CN109221294A - A kind of heavy duty detergent compound bio crops pesticide and preparation method thereof - Google Patents

A kind of heavy duty detergent compound bio crops pesticide and preparation method thereof Download PDF

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Publication number
CN109221294A
CN109221294A CN201811075752.9A CN201811075752A CN109221294A CN 109221294 A CN109221294 A CN 109221294A CN 201811075752 A CN201811075752 A CN 201811075752A CN 109221294 A CN109221294 A CN 109221294A
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parts
compound
heavy duty
oil
duty detergent
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Inventor
徐益峰
方润
刘明浩
何海峰
吴兵
袁成军
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ANHUI YINONG CHEMICAL Co Ltd
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ANHUI YINONG CHEMICAL Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/02Sulfur; Selenium; Tellurium; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • A01N59/14Boron; Compounds thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10Animals; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/30Microbial fungi; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/12Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/24Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/26Meliaceae [Chinaberry or Mahogany family], e.g. mahogany, langsat or neem
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
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  • Agronomy & Crop Science (AREA)
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  • Plant Pathology (AREA)
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  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Mycology (AREA)
  • Pest Control & Pesticides (AREA)
  • Virology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Botany (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of heavy duty detergent compound bio crops pesticides, the parts by weight of its raw material components are as follows: compound nonionic emulsifier 20-28 parts, 7-12 parts of borax, 1-4 parts of Bitter Melon P.E, 1-4 parts of chitosan, 2-4 parts of composite bacteria preparation, 1-3 parts of purslane, 1-3 parts of rhizome of cyrtomium, 1-3 parts of cordate houttuynia, 1-3 parts of azedarach, 1-3 parts of Dalmatian chrysanthemum, 0.5-1.5 parts of leaf tobacco extract, 0.5-1.5 parts of Asian puccoon, 0.5-1.5 parts of microelement, 0.5-1.5 parts of allicin, 2-6 parts of litsea citrate oil, 2-4 parts of cassia oil, 1-5 parts of coumarin kind compound, 1-2 parts of zinc sulfate, 3-8 parts of wetting agent, water is surplus, total amount is 100 parts, the present invention cooperates composite bacteria preparation by a variety of Chinese herbal medicines, chitosan, mountain is grey Seed oil, cassia oil and coumarin kind compound have good insecticidal and antibacterial effect, can controlling plant diseases, and natural environmental-protective.

Description

A kind of heavy duty detergent compound bio crops pesticide and preparation method thereof
Technical field
The present invention relates to pesticide field, specifically a kind of heavy duty detergent compound bio crops pesticide and preparation method thereof.
Background technique
Biological pesticide refers to directly using biogenic bioactive substance or biological living as pesticide, and artificial The pesticide identical with native compound structure of synthesis.Biological pesticide includes that microbial pesticide, botanical pesticide, bioid are learned to farm The biological pesticides such as medicine, genetically modified organism and natural enemy biology.According to the standard of FAO (Food and Agriculture Organization of the United Nation), biological pesticide is usually natural Compound or genetic dressing agent, mainly include biochemical pesticides (pheromones, hormone, plant modifying agent, insect growth tune Save agent) and microbial pesticide (fungi, bacterium, insect viruses, protozoan, or the microorganism through genetic modification).
Biological pesticide product, they only have effect to pest and disease damage, generally safer to people and animals and various beneficial organisms, right The influence of non-target organism is also smaller.Biological pesticide is biological living, if eco environment facto is not considered, then biological agriculture Medicine is to non-target organism substantially without lethality.Insect pathogenic fungus, bacterium, virus etc. are from susceptible in biological pesticide It is separated in insect, acts on this kind of insect by artificial propagation, in addition most of biological pesticide is all by influencing to do harm to Worm feeds and reaches desinsection purpose, therefore the use of biological pesticide is very safe.
Summary of the invention
The purpose of the present invention is to provide a kind of heavy duty detergent compound bio crops pesticides and preparation method thereof, to solve The problems mentioned above in the background art.
To achieve the above object, the invention provides the following technical scheme:
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
Compound nonionic emulsifier 20-28 parts, it is 7-12 parts of borax, 1-4 parts of Bitter Melon P.E, 1-4 parts of chitosan, compound 2-4 parts of bacteria preparation, 1-3 parts of purslane, 1-3 parts of rhizome of cyrtomium, 1-3 parts of cordate houttuynia, 1-3 parts of azedarach, 1-3 parts of Dalmatian chrysanthemum, tobacco leaf mention Take 0.5-1.5 parts of object, 0.5-1.5 parts of Asian puccoon, 0.5-1.5 parts of microelement, 0.5-1.5 parts of allicin, 2-6 parts of litsea citrate oil, 2-4 parts of cassia oil, 1-5 parts of coumarin kind compound, 1-2 parts of zinc sulfate, 3-8 parts of wetting agent, water are surplus, and total amount is 100 parts.
The composite bacteria preparation is bacillus subtilis bacterium solution, beauveria bassiana liquid and yeast liquid according to 2:1:1 mass ratio It mixes.
The wetting agent is in the polyoxyethylene ether of sulfonated oil, soybean lecithin, thio-alcohol, mercaptan acetals, alkyl phenol Any nonionic surface active agent.
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
20 parts of compound nonionic emulsifier, 7 parts of borax, 1 part of Bitter Melon P.E, 1 part of chitosan, 2 parts of composite bacteria preparation, It is 1 part of purslane, 1 part of rhizome of cyrtomium, 1 part of cordate houttuynia, 1 part of azedarach, 1 part of Dalmatian chrysanthemum, 0.5 part of leaf tobacco extract, 0.5 part of Asian puccoon, micro- It is 0.5 part of secondary element, 0.5 part of allicin, 2 parts of litsea citrate oil, 2 parts of cassia oil, 1 part of coumarin kind compound, 1 part of zinc sulfate, wet 3 parts of agent of profit, water are surplus, and total amount is 100 parts.
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
28 parts of compound nonionic emulsifier, 12 parts of borax, 4 parts of Bitter Melon P.E, 4 parts of chitosan, composite bacteria preparation 4 Part, 3 parts of purslane, 3 parts of rhizome of cyrtomium, 3 parts of cordate houttuynia, 3 parts of azedarach, 3 parts of Dalmatian chrysanthemum, 1.5 parts of leaf tobacco extract, 1.5 parts of Asian puccoon, 1.5 parts of microelement, 1.5 parts of allicin, 6 parts of litsea citrate oil, 4 parts of cassia oil, 5 parts of coumarin kind compound, 2 parts of zinc sulfate, 8 parts of wetting agent, water are surplus, and total amount is 100 parts.
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
24 parts of compound nonionic emulsifier, 9 parts of borax, 3 parts of Bitter Melon P.E, 2 parts of chitosan, 3 parts of composite bacteria preparation, 2 parts of purslane, 2 parts of rhizome of cyrtomium, 2 parts of cordate houttuynia, 2 parts of azedarach, 2 parts of Dalmatian chrysanthemum, 1 part of leaf tobacco extract, 1 part of Asian puccoon, micro member Plain 1 part, 1 part of allicin, 4 parts of litsea citrate oil, 3 parts of cassia oil, 3 parts of coumarin kind compound, 1.5 parts of zinc sulfate, wetting agent 6 Part, water are surplus, and total amount is 100 parts.
A kind of preparation method of heavy duty detergent compound bio crops pesticide, comprising the following steps:
(1) by composite bacteria preparation, purslane, rhizome of cyrtomium, cordate houttuynia, azedarach, Dalmatian chrysanthemum, leaf tobacco extract, microelement, It after allicin drying, is crushed respectively by micronizer, crosses 50-100 mesh, then by after the mixing of various traditional Chinese medicine powders, be packed into extraction It takes in kettle, flow is passed through into extraction kettle and is the CO2 of 15-25L/h, and is extracted 3-6 hours, after extraction, institute is collected in decompression Obtained Chinese medical extract;
(2) oily phase is prepared: by Chinese medical extract, compound nonionic emulsifier, cassia oil, coumarin kind compound, wet Moisten agent, is mixed into uniform oily phase;
(3) it prepares water phase: borax, Bitter Melon P.E, chitosan, zinc sulfate, Asian puccoon, litsea citrate oil, He Shui is mixed into Uniform water phase;
(4) shear: water phase is slowly added in oily phase under conditions of magnetic stirrer, make two-phase mixtures uniformly at Thick lotion, and high-shear emulsion machine emulsification pretreatment.
Compared with prior art, the beneficial effects of the present invention are:
The present invention cooperates composite bacteria preparation, chitosan, litsea citrate oil, cassia oil and Coumarins by a variety of Chinese herbal medicines Close object, there is good insecticidal and antibacterial effect, at the same can controlling plant diseases, and it is natural environmental-protective, without any side effects, Product of the present invention is because of materials Chinese herbal medicine and agricultural wastes, so do not have toxic side effect to crops when killing pest, it can So that the agricultural product of people's relievedly edible safety, to human health totally nontoxic side effect;It can make the matter of agricultural product simultaneously Amount is significantly improved, therefore this biological agricultural chemical insecticide is suited large area to popularize and applied.A variety of Chinese herbal medicines of addition are day Right active material, it is degradable in the environment, to the mammals such as people and animals low toxicity, to pest natural enemy and other beneficial organisms safety.
Cassia oil can completely inhibit the growth of Candida albicans, and litsea citrate oil can completely inhibit staphylococcus aureus.It is miscellaneous Antibacterial work of the cyclosubstituted coumarin kind compound to the aquatic products common pathogen such as Streptococcusagalactiae, flavobacterium columnare, Vibrio anguillarum Property.As the result is shown: compound shows different degrees of inhibitory activity to pathogens such as flavobacterium columnare and Streptococcusagalactiaes
Specific embodiment
Embodiment 1
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
20 parts of compound nonionic emulsifier, 7 parts of borax, 1 part of Bitter Melon P.E, 1 part of chitosan, 2 parts of composite bacteria preparation, It is 1 part of purslane, 1 part of rhizome of cyrtomium, 1 part of cordate houttuynia, 1 part of azedarach, 1 part of Dalmatian chrysanthemum, 0.5 part of leaf tobacco extract, 0.5 part of Asian puccoon, micro- It is 0.5 part of secondary element, 0.5 part of allicin, 2 parts of litsea citrate oil, 2 parts of cassia oil, 1 part of coumarin kind compound, 1 part of zinc sulfate, wet 3 parts of agent of profit, water are surplus, and total amount is 100 parts.
The composite bacteria preparation is bacillus subtilis bacterium solution, beauveria bassiana liquid and yeast liquid according to 2:1:1 mass ratio It mixes.
The wetting agent is in the polyoxyethylene ether of sulfonated oil, soybean lecithin, thio-alcohol, mercaptan acetals, alkyl phenol Any nonionic surface active agent.
A kind of preparation method of heavy duty detergent compound bio crops pesticide, comprising the following steps:
(1) by after purslane, rhizome of cyrtomium, cordate houttuynia, azedarach, Dalmatian chrysanthemum, Asian puccoon drying, pass through micronizer powder respectively It is broken, 50-100 mesh is crossed, then by after the mixing of various traditional Chinese medicine powders, be fitted into extraction kettle, it is 15-25L/ that flow is passed through into extraction kettle The CO2 of h, and extract 3-6 hours, after extraction, obtained Chinese medical extract is collected in decompression;
(2) oily phase is prepared: by Chinese medical extract, compound nonionic emulsifier, cassia oil, coumarin kind compound, mountain Grey seed oil, wetting agent are mixed into uniform oily phase;
(3) prepare water phase: by composite bacteria preparation, leaf tobacco extract, microelement, allicin, borax, Bitter Melon P.E, Chitosan, zinc sulfate and water are mixed into uniform water phase;
(4) shear: water phase is slowly added in oily phase under conditions of magnetic stirrer, make two-phase mixtures uniformly at Thick lotion, and high-shear emulsion machine emulsification pretreatment.
Embodiment 2
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
28 parts of compound nonionic emulsifier, 12 parts of borax, 4 parts of Bitter Melon P.E, 4 parts of chitosan, composite bacteria preparation 4 Part, 3 parts of purslane, 3 parts of rhizome of cyrtomium, 3 parts of cordate houttuynia, 3 parts of azedarach, 3 parts of Dalmatian chrysanthemum, 1.5 parts of leaf tobacco extract, 1.5 parts of Asian puccoon, 1.5 parts of microelement, 1.5 parts of allicin, 6 parts of litsea citrate oil, 4 parts of cassia oil, 5 parts of coumarin kind compound, 2 parts of zinc sulfate, 8 parts of wetting agent, water are surplus, and total amount is 100 parts.
The composite bacteria preparation is bacillus subtilis bacterium solution, beauveria bassiana liquid and yeast liquid according to 2:1:1 mass ratio It mixes.
The wetting agent is in the polyoxyethylene ether of sulfonated oil, soybean lecithin, thio-alcohol, mercaptan acetals, alkyl phenol Any nonionic surface active agent.
A kind of preparation method of heavy duty detergent compound bio crops pesticide, comprising the following steps:
(1) by after purslane, rhizome of cyrtomium, cordate houttuynia, azedarach, Dalmatian chrysanthemum, Asian puccoon drying, pass through micronizer powder respectively It is broken, 50-100 mesh is crossed, then by after the mixing of various traditional Chinese medicine powders, be fitted into extraction kettle, it is 15-25L/ that flow is passed through into extraction kettle The CO2 of h, and extract 3-6 hours, after extraction, obtained Chinese medical extract is collected in decompression;
(2) oily phase is prepared: by Chinese medical extract, compound nonionic emulsifier, cassia oil, coumarin kind compound, mountain Grey seed oil, wetting agent are mixed into uniform oily phase;
(3) prepare water phase: by composite bacteria preparation, leaf tobacco extract, microelement, allicin, borax, Bitter Melon P.E, Chitosan, zinc sulfate and water are mixed into uniform water phase;
(4) shear: water phase is slowly added in oily phase under conditions of magnetic stirrer, make two-phase mixtures uniformly at Thick lotion, and high-shear emulsion machine emulsification pretreatment.
Embodiment 3
A kind of heavy duty detergent compound bio crops pesticide, the parts by weight of raw material components are as follows:
24 parts of compound nonionic emulsifier, 9 parts of borax, 3 parts of Bitter Melon P.E, 2 parts of chitosan, 3 parts of composite bacteria preparation, 2 parts of purslane, 2 parts of rhizome of cyrtomium, 2 parts of cordate houttuynia, 2 parts of azedarach, 2 parts of Dalmatian chrysanthemum, 1 part of leaf tobacco extract, 1 part of Asian puccoon, micro member Plain 1 part, 1 part of allicin, 4 parts of litsea citrate oil, 3 parts of cassia oil, 3 parts of coumarin kind compound, 1.5 parts of zinc sulfate, wetting agent 6 Part, water are surplus, and total amount is 100 parts.
The composite bacteria preparation is bacillus subtilis bacterium solution, beauveria bassiana liquid and yeast liquid according to 2:1:1 mass ratio It mixes.
The wetting agent is in the polyoxyethylene ether of sulfonated oil, soybean lecithin, thio-alcohol, mercaptan acetals, alkyl phenol Any nonionic surface active agent.
A kind of preparation method of heavy duty detergent compound bio crops pesticide, comprising the following steps:
(1) by after purslane, rhizome of cyrtomium, cordate houttuynia, azedarach, Dalmatian chrysanthemum, Asian puccoon drying, pass through micronizer powder respectively It is broken, 50-100 mesh is crossed, then by after the mixing of various traditional Chinese medicine powders, be fitted into extraction kettle, it is 15-25L/ that flow is passed through into extraction kettle The CO2 of h, and extract 3-6 hours, after extraction, obtained Chinese medical extract is collected in decompression;
(2) oily phase is prepared: by Chinese medical extract, compound nonionic emulsifier, cassia oil, coumarin kind compound, mountain Grey seed oil, wetting agent are mixed into uniform oily phase;
(3) prepare water phase: by composite bacteria preparation, leaf tobacco extract, microelement, allicin, borax, Bitter Melon P.E, Chitosan, zinc sulfate and water are mixed into uniform water phase;
(4) shear: water phase is slowly added in oily phase under conditions of magnetic stirrer, make two-phase mixtures uniformly at Thick lotion, and high-shear emulsion machine emulsification pretreatment.

Claims (7)

1. a kind of heavy duty detergent compound bio crops pesticide, which is characterized in that the parts by weight of its raw material components are as follows:
Compound nonionic emulsifier 20-28 parts, 7-12 parts of borax, 1-4 parts of Bitter Melon P.E, 1-4 parts of chitosan, compound bacteria system 2-4 parts of agent, 1-3 parts of purslane, 1-3 parts of rhizome of cyrtomium, 1-3 parts of cordate houttuynia, 1-3 parts of azedarach, 1-3 parts of Dalmatian chrysanthemum, leaf tobacco extract 0.5-1.5 parts, 0.5-1.5 parts of Asian puccoon, 0.5-1.5 parts of microelement, 0.5-1.5 parts of allicin, 2-6 parts of litsea citrate oil, cassia bark 2-4 parts oily, 1-5 parts of coumarin kind compound, 1-2 parts of zinc sulfate, 3-8 parts of wetting agent, water are surplus, and total amount is 100 parts.
2. heavy duty detergent compound bio crops pesticide according to claim 1, which is characterized in that the weight of its raw material components Measure part are as follows:
20 parts of compound nonionic emulsifier, 7 parts of borax, 1 part of Bitter Melon P.E, 1 part of chitosan, 2 parts of composite bacteria preparation, dent 1 part of amaranth, 1 part of rhizome of cyrtomium, 1 part of cordate houttuynia, 1 part of azedarach, 1 part of Dalmatian chrysanthemum, 0.5 part of leaf tobacco extract, 0.5 part of Asian puccoon, micro member Plain 0.5 part, 0.5 part of allicin, 2 parts of litsea citrate oil, 2 parts of cassia oil, 1 part of coumarin kind compound, 1 part of zinc sulfate, wetting agent 3 Part, water are surplus, and total amount is 100 parts.
3. heavy duty detergent compound bio crops pesticide according to claim 1, which is characterized in that the weight of its raw material components Measure part are as follows:
28 parts of compound nonionic emulsifier, 12 parts of borax, 4 parts of Bitter Melon P.E, 4 parts of chitosan, 4 parts of composite bacteria preparation, horse It is 3 parts of bitterroot, 3 parts of rhizome of cyrtomium, 3 parts of cordate houttuynia, 3 parts of azedarach, 3 parts of Dalmatian chrysanthemum, 1.5 parts of leaf tobacco extract, 1.5 parts of Asian puccoon, micro 1.5 parts of element, 6 parts of litsea citrate oil, 4 parts of cassia oil, 5 parts of coumarin kind compound, 2 parts of zinc sulfate, moistens 1.5 parts of allicin 8 parts of agent, water are surplus, and total amount is 100 parts.
4. heavy duty detergent compound bio crops pesticide according to claim 1, which is characterized in that the weight of its raw material components Measure part are as follows:
24 parts of compound nonionic emulsifier, 9 parts of borax, 3 parts of Bitter Melon P.E, 2 parts of chitosan, 3 parts of composite bacteria preparation, dent 2 parts of amaranth, 2 parts of rhizome of cyrtomium, 2 parts of cordate houttuynia, 2 parts of azedarach, 2 parts of Dalmatian chrysanthemum, 1 part of leaf tobacco extract, 1 part of Asian puccoon, microelement 1 Part, 1 part of allicin, 4 parts of litsea citrate oil, 3 parts of cassia oil, 3 parts of coumarin kind compound, 1.5 parts of zinc sulfate, 6 parts of wetting agent, water For surplus, total amount is 100 parts.
5. heavy duty detergent compound bio crops pesticide according to claim 1, which is characterized in that the composite bacteria preparation It is mixed for bacillus subtilis bacterium solution, beauveria bassiana liquid and yeast liquid according to 2:1:1 mass ratio.
6. heavy duty detergent compound bio crops pesticide according to claim 1, which is characterized in that the wetting agent is sulphur Carburetion, soybean lecithin, thio-alcohol, mercaptan acetals, alkyl phenol polyoxyethylene ether in any non-ionic surfactant Agent.
7. a kind of preparation method of heavy duty detergent compound bio crops pesticide, which comprises the following steps:
(1) it by after purslane, rhizome of cyrtomium, cordate houttuynia, azedarach, Dalmatian chrysanthemum, Asian puccoon drying, is crushed respectively by micronizer, 50-100 mesh is crossed, then by after the mixing of various traditional Chinese medicine powders, is fitted into extraction kettle, it is 15-25L/h's that flow is passed through into extraction kettle CO2, and extract 3-6 hours, after extraction, obtained Chinese medical extract is collected in decompression;
(2) oily phase is prepared: by Chinese medical extract, compound nonionic emulsifier, cassia oil, coumarin kind compound, the fruit of a cubeb litsea tree Oil, wetting agent are mixed into uniform oily phase;
(3) it prepares water phase: composite bacteria preparation, leaf tobacco extract, microelement, allicin, borax, Bitter Melon P.E, shell is gathered Sugar, zinc sulfate and water are mixed into uniform water phase;
(4) it shears: water phase being slowly added in oily phase under conditions of magnetic stirrer, makes two-phase mixtures uniformly at thick cream Liquid, and high-shear emulsion machine emulsification pretreatment.
CN201811075752.9A 2018-09-14 2018-09-14 A kind of heavy duty detergent compound bio crops pesticide and preparation method thereof Pending CN109221294A (en)

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CN112125731A (en) * 2020-09-10 2020-12-25 河南省科学院 Plant-source multifunctional liquid pesticide fertilizer and preparation method thereof
WO2021009164A1 (en) * 2019-07-16 2021-01-21 Universiteit Gent Plant extract for controlling parasitic nematodes

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Publication number Priority date Publication date Assignee Title
WO2021009164A1 (en) * 2019-07-16 2021-01-21 Universiteit Gent Plant extract for controlling parasitic nematodes
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