CN109181860A - A kind of aroma type snake oil and preparation method thereof - Google Patents
A kind of aroma type snake oil and preparation method thereof Download PDFInfo
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- CN109181860A CN109181860A CN201811117900.9A CN201811117900A CN109181860A CN 109181860 A CN109181860 A CN 109181860A CN 201811117900 A CN201811117900 A CN 201811117900A CN 109181860 A CN109181860 A CN 109181860A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/12—Production of fats or fatty oils from raw materials by melting out
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
Abstract
The present invention provides a kind of aroma type snake oil and preparation method thereof, and in particular to animal fat produces and processes technical field.The present invention includes the raw material for including following weight part ratio: 50-60 parts of snake adipose tissue, 2-8 parts of beech juice, 2-6 parts of Randia canthioides leaf juice, fragrant 0.5-1.5 parts of knotweed juice, 0.1-0.2 parts of lecithin, 0.13-0.17 parts of carrotene and 0.07-0.13 parts of sodium alginate；It advanced optimizes are as follows: 54-56 parts of snake adipose tissue, 4-6 parts of beech juice, 3-5 parts of Randia canthioides leaf juice, fragrant 0.8-1.2 parts of knotweed juice, 0.17-0.19 parts of lecithin, 0.14-0.16 parts of carrotene and 0.09-0.11 parts of sodium alginate.Beech juice, Randia canthioides leaf juice, fragrant three Plant Extracts of knotweed juice are added in the present invention in snake oil, deodorization flavouring can be played, the effect to extend the shelf life, aroma type snake oil smell faint scent, the pale yellow, clear made, unsaturated fatty acid content is high, and long shelf-life was up to 36-48 months.
Description
[technical field]
The present invention relates to animal fats to produce and process technical field, and in particular to a kind of aroma type snake oil and its preparation side
Method.
[background technique]
Snake oil is that the fat of snake section animal snake is extracted through refining.Applying for snake oil has long history in China, enters
Medicine is first appeared in " 52 Bingfang ".Li Shizhen (1518-1593 A.D.) describes the effect of snake oil in Compendium of Material Medica: " it is deaf that silk floss wraps up in ear plug to snake rouge, also
Fu's pyogenic infections " illustrates that snake oil penetration is strong, and play the role of detumescence poison again " rub object, all thoroughly ".Civil common snake oil is controlled
Pernio, chap, eczema and scald are treated, in cosmetic industry, snake oil is also a kind of advanced skin care product, has anti-wrinkle, except scar, guarantor
It is wet, adjust endocrine effect, be usually used in that tender skin is crease-resistant, eliminates abdominal pregnancy line.
Snake oil in its fat from snake because refining, and the grease taste of the bad smell with snake body and fat, is caused often
Usage experience is bad, and its active constituent unsaturated fatty acid will affect its shelf-life, therefore is restricted in application.Mesh
Before, refinement and refining methd about snake oil have following pertinent literature to report: Chinese patent grant number is CN103468390B, name
Disclosed in a kind of patent document for method for refining snake oil it is a kind of crude product is refined into obtain in the heating of snake adipose tissue, then with having
The method that solvent carries out extracting and refining, although having fishy smell, and have after extraction although obtained snake oil is more clarified
The loss of trace active ingredient, the effect of influencing snake oil；Chinese patent grant number is CN100450468C, and a kind of entitled snake oil is received
A kind of various chemical antioxidants of addition, solubilizer, thickening are disclosed in Mizhi liposome preparation and its patent document of preparation process
Snake oil dilution is made nanosized emulsion, makes snake oil transparent color and luster, without flocculation by the method for the additives such as agent, isotonic agent, diluent
And precipitating, but additive amount is excessive, and snake oil content after the dilution of a large amount of solvents is lower, it is difficult to play unique function of snake oil comprehensively
Effect；China Patent Publication No. is CN108096074A, the patent document of entitled a kind of snake oil composition and preparation method thereof, purposes
In disclose snake oil extracted from snake adipose tissue using room temperature and low temperature process, later using addition adsorbent and using overcritical
CO2The method method being decolourized and deodorized, the good snake oil composition without fishy smell of stability, but its process equipment can be obtained
Cost is high, and production cost is quite high.
Therefore, it is necessary to develop a kind of novel snake oil, solves the problems, such as that the snake oil shelf-life is short, smells as of rotten fish that highly seasoned, clarity is not high,
To promote the utilization space of snake oil, increase the market competitiveness of snake oil.
[summary of the invention]
Goal of the invention of the invention is: for the snake oil shelf-life is short, the not high problem of highly seasoned, clarity of smelling as of rotten fish, providing
A kind of aroma type snake oil.Beech juice, Randia canthioides leaf juice, fragrant three Plant Extracts of knotweed juice are added in the present invention in snake oil, can play
Deodorization flavouring, the effect to extend the shelf life make snake oil smell faint scent, pale yellow, clear, unsaturated fatty acid content
Height, long shelf-life was up to 36-48 months.
To achieve the goals above, The technical solution adopted by the invention is as follows:
A kind of aroma type snake oil, the raw material including following weight part ratio: 50-60 parts of snake adipose tissue, 2-8 parts of beech juice,
2-6 parts of Randia canthioides leaf juice, fragrant 0.5-1.5 parts of knotweed juice, 0.1-0.2 parts of lecithin, 0.13-0.17 parts of carrotene and sodium alginate
0.07-0.13 parts.
Optimization, the raw material including following weight part ratio: 54-56 parts of snake adipose tissue, 4-6 parts of beech juice, Randia canthioides leaf juice
3-5 parts, fragrant 0.8-1.2 parts of knotweed juice, 0.17-0.19 parts of lecithin, 0.14-0.16 parts of carrotene and sodium alginate 0.09-0.11
Part.
It advanced optimizes, the snake is selected from Elaphe Carinatas；Aroma type snake oil shelf-life at 4-8 DEG C is 36-48
Month.
Further optimize, the beech juice the preparation method comprises the following steps: by weight, taking 1-3 parts of beech bark and beech
Wooden leaf 0.6-1 parts, 50-60 mesh is smashed it through, then the powder after collecting sieving takes powder to add 5-9 parts of water, stirs evenly,
After standing 25-35 minutes, it is placed in squeezer and squeezes the juice, obtain beech crude extract, beech crude extract is then taken to subtract at 70-80 DEG C
Pressure is dried to the medicinal extract that relative density is 1.24-1.28, and acetone 8-14 parts, 30-40 points of ultrasonic treatment is then added in medicinal extract
Clock, filtering, obtains filter residue, and then filter residue volatilizes acetone at 40-50 DEG C, and mixed solvent is then added in two portions in filter residue,
The amount that mixed solvent is added every time is respectively 10-20 parts and 8-12 parts, and 45-65 points of ultrasonic treatment are added after mixed solvent for the first time
Clock is ultrasonically treated 20-30 minutes after mixed solvent is added for the second time, then through 0.2-0.3 μm of membrane filtration, collects and merge two
The filtrate of secondary filtering, then filtrate adds 1-2 parts of water, and then recycling design obtains beech juice；The mixed solvent includes following heavy
Measure the solution of part ratio: 5-9 parts and ethyl acetate 1-3 parts of ethanol water that concentration of volume percent is 70%-80%.
Further optimize again, the beech juice the preparation method comprises the following steps: the bark of beech trunk is cut open with knife, by weight
Part ratio is measured, then mixed solvent is added in two portions in 5-9 parts of juice for collecting outflow, the amount that mixed solvent is added every time is respectively
It 10-20 parts and 8-12 parts, is ultrasonically treated 32-42 minutes after mixed solvent is added for the first time, surpasses after second of addition mixed solvent
It sonication 15-25 minutes, then through 0.2-0.3 μm of membrane filtration, collects and merges the filtrate filtered twice, then filtrate is recycled
Solvent obtains beech juice；The mixed solvent includes the solution of following weight part ratio: concentration of volume percent is 70%-80%
5-9 parts and ethyl acetate 1-3 parts of ethanol water.
Further optimize again, the Randia canthioides leaf juice the preparation method comprises the following steps: by weight, taking 2-4 parts of Randia canthioides leaf, setting
It squeezes the juice in squeezer, obtains Randia canthioides leaf crude extract, acetone 12-22 parts is then added in Randia canthioides leaf crude extract, ultrasonic treatment
50-60 minutes, filtering obtained filter residue, filter residue acetone rinse 2-3 times, and the dosage of each acetone is 1-2 parts, and then filter residue exists
Acetone is volatilized at 40-50 DEG C, mixed solvent is then added in two portions in filter residue, and the amount that mixed solvent is added every time is respectively
It 14-28 parts and 10-20 parts, is ultrasonically treated 60-70 minutes after mixed solvent is added for the first time, surpasses after second of addition mixed solvent
It sonication 30-40 minutes, then through 0.2-0.3 μm of membrane filtration, collects and merges the filtrate filtered twice, then recycling design
Obtain Randia canthioides juice；The mixed solvent includes the solution of following weight part ratio: concentration of volume percent is the ethyl alcohol of 70%-80%
5-9 parts and ethyl acetate 1-3 parts of aqueous solution.
Further optimize again, the perfume knotweed juice the preparation method comprises the following steps: by weight, taking whole strain 2-4 parts of fragrant knotweed, setting
It squeezes the juice in squeezer, obtains fragrant knotweed crude extract, it is 75%-85% that concentration of volume percent is then added in fragrant knotweed crude extract
16-30 parts of ethanol water, be ultrasonically treated 45-55 minute, then filter, collect filtrate I, then in filter residue addition volume hundred
Dividing specific concentration is 12-20 parts of ethanol water of 80%-90%, is ultrasonically treated 25-35 minutes, then filters, and collects filtrate II,
Then merging filtrate I and filtrate II, then recycling design is up to no alcohol taste is to get fragrant knotweed juice.
The preparation method of above-mentioned aroma type snake oil, comprising the following steps:
A. fat decoct oil: by weight, take snake adipose tissue, be put into iron pan, be then cooked by slow fire 16-18 minute up to
Produce oil oil colours be it is light yellow when, stop heating, obtain crude oil；
B. it filters: taking crude oil, keep oil temperature to filter 2-4 times at 30-38 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in
It squeezes the juice in squeezer, collect juice and is filtered 2-4 times at 30-38 DEG C, obtain refined filtration oil II, then merge refined filtration oil I, refined filtration
Oil II, obtains snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 6-10 minutes, obtain
Mixed juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, mixed juice is then taken to divide 2-3 addition snake oil
In mixed liquor, each additional amount is the 30%-50% of mixed juice total weight, shakes 3-7 minutes after being added every time, obtains thick cream,
Thick cream is placed in high pressure homogenizer again and carries out homogeneous, setting high pressure homogenizer pressure be 50-60MPa, homogenization cycles 4-5
Secondary, homogenizing temperature is 35-45 DEG C, collects homogenizing fluid, carrotene is then added, and is uniformly mixed to get aroma type snake oil finished product.
In conclusion by adopting the above-described technical solution, the beneficial effects of the present invention are:
1. the extracting solution of three kinds of plants is added in the present invention in snake oil, and obtains best original by creative work many times
Material proportion, had not only dispelled the grease taste of snake oil but also had made it have fragrant, and the addition of extracting solution cooperation carrotene also makes snake oil sour
Value is less than 0.3, and the shelf-life can extend 1-2, while the snake oil pale yellow of preparation, clear, iodine number are up to 82.9, make it
Unsaturated fatty acid with high-content.
2. the present invention extracts the fragrance ingredient or antioxidant content of three kinds of plants using specific extraction process, snake can be dispelled
The grease taste of oil, and make snake oil giving out fragrance, antioxidant content in the middle can effectively reduce acid value, extend the storage life of snake oil
Limit.Wherein, the juice of the bark of beech, leaf and trunk has distributed fresh and sweet fragrance, can be fragrant by the Extraction and enrichment of mixed solvent
Taste ingredient；Randia canthioides leaf is the leaf of nanmu, and smell faint scent is pleasant, and nanmu has the characteristic being stale-proof in thousand, shows wherein antioxygen
It is high to change component content, by the extraction of mixed solvent, these two types of ingredients effectively can be extracted into simultaneously successful fusion to greatest extent
Together；Fragrant knotweed becomes the production raw material of screw powder because of its distinctive fragrance component, by the volume hundred for limiting ethanol water
Divide specific concentration, flavor component therein is efficiently extracted into concentration and is come out.The mixed solvent that the present invention uses is by designated volume hundred
The ethanol water and ethyl acetate for dividing specific concentration are formulated, by volumes of aqueous ethanol percent concentration and two kinds of solvents
The many experiments of proportion are groped, and have obtained optimum ethanol water concentration and two kinds of optimal ratio ranges of solvent, have made to mention
The beech juice and Randia canthioides leaf juice taken reaches optimal deodorization Titian and antioxidant effect.
3. beech juice, Randia canthioides leaf juice, fragrant knotweed juice and snake oil are mutual exclusive two classes solution in the present invention, by sodium alginate
Ultrasonic mixing is carried out with beech juice, Randia canthioides leaf juice, fragrant knotweed juice, mixed juice is made, snake oil, lecithin are stirred, snake is made
Oily mixed liquor can be made into the Heterodisperse system with high clarity, makes snake oil not occur flocculating and precipitating for a long time, increases it
Stability.Wherein, it goes back after sodium alginate is added in the juice of above-mentioned three kinds of plants, the viscosity of juice can be increased, be conducive to
Improve the subsequent degree of scatter in snake oil mixed liquor；Lecithin can reduce the surface tension of snake oil, and snake oil is made to be easy to wrap up
Water；Sodium alginate and lecithin are added in two above-mentioned class solution correspondingly, and additional amount are carried out tight
Lattice control, prevents from being added very few, dispersion is difficult to be formed, and snake oil is made milkiness occur；It is excessive to be also prevented from addition, causes snake oil viscous
It spends greatly, two class solution therein cohesiveness are excessive, reduce degree of scatter of the mixed juice in snake oil mixed liquor instead.
4. the present invention refines snake oil using Elaphe Carinatas adipose tissue, it is different from the snake oil of other class, only distributes slight oil
Rouge taste and without bad smell, avoid except the loss caused by snake oil effective component of fishy smell step, also improve people using snake oil
Adaptability.
[specific embodiment]
Below with reference to embodiment, the invention will be further described.
Embodiment 1
A kind of aroma type snake oil, the raw material including following weight part ratio: 50 parts of snake adipose tissue, 2 parts of beech juice, Randia canthioides leaf
2 parts of juice, fragrant 0.5 part of knotweed juice, 0.1 part of lecithin, 0.13 part of carrotene and 0.07 part of sodium alginate.
Above-mentioned aroma type snake oil the preparation method comprises the following steps:
A. fat decocts oil: by weight, taking snake adipose tissue, is put into iron pan, is then cooked by slow fire 16 minutes until refining
When fuel-displaced oil colours is light yellow, stops heating, obtain crude oil；
Wherein, snake is selected from Elaphe Carinatas.
B. it filters: taking crude oil, keep oil temperature to filter 2 times at 30 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in squeezing
It squeezes the juice in machine, collect juice and is filtered 2 times at 30 DEG C, obtain refined filtration oil II, then merge refined filtration oil I, refined filtration oil II, obtain
Snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 6 minutes, mixed
Juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, then takes 2 addition snake oil mixed liquors of mixed juice point
In, each additional amount is the 50% of mixed juice total weight, shakes 3 minutes after being added every time, obtains thick cream, then thick cream is placed in height
Homogeneous is carried out in pressure homogenizer, setting high pressure homogenizer pressure is 50MPa, homogenization cycles are 4 times, homogenizing temperature is 35 DEG C, is received
Collect homogenizing fluid, carrotene is then added, is uniformly mixed to get aroma type snake oil finished product；Aroma type snake oil is placed at 4 DEG C and is protected
It deposits.
Wherein, beech juice the preparation method comprises the following steps: by weight, take 1 part and 0.6 part of beech leaf of beech bark, after crushing
50 meshes are crossed, then the powder after collecting sieving takes powder to add 5 parts of water, stirs evenly, after standing 25 minutes, be placed in squeezer
Middle juicing, obtains beech crude extract, and beech crude extract is then taken to be dried under reduced pressure into the medicinal extract that relative density is 1.24 at 70 DEG C,
Then 8 parts of acetone are added in medicinal extract, is ultrasonically treated 30 minutes, filtering obtains filter residue, then filter residue volatilizes third at 40 DEG C
Then mixed solvent is added in two portions in ketone in filter residue, the amount that mixed solvent is added every time is respectively 10 parts and 8 parts, first time
It is ultrasonically treated 45 minutes after mixed solvent is added, is ultrasonically treated 20 minutes after second of addition mixed solvent, is then filtered through 0.2 μm
Film filtering, collects and merges the filtrate filtered twice, then filtrate adds 1 part of water, and then recycling design obtains beech juice；It mixes molten
Agent includes the solution of following weight part ratio: 5 parts and 1 part of ethyl acetate of the ethanol water that concentration of volume percent is 70%.
Randia canthioides leaf juice the preparation method comprises the following steps: by weight, taking 2 parts of Randia canthioides leaf, being placed in squeezer and squeeze the juice, obtain Randia canthioides
Then leaf crude extract is added 12 parts of acetone in Randia canthioides leaf crude extract, be ultrasonically treated 50 minutes, filtering, obtains filter residue, and filter residue is used
Acetone rinse 2 times, the dosage of each acetone is 1 part, and then filter residue volatilizes acetone at 40 DEG C, is then added in two times in filter residue
Enter mixed solvent, the amount that mixed solvent is added every time is respectively 14 parts and 10 parts, is ultrasonically treated after mixed solvent is added for the first time
It 60 minutes, is ultrasonically treated 30 minutes after mixed solvent is added for the second time, then through 0.2 μm of membrane filtration, collects and merge twice
The filtrate of filtering, then recycling design obtains Randia canthioides juice；Mixed solvent includes the solution of following weight part ratio: percent by volume is dense
5 parts and 1 part of ethyl acetate of the ethanol water that degree is 70%.
Fragrant knotweed juice the preparation method comprises the following steps: by weight, taking 2 parts of the whole strain of fragrant knotweed, being placed in squeezer and squeeze the juice, obtain fragrant knotweed
Then 16 parts of ethanol water that concentration of volume percent is 75%, ultrasonic treatment 45 is added in crude extract in fragrant knotweed crude extract
Minute, it then filters, collects filtrate I, then it is 12 parts of ethanol water of 75% that concentration of volume percent, which is added, in filter residue, is surpassed
It sonication 25 minutes, then filters, collects filtrate II, then merging filtrate I and filtrate II, then recycling design is up to no alcohol
Taste is to get fragrant knotweed juice.
Embodiment 2
A kind of aroma type snake oil, the raw material including following weight part ratio: 60 parts of snake adipose tissue, 8 parts of beech juice, Randia canthioides leaf
6 parts of juice, fragrant 1.5 parts of knotweed juice, 0.2 part of lecithin, 0.17 part of carrotene and 0.13 part of sodium alginate.
Above-mentioned aroma type snake oil the preparation method comprises the following steps:
A. fat decocts oil: by weight, taking snake adipose tissue, is put into iron pan, is then cooked by slow fire 18 minutes until refining
When fuel-displaced oil colours is light yellow, stops heating, obtain crude oil；
Wherein, snake is selected from Elaphe Carinatas.
B. it filters: taking crude oil, keep oil temperature to filter 4 times at 38 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in squeezing
It squeezes the juice in machine, collect juice and is filtered 4 times at 38 DEG C, obtain refined filtration oil II, then merge refined filtration oil I, refined filtration oil II, obtain
Snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 10 minutes, mixed
Close juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, mixed juice is then taken to be added three times snake oil mixing
In liquid, each additional amount is the 30%-40% of mixed juice total weight, shakes 7 minutes after being added every time, obtains thick cream, then will be thick
Cream, which is placed in high pressure homogenizer, carries out homogeneous, and setting high pressure homogenizer pressure is 60MPa, homogenization cycles are 5 times, homogenizing temperature is
45 DEG C, homogenizing fluid is collected, carrotene is then added, is uniformly mixed to get aroma type snake oil finished product；Aroma type snake oil is placed in 8
It is saved at DEG C.
Wherein, beech juice the preparation method comprises the following steps: by weight, take 3 parts and 1 part of beech leaf of beech bark, smash it through
60 meshes, the powder after collecting sieving, then take powder to add 9 parts of water, stir evenly, and after standing 35 minutes, are placed in squeezer
Juicing, obtains beech crude extract, then takes beech crude extract to be dried under reduced pressure into the medicinal extract that relative density is 1.28 at 80 DEG C, so
14 parts of acetone are added in medicinal extract afterwards, is ultrasonically treated 40 minutes, filtering obtains filter residue, and then filter residue volatilizes acetone at 50 DEG C,
Then mixed solvent is added in two portions in filter residue, the amount that mixed solvent is added every time is respectively 20 parts and 12 parts, is added for the first time
It is ultrasonically treated 65 minutes, is ultrasonically treated 30 minutes after second of addition mixed solvent, then through 0.3 μm of filter membrane after entering mixed solvent
Filtering, collects and merges the filtrate filtered twice, then filtrate adds 2 parts of water, and then recycling design obtains beech juice；Mixed solvent
Solution including following weight part ratio: 9 parts and 3 parts of ethyl acetate of the ethanol water that concentration of volume percent is 80%.
Randia canthioides leaf juice the preparation method comprises the following steps: by weight, taking 4 parts of Randia canthioides leaf, being placed in squeezer and squeeze the juice, obtain Randia canthioides
Then leaf crude extract is added 22 parts of acetone in Randia canthioides leaf crude extract, be ultrasonically treated 60 minutes, filtering, obtains filter residue, and filter residue is used
Acetone rinse 3 times, the dosage of each acetone is 2 parts, and then filter residue volatilizes acetone at 50 DEG C, is then added in two times in filter residue
Enter mixed solvent, the amount that mixed solvent is added every time is respectively 28 parts and 20 parts, is ultrasonically treated after mixed solvent is added for the first time
It 60-70 minutes, is ultrasonically treated 40 minutes after mixed solvent is added for the second time, then through 0.3 μm of membrane filtration, collects and merge two
The filtrate of secondary filtering, then recycling design obtains Randia canthioides juice；Mixed solvent includes the solution of following weight part ratio: percent by volume
9 parts and 3 parts of ethyl acetate of ethanol water that concentration is 70%-80%.
Fragrant knotweed juice the preparation method comprises the following steps: by weight, taking 4 parts of the whole strain of fragrant knotweed, being placed in squeezer and squeeze the juice, obtain fragrant knotweed
Then 30 parts of ethanol water that concentration of volume percent is 85%, ultrasonic treatment 55 is added in crude extract in fragrant knotweed crude extract
Minute, it then filters, collects filtrate I, then it is 20 parts of ethanol water of 85% that concentration of volume percent, which is added, in filter residue, is surpassed
It sonication 35 minutes, then filters, collects filtrate II, then merging filtrate I and filtrate II, then recycling design is up to no alcohol
Taste is to get fragrant knotweed juice.
Embodiment 3
A kind of aroma type snake oil, the raw material including following weight part ratio: 54 parts of snake adipose tissue, 4 parts of beech juice, Randia canthioides leaf
3 parts of juice, fragrant 0.8 part of knotweed juice, 0.17 part of lecithin, 0.14 part of carrotene and 0.09 part of sodium alginate.
Above-mentioned aroma type snake oil the preparation method comprises the following steps:
A. fat decoct oil: by weight, take snake adipose tissue, be put into iron pan, be then cooked by slow fire 16.5 minutes until
Produce oil oil colours be it is light yellow when, stop heating, obtain crude oil；
Wherein, snake is selected from Elaphe Carinatas.
B. it filters: taking crude oil, keep oil temperature filter 23 at 32 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in squeezer
Middle juicing is collected juice and is filtered 2 times at 328 DEG C, obtain refined filtration oil II, then merges refined filtration oil I, refined filtration oil II, obtain
Snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 7 minutes, mixed
Juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, mixed juice is then taken to be added three times snake oil mixed liquor
In, preceding additional amount twice is the 40% of mixed juice total weight, shakes 4 minutes after being added every time, obtains thick cream, then thick cream is placed in
Homogeneous is carried out in high pressure homogenizer, setting high pressure homogenizer pressure is 53MPa, homogenization cycles are 4 times, homogenizing temperature is 37 DEG C,
Homogenizing fluid is collected, carrotene is then added, is uniformly mixed to get aroma type snake oil finished product；Aroma type snake oil is placed at 5 DEG C
It saves.
Wherein, beech juice the preparation method comprises the following steps: the bark of beech trunk is cut open with knife, by weight, collect outflow
5 parts of juice, mixed solvent is then added in two portions, the amount that mixed solvent is added every time is respectively 10 parts and 8 parts, is added for the first time
It is ultrasonically treated 32 minutes, is ultrasonically treated 15 minutes after second of addition mixed solvent, then through 0.2 μm of filter membrane after entering mixed solvent
Filtering, collects and merges the filtrate filtered twice, then filtrate recycling design obtains beech juice；Mixed solvent includes following weight
The solution of part ratio: 5 parts and 1 part of ethyl acetate of the ethanol water that concentration of volume percent is 70%.
Randia canthioides leaf juice the preparation method comprises the following steps: by weight, taking 2.5 parts of Randia canthioides leaf, being placed in squeezer and squeeze the juice, obtain perfume (or spice)
Then nanmu leaf crude extract is added 15 parts of acetone in Randia canthioides leaf crude extract, be ultrasonically treated 52 minutes, and filtering obtains filter residue, filter residue
With acetone rinse 2 times, the dosage of each acetone is 1.2 parts, and then filter residue volatilizes acetone at 43 DEG C, and two are then divided in filter residue
Secondary addition mixed solvent, the amount that mixed solvent is added every time is respectively 18 parts and 12 parts, and ultrasound after mixed solvent is added for the first time
Processing 63 minutes is ultrasonically treated 32 minutes after mixed solvent is added for the second time, then through 0.22 μm of membrane filtration, collects and merge
The filtrate filtered twice, then recycling design obtains Randia canthioides juice；Mixed solvent includes the solution of following weight part ratio: volume basis
6 parts and 1.5 parts of ethyl acetate of the ethanol water that specific concentration is 73%.
Fragrant knotweed juice the preparation method comprises the following steps: by weight, taking 3 parts of the whole strain of fragrant knotweed, being placed in squeezer and squeeze the juice, obtain fragrant knotweed
Then 20 parts of ethanol water that concentration of volume percent is 78%, ultrasonic treatment 47 is added in crude extract in fragrant knotweed crude extract
Minute, it then filters, collects filtrate I, then it is 14 parts of ethanol water of 78% that concentration of volume percent, which is added, in filter residue, is surpassed
It sonication 28 minutes, then filters, collects filtrate II, then merging filtrate I and filtrate II, then recycling design is up to no alcohol
Taste is to get fragrant knotweed juice.
Embodiment 4
A kind of aroma type snake oil, the raw material including following weight part ratio: 56 parts of snake adipose tissue, 6 parts of beech juice, Randia canthioides leaf
5 parts of juice, fragrant 1.2 parts of knotweed juice, 0.19 part of lecithin, 0.16 part of carrotene and 0.11 part of sodium alginate.
Above-mentioned aroma type snake oil the preparation method comprises the following steps:
A. fat decoct oil: by weight, take snake adipose tissue, be put into iron pan, be then cooked by slow fire 17.5 minutes until
Produce oil oil colours be it is light yellow when, stop heating, obtain crude oil；
Wherein, snake is selected from Elaphe Carinatas.
B. it filters: taking crude oil, keep oil temperature filter 23 at 36 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in squeezing
It squeezes the juice in machine, collects juice and the filter 23 at 6 DEG C, obtain refined filtration oil II, then merge refined filtration oil I, refined filtration oil II, obtain
Snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 9 minutes, mixed
Juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, mixed juice is then taken to be added three times snake oil mixed liquor
In, preceding additional amount twice is the 45% of mixed juice total weight, shakes 6 minutes after being added every time, obtains thick cream, then thick cream is placed in
Homogeneous is carried out in high pressure homogenizer, setting high pressure homogenizer pressure is 58MPa, homogenization cycles are 5 times, homogenizing temperature is 43 DEG C,
Homogenizing fluid is collected, carrotene is then added, is uniformly mixed to get aroma type snake oil finished product；Aroma type snake oil is placed at 7 DEG C
It saves.
Wherein, beech juice the preparation method comprises the following steps: the bark of beech trunk is cut open with knife, by weight, collect outflow
9 parts of juice, mixed solvent is then added in two portions, the amount that mixed solvent is added every time is respectively 20 parts and 12 parts, first time
It is ultrasonically treated 42 minutes after mixed solvent is added, is ultrasonically treated 25 minutes after second of addition mixed solvent, is then filtered through 0.3 μm
Film filtering, collects and merges the filtrate filtered twice, then filtrate recycling design obtains beech juice；Mixed solvent includes following heavy
Measure the solution of part ratio: 9 parts and 3 parts of ethyl acetate of the ethanol water that concentration of volume percent is 80%.
Randia canthioides leaf juice the preparation method comprises the following steps: by weight, taking 3.5 parts of Randia canthioides leaf, being placed in squeezer and squeeze the juice, obtain perfume (or spice)
Then nanmu leaf crude extract is added 20 parts of acetone in Randia canthioides leaf crude extract, be ultrasonically treated 58 minutes, and filtering obtains filter residue, filter residue
With acetone rinse 3 times, the dosage of each acetone is 1.8 parts, and then filter residue volatilizes acetone at 48 DEG C, and two are then divided in filter residue
Secondary addition mixed solvent, the amount that mixed solvent is added every time is respectively 24 parts and 17 parts, and ultrasound after mixed solvent is added for the first time
Processing 67 minutes is ultrasonically treated 38 minutes after mixed solvent is added for the second time, then through 0.27 μm of membrane filtration, collects and merge
The filtrate filtered twice, then recycling design obtains Randia canthioides juice；Mixed solvent includes the solution of following weight part ratio: volume basis
8 parts and 2.5 parts of ethyl acetate of the ethanol water that specific concentration is 77%.
Fragrant knotweed juice the preparation method comprises the following steps: by weight, taking 3.5 parts of the whole strain of fragrant knotweed, being placed in squeezer and squeeze the juice, obtain perfume (or spice)
Then 26 parts of ethanol water that concentration of volume percent is 82%, ultrasonic treatment is added in knotweed crude extract in fragrant knotweed crude extract
It 53 minutes, then filters, collects filtrate I, then addition concentration of volume percent is 18 parts of ethanol water of 83% in filter residue,
Ultrasonic treatment 33 minutes, is then filtered, and collects filtrate II, then merging filtrate I and filtrate II, then recycling design is up to no alcohol
Taste is to get fragrant knotweed juice.
Embodiment 5
A kind of aroma type snake oil, the raw material including following weight part ratio: 55 parts of snake adipose tissue, 5 parts of beech juice, Randia canthioides leaf
4 parts of juice, fragrant 1 part of knotweed juice, 0.15 part of lecithin, 0.15 part of carrotene and 0.1 part of sodium alginate.
Above-mentioned aroma type snake oil the preparation method comprises the following steps:
A. fat decocts oil: by weight, taking snake adipose tissue, is put into iron pan, is then cooked by slow fire 17 minutes until refining
When fuel-displaced oil colours is light yellow, stops heating, obtain crude oil；
Wherein, snake is selected from Elaphe Carinatas.
B. it filters: taking crude oil, keep oil temperature filter 23 at 34 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in squeezing
It squeezes the juice in machine, collects juice and the filter 23 at 34 DEG C, obtain refined filtration oil II, then merge refined filtration oil I, refined filtration oil II, obtain
Snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 8 minutes, mixed
Juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, mixed juice is then taken to be added three times snake oil mixed liquor
In, preceding additional amount twice is the 30% of mixed juice total weight, shakes 5 minutes after being added every time, obtains thick cream, then thick cream is placed in
Homogeneous is carried out in high pressure homogenizer, setting high pressure homogenizer pressure is 55MPa, homogenization cycles are 5 times, homogenizing temperature is 40 DEG C,
Homogenizing fluid is collected, carrotene is then added, is uniformly mixed to get aroma type snake oil finished product；Aroma type snake oil is placed at 6 DEG C
It saves.
Wherein, beech juice the preparation method comprises the following steps: by weight, take 2 parts and 0.8 part of beech leaf of beech bark, after crushing
55 meshes are crossed, then the powder after collecting sieving takes powder to add 7 parts of water, stirs evenly, after standing 30 minutes, be placed in squeezer
Middle juicing, obtains beech crude extract, and beech crude extract is then taken to be dried under reduced pressure into the medicinal extract that relative density is 1.26 at 75 DEG C,
Then 11 parts of acetone are added in medicinal extract, is ultrasonically treated 35 minutes, filtering obtains filter residue, then filter residue volatilizes third at 45 DEG C
Then mixed solvent is added in two portions in ketone in filter residue, the amount that mixed solvent is added every time is respectively 15 parts and 10 parts, first time
It is ultrasonically treated 55 minutes, is ultrasonically treated 25 minutes after second of addition mixed solvent, then through 0.25 μm after mixed solvent is added
Membrane filtration is collected and merges the filtrate filtered twice, and then filtrate adds 1.5 parts of water, and then recycling design obtains beech juice；It is mixed
Bonding solvent includes the solution of following weight part ratio: 7 parts of the ethanol water and ethyl acetate 2 that concentration of volume percent is 75%
Part.
Randia canthioides leaf juice the preparation method comprises the following steps: by weight, taking 3 parts of Randia canthioides leaf, being placed in squeezer and squeeze the juice, obtain Randia canthioides
Then leaf crude extract is added 17 parts of acetone in Randia canthioides leaf crude extract, be ultrasonically treated 55 minutes, filtering, obtains filter residue, and filter residue is used
Acetone rinse 3 times, the dosage of each acetone is 1.5 parts, and then filter residue volatilizes acetone at 45 DEG C, then in filter residue in two times
Mixed solvent is added, the amount that mixed solvent is added every time is respectively 21 parts and 15 parts, for the first time after addition mixed solvent at ultrasound
Reason 65 minutes is ultrasonically treated 35 minutes after mixed solvent is added for the second time, then through 0.25 μm of membrane filtration, collects and merge two
The filtrate of secondary filtering, then recycling design obtains Randia canthioides juice；Mixed solvent includes the solution of following weight part ratio: percent by volume
7 parts and 2 parts of ethyl acetate of the ethanol water that concentration is 75%.
Fragrant knotweed juice the preparation method comprises the following steps: by weight, taking 3 parts of the whole strain of fragrant knotweed, being placed in squeezer and squeeze the juice, obtain fragrant knotweed
Then 23 parts of ethanol water that concentration of volume percent is 80%, ultrasonic treatment 50 is added in crude extract in fragrant knotweed crude extract
Minute, it then filters, collects filtrate I, then it is 16 parts of ethanol water of 80% that concentration of volume percent, which is added, in filter residue, is surpassed
It sonication 30 minutes, then filters, collects filtrate II, then merging filtrate I and filtrate II, then recycling design is up to no alcohol
Taste is to get fragrant knotweed juice.
Embodiment 6
Except 9 parts of beech juice, 1 part of Randia canthioides leaf juice, fragrant knotweed juice 0.4 by weight, is taken especially, remaining method is the same as embodiment 5.
Embodiment 7
Except used in step b concentration of volume percent by 9 parts of ethanol water of 70%-80% replace mixed solvent prepare
Outside beech juice, remaining method is the same as embodiment 5.
Embodiment 8
In addition to using 9 parts of ethyl acetate to replace mixed solvent preparation Randia canthioides leaf juice in step b, remaining method is the same as embodiment 5.
Embodiment 9
Except lecithin and beech juice, Randia canthioides leaf juice, fragrant knotweed juice are mixed in step c, by sodium alginate and snake oil into
Row mixing is outer, remaining method is the same as embodiment 5.
Embodiment 10
By Chinese patent grant number be CN103468390B, it is entitled it is a kind of refine snake oil method patent of invention in implement
It is prepared by the method for example 3.
The comparison of 11 implementation result of embodiment
1. prepared by laboratory sample: taking with a collection of raw material, laboratory sample 1- is prepared according to embodiment 1-10 preparation method
10。
2. evaluation method: being investigated respectively to the appearance of laboratory sample 1-10, smell, and measure its iodine number, acid value, commented
Valence the results are shown in Table 1.Meanwhile laboratory sample 1,3,5,6,8,10 being placed in temperature is 25 ± 2 DEG C, relative humidity is 60% ± 5%
Climatic chamber in carry out 6 months by a definite date accelerated tests, investigate appearance, the smell of laboratory sample, and measure its acid value, with
This confirms the anticipated impact to the shelf-life, and evaluation result is shown in Table 2.
3. evaluation result
1 overall assessment result of table
2 accelerated test result of table
4. experimental result
As can be seen from Table 1, the result of the appearance of laboratory sample 1-5, smell, iodine number, acid value is superior to laboratory sample 6-10；By
Table 2 finds out that for laboratory sample 1,3,5 after the Acceleration study by 6 months, indices do not have significant change, and test sample
There is different degrees of significant change in 6,8,10 appearance of product, smell, acid value, when acid value is greater than 2.5, it may appear that different smell.
In conclusion showing aroma type snake oil excellent quality of the invention, long shelf-life.
Laboratory sample 6 uses different beech juice, Randia canthioides leaf juice and fragrant knotweed juice additional amount from laboratory sample 1-5, so that snake
The smell of oily finished product is affected, while but also sample solution goes bad.
The use of laboratory sample 7 and laboratory sample 1-5 difference ethanol water concentration, so that the smell of snake oil is affected,
Fragrance is insufficient and has grease taste.
Laboratory sample 8 prepares Randia canthioides leaf juice only with ethyl acetate, is not only snake oil fragrance deficiency or snake oil is easy to become
Matter, shortened shelf life.
Laboratory sample 9 is layered snake oil finished product, is shown various using the mixed method for being different from laboratory sample 1-5
Ingredient fails sufficiently to merge, and influences finished appearance and acid value.
Laboratory sample 10 prepares snake oil using known, and obvious layering and precipitating occurs in finished product, and grease taste is heavier,
Go bad under the conditions of accelerated test fast, shows that the shelf-life is short.
Above description is the detailed description for the present invention preferably possible embodiments, but embodiment is not limited to this hair
Bright patent claim, it is all the present invention suggested by technical spirit under completed same changes or modifications change, should all belong to
In the covered the scope of the patents of the present invention.
Claims (8)
1. a kind of aroma type snake oil, which is characterized in that the raw material including following weight part ratio: 50-60 parts of snake adipose tissue, beech
2-8 parts of juice, 2-6 parts of Randia canthioides leaf juice, fragrant 0.5-1.5 parts of knotweed juice, 0.1-0.2 parts of lecithin, 0.13-0.17 parts of carrotene and sea
0.07-0.13 parts of mosanom.
2. aroma type snake oil according to claim 1, which is characterized in that the raw material including following weight part ratio: snake fat
54-56 parts of tissue, 4-6 parts of beech juice, 3-5 parts of Randia canthioides leaf juice, fragrant 0.8-1.2 parts of knotweed juice, 0.17-0.19 parts of lecithin, carrot
Plain 0.14-0.16 parts and sodium alginate 0.09-0.11 parts.
3. a kind of aroma type snake oil according to claim 1 or 2, which is characterized in that the snake is selected from Elaphe Carinatas；The virtue
Odor type snake oil shelf-life at 4-8 DEG C is 36-48 months.
4. aroma type snake oil according to claim 1 or 2, which is characterized in that the beech juice weighs the preparation method comprises the following steps: pressing
Part ratio is measured, 1-3 parts and 0.6-1 parts of beech leaf of beech bark is taken, smashes it through 50-60 mesh, the powder after collecting sieving, then
It takes powder to add 5-9 parts of water, stirs evenly, after standing 25-35 minutes, be placed in squeezer and squeeze the juice, obtain beech crude extract, then
It takes beech crude extract to be dried under reduced pressure into the medicinal extract that relative density is 1.24-1.28 at 70-80 DEG C, third is then added in medicinal extract
It 8-14 parts of ketone, is ultrasonically treated 30-40 minutes, filtering obtains filter residue, then filter residue volatilizes acetone at 40-50 DEG C, is then filtering
Mixed solvent is added in two portions in slag, the amount that mixed solvent is added every time is respectively 10-20 parts and 8-12 parts, is added for the first time mixed
It is ultrasonically treated 45-65 minutes, is ultrasonically treated 20-30 minutes after second of addition mixed solvent, then through 0.2-0.3 after bonding solvent
μm membrane filtration, collects and merges the filtrate filtered twice, then filtrate adds 1-2 parts of water, and then recycling design obtains beech juice；
The mixed solvent includes the solution of following weight part ratio: concentration of volume percent is 5-9 parts of ethanol water of 70%-80%
With 1-3 parts of ethyl acetate.
5. aroma type snake oil according to claim 1 or 2, which is characterized in that the beech juice the preparation method comprises the following steps: using knife
The bark of beech trunk is cut open, by weight, then mixed solvent is added in two portions, often in 5-9 parts of juice for collecting outflow
The secondary amount that mixed solvent is added is respectively 10-20 parts and 8-12 parts, and 32-42 points of ultrasonic treatment are added after mixed solvent for the first time
Clock is ultrasonically treated 15-25 minutes after mixed solvent is added for the second time, then through 0.2-0.3 μm of membrane filtration, collects and merge two
The filtrate of secondary filtering, then filtrate recycling design obtains beech juice；The mixed solvent includes the solution of following weight part ratio: body
5-9 parts and ethyl acetate 1-3 parts of ethanol water that product percent concentration is 70%-80%.
6. aroma type snake oil according to claim 1 or 2, which is characterized in that the Randia canthioides leaf juice the preparation method comprises the following steps: pressing
Weight part ratio takes 2-4 parts of Randia canthioides leaf, is placed in squeezer and squeezes the juice, and obtains Randia canthioides leaf crude extract, then in Randia canthioides leaf crude extract
It is added acetone 12-22 parts, is ultrasonically treated 50-60 minutes, filtering obtains filter residue, filter residue acetone rinse 2-3 times, each acetone
Dosage be 1-2 parts, then filter residue volatilizes acetone at 40-50 DEG C, mixed solvent is then added in two portions in filter residue, every time
The amount that mixed solvent is added is respectively 14-28 parts and 10-20 parts, is ultrasonically treated 60-70 minutes after mixed solvent is added for the first time,
It is ultrasonically treated 30-40 minutes after second of addition mixed solvent, then through 0.2-0.3 μm of membrane filtration, collects and merge twice
The filtrate of filtering, then recycling design obtains Randia canthioides juice；The mixed solvent includes the solution of following weight part ratio: volume basis
5-9 parts and ethyl acetate 1-3 parts of ethanol water that specific concentration is 70%-80%.
7. aroma type snake oil according to claim 1 or 2, which is characterized in that the perfume knotweed juice weighs the preparation method comprises the following steps: pressing
Part ratio is measured, whole strain 2-4 parts of fragrant knotweed is taken, is placed in squeezer and squeezes the juice, obtain fragrant knotweed crude extract, be then added in fragrant knotweed crude extract
Concentration of volume percent is 16-30 parts of ethanol water of 75%-85%, is ultrasonically treated 45-55 minutes, then filters, and is collected
Filtrate I, then it is 12-20 parts of ethanol water of 80%-90% that concentration of volume percent, which is added, in filter residue, is ultrasonically treated 25-
35 minutes, then filter, collect filtrate II, then merging filtrate I and filtrate II, then recycling design up to no alcohol taste to get
Fragrant knotweed juice.
8. a kind of preparation method of aroma type snake oil as claimed in claim 1 or 2, which comprises the following steps:
A. fat decocts oil: by weight, taking snake adipose tissue, is put into iron pan, is then cooked by slow fire 16-18 minutes until producing
When the oil colours of oil is light yellow, stops heating, obtain crude oil；
B. it filters: taking crude oil, keep oil temperature to filter 2-4 times at 30-38 DEG C, obtain refined filtration oil I, and collect filter residue and be placed in squeezing
It squeezes the juice in machine, collect juice and is filtered 2-4 times at 30-38 DEG C, obtain refined filtration oil II, then merge refined filtration oil I, refined filtration oil
II, obtain snake oil；
C. it mixes to obtain finished product: taking beech juice, Randia canthioides leaf juice, fragrant knotweed juice, sodium alginate, be ultrasonically treated 6-10 minutes, mixed
Juice；Then snake oil, lecithin are taken, is stirred evenly, snake oil mixed liquor is obtained, mixed juice is then taken to divide 2-3 addition snake oil mixing
In liquid, each additional amount is the 30%-50% of mixed juice total weight, is shaken 3-7 minutes after being added every time, obtains thick cream, then will
Thick cream, which is placed in high pressure homogenizer, carries out homogeneous, and setting high pressure homogenizer pressure is 50-60MPa, homogenization cycles are 4-5 times, equal
Matter temperature is 35-45 DEG C, collects homogenizing fluid, carrotene is then added, and is uniformly mixed to get aroma type snake oil finished product.
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Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58146030A (en) * | 1982-11-19 | 1983-08-31 | Yoshiro Nakamatsu | Magnetic recording medium having inclined snake oil surface |
| CN1345588A (en) * | 2000-09-29 | 2002-04-24 | 国家海洋药物工程技术研究中心 | No-stinking fish-oil composite micro-capsule and preparation process |
| CN101475807A (en) * | 2009-01-12 | 2009-07-08 | 高政 | Ultrasonic assisted production technology for extracting rosemary antioxidant |
| CN101961352A (en) * | 2010-10-27 | 2011-02-02 | 南通迈特生物工程有限公司 | Self-emulsified fish oil soft capsules without fishy smell |
| CN102293438A (en) * | 2011-05-27 | 2011-12-28 | 南京农业大学 | Color, flavor and safety three-effect food fumeol and its preparation method |
| CN103468390A (en) * | 2013-09-29 | 2013-12-25 | 武夷山元生泰生物科技有限公司 | Snake oil refining method |
| CN103483134A (en) * | 2013-04-18 | 2014-01-01 | 杨红梅 | Ultrasonic countercurrent extraction method for lycopene |
| CN105287715A (en) * | 2015-10-19 | 2016-02-03 | 南昌大学 | Perilla oil oral emulsion with lipid-lowering nutritious function and preparation method thereof |
| CN105326736A (en) * | 2015-11-06 | 2016-02-17 | 陕西唐兰商贸有限公司 | Manufacturing method of natural snake oil cream |
| CN105602730A (en) * | 2016-01-12 | 2016-05-25 | 四川农业大学 | Phoebe zhennan essential oil and preparation method thereof |
| CN108096074A (en) * | 2017-12-28 | 2018-06-01 | 江苏隆力奇生物科技股份有限公司 | A kind of snake oil composition and preparation method thereof, purposes |
-
2018
- 2018-09-21 CN CN201811117900.9A patent/CN109181860A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58146030A (en) * | 1982-11-19 | 1983-08-31 | Yoshiro Nakamatsu | Magnetic recording medium having inclined snake oil surface |
| CN1345588A (en) * | 2000-09-29 | 2002-04-24 | 国家海洋药物工程技术研究中心 | No-stinking fish-oil composite micro-capsule and preparation process |
| CN101475807A (en) * | 2009-01-12 | 2009-07-08 | 高政 | Ultrasonic assisted production technology for extracting rosemary antioxidant |
| CN101961352A (en) * | 2010-10-27 | 2011-02-02 | 南通迈特生物工程有限公司 | Self-emulsified fish oil soft capsules without fishy smell |
| CN102293438A (en) * | 2011-05-27 | 2011-12-28 | 南京农业大学 | Color, flavor and safety three-effect food fumeol and its preparation method |
| CN103483134A (en) * | 2013-04-18 | 2014-01-01 | 杨红梅 | Ultrasonic countercurrent extraction method for lycopene |
| CN103468390A (en) * | 2013-09-29 | 2013-12-25 | 武夷山元生泰生物科技有限公司 | Snake oil refining method |
| CN105287715A (en) * | 2015-10-19 | 2016-02-03 | 南昌大学 | Perilla oil oral emulsion with lipid-lowering nutritious function and preparation method thereof |
| CN105326736A (en) * | 2015-11-06 | 2016-02-17 | 陕西唐兰商贸有限公司 | Manufacturing method of natural snake oil cream |
| CN105602730A (en) * | 2016-01-12 | 2016-05-25 | 四川农业大学 | Phoebe zhennan essential oil and preparation method thereof |
| CN108096074A (en) * | 2017-12-28 | 2018-06-01 | 江苏隆力奇生物科技股份有限公司 | A kind of snake oil composition and preparation method thereof, purposes |
Non-Patent Citations (1)
| Title |
|---|
| 苟体忠 等: ""香蓼总多酚超声波辅助提取工艺优化及其体外抗氧活性评价"", 《食品工业科技》 * |
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