CN105287715A - Perilla oil oral emulsion with lipid-lowering nutritious function and preparation method thereof - Google Patents
Perilla oil oral emulsion with lipid-lowering nutritious function and preparation method thereof Download PDFInfo
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- CN105287715A CN105287715A CN201510679113.3A CN201510679113A CN105287715A CN 105287715 A CN105287715 A CN 105287715A CN 201510679113 A CN201510679113 A CN 201510679113A CN 105287715 A CN105287715 A CN 105287715A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
Abstract
The invention discloses a perilla oil oral emulsion with a lipid-lowering nutritious function, and a preparation method thereof. The invention discloses an oil-in-water type perilla oil oral emulsion and the preparation method thereof. The emulsion takes perilla oil as a main raw material, and is characterized by being prepared through the following components according to proportion: 5 to 50 percent of the perilla oil, 0.5 to 30 percent of an emulgator, 0 to 0.5 percent of a corrigent and the balance of purified water, and emulsification is adopted as the preparation method. Based on the perilla oil, the perilla oil oral emulsion has a delicate flavor and also has an anti-oxidation effect, and an antioxidant and a smell mask are not required to add. Compared with a conventional product, the emulsion provided by the invention is high in perilla oil content, good in taste and convenient to eat, is wide in applicable human populations, and can obtain a better effect under low dosage; the emulsion is relatively good in dispersibility and thermodynamic stability, has low probability of phase splitting and precipitating, is easy to store, simple in process, convenient for large scale production, and has great social value and economic value.
Description
Technical field
The present invention relates to and a kind ofly there is lipid-lowering nourishing effect and can the preparation method of perilla oil Orally taken emulsion of auxiliary antilipemic blood pressure lowering.
Background technology
Alpha-linolenic acid is essential fatty acid, two kinds of material eicosapentaenoic acid (EPA) and docosahexenoic acid (DHA) that human body is played an important role are generated through a series of metabolism in human body, they are to raising memory, improve cardiovascular and cerebrovascular vessel function, delaying body aging all has remarkable effect.And containing the alpha-linolenic acid of 50% ~ 70% in perilla oil, also just mean and take in the amount that 3-5g perilla oil can meet needed by human body alpha-linolenic acid every day.Because the double bond of alpha-linolenic acid is fewer than EPA and DHA, therefore Fructus Perillae oil oxidation stability is stronger than fish oil, and perilla oil is not containing the cholesterol contained in fish oil, and nutritive value is higher.
At present, the perilla oil product circulated in market is based on Fructus Perillae crude oil, soft capsule of perilla seed oil, and wherein Fructus Perillae crude oil directly drinks comparatively inconvenience as health promoting product, and mouthfeel is greasy; And soft capsule of perilla seed oil is expensive and be unsuitable for infant and digestive tract has the patient of ulcer to take.
To sum up, a kind of applicable all kinds of crowd is daily oral in development, and be easy to quantitative, good absorbing, delicious perilla oil Orally taken emulsion can solve above-mentioned Problems existing.
Summary of the invention
The object of the present invention is to provide a kind of have mouthfeel good, be easy to take, the perilla oil Orally taken emulsion of the feature such as good stability.
The present invention also aims to provide a kind of preparation method being beneficial to the perilla oil Orally taken emulsion of suitability for industrialized production.
Perilla oil Emulsion provided by the invention is a kind of Orally taken emulsion with lipid-lowering nourishing effect, it is characterized in that it is made up of following compositions and proportioning, perilla oil 5%-50%; Emulsifying agent 0.5%-30%; Correctives 0-0.5%; All the other are water.
Perilla oil Orally taken emulsion provided by the invention, it is characterized in that described perilla oil preparation method is: (1) selects materials, remove impurity and drying: cleaned by Fructus Perillae clear water, after the impurity such as dust, earth, be placed in dry in the sun or baking oven under the sun and dry; (2) microwave: take out after Fructus Perillae 700w microwave 60s; (3) modified: in Fructus Perillae, to add certain moisture carry out modified to it, regulate Fructus Perillae moisture to be 2%; (4) extract oil: choosing rotor aperture is 5mm, assemble KOMET-CA59G low temperature pressing machine and preheating, make the 4th hole temperature on squeezing head remain on 55 DEG C, adjustment oil press rotating speed is 32rpm, carries out low temperature pressing to the Fructus Perillae that (3) obtain; (5) filter: undertaken centrifugal by the oil that (4) step obtains, filtration or sucking filtration obtain limpid transparent perilla oil.
Perilla oil Orally taken emulsion provided by the invention, emulsifying agent can be one or more in amphoteric surfactant, non-ionic surface active agent.Wherein amphoteric surfactant is selected from one or more that amphoteric surfactant is selected from fabaceous lecithin, egg yolk lecithin, phosphatidylcholine, PHOSPHATIDYL ETHANOLAMINE, serinephosphatide, lipositol, phosphatidic acid, cephalin or hydrogenated phospholipid; Non-ionic surface active agent is selected from one or more of sucrose-fatty esters, spans, Tweens, polyethylene Topiramate Los oxazolidinone, polyoxyethylene fatty acid ester class, polyoxyethylene aliphatic alcohol ether class, glyceryl monostearate, Cetomacrogol class, CremophoreEL class or poloxamer apoplexy due to endogenous wind.Be preferably one or more in lecithin, sucrose fatty acid ester, Tweens, spans, glyceryl monostearate.
Perilla oil Orally taken emulsion provided by the invention, can also contain correctives, correctives can be acidic flavoring agent; It can be sweeting agent; It can be thickening agent; Can be glycerol.Wherein acidic flavoring agent preferably from but be not limited to citric acid, tartaric acid, malic acid, lactic acid, fumaric acid, succinic acid and glucono-δ-lactone; Sweeting agent preferably from but be not limited to stevioside, Radix Glycyrrhizae, disodium glycyrrhizinate, trisodium glycyrrhetinate (potassium), Rhizoma Marantae arundinaceae glucin, saccharin sodium, sodium cyclamate (cyclamate), L-aspartyl-L-phenylalanine Methylester (sweetener or aspartame), acesulfame potassium (acesulfame potassium), sucralose.
The preparation method of perilla oil Orally taken emulsion of the present invention is emulsion process, it is characterized in that concrete steps are as follows: emulsifying agent, fat-soluble additive and perilla oil mix, are uniformly dispersed as oil phase; Add 1/3 of water full dose, emulsifying is helped with high shear, 2-4 time repeatedly, within each 2-4 minute, obtain colostrum, other water-soluble additives are added in residue aqueous phase, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, rotates water-bath sterilization 30min, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
The invention still further relates to the aforementioned perilla oil Orally taken emulsion with lipid-lowering nourishing effect and prepare the purposes in health food.
Advantage of the present invention is as follows: perilla oil Orally taken emulsion of the present invention, compared with existing perilla oil Related product, has that mouthfeel is good, good absorbing, good stability, is easy to advantages such as quantitatively taking, adaptation population is extensive; Compared with other oil emulsion, in perilla oil Orally taken emulsion, alpha-linolenic acid content is higher, and dispersibility, thermodynamic stability are better; not easily phase-splitting, precipitation, easily store, and present invention process is simple; be convenient to large-scale production, there is very large social value and economic worth.
Detailed description of the invention
Below by way of detailed description of the invention, the present invention will be further described, but this can not limit protection scope of the present invention, can make amendment and improve according to basic thought of the present invention, only otherwise depart from basic thought of the present invention all within the scope of the present invention.
Perilla oil preparation method is: (1) selects materials, remove impurity and drying: cleaned by Fructus Perillae clear water, after the impurity such as dust, earth, is placed in dry in the sun or baking oven under the sun and dries; (2) microwave: Fructus Perillae is placed in microwave oven, takes out with after 700w microwave 60s; (3) modified: in Fructus Perillae, add certain moisture carry out modified to it, the Fructus Perillae mortar that takes a morsel is milled broken, measure Fructus Perillae moisture with moisture test apparatus, regulate Fructus Perillae moisture to be 2%; (4) extract oil: choosing rotor aperture is 5mm, assemble KOMET-CA59G low temperature pressing machine and preheating, make the 4th hole temperature on squeezing head remain on 55 DEG C, adjustment oil press rotating speed is 32rpm, carries out low temperature pressing to the Fructus Perillae that (3) obtain; (5) filter: the oil that (4) step obtains is carried out centrifugal (4000rpm, 10min), uses bottle,suction sucking filtration, obtain limpid transparent perilla oil.
Embodiment 1:
Get 2ml perilla oil, Tween 80 0.6g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Add 3ml water, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, rotates water-bath sterilization 30min, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.The content recording alpha-linolenic acid is: 2.5%-30%.
The dewatering ability test of Emulsion: perilla oil Orally taken emulsion is placed in 10ml centrifuge tube, under the condition of 4000r/min after centrifugal 30min, takes out and observes, do not find layering, prove that stability is better.
The heat stability testing of Emulsion: perilla oil Orally taken emulsion is placed in test tube, sealing, after being placed in 37 DEG C of constant water bath box placement 14d, taking out and observes, do not find layering, prove that stability is better.
Embodiment 2:
Get 2ml perilla oil, Tween 80 0.6g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Getting 0.001g saccharin sodium is dissolved in 3ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 3:
Get 2ml perilla oil, Tween 80 0.6g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Get 0.001g saccharin sodium, 0.02g citric acid is dissolved in 3ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 4:
Get 2ml perilla oil, polysorbate60 0.6g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Getting 0.001g saccharin sodium is dissolved in 3ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 5:
Get 2ml perilla oil, polysorbate60 0.6g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Get 0.001g saccharin sodium, 0.02g citric acid is dissolved in 3ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 6:
Get 2ml perilla oil, sucrose ester 0.7g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Get 0.001g saccharin sodium, 0.02g citric acid is dissolved in 3ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 7:
Get 4ml perilla oil, Tween 80 0.6g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Get 0.001g saccharin sodium, 0.02g citric acid is dissolved in 2ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 3ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 8:
Get 4ml perilla oil, sucrose ester 0.7g, glyceryl monostearate 0.5g mixing, be uniformly dispersed as oil phase; Get 0.001g saccharin sodium, 0.02g citric acid is dissolved in 2ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 3ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 9:
Get 4ml perilla oil, polysorbate60 0.6g, glyceryl monostearate 0.5g stir, are uniformly dispersed as oil phase; Get 0.001g saccharin sodium, 0.02g citric acid is dissolved in 3ml water, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 4ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Embodiment 10:
Get 4ml perilla oil, polysorbate60 0.6g, glyceryl monostearate 0.5g stir, are uniformly dispersed as oil phase; Add water 2ml, after mixing with oil phase, help emulsifying with high shear, 3 times repeatedly, within each 3 minutes, obtain colostrum, add residue 3ml water, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, water-bath sterilization 30min is rotated, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
Claims (3)
1. there is a perilla oil Orally taken emulsion for lipid-lowering nourishing effect, it is characterized in that it is made up of following compositions and proportioning, perilla oil 5%-50%; Emulsifying agent 0.5%-30%; Correctives 0-0.5%; All the other are water; Described perilla oil preparation method is: (1) selects materials, remove impurity and drying: cleaned by Fructus Perillae clear water, after the impurity such as dust, earth, is placed in dry in the sun or baking oven under the sun and dries; (2) microwave: take out after Fructus Perillae 700w microwave 60s; (3) modified: in Fructus Perillae, to add certain moisture carry out modified to it, regulate Fructus Perillae moisture to be 2%; (4) extract oil: choosing rotor aperture is 5mm, assemble KOMET-CA59G low temperature pressing machine and preheating, make the 4th hole temperature on squeezing head remain on 55 DEG C, adjustment oil press rotating speed is 32rpm, carries out low temperature pressing to the Fructus Perillae that (3) obtain; (5) filter: the oil that (4) step obtains is carried out centrifugal, obtains limpid transparent perilla oil; The described perilla oil Orally taken emulsion with lipid-lowering nourishing effect, is characterized in that described emulsifying agent is selected from: amphoteric surfactant or non-ionic surface active agent; Amphoteric surfactant is selected from one or more in fabaceous lecithin, egg yolk lecithin, phosphatidylcholine, PHOSPHATIDYL ETHANOLAMINE, serinephosphatide, lipositol, phosphatidic acid, cephalin or hydrogenated phospholipid; Non-ionic surface active agent is selected from one or more of sucrose-fatty esters, spans, Tweens, polyethylene Topiramate Los oxazolidinone, polyoxyethylene fatty acid ester class, polyoxyethylene aliphatic alcohol ether class, glyceryl monostearate, Cetomacrogol class, CremophoreEL class or poloxamer apoplexy due to endogenous wind, is preferably glyceryl monostearate; Described emulsifying agent is preferably one or more in lecithin, sucrose fatty acid ester, Tweens, spans, glyceryl monostearate, is preferably Tween 80; Correctives is acidic flavoring agent, sweeting agent, thickening agent or glycerol; Acidic flavoring agent is selected from citric acid, tartaric acid, malic acid, lactic acid, fumaric acid, succinic acid and glucono-δ-lactone; Sweeting agent is selected from stevioside, Radix Glycyrrhizae, disodium glycyrrhizinate, trisodium glycyrrhetinate, tripotassium glycyrrhetate, Rhizoma Marantae arundinaceae glucin, saccharin sodium, sodium cyclamate, L-aspartyl-L-phenylalanine Methylester, acesulfame potassium, sucralose.
2. prepare the method with lipid-lowering nourishing effect perilla oil Orally taken emulsion according to claim 1, be emulsion process, it is characterized in that concrete steps are as follows: emulsifying agent, fat-soluble additive and perilla oil mix, are uniformly dispersed as oil phase; Add 1/3 of water full dose, use high-shearing dispersion emulsifying machine emulsifying, 2-4 time repeatedly, within each 2-4 minute, obtain colostrum, other water-soluble additives are added in residue aqueous phase, mix homogeneously with colostrum, to proceed in high pressure homogenizer under 50-90MPa pressure homogenizing 5-10 time, embedding after filtering, rotates water-bath sterilization 30min, 4-20 DEG C of lucifuge cold preservation at 115 DEG C-121 DEG C.
3. there is lipid-lowering nourishing effect perilla oil Orally taken emulsion as claimed in claim 1 and preparing the purposes in health food.
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Cited By (5)
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CN108208838A (en) * | 2018-03-09 | 2018-06-29 | 北京素维生物科技有限公司 | A kind of taste masking composition and application thereof |
CN108514118A (en) * | 2018-03-09 | 2018-09-11 | 北京素维生物科技有限公司 | A kind of taste masking composition and its application |
CN109181860A (en) * | 2018-09-21 | 2019-01-11 | 三江县连兴蛇业有限公司 | A kind of aroma type snake oil and preparation method thereof |
CN109601798A (en) * | 2019-02-01 | 2019-04-12 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of Wudalianchi metasilicic acid mineral water hemp beverage |
CN110447886A (en) * | 2019-08-29 | 2019-11-15 | 吉林大学 | Purple perilla black fungus cream and manufacturing method |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN108208838A (en) * | 2018-03-09 | 2018-06-29 | 北京素维生物科技有限公司 | A kind of taste masking composition and application thereof |
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CN109181860A (en) * | 2018-09-21 | 2019-01-11 | 三江县连兴蛇业有限公司 | A kind of aroma type snake oil and preparation method thereof |
CN109601798A (en) * | 2019-02-01 | 2019-04-12 | 黑龙江省科学院火山与矿泉研究所 | Preparation method of Wudalianchi metasilicic acid mineral water hemp beverage |
CN110447886A (en) * | 2019-08-29 | 2019-11-15 | 吉林大学 | Purple perilla black fungus cream and manufacturing method |
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