CN109183184A - A kind of preparation method and capsule fiber of capsule fiber - Google Patents
A kind of preparation method and capsule fiber of capsule fiber Download PDFInfo
- Publication number
- CN109183184A CN109183184A CN201810920899.7A CN201810920899A CN109183184A CN 109183184 A CN109183184 A CN 109183184A CN 201810920899 A CN201810920899 A CN 201810920899A CN 109183184 A CN109183184 A CN 109183184A
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- Prior art keywords
- capsule
- core
- fiber
- powder
- aromatic
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/103—Agents inhibiting growth of microorganisms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/39—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/341—Material containing ester groups using acid dyes
Abstract
The preparation method and capsule fiber of capsule fiber provided by the invention, for improveing the functional characteristic of existing capsule fiber, wherein preparation method includes the following steps: that 450 meshes fine maifanite powder below for medical stone is made；Pollen particles are uniformly mixed with fine maifanite powder by weight 3:2, aromatic powder is obtained；Acid dyes and Carbon fibe element are mixed to prepare capsule-core under vacuum conditions；Under 40-55 degree Celsius range, aromatic powder and liquid water are modulated into aromatic liquid；At normal temperature, capsule-core is immersed in aromatic liquid to take out after 20-30 minutes and is dried, functionality capsule-core is made；Hydrophilic colloid and capsule-core are wrapped to form microcapsules, microcapsules are added in the polyester slice under molten condition and are uniformly mixed, spinning material is obtained；Spinning material addition spinning machine high-speed spinning is woven into as-spun fibre；Capsule fiber is obtained after as-spun fibre is formed by parallel drafting machine.The technological merit that there is the present invention capsule fiber additional function can keep for a long time.
Description
Technical field
The present invention relates to capsule fibre technology fields, and the preparation method and capsule more particularly, to a kind of capsule fiber are fine
Dimension.
Background technique
Textile in the prior art constantly pursues the diversification in terms of function, textile high performance, multifunction and
Intelligence always is main flow direction of this field in terms of new-product development.Capsule fiber in the prior art is in functionality side
Face is difficult to keep for a long time, and after a period of use, to gradually lose original fabric institute due for accompaniment functions ingredient lost
Additional function；Further, the cyst wall of capsule fiber is not usually good enough in terms of structural strength in the prior art, rubs shape in washing
Breakage easily occurs under state, the functional components being located in capsule is caused to generate too fast lost, Jin Ergeng after clothes washing
Further shorten the service life of functional fabric.
Therefore it provides a kind of capsule fiber and preparation method thereof, for solving at least one of above-mentioned technological deficiency just
The technical problem urgently to be resolved as those skilled in the art.
Summary of the invention
The object of the present invention is to provide a kind of preparation method of capsule fiber and capsule fibers, fine for solving existing capsule
Dimension additional function is not easy the technical issues of keeping for a long time.
To achieve the goals above, on the one hand, the present invention provides a kind of preparation method of capsule fiber, the method includes
Following steps:
450 meshes fine maifanite powder below is made in medical stone；
Pollen particles are ground to after nano-scale particle degree and are uniformly mixed with the fine maifanite powder by weight 3:2
It closes, obtains aromatic powder；
Capsule-core is made in acid dyes and Carbon fibe element after mixing under vacuum conditions；
Under 40-55 degree Celsius range, the aromatic powder and liquid water are modulated after evenly mixing by weight 1:50-80
At aromatic liquid；
At normal temperature, the capsule-core is immersed in the aromatic liquid to take out after 20-30 minutes and is dried, functionality capsule is made
Core；
Hydrophilic colloid and the capsule-core are wrapped to form microcapsules, the polyester that the microcapsules are added under molten condition is cut
It is uniformly mixed in piece, obtains spinning material；
Spinning material addition spinning machine high-speed spinning is woven into as-spun fibre；
Capsule fiber is obtained after the as-spun fibre is formed by parallel drafting machine.
Preferably, the pollen includes but is not limited to: Flos Rosae Rugosas pollen, Jasmine are fragrant, lilac is fragrant and lilium pollen.
Preferably, the hydrophilic colloid is gelatin.
Preferably, peppermint and wintergreen are also added in the aromatic powder；The pollen particles, fine maifanite powder,
Peppermint and wintergreen are configured that 3:2:0.5:0.3 by weight.
Preferably, the liquid water is deionized water.
Preferably, in step: " at normal temperature, the capsule-core being immersed in the aromatic liquid to take out after 20-30 minutes and be dried
It is dry, functionality capsule-core is made；" in, further includes: one layer is sprayed by the poly- cream of polyethylene glycol-b- in the functional capsule-core outer surface
The inner membrance formed after sour methyl ether and polymethyl acrylate mixing；The polyethylene-b-polylactic acid methyl ether and the polyacrylic acid
The mixed weight proportion of methyl esters is 2:1.
Preferably, rendering is further comprised the steps of:；Wherein, the formula used in rendering step is as follows: weak acid dye raw material
35~40g/l, 2~6g/l of auxiliary agent, surplus are water.
Preferably, the operating procedure of the rendering is as follows:
Under room temperature and vacuum environment, by capsule fiber impregnation in the rendering agent made of being formulated according to the rendering；
With the temperature speedup of 2 centigrade per minutes, dye temperature is warming up to 40 degrees Celsius；
Capsule fiber is continued to keep the temperature and is taken out after 15 minutes in 40 degrees Celsius of dyestuff；
It is rinsed described capsule fibre 2~3 times with 90~100 degrees Celsius of clear water, and is dried at a temperature of 110~120；
Finished product is obtained after the capsule fibre is formed again on forming machine.
Preferably, anti-mite deodorization nano powder is also added in the aromatic powder；The weight of the anti-mite deodorization nano powder is matched
Than as follows:
5-8 parts of Ag-carried nanometer titanium dioxide antibacterial agent；
2-3 parts of zinc oxide nano；
3-6 parts of hygroscopic fibre；
20-40 parts of tourmaline nano powder.
To achieve the goals above, on the other hand, the present invention also provides a kind of capsule fiber, the capsule fiber is by before such as
The preparation method of the capsule fiber is made.
Compared with capsule fiber in the prior art, this patent is had the advantage that
1, functionality capsule-core made from the preparation method according to capsule fiber provided by the present invention volatilizees with effective component
Persistently, and reusable technological merit；The Carbon fibe element added in capsule-core has extremely strong weigh for functional components
Multiple adsorptivity；When capsule fiber functional components volatilize totally, capsule fiber need to only be soaked under 40-55 degree Celsius range
Bubble can restore original effect of capsule fiber 10 minutes or more in aromatic liquid, and there is functional fabric additional function can weigh
The technological merit of renaturation continuation of the journey；Further, there is higher structural strength, water-washing process using cyst wall made from hydrophilic colloid
Middle cyst wall is not easily broken, and then is capable of the service life of substantially reinfored glue capsular fibers, and is the equal of the functional components in capsule
Even slow release provides strong structure guarantee.
2, the peppermint and wintergreen further added in aromatic powder can further be added for functional capsule-core refresh oneself it is awake
The function of brain is suitble to using capsule fiber production jacket or scrambled eggs, and then provides basic fabric for functional clothes or dress ornament.
3, the inner membrance being sprayed on functional capsule-core can effectively keep the functional components adsorbed in capsule-core in a timing
Slow uniform release in limit, inhibits functional components contained on capsule fiber using initial stage fragrance excessively strong, latter stage
Fragrance is excessively light, and then reaches functional components in the release of relatively longer following period of time lasting stability.
4, it is able to ascend the dyefastness of capsule fiber surface for the Rendering operations that preparation process further adds, causes glue
Technical parameter in terms of the washable, fast light of capsular fibers, rub resistance, perspiration resistance, resistance to ironing and weatherability is increased dramatically；
Wherein, treated, and its color fastness to light of capsule fiber is not less than 6 grades, rub resistance, perspiration resistance, resistance to ironing and weatherability aspect
Technical parameter be 3 grades or more；For rub resistance no matter dry state friction or hygrometric state friction, can reach 5 grades of technology
Effect.
5, the anti-mite deodorization nano powder further added in aromatic powder can further add anti-mite for capsule fiber
The technical effect of deodorization, can be substantially improved the wearing comfort of capsule fiber, and can be by big model in smell and in a manner of absorption
It encloses and inhibits distributing for body odour, suitable for catering to the demand of wearing for savouring heavier consumer groups.
Specific embodiment
The embodiment of the present invention is described below in detail, since following embodiments are exemplary, it is intended to for explaining this hair
It is bright, and then be not considered as limiting the invention.
The present invention proposes a kind of preparation method of capsule fiber, concrete scheme includes the following steps:
450 meshes fine maifanite powder below is made in medical stone；
Pollen particles are ground to after nano-scale particle degree and are uniformly mixed with the fine maifanite powder by weight 3:2
It closes, obtains aromatic powder；
Capsule-core is made in acid dyes and Carbon fibe element after mixing under vacuum conditions；
Under 40-55 degree Celsius range, the aromatic powder and liquid water are modulated after evenly mixing by weight 1:50-80
At aromatic liquid；
At normal temperature, the capsule-core is immersed in the aromatic liquid to take out after 20-30 minutes and is dried, functionality capsule is made
Core；
Hydrophilic colloid and the capsule-core are wrapped to form microcapsules, the polyester that the microcapsules are added under molten condition is cut
It is uniformly mixed in piece, obtains spinning material；
Spinning material addition spinning machine high-speed spinning is woven into as-spun fibre；
Capsule fiber is obtained after the as-spun fibre is formed by parallel drafting machine.
Further, in one of optimal technical scheme of the present embodiment, to cater to different consumers to pollen gas
The hobby of taste, above-mentioned pollen includes but is not limited to: Flos Rosae Rugosas pollen, Jasmine are fragrant, lilac is fragrant and lilium pollen.
Further, in one of optimal technical scheme of the present embodiment, the hydrophilic colloid is gelatin.
Further, in one of optimal technical scheme of the present embodiment, peppermint is also added in the aromatic powder
And wintergreen；The pollen particles, fine maifanite powder, peppermint and wintergreen are configured that 3:2:0.5:0.3 by weight.
Further, in one of optimal technical scheme of the present embodiment, the liquid water is deionized water.
Further, in one of optimal technical scheme of the present embodiment, in step: " at normal temperature, by the capsule
Core, which was immersed in the aromatic liquid after 20-30 minutes, takes out drying, and functionality capsule-core is made；" in, further includes: in the function
Property capsule-core outer surface spray one layer by the inner membrance that is formed after polyethylene-b-polylactic acid methyl ether and polymethyl acrylate mixing；Institute
The mixed weight proportion for stating polyethylene-b-polylactic acid methyl ether and the polymethyl acrylate is 2:1.
Further, in one of optimal technical scheme of the present embodiment, rendering is further comprised the steps of:；Wherein, in wash with watercolours
It is as follows to contaminate formula used in step: 35~40g/l of weak acid dye raw material, 2~6g/l of auxiliary agent, surplus are water.
Further, in one of optimal technical scheme of the present embodiment, the operating procedure of the rendering is as follows:
Under room temperature and vacuum environment, by capsule fiber impregnation in the rendering agent made of being formulated according to the rendering；
With the temperature speedup of 2 centigrade per minutes, dye temperature is warming up to 40 degrees Celsius；
Capsule fiber is continued to keep the temperature and is taken out after 15 minutes in 40 degrees Celsius of dyestuff；
It is rinsed described capsule fibre 2~3 times with 90~100 degrees Celsius of clear water, and is dried at a temperature of 110~120；
Finished product is obtained after the capsule fibre is formed again on forming machine.
Further, in one of optimal technical scheme of the present embodiment, anti-mite is also added in the aromatic powder
Deodorization nano powder；The weight proportion of the anti-mite deodorization nano powder is as follows:
5-8 parts of Ag-carried nanometer titanium dioxide antibacterial agent；
2-3 parts of zinc oxide nano；
3-6 parts of hygroscopic fibre；
20-40 parts of tourmaline nano powder.
It should be noted that be also protection emphatically required by the present invention according to the capsule fiber that above-mentioned preparation method obtains,
Also protection scope of the present invention should be fallen into.
Compared with capsule fiber in the prior art, this patent is had the advantage that
1, functionality capsule-core made from the preparation method according to capsule fiber provided by the present invention volatilizees with effective component
Persistently, and reusable technological merit；The Carbon fibe element added in capsule-core has extremely strong weigh for functional components
Multiple adsorptivity；When capsule fiber functional components volatilize totally, capsule fiber need to only be soaked under 40-55 degree Celsius range
Bubble can restore original effect of capsule fiber 10 minutes or more in aromatic liquid, and there is functional fabric additional function can weigh
The technological merit of renaturation continuation of the journey；Further, there is higher structural strength, water-washing process using cyst wall made from hydrophilic colloid
Middle cyst wall is not easily broken, and then is capable of the service life of substantially reinfored glue capsular fibers, and is the equal of the functional components in capsule
Even slow release provides strong structure guarantee.
2, the peppermint and wintergreen further added in aromatic powder can further be added for functional capsule-core refresh oneself it is awake
The function of brain is suitble to using capsule fiber production jacket or scrambled eggs, and then provides basic fabric for functional clothes or dress ornament.
3, the inner membrance being sprayed on functional capsule-core can effectively keep the functional components adsorbed in capsule-core in a timing
Slow uniform release in limit, inhibits functional components contained on capsule fiber using initial stage fragrance excessively strong, latter stage
Fragrance is excessively light, and then reaches functional components in the release of relatively longer following period of time lasting stability.
4, it is able to ascend the dyefastness of capsule fiber surface for the Rendering operations that preparation process further adds, causes glue
Technical parameter in terms of the washable, fast light of capsular fibers, rub resistance, perspiration resistance, resistance to ironing and weatherability is increased dramatically；
Wherein, treated, and its color fastness to light of capsule fiber is not less than 6 grades, rub resistance, perspiration resistance, resistance to ironing and weatherability aspect
Technical parameter be 3 grades or more；For rub resistance no matter dry state friction or hygrometric state friction, can reach 5 grades of technology
Effect.
5, the anti-mite deodorization nano powder further added in aromatic powder can further add anti-mite for capsule fiber
The technical effect of deodorization, can be substantially improved the wearing comfort of capsule fiber, and can be by big model in smell and in a manner of absorption
It encloses and inhibits distributing for body odour, suitable for catering to the demand of wearing for savouring heavier consumer groups.
The various embodiments described above are only the preferred embodiment of the present invention, in the art, all to be based on skill of the present invention
Changes and improvements in art scheme should not exclude except protection scope of the present invention.
Claims (10)
1. a kind of preparation method of capsule fiber, which is characterized in that described method includes following steps:
450 meshes fine maifanite powder below is made in medical stone；
Pollen particles are ground to after nano-scale particle degree and are uniformly mixed with the fine maifanite powder by weight 3:2, are obtained
To aromatic powder；
Capsule-core is made in acid dyes and Carbon fibe element after mixing under vacuum conditions；
Under 40-55 degree Celsius range, the aromatic powder and liquid water are modulated into virtue by weight 1:50-80 after evenly mixing
Fragrant liquid；
At normal temperature, the capsule-core is immersed in the aromatic liquid to take out after 20-30 minutes and is dried, functionality capsule-core is made；
Hydrophilic colloid and the capsule-core are wrapped to form microcapsules, the microcapsules are added in the polyester slice under molten condition
It is uniformly mixed, obtains spinning material；
Spinning material addition spinning machine high-speed spinning is woven into as-spun fibre；
Capsule fiber is obtained after the as-spun fibre is formed by parallel drafting machine.
2. the method according to claim 1, wherein the pollen includes but is not limited to: Flos Rosae Rugosas pollen, Jasmine
Fragrant, lilac sweet smell and lilium pollen.
3. the method according to claim 1, wherein the hydrophilic colloid is gelatin.
4. the method according to claim 1, wherein being also added with peppermint and wintergreen in the aromatic powder；Institute
It states pollen particles, fine maifanite powder, peppermint and wintergreen and is configured that 3:2:0.5:0.3 by weight.
5. the method according to claim 1, wherein the liquid water is deionized water.
6. the method according to claim 1, wherein in step: " capsule-core at normal temperature, being immersed in institute
It states and takes out drying in aromatic liquid after 20-30 minutes, functionality capsule-core is made；" in, further includes: in the functional capsule-core appearance
Face sprays one layer of inner membrance by being formed after polyethylene-b-polylactic acid methyl ether and polymethyl acrylate mixing；The polyethylene glycol-
B- polylactic acid methyl ether and the mixed weight of polymethyl acrylate proportion are 2:1.
7. the method according to claim 1, wherein further comprising the steps of: rendering；Wherein, the institute in rendering step
Formula is as follows: 35~40g/l of weak acid dye raw material, 2~6g/l of auxiliary agent, surplus are water.
8. the method according to the description of claim 7 is characterized in that the operating procedure of the rendering is as follows:
Under room temperature and vacuum environment, by capsule fiber impregnation in the rendering agent made of being formulated according to the rendering；
With the temperature speedup of 2 centigrade per minutes, dye temperature is warming up to 40 degrees Celsius；
Capsule fiber is continued to keep the temperature and is taken out after 15 minutes in 40 degrees Celsius of dyestuff；
It is rinsed described capsule fibre 2~3 times with 90~100 degrees Celsius of clear water, and is dried at a temperature of 110~120；
Finished product is obtained after the capsule fibre is formed again on forming machine.
9. the method according to claim 1, wherein being also added with anti-mite deodorization nano powder in the aromatic powder；
The weight proportion of the anti-mite deodorization nano powder is as follows:
5-8 parts of Ag-carried nanometer titanium dioxide antibacterial agent；
2-3 parts of zinc oxide nano；
3-6 parts of hygroscopic fibre；
20-40 parts of tourmaline nano powder.
10. a kind of capsule fiber, which is characterized in that capsule fiber capsule as described in any one of claim 1 to 9
The preparation method of fiber is made.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810920899.7A CN109183184A (en) | 2018-08-14 | 2018-08-14 | A kind of preparation method and capsule fiber of capsule fiber |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810920899.7A CN109183184A (en) | 2018-08-14 | 2018-08-14 | A kind of preparation method and capsule fiber of capsule fiber |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110004510A (en) * | 2019-04-25 | 2019-07-12 | 希肤科技（上海）有限公司 | A kind of preparation process of jade viscose rayon and mask substrate |
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Application publication date: 20190111 |
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| RJ01 | Rejection of invention patent application after publication |