CN107523897A - A kind of preparation method of health care's polyester fiber - Google Patents
A kind of preparation method of health care's polyester fiber Download PDFInfo
- Publication number
- CN107523897A CN107523897A CN201710855770.8A CN201710855770A CN107523897A CN 107523897 A CN107523897 A CN 107523897A CN 201710855770 A CN201710855770 A CN 201710855770A CN 107523897 A CN107523897 A CN 107523897A
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- CN
- China
- Prior art keywords
- polyester fiber
- preparation
- health care
- health
- spinning
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
Abstract
The present invention relates to a kind of preparation method of polyester fiber, in order to solve the problems, such as the health-care components during health fiber modified poly ester rapidly volatilize distillation and the duration it is short, the present invention proposes a kind of preparation method of health care's polyester fiber, using abstraction technique by lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon has the extraction of health functionses composition to human body, spansule is made, master batch is made with slow capsule is released, then it is added in spinning process in melt, health care's polyester fiber is made after the completion of spinning, the available polyester fiber that can release slow health-care components for a long time, it is effectively improved the healthcare function of polyester fiber.
Description
Technical field
The present invention relates to a kind of preparation method of polyester fiber, more particularly to a kind of preparation side of health care's polyester fiber
Method.
Background technology
Polyester fiber have the advantages that intensity is high, wearability is good, surface is smooth, can thermal finalization, physical and chemical performance it is stable, it is wide
It is general to be applied to dress ornament field.But continuation essential oil ongoing health care's function of polyester fiber is not developed, patent
Product disclosed in CN102134769A, it is in a kind of chemical fibre strip body containing multiple micropores, adheres to essential oil particle.It is this
Method attachment fastness is poor, and poor durability is not water-fastness.In order to improve health functionses, Many researchers largely add Chinese medicine
Composition, make polyester fiber there are a kind of flavour of a drug to volatilize, welding sense with fresh air, also give people a kind of heavy sensation.
The content of the invention
In order to solve, the health-care components during health fiber modified poly ester volatilize rapidly distillation and the duration short asks
Topic, the present invention propose a kind of preparation method of health care's polyester fiber, when adding spansule, first carry out spansule
High temperature resistant processing, is then quickly cooled down in the spinning later stage, the available polyester fiber that can release slow health-care components for a long time, is had
Effect improves the healthcare function of polyester fiber.
The present invention is achieved by the following technical solutions:A kind of preparation method of health care's polyester fiber is following step
Suddenly:
(1)Lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon active ingredient are extracted;
Preferably, lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, the mass ratio of lemon is 15:15:20:15:20:15.
(2)Extract and polyurethane are fabricated to spansule at 130-180 DEG C,
Preferably, release slow capsule dries 6-10 hours in 80-120 DEG C of baking oven;
Preferably, the mass ratio of extract and polyurethane is 5:95-10:90.Spansule is fabricated to by interfacial polymerization,
Core is emulsified or is dispersed in one dissolved with the continuous phase of wall material, is then polymerize on the surface of core material by monomer
React and form microcapsules, be core to health-preserving function composition in the present invention, using polyurethane as wall, ensure the poly- of essential oil active ingredient
Collected explanations delays.
(3)Slow capsule and polybutylene terephthalate will be released(pet)Section is with mass percent 50:50-60:40 is abundant
Mixing, slow capsule master batch is released through twin (double) screw extruder, extruder head is fabricated under conditions of 220 DEG C -250 DEG C;
(4)Polyester slice makes polyester slice aqueous in below 30ppm, so by 120-180 DEG C of drying temperature progress crystallizing and drying
Afterwards by spansule master batch and polyester slice using mass ratio as 5:95-10:90 well mixed co-blended spinnings, obtain a kind of health care and support
Raw polyester fiber.
Spansule master batch is added by volume type master batch machine in screw rod mouth, is then added to melt in spinning process
In.
Preferably, spinneret draw ratio is 2.5 ~ 3.5 in spinning technique, component sand loading amount(Up/down)For(40~80)/
(100~300), 10 ~ 15MPa of component pressure, 285 ~ 292 DEG C of spinning temperature, 0.30 ~ 0.50m/s of cross air blasting wind speed;Oil applying rate is
1.0%~1.3%。
Preferably, POY spinning speed is 2500 ~ 3500m/min.
Preferably, FDY spinning speed is 4000 ~ 5500m/min, and draw ratio 2.6~3.2,70~90 DEG C of a roll temperature, two
115 ~ 135 DEG C of roll temperature.
Compared with prior art, the beneficial effects of the invention are as follows:
(1)Manufactured fiber dress ornament by with human body triboabsorption, have toxin expelling, restoring consciouness, refresh oneself, deodorizing, the work(such as relaxing tendons and activating collaterals
Effect;
(2)The available polyester fiber that can release slow health-care components for a long time, it is effectively improved the healthcare function of polyester fiber.
Embodiment
The present invention is described in further detail below by embodiment, it is raw materials used commercially available in embodiment.
Embodiment 1
(1)It is 15 in mass ratio by lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon:15:20:15:20:15 are extracted
Take, obtain extract;
(2)It is 5 in mass ratio by extract and polyurethane:95 are fabricated to spansule at 130 DEG C, release baking of the slow capsule at 80 DEG C
Dried 10 hours in case;
(3)Slow capsule will be released with polybutylene terephthalate section with mass percent 55:45 mixing, then through twin-screw extruder
Machine, extruder head are fabricated to essential oil under conditions of 230 DEG C and release slow capsule master batch;
(4)Polyester slice is made polyester slice aqueous in below 30ppm, will be sustained by 150 DEG C of drying temperature progress crystallizing and dryings
Capsule master batch is with polyester slice with 5:95 mass ratio is well mixed, 285 degrees Celsius of spinning 75d/24f circles fdy of spinning temperature
Product.
Effective efficiency composition 2.13% in finished product test product;Product is washed 30 times, effective efficiency component content in product
2.0%.Hung up under body temperature 1 year, effective efficiency composition 1.5% in product.
Embodiment 2
(1)It is 15 in mass ratio by lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon:15:20:15:20:15 are extracted
Take, obtain extract;
(2)It is 10 in mass ratio by extract and polyurethane:90 are fabricated to spansule at 180 DEG C, release slow capsule at 120 DEG C
Dried 6 hours in baking oven;
(3)Slow capsule will be released with polybutylene terephthalate section with mass percent 57:43 mixing, then through twin-screw extruder
Machine, extruder head are fabricated to essential oil under conditions of 240 DEG C and release slow capsule master batch;
(4)Polyester slice is made polyester slice aqueous in below 30ppm, will be sustained by 120 DEG C of drying temperature progress crystallizing and dryings
Capsule master batch is with polyester slice with 10:90 mass ratio is well mixed, 290 degrees Celsius of spinning 75d/72f circles fdy of spinning temperature
Product.
Effective efficiency composition 2.1% in finished product test product;Product is washed 30 times, effective efficiency component content in product
1.96 %.Hung up under body temperature 1 year, effective efficiency composition 1.45% in product.
Embodiment 3
(1)It is 15 in mass ratio by lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon:15:20:15:20:15 are extracted
Take, obtain extract;
(2)It is 7 in mass ratio by extract and polyurethane:93 are fabricated to spansule at 150 DEG C, release slow capsule at 100 DEG C
Dried 8 hours in baking oven;
(3)Slow capsule will be released with polybutylene terephthalate section with mass percent 50:50 mixing, then through twin-screw extruder
Machine, extruder head are fabricated to essential oil under conditions of 220 DEG C and release slow capsule master batch;
(4)Polyester slice is made polyester slice aqueous in below 30ppm, will be sustained by 180 DEG C of drying temperature progress crystallizing and dryings
Capsule master batch is with polyester slice with 7:93 mass ratio is well mixed, 295 degrees Celsius of spinning 75d/72f triangles of spinning temperature
Fdy products,
Effective efficiency composition 2.05% in finished product test product;Product is washed 30 times, effective efficiency component content 1.9% in product.
Hung up under body temperature 1 year, effective efficiency composition 1.4% in product.
Embodiment 4
(1)It is 15 in mass ratio by lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon:15:20:15:20:15 are extracted
Take, obtain extract;
(2)It is 8 in mass ratio by extract and polyurethane:92 are fabricated to spansule at 170 DEG C, release baking of the slow capsule at 90 DEG C
Dried 9 hours in case;
(3)Slow capsule will be released with polybutylene terephthalate section with mass percent 60:40 mixing, then through twin-screw extruder
Machine, extruder head are fabricated to essential oil under conditions of 250 DEG C and release slow capsule master batch;
(4)Polyester slice makes polyester slice aqueous in below 30ppm, general by 120-180 DEG C of progress crystallizing and drying of drying temperature
Spansule master batch is with polyester slice with 8:92 mass ratio is well mixed, 292 degrees Celsius of five jiaos of 75d/36f of spinning of spinning temperature
Star fdy products.
Effective efficiency composition 2.11% in finished product test product;Product is washed 30 times, effective efficiency component content in product
2.03%.Hung up under body temperature 1 year, effective efficiency composition 1.48% in product.
It will be appreciated by those skilled in the art that:The foregoing is only the present invention specific embodiment and
, it is not intended to limit the invention, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done
Deng should be included in the scope of the protection.
Claims (6)
1. a kind of preparation method of health care's polyester fiber, it is characterised in that described preparation method is following steps:
(1)Lavender, You Jiali, Buddha's hand, fish pelargonium, peppermint, lemon active ingredient are extracted;
(2)Extract and polyurethane are fabricated to spansule at 130-180 DEG C;
(3)Slow capsule will be released with polybutylene terephthalate section with mass percent 50:50-60:40 mixing, through double spiral shells
Bar extruder, extruder head are fabricated to essential oil under conditions of 220 DEG C -250 DEG C and release slow capsule master batch;
(4)Polyester slice makes polyester slice aqueous in below 30ppm by 120-180 DEG C of progress crystallizing and drying of drying temperature;So
Afterwards by spansule master batch and polyester slice using mass ratio as 5:95-10:90 well mixed co-blended spinnings, obtain a kind of health care and support
Raw polyester fiber.
A kind of 2. preparation method of health care's polyester fiber according to claim 1, it is characterised in that lavender, especially
Add profit, Buddha's hand, fish pelargonium, peppermint, the mass ratio of lemon is 15:15:20:15:20:15.
3. the preparation method of a kind of health care's polyester fiber according to claim 1, it is characterised in that extract is with gathering
The mass ratio of urethane is 5:95-10:90.
A kind of 4. preparation method of health care's polyester fiber according to claim 1, it is characterised in that step(4)In
Spinneret draw ratio is 2.5 ~ 3.5 in spinning technique, component sand loading amount(Up/down)For(40~80)/(100~300), component pressure
10 ~ 15MPa, 285 ~ 292 DEG C of spinning temperature, 0.30 ~ 0.50m/s of cross air blasting wind speed;Oil applying rate is 1.0% ~ 1.3%.
A kind of 5. preparation method of health care's polyester fiber according to claim 1, it is characterised in that POY spinning
Speed is 2500 ~ 3500m/min.
A kind of 6. preparation method of health care's polyester fiber according to claim 1, it is characterised in that FDY spinning
Speed is 4000 ~ 5500m/min, draw ratio 2.6~3.2,70~90 DEG C of a roll temperature, two 115 ~ 135 DEG C of roll temperatures.
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CN201710855770.8A CN107523897A (en) | 2017-09-20 | 2017-09-20 | A kind of preparation method of health care's polyester fiber |
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CN201710855770.8A CN107523897A (en) | 2017-09-20 | 2017-09-20 | A kind of preparation method of health care's polyester fiber |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109183184A (en) * | 2018-08-14 | 2019-01-11 | 北京麻世纪麻业科技发展有限公司 | A kind of preparation method and capsule fiber of capsule fiber |
CN110106577A (en) * | 2019-04-22 | 2019-08-09 | 中科纺织研究院(青岛)有限公司 | A kind of cassia seed composite fiber of terylene carrier and preparation method thereof |
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CN102031581A (en) * | 2009-09-25 | 2011-04-27 | 上海德福伦化纤有限公司 | Method for producing super-refreshing cool-feel health care polyester fiber |
CN104178844A (en) * | 2014-08-13 | 2014-12-03 | 江苏月源纤维科技有限公司 | Aromatic chinlon-spandex air wrapped yarn and production method thereof |
CN104248273A (en) * | 2014-09-09 | 2014-12-31 | 江苏蓝品纤维科技发展有限公司 | Production technique of multifunctional polyester fiber quilt mat |
CN107012530A (en) * | 2017-05-12 | 2017-08-04 | 福建鑫森合纤科技有限公司 | A kind of mosquito repellent nylon-6 fiber and preparation method thereof |
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2017
- 2017-09-20 CN CN201710855770.8A patent/CN107523897A/en active Pending
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102031581A (en) * | 2009-09-25 | 2011-04-27 | 上海德福伦化纤有限公司 | Method for producing super-refreshing cool-feel health care polyester fiber |
CN104178844A (en) * | 2014-08-13 | 2014-12-03 | 江苏月源纤维科技有限公司 | Aromatic chinlon-spandex air wrapped yarn and production method thereof |
CN104248273A (en) * | 2014-09-09 | 2014-12-31 | 江苏蓝品纤维科技发展有限公司 | Production technique of multifunctional polyester fiber quilt mat |
CN107012530A (en) * | 2017-05-12 | 2017-08-04 | 福建鑫森合纤科技有限公司 | A kind of mosquito repellent nylon-6 fiber and preparation method thereof |
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朱立春主编: "《家庭养花和阳台种菜一本全》", 31 July 2015, 中国华侨出版社 * |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109183184A (en) * | 2018-08-14 | 2019-01-11 | 北京麻世纪麻业科技发展有限公司 | A kind of preparation method and capsule fiber of capsule fiber |
CN110106577A (en) * | 2019-04-22 | 2019-08-09 | 中科纺织研究院(青岛)有限公司 | A kind of cassia seed composite fiber of terylene carrier and preparation method thereof |
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