parts of bamboo vinegar, 7 parts of microelement, 29 parts of attapulgite, wherein microelement by borax and Chelating state calcium, magnesium, manganese, copper,
Zinc composition, weight ratio 2.5:2.5:1.5:1:1:1, above-mentioned Chelating state calcium, magnesium, manganese, copper, zinc is respectively calcium glycine, sweet
Propylhomoserin magnesium, Mn-Gly, basic copper chloride, basic zinc chloride.
Embodiment 4:
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, fertilizer are made
Grain, specific steps advanced optimize as follows:
1) 6 parts of rheum officinale, 6 parts of scutellaria, 8 parts of Schisandra chinensis, 5 parts of Cortex Phellodendri, 5 parts of Herba Andrographitis, 8 parts of Chinese gall, stone are taken by weight
Each herbal raw material is carried out powder by 7 parts of pomegranate skin, 9 parts of honeysuckle, 6 parts of dandelion, 11 parts of the tuber of stemona, 13 parts of kuh-seng, 12 parts of fructus lycii
It is broken, after crossing 50 meshes, it is spare to obtain traditional Chinese medicine powder；
2) water of 7 times of amounts is added into traditional Chinese medicine powder, it is micro- under conditions of power 500W, 110 DEG C of temperature after impregnating 30min
Wave extracts 50min, then filters, filtrate is the Chinese herbal medicine extract；
3) organic solvent of 4 times of amounts is added into the Chinese herbal medicine extract, after stirring evenly and standing 4.5h, filtering, then take
Organic solvent is heated and recycled to filtrate, and gained concentrate is Chinese herbal and crude drugs preparations, above-mentioned organic solvent be ethyl alcohol, usnic acid sodium and
Sodium butyrate, weight ratio 13:1:1；
4) sodium humate, potassium fulvate, bamboo vinegar and microelement are added into Chinese herbal and crude drugs preparations, after mixing evenly, then
Attapulgite is added, and account for respectively attapulgite weight 0.065% D-MANNOSE and 0.077% nipagin A sodium it is mixed
It is even, it is then sent in pelletizer and is granulated, fertilizer size controlling trains algae fertilizer after dry in 3mm to obtain the final product, above-mentioned D-MANNOSE
Phenolic hydroxyl structure in polyhydroxy configuration and nipagin A sodium can preferentially with organic acid, the terpenoid in Chinese herbal and crude drugs preparations
Between formed overlap joint, and then form polymolecular long-chain, after being adsorbed by attapulgite, be deposited on particle surface and capillary interstice
It is interior, make the further extruding of its molecular grating, increase its adsorption capacity, while by the effect of long-chain, by attapulgite package, twining
It is wound up, increases the thickness of attapulgite's surface adsorbed film with this, thus it is enable to generate bigger surface and adsorption capacity, energy
It is pellet inside acceleration particle in granulation process, so that shaping speed is accelerated, reduce production energy consumption.
Embodiment 5:
A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, fertilizer are made
Grain is wherein used only ethyl alcohol as organic solvent and carries out precipitation operation in settling step, other steps are same as Example 3, system
Algae fertilizer must be trained.
Embodiment 6:
Train the application test of algae fertilizer
In certain aquaculture base, using the made training algae fertilizer of Examples 1 to 4 as test group 1~4, the made training algae of embodiment 5
Fertilizer as a control group, using certain commercially available training algae fertilizer as blank group, carries out control examination to aquaculture field under identical cultivating condition
It tests, chooses 6 groups of test pools, every group has pilot at 2 respectively, after applying each training algae fertilizer respectively, after application 7 days, to test pool water
Body and algae are mutually detected, specific value such as the following table 1, and 2.
Table 1 trains algae fertilizer application front and back water quality monitoring Comparative result
Table 2 trains the variation of algae fertilizer application front and back algae bio amount
By upper table 1, table 2 it is found that there is water quality in breeding water body obviously changes after the made training algae fertilizer of the application embodiment of the present invention
Kind, especially transparency significantly reduces, and is conducive to the photosynthesis of algae in water, so that on the dissolved oxygen amount in water body is also significant
It rises, is conducive to the growth of aquatic livestock, and ammonia nitrogen in water body and nitrite are significantly reduced, water quality optimizing effect is aobvious
It writes, so that water body is more suitable for the growth of algae, in the cultivation later period, training algae fertilizer is obvious to the growth gain effect of algae, illustrates this
Water body muddiness can be improved by inventing made training algae fertilizer, purified water, improved algae bio amount and diversity, and rich water training algae is reached
Purpose.
Routine operation in operation of the present invention step is well known to those skilled in the art, herein without repeating.
Technical solution of the present invention is described in detail in embodiment described above, it should be understood that the above is only
For specific embodiments of the present invention, it is not intended to restrict the invention, all any modifications made in spirit of the invention,
Supplement or similar fashion substitution etc., should all be included in the protection scope of the present invention.
Claims (9)
1. a kind of preparation method of the training algae fertilizer containing Chinese herbal medicine, including Chinese herbal medicine ingredient, Microwave Extraction, precipitating, granulation of fertilizer,
It is characterized by: organic solvent is added into the Chinese herbal medicine extract, and after staticly settling, filtering, then filtrate is taken to be concentrated to get medium-height grass
Medicine preparation；The organic solvent contains ethyl alcohol, usnic acid sodium and sodium butyrate.
2. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 1, it is characterised in that: the precipitating
Specific steps are as follows: the organic solvent of 3 ~ 4 times of amounts is added into the Chinese herbal medicine extract, after stirring evenly and standing 4 ~ 5h, filtering is taken
Organic solvent is heated and recycled to filtrate, and gained concentrate is Chinese herbal and crude drugs preparations.
3. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 1 or 2, it is characterised in that: described
The weight ratio of ethyl alcohol, usnic acid sodium and sodium butyrate is 11 ~ 15:1 ~ 1.5:1.
4. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 1, it is characterised in that: the medium-height grass
Medicine batching step are as follows: take by weight 4 ~ 7 parts of rheum officinale, 5 ~ 6 parts of scutellaria, 6 ~ 9 parts of Schisandra chinensis, 3 ~ 5 parts of Cortex Phellodendri, 4 ~ 5 parts of Herba Andrographitis,
6 ~ 8 parts of Chinese gall, 5 ~ 7 parts of granatum, 6 ~ 9 parts of honeysuckle, 3 ~ 7 parts of dandelion, 9 ~ 12 parts of the tuber of stemona, 8 ~ 13 parts of kuh-seng, fructus lycii 10 ~
13 parts, each herbal raw material is crushed, after crossing 40 ~ 50 meshes, it is spare to obtain traditional Chinese medicine powder.
5. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 1, it is characterised in that: the microwave
Extraction step are as follows: the water of 6 ~ 8 times of amounts are added into traditional Chinese medicine powder, after impregnating 20 ~ 30min, 35 ~ 55min of Microwave Extraction, then mistake
Filter, filtrate is the Chinese herbal medicine extract.
6. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 5, it is characterised in that: the microwave
Extraction power is 400 ~ 700W, and temperature is 100 ~ 110 DEG C.
7. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 1, it is characterised in that: the fertilizer
Granulation step are as follows: sodium humate, potassium fulvate, bamboo vinegar and microelement are added into Chinese herbal and crude drugs preparations, after mixing evenly, then
Attapulgite is added to mix, is then granulated and dry to get training algae fertilizer.
8. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 7, it is characterised in that: the fertilizer
It is granulated as follows with the parts by weight of raw material: 20 ~ 25 parts of Chinese herbal and crude drugs preparations, 11 ~ 14 parts of sodium humate, 10 ~ 15 parts of potassium fulvate, bamboo vinegar
6 ~ 8 parts of liquid, 5 ~ 7 parts of microelement, 24 ~ 29 parts of attapulgite.
9. a kind of preparation method of training algae fertilizer containing Chinese herbal medicine according to claim 7, it is characterised in that: described micro
Element is made of borax and Chelating state calcium, magnesium, manganese, copper, zinc, and weight ratio is 2 ~ 2.5:1.5 ~ 2.5:1 ~ 2:1:1:1.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811016994.0A CN109232126A (en) | 2018-09-03 | 2018-09-03 | A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811016994.0A CN109232126A (en) | 2018-09-03 | 2018-09-03 | A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109232126A true CN109232126A (en) | 2019-01-18 |
Family
ID=65060302
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811016994.0A Withdrawn CN109232126A (en) | 2018-09-03 | 2018-09-03 | A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109232126A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113149774A (en) * | 2021-05-27 | 2021-07-23 | 浙江农林大学 | Disease-resistant growth-promoting bio-organic fertilizer for solanaceous vegetables and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101423439A (en) * | 2008-12-02 | 2009-05-06 | 史掌元 | Chinese herbal medicine essence for culturing algae |
| CN101792352A (en) * | 2010-04-20 | 2010-08-04 | 北京鑫洋水产高新技术有限公司 | Special high-efficiency compound fertilizer for freshwater aquiculture |
| CN104381606A (en) * | 2014-11-18 | 2015-03-04 | 湖北任森农业科技发展有限公司 | Aquaculture growth hormone and preparation technology thereof |
| CN106509479A (en) * | 2016-09-30 | 2017-03-22 | 防城港市金沙海洋科技有限责任公司 | Special alga culturing fertilizer for aquaculture |
-
2018
- 2018-09-03 CN CN201811016994.0A patent/CN109232126A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101423439A (en) * | 2008-12-02 | 2009-05-06 | 史掌元 | Chinese herbal medicine essence for culturing algae |
| CN101792352A (en) * | 2010-04-20 | 2010-08-04 | 北京鑫洋水产高新技术有限公司 | Special high-efficiency compound fertilizer for freshwater aquiculture |
| CN104381606A (en) * | 2014-11-18 | 2015-03-04 | 湖北任森农业科技发展有限公司 | Aquaculture growth hormone and preparation technology thereof |
| CN106509479A (en) * | 2016-09-30 | 2017-03-22 | 防城港市金沙海洋科技有限责任公司 | Special alga culturing fertilizer for aquaculture |
Non-Patent Citations (4)
| Title |
|---|
| 叶勇: "《制药工艺学》", 28 February 2014, 华南理工大学出版社 * |
| 张兆旺: "《中药药剂学 供中药类专业用 新世纪 第2版》", 31 July 2017, 中国中医药出版社 * |
| 徐卫国: "《嘉兴新型职业农民培训系列教材 嘉兴特色水产养殖技术》", 31 January 2017, 中国农业大学出版社 * |
| 沈阳药学院《常用药物制剂》编写组: "《常用药物制剂》", 30 November 1975, 辽宁人民出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113149774A (en) * | 2021-05-27 | 2021-07-23 | 浙江农林大学 | Disease-resistant growth-promoting bio-organic fertilizer for solanaceous vegetables and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102674961B (en) | Organic fertilizer produced from tea cakes | |
| CN104311335B (en) | Have soil-repairing agent and the preparation technology of process heavy metal contamination and getting fat effect concurrently | |
| CN102584432A (en) | Total-nutrient kelp oligosaccharide biological synergistic fertilizer and preparation method thereof | |
| CN106973744A (en) | A kind of high-yield planting method of positive hair Exocarpium Citri Rubrum | |
| CN106219705B (en) | A kind of pure natural flocculant and preparation method thereof changed for aquaculture pond bottom | |
| CN104058880A (en) | Pesticide fertilizer for danshen root GAP standard planting and production method thereof | |
| CN108283191B (en) | Preparation method of pesticide for preventing and treating Chinese chive maggots | |
| CN105541448A (en) | Fertilizer powder for cultivating high-selenium and germanium, cancer prevention and life prolongation broccoli | |
| CN107006538A (en) | A kind of plant environment-friendly type bactericide used for aquiculture and preparation method thereof | |
| CN109221795A (en) | A kind of purposes of the aquatic feeds rich in protein | |
| CN109503251A (en) | A kind of preparation method and applications of biostimulant | |
| CN105859378A (en) | Biological organic fertilizer and preparation method thereof | |
| CN103333014B (en) | Rich selenium germanium ferment ketone gathers the Kidney bean oil of enzyme | |
| CN109232126A (en) | A kind of preparation method of the training algae fertilizer containing Chinese herbal medicine | |
| CN109329322A (en) | The preparation method for the fungicide that can be purified water | |
| CN107467045A (en) | Preparation method using biogas slurry as the jamaicin aqua of solvent | |
| CN106630088A (en) | Preparation for preventing and treating citrus yellow shoot and preparation method of preparation | |
| CN107056441A (en) | A kind of preparation method of the bio-feritlizer containing willow leaf | |
| CN108373389A (en) | A kind of gardens broadleaf tree nutrient solution and preparation method | |
| CN107027828A (en) | A kind of plant environment-friendly type bactericide used for aquiculture and preparation method thereof | |
| CN106854112A (en) | A kind of production method of the liquid seaweed manure for being exclusively used in rhizoma Gastrodiae | |
| CN107445745A (en) | A kind of organic fertilizer for planting white jade cherry | |
| CN107223527A (en) | A kind of cuttage and seedling culture method of grape | |
| CN113072406A (en) | Plant fermentation extract for preventing rice from absorbing heavy metals and preparation method thereof | |
| CN106631380A (en) | Preparation method of seaweed organic fertilizer for promoting plant growth |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20190118 |
|
| WW01 | Invention patent application withdrawn after publication |