CN109135969B - Zinc chlorophyll facial soap and preparation method thereof - Google Patents
Zinc chlorophyll facial soap and preparation method thereof Download PDFInfo
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- CN109135969B CN109135969B CN201810985045.7A CN201810985045A CN109135969B CN 109135969 B CN109135969 B CN 109135969B CN 201810985045 A CN201810985045 A CN 201810985045A CN 109135969 B CN109135969 B CN 109135969B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Cosmetics (AREA)
- Detergent Compositions (AREA)
Abstract
The invention provides a zinc chlorophyll facial soap which is composed of the following components in parts by weight: 31-71 parts of vegetable oil, 20-40 parts of alkali liquor, 7-13 parts of ethanol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, 0.05-1 part of zinc chlorophyll and 0.1-3 parts of essential oil; wherein the vegetable oil comprises 5-15 parts of castor oil, 10-20 parts of coconut oil, 10-20 parts of shea butter, 3-8 parts of jojoba oil and 3-8 parts of peanut oil; the alkali liquor is deionized water solution of sodium hydroxide, and the concentration of the solution is 20-40 wt%; the essential oil is one or more of rose essential oil, jasmine essential oil, orange flower essential oil, sweet essence oil, cananga odorata essential oil, rosemary essential oil, peppermint essential oil and eucalyptus essential oil. According to the invention, the zinc chlorophyll and the sodium zinc chlorophyllin are added into the facial soap, so that metal ions deposited on the face can be removed, the skin of the face can be protected, and the skin activity can be recovered.
Description
Technical Field
The invention relates to the technical field of daily necessities, in particular to a zinc chlorophyll facial soap and a preparation method thereof.
Background
Chlorophyll has attracted much attention since the beginning of its discovery, and its properties have been extensively studied at home and abroad, and it has been found that it not only catalyzes photosynthesis, but also has peculiar effects on human body. Richard award for Nobel prize
And Hans Fischer, indicate the relationship of chlorophyll to hemoglobin in red blood cells: the chlorophyll molecule can be converted into heme under a certain condition similar to heme molecule, and has blood replenishing effect. In addition, chlorophyll has the function of expelling toxin, can complex a plurality of heavy metal ions, reduce oxides, eliminate free radicals and inhibit sulfide generated in the metabolic process so as to deodorize, and is widely applied to health care products at present. However, the cost for extracting the natural chlorophyll is high at present, the artificial synthesis is very complicated, the natural chlorophyll is easy to decompose under the light, and is extremely unstable and easy to remove magnesium under the acid condition, and the natural chlorophyll is further shapedThe pyropheophytin is formed, so the storage is difficult. At present, methods for improving chlorophyll stability by replacing magnesium ions in a porphyrin ring with copper, iron and zinc ions are mainly used. Today, cosmetics are widely used, heavy metal deposition on skin caused by cosmetics of various colors is serious day by day, so that a product is urgently needed to solve the technical problem.
Disclosure of Invention
Therefore, the invention aims to provide a zinc chlorophyll facial soap and a preparation method thereof, and solves the technical problems.
The technical scheme of the invention is realized as follows:
the zinc chlorophyll facial soap comprises the following components in parts by weight: 31-71 parts of vegetable oil, 20-40 parts of alkali liquor, 7-13 parts of ethanol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, 0.05-1 part of zinc chlorophyll and 0.1-3 parts of essential oil.
Further, the vegetable oil comprises the following components in parts by weight: 5-15 parts of castor oil, 10-20 parts of coconut oil, 10-20 parts of shea butter, 3-8 parts of jojoba oil and 3-8 parts of peanut oil.
Further, the zinc chlorophyll can be replaced by sodium zinc chlorophyll.
Further, the alkali liquor is deionized water solution of sodium hydroxide, and the concentration of the solution is 20-40% wt.
Further, the essential oil is one or more of rose essential oil, jasmine essential oil, orange flower essential oil, sweet essence oil, cananga essential oil, rosemary essential oil, peppermint essential oil and eucalyptus essential oil.
Further, the zinc chlorophyll facial soap comprises the following components in parts by weight: 50 parts of vegetable oil, 30 parts of alkali liquor, 10 parts of ethanol, 8 parts of cane sugar, 2 parts of propylene glycol, 0.3 part of zinc chlorophyll and 1 part of essential oil.
Further, the vegetable oil comprises the following components in parts by weight: 10 parts of castor oil, 15 parts of coconut oil, 15 parts of shea butter, 5 parts of jojoba oil and 5 parts of peanut oil.
A zinc chlorophyll facial soap is prepared by the following steps:
step 1: keeping oleum ricini, oleum Cocois, shea butter, jojoba oil, and oleum Arachidis Hypogaeae at 50-70 deg.C for 0.4-0.6h, adding alkali solution, and saponifying at 60-80 deg.C for 2-4h to obtain vegetable oil mixture;
step 2: adding ethanol, propylene glycol and sucrose into the vegetable oil mixture obtained in the step 1, fully mixing, and keeping the temperature at 60-80 ℃ for 2-4 h;
and step 3: cooling the mixture obtained in step 2 to 40-50 ℃, adding zinc chlorophyll and essential oil, fully mixing, filling into a mold, cooling, curing for 2-4 days, and packaging.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, the zinc chlorophyll and the sodium zinc chlorophyllin are added into the facial soap, so that metal ions deposited on the face can be removed, the skin of the face can be protected, the skin metabolism can be promoted, the skin repair can be promoted, and the skin activity can be recovered.
Detailed Description
For clear and complete description of the technical solutions in the present invention, it is obvious that the inventor combines the embodiments to describe, but the following embodiments describe only some embodiments of the present invention, not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The zinc chlorophyll facial soap comprises the following components in parts by weight: 31-71 parts of vegetable oil, 20-40 parts of alkali liquor, 7-13 parts of ethanol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, 0.05-1 part of zinc chlorophyll and 0.1-3 parts of essential oil.
Further, the vegetable oil comprises the following components in parts by weight: 5-15 parts of castor oil, 10-20 parts of coconut oil, 10-20 parts of shea butter, 3-8 parts of jojoba oil and 3-8 parts of peanut oil.
Further, the zinc chlorophyll can be replaced by sodium zinc chlorophyll.
Further, the alkali liquor is deionized water solution of sodium hydroxide, and the concentration of the solution is 20-40% wt.
Further, the essential oil is one or more of rose essential oil, jasmine essential oil, orange flower essential oil, sweet essence oil, cananga essential oil, rosemary essential oil, peppermint essential oil and eucalyptus essential oil.
A zinc chlorophyll facial soap is prepared by the following steps:
step 1: keeping oleum ricini, oleum Cocois, shea butter, jojoba oil, and oleum Arachidis Hypogaeae at 50-70 deg.C for 0.4-0.6h, adding alkali solution, and saponifying at 60-80 deg.C for 2-4h to obtain vegetable oil mixture;
step 2: adding ethanol, propylene glycol and sucrose into the vegetable oil mixture obtained in the step 1, fully mixing, and keeping the temperature at 60-80 ℃ for 2-4 h;
and step 3: cooling the mixture obtained in step 2 to 40-50 ℃, adding zinc chlorophyll and essential oil, fully mixing, filling into a mold, cooling, curing for 2-4 days, and packaging.
The cleansing soaps of examples 1 to 5 and comparative examples 1 to 6 were prepared according to the formulations shown in tables 1 to 2, the above preparation steps:
table 1:
| unit of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 | |
| Castor oil | Portions are | 5 | 8 | 10 | 10 | 15 |
| Coconut oil | Portions are | 13 | 18 | 20 | 15 | 10 |
| Shea butter | Portions are | 20 | 18 | 15 | 15 | 10 |
| Jojoba oil | Portions are | 6 | 3 | 5 | 5 | 8 |
| Peanut oil | Portions are | 5 | 6 | 8 | 5 | 3 |
| Alkali liquor | Portions are | 32 | 40 | 20 | 30 | 38 |
| Ethanol | Portions are | 7 | 10 | 13 | 10 | 11 |
| Sucrose | Portions are | 8 | 5 | 10 | 8 | 12 |
| Propylene glycol | Portions are | 1 | 2 | 2 | 2 | 1 |
| Chlorophyll zinc | Portions are | —— | 1 | 0.5 | 0.3 | 0.05 |
| Chlorophyll zinc sodium salt | Portions are | 0.5 | —— | —— | —— | —— |
| Essential oil | Portions are | 0.1 | 0.5 | 2 | 1 | 3 |
Table 2:
120 volunteers having experience of using the washing and makeup articles for more than 2 years were selected from the population, and the facial soap of examples 1 to 5 and comparative examples 1 to 6 were used twice a day in the morning and at the evening, and after 1 month of continuous use, the investigation was conducted, and the remaining 10 volunteers used only clean faces with clean water, and the results were as follows:
table 3, examples 1-5:
table 4, comparative examples 1-6 and control:
it can be seen that the formula adopted by the application can not cause allergy, and the facial soap prepared according to the formula can improve the blackheads of the skin, keep the water content of the skin and have a better oil control effect after being used.
And (3) testing metal ions:
configuration of Hg2+、Cd2+、Pb2+、Cu2+、As3+And Sb3+Selecting fresh pork on the market, removing pig hair, cleaning, drawing 4 x 4cm square grids on the pigskin, respectively dipping the 6 solutions by cotton swabs, coating the pigskin, completely drying in the air, cutting 1 x 1cm square grids, and testing the metal ion content. Then, the pigskins were washed with examples 1 to 5, comparative examples 1 to 6 and clean water (control), and after washing and air-drying, the pigskins were cut into 1 × 1cm squares again to measure the metal ion content. The percentage of metal ions washed off after washing the pigskin was calculated and the average was taken after repeating the above experiment 5 times, as shown in tables 5 and 6.
Table 5, examples 1-5:
| metal ion | Unit of | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 |
| Hg | ％ | 97 | 100 | 99 | 98 | 95 |
| Cd | ％ | 96 | 95 | 99 | 99 | 98 |
| Pb | ％ | 98 | 99 | 95 | 100 | 98 |
| Cu | ％ | 99 | 96 | 98 | 99 | 98 |
| As | ％ | 96 | 99 | 100 | 99 | 100 |
| Sb | ％ | 100 | 98 | 99 | 100 | 97 |
Table 6, comparative examples 1-6 and control:
| metal ion | Unit of | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | Comparative example 6 | Control group |
| Hg | ％ | 88 | 96 | 87 | 95 | 86 | 79 | 70 |
| Cd | ％ | 85 | 95 | 86 | 99 | 87 | 86 | 69 |
| Pb | ％ | 86 | 94 | 93 | 91 | 88 | 85 | 75 |
| Cu | ％ | 88 | 97 | 90 | 97 | 85 | 83 | 76 |
| As | ％ | 85 | 98 | 84 | 96 | 90 | 79 | 82 |
| Sb | ％ | 81 | 99 | 86 | 97 | 86 | 80 | 77 |
It can be seen that the facial soap prepared according to the application can better remove residual metal ions on the surface of skin, and the facial soap prepared by adopting clear water or a formula provided by the invention has poorer removal effect on the metal ions.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (5)
1. The zinc chlorophyll facial soap is characterized by comprising the following components in parts by weight: 31-71 parts of vegetable oil, 20-40 parts of alkali liquor, 7-13 parts of ethanol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, 0.05-1 part of zinc chlorophyll and 0.1-3 parts of essential oil; the vegetable oil comprises the following components in parts by weight: 5-15 parts of castor oil, 10-20 parts of coconut oil, 10-20 parts of shea butter, 3-8 parts of jojoba oil and 3-8 parts of peanut oil, wherein the essential oil is one or a mixture of more of rose essential oil, jasmine essential oil, neroli essential oil, allspice essential oil, ylang essential oil, rosemary essential oil, peppermint essential oil and eucalyptus essential oil;
the zinc chlorophyll facial soap is prepared by the following steps:
step 1: keeping oleum ricini, oleum Cocois, shea butter, jojoba oil, and oleum Arachidis Hypogaeae at 50-70 deg.C for 0.4-0.6h, adding alkali solution, and saponifying at 60-80 deg.C for 2-4h to obtain vegetable oil mixture;
step 2: adding ethanol, propylene glycol and sucrose into the vegetable oil mixture obtained in the step 1, fully mixing, and keeping the temperature at 60-80 ℃ for 2-4 h;
and step 3: cooling the mixture obtained in step 2 to 40-50 ℃, adding zinc chlorophyll and essential oil, fully mixing, filling into a mold, cooling, curing for 2-4 days, and packaging.
2. The zinc chlorophyll facial soap according to claim 1, wherein said zinc chlorophyll is replaced with zinc sodium chlorophyll.
3. The zinc chlorophyll facial soap of claim 1, wherein said alkaline solution is a deionized water solution of sodium hydroxide, having a concentration of 20-40% wt.
4. The zinc chlorophyllin facial soap according to claim 1, wherein the zinc chlorophyllin facial soap comprises the following components in parts by weight: 50 parts of vegetable oil, 30 parts of alkali liquor, 10 parts of ethanol, 8 parts of cane sugar, 2 parts of propylene glycol, 0.3 part of zinc chlorophyll and 1 part of essential oil.
5. The zinc chlorophyll facial soap of claim 4, wherein the vegetable oil comprises the following components in parts by weight: 10 parts of castor oil, 15 parts of coconut oil, 15 parts of shea butter, 5 parts of jojoba oil and 5 parts of peanut oil.
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1857192A (en) * | 2006-03-28 | 2006-11-08 | 柳州两面针股份有限公司 | Application of sodium zinc chlorophyllin in preparing oral cavity care article |
| US20080317836A1 (en) * | 2007-06-19 | 2008-12-25 | Discovery Partners Llc | Topical compositions for anti-aging skin treatment |
| US20120283235A1 (en) * | 2009-10-20 | 2012-11-08 | Discovery Partners Llc | Dermatologic and Cosmetic Compositions |
| CN106236687A (en) * | 2016-08-26 | 2016-12-21 | 广东科玮生物技术股份有限公司 | A kind of crease-resistant facial cream of chlorophyll and preparation method thereof |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS61190598A (en) * | 1985-02-18 | 1986-08-25 | 株式会社 寺尾 | Cosmetic soap and its production |
| CN108384643A (en) * | 2018-03-22 | 2018-08-10 | 徐州巨龙新材料科技有限公司 | A kind of preparation method of kitchen greasy dirt cleaning agent |
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1857192A (en) * | 2006-03-28 | 2006-11-08 | 柳州两面针股份有限公司 | Application of sodium zinc chlorophyllin in preparing oral cavity care article |
| US20080317836A1 (en) * | 2007-06-19 | 2008-12-25 | Discovery Partners Llc | Topical compositions for anti-aging skin treatment |
| US20120283235A1 (en) * | 2009-10-20 | 2012-11-08 | Discovery Partners Llc | Dermatologic and Cosmetic Compositions |
| CN106236687A (en) * | 2016-08-26 | 2016-12-21 | 广东科玮生物技术股份有限公司 | A kind of crease-resistant facial cream of chlorophyll and preparation method thereof |
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