CN109135969A - A kind of zinc is for chlorophyll facial soap and preparation method thereof - Google Patents

A kind of zinc is for chlorophyll facial soap and preparation method thereof Download PDF

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Publication number
CN109135969A
CN109135969A CN201810985045.7A CN201810985045A CN109135969A CN 109135969 A CN109135969 A CN 109135969A CN 201810985045 A CN201810985045 A CN 201810985045A CN 109135969 A CN109135969 A CN 109135969A
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CN
China
Prior art keywords
parts
oil
chlorophyll
zinc
facial soap
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Granted
Application number
CN201810985045.7A
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Chinese (zh)
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CN109135969B (en
Inventor
秦玉春
秦玉华
徐秋阳
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Sanya Rongxiang Technology Co.,Ltd.
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Hainan Tropical Ocean University
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Priority to CN201810985045.7A priority Critical patent/CN109135969B/en
Publication of CN109135969A publication Critical patent/CN109135969A/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/005—Synthetic soaps
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/26—Organic compounds, e.g. vitamins containing oxygen
    • C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22—Organic compounds, e.g. vitamins
    • C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents

Abstract

The invention proposes a kind of zinc for chlorophyll facial soap, is grouped as by the group of following parts by weight: 31-71 parts of vegetable oil, 20-40 parts of lye, 7-13 parts of ethyl alcohol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, zinc is for 0.05-1 parts and essential oil 0.1-3 parts of chlorophyll；Wherein, the vegetable oil includes 5-15 parts of castor oil, 10-20 parts of coconut oil, 10-20 parts of shea butter, 3-8 parts and peanut oil 3-8 parts of SIMMONDSIA CHINENSIS SEED OIL；The lye is the deionized water solution of sodium hydroxide, solution concentration 20-40%wt；The essential oil is Rosa Damascana, refined jasmine oil, flores aurantii essential oil, the mixture for one or more of entering essential oil, Cananga odorata quintessence oil, Rosemary Oil, lavender essential oil, eucalyptus quintessence oil.The present invention is added to zinc for chlorophyll, sodium zinc chlorophyllin in facial soap, can dispel the metal ion of face deposition, protect skin of face, restore skin vitality.

Description

A kind of zinc is for chlorophyll facial soap and preparation method thereof
Technical field
The present invention relates to technical field of daily necessities, in particular to a kind of zinc is for chlorophyll facial soap and preparation method thereof.
Background technique
It is just concerned at the beginning of chlorophyll self-discovery, extensive research has been carried out to its property both at home and abroad, it is found that it is not only urged Change photosynthesis or even also plays the role of to human body peculiar.Nobel Laureate RichardAnd Hans Fischer just goes out to indicate the relationship of the hemoglobin in chlorophyll and erythrocyte: chlorophyll molecule and haemachrome molecule class Like ferroheme can be converted under certain condition, there is blood tonification effect.Furthermore a numerous huge sum of moneys can be complexed there are also toxin expelling effect in chlorophyll Belong to ion, reduced oxide, eliminate free radical, inhibit to generate sulfide in metabolic process to deodorization, is answered extensively at present For health care product.But at present extract natural chlorophyll cost it is very high, it is artificial synthesized be also it is extremely complex, natural chlorophyll is shown in Light easily decomposes, and extremely unstable easy de-magging and is further formed burnt pheophytin in acid condition, therefore not easy to maintain.Mesh The preceding method mainly having with the magnesium ion in copper, iron, zinc ion substitution porphyrin ring to improve chlorophyll stability.Make in cosmetics With increasingly extensive today, skin heavy metal deposition caused by assorted cosmetics is got worse, therefore is badly in need of a kind of product, in solution State technical problem.
Summary of the invention
For mirror with this, it is an object of the invention to propose that a kind of zinc for chlorophyll facial soap and preparation method thereof, solves above-mentioned Technical problem.
The technical scheme of the present invention is realized as follows:
A kind of zinc is grouped as chlorophyll facial soap by the group of following parts by weight: 31-71 parts of vegetable oil, lye 20-40 Part, 7-13 parts of ethyl alcohol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, zinc is for 0.05-1 parts and essential oil 0.1-3 parts of chlorophyll.
Further, the vegetable oil is grouped as by the group of following parts by weight: 5-15 parts of castor oil, coconut oil 10-20 Part, 10-20 parts of shea butter, 3-8 parts and peanut oil 3-8 parts of SIMMONDSIA CHINENSIS SEED OIL.
Further, the zinc could alternatively be sodium zinc chlorophyllin for chlorophyll.
Further, the lye is the deionized water solution of sodium hydroxide, solution concentration 20-40%wt.
Further, the essential oil be Rosa Damascana, refined jasmine oil, flores aurantii essential oil, enter essential oil, Cananga odorata quintessence oil, fan change The mixture of one or more of essential oil, lavender essential oil, eucalyptus quintessence oil.
Further, the zinc is grouped as chlorophyll facial soap by the group of following parts by weight: 50 parts of vegetable oil, lye 30 parts, 10 parts of ethyl alcohol, 8 parts of sucrose, 2 parts of propylene glycol, zinc is for 0.3 part and 1 part of essential oil of chlorophyll.
Further, the vegetable oil is grouped as by the group of following parts by weight: 10 parts of castor oil, 15 parts of coconut oil, and cream Wooden 15 parts of fruit oil, 5 parts and 5 parts of peanut oil of SIMMONDSIA CHINENSIS SEED OIL.
A kind of zinc is made for chlorophyll facial soap of following steps:
Step 1: by castor oil, coconut oil, shea butter, SIMMONDSIA CHINENSIS SEED OIL, peanut oil at 50-70 DEG C constant temperature 0.4- 0.6h is added lye, and is saponified 2-4h at 60-80 DEG C, obtains vegetable oil mixt；
Step 2: ethyl alcohol, propylene glycol, sucrose being added in step 1 gained vegetable oil mixt, after being sufficiently mixed, in 60- Constant temperature 2-4h at 80 DEG C；
Step 3: step 2 gained mixture is cooled to 40-50 DEG C, addition zinc is for chlorophyll and essential oil, after being sufficiently mixed, It is packed into mold, it is cooling, it cures 2-4 days, packaging.
Compared with prior art, the invention has the benefit that the present invention is added to zinc for chlorophyll, leaf in facial soap Green element zinc sodium salt, can dispel the metal ion of face deposition, protect skin of face, promote skin metabolism, promote skin It repairs, restores skin vitality.
Specific embodiment
For the technical solution in the present invention is clearly and completely described in conjunction with the embodiments, it is clear that inventor says It is bright, but it is only a part of the embodiment of the present invention that following embodiment is described, instead of all the embodiments.Based on the present invention In embodiment, every other implementation obtained by those of ordinary skill in the art without making creative efforts Example, shall fall within the protection scope of the present invention.
A kind of zinc is grouped as chlorophyll facial soap by the group of following parts by weight: 31-71 parts of vegetable oil, lye 20-40 Part, 7-13 parts of ethyl alcohol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, zinc is for 0.05-1 parts and essential oil 0.1-3 parts of chlorophyll.
Further, the vegetable oil is grouped as by the group of following parts by weight: 5-15 parts of castor oil, coconut oil 10-20 Part, 10-20 parts of shea butter, 3-8 parts and peanut oil 3-8 parts of SIMMONDSIA CHINENSIS SEED OIL.
Further, the zinc could alternatively be sodium zinc chlorophyllin for chlorophyll.
Further, the lye is the deionized water solution of sodium hydroxide, solution concentration 20-40%wt.
Further, the essential oil be Rosa Damascana, refined jasmine oil, flores aurantii essential oil, enter essential oil, Cananga odorata quintessence oil, fan change The mixture of one or more of essential oil, lavender essential oil, eucalyptus quintessence oil.
A kind of zinc is made for chlorophyll facial soap of following steps:
Step 1: by castor oil, coconut oil, shea butter, SIMMONDSIA CHINENSIS SEED OIL, peanut oil at 50-70 DEG C constant temperature 0.4- 0.6h is added lye, and is saponified 2-4h at 60-80 DEG C, obtains vegetable oil mixt；
Step 2: ethyl alcohol, propylene glycol, sucrose being added in step 1 gained vegetable oil mixt, after being sufficiently mixed, in 60- Constant temperature 2-4h at 80 DEG C；
Step 3: step 2 gained mixture is cooled to 40-50 DEG C, addition zinc is for chlorophyll and essential oil, after being sufficiently mixed, It is packed into mold, it is cooling, it cures 2-4 days, packaging.
It is formulated according to shown in table 1-2, step made above, configures embodiment 1-5, the facial soap of comparative example 1-6:
Table 1:
Unit Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Castor oil Part 5 8 10 10 15
Coconut oil Part 13 18 20 15 10
Shea butter Part 20 18 15 15 10
SIMMONDSIA CHINENSIS SEED OIL Part 6 3 5 5 8
Peanut oil Part 5 6 8 5 3
Lye Part 32 40 20 30 38
Ethyl alcohol Part 7 10 13 10 11
Sucrose Part 8 5 10 8 12
Propylene glycol Part 1 2 2 2 1
Zinc is for chlorophyll Part —— 1 0.5 0.3 0.05
Sodium zinc chlorophyllin Part 0.5 —— —— —— ——
Essential oil Part 0.1 0.5 2 1 3
Table 2:
120 volunteers for possessing 2 years or more washing products and cosmetic use experience are selected in crowd, are made respectively With the facial soap of embodiment 1-5 and comparative example 1-6, sooner or later twice daily, continuous use is investigated after 1 month, 10 remaining Clear water face cleaning is used only in volunteer, and result is as follows:
Table 3, embodiment 1-5:
Table 4, comparative example 1-6 and control group:
As can be seen that formula used by the application not will cause allergy, according to facial soap prepared by the application formula, make Skin blackhead can be improved after, keep moisture content of skin, and oil-control effect is preferable.
Metal ion test:
Configure Hg2+、Cd2+、Pb2+、Cu2+、As3+And Sb3+Each 100ml of the solution of ion 0.01mol/L chooses new in the market Fresh pork, removal pig hair, after cleaning, the grid of 4*4cm size is drawn on pigskin, dips above 6 kinds of solution with cotton swab respectively, applied Film is on pigskin, and after thoroughly drying, the grid of clip 1*1cm size tests its metal ion content.Then embodiment is used 1-5, comparative example 1-6 and clear water (control group) wash pigskin, clean after drying, the grid of clip 1*1cm size tests it again Metal ion content.After calculating pigskin washing, the percentage that metal ion washes away is averaged after repeating the above experiment 5 times, As shown in Table 5,6.
Table 5, embodiment 1-5:
Metal ion Unit Embodiment 1 Embodiment 2 Embodiment 3 Embodiment 4 Embodiment 5
Hg % 97 100 99 98 95
Cd % 96 95 99 99 98
Pb % 98 99 95 100 98
Cu % 99 96 98 99 98
As % 96 99 100 99 100
Sb % 100 98 99 100 97
Table 6, comparative example 1-6 and control group:
Metal ion Unit Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4 Comparative example 5 Comparative example 6 Control group
Hg % 88 96 87 95 86 79 70
Cd % 85 95 86 99 87 86 69
Pb % 86 94 93 91 88 85 75
Cu % 88 97 90 97 85 83 76
As % 85 98 84 96 90 79 82
Sb % 81 99 86 97 86 80 77
As can be seen that the facial soap being prepared according to the application, can preferably dispel the remaining metal of skin surface Ion gives formula using clear water or beyond the present invention, and the facial soap prepared is poor to dispelling for metal ion.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.

Claims (8)

1. a kind of zinc is for chlorophyll facial soap, which is characterized in that the zinc is for chlorophyll facial soap by the group of following parts by weight Be grouped as: 31-71 parts of vegetable oil, 20-40 parts of lye, 7-13 parts of ethyl alcohol, 5-12 parts of sucrose, 1-2 parts of propylene glycol, zinc is for chlorophyll 0.05-1 parts and essential oil 0.1-3 parts.
2. zinc according to claim 1 is for chlorophyll facial soap, which is characterized in that the vegetable oil is by following parts by weight Group be grouped as: 5-15 parts of castor oil, 10-20 parts of coconut oil, 10-20 parts of shea butter, 3-8 parts of SIMMONDSIA CHINENSIS SEED OIL and peanut oil 3- 8 parts.
3. zinc according to claim 1 is for chlorophyll facial soap, which is characterized in that it is green that the zinc for chlorophyll replaces with leaf Plain zinc sodium salt.
4. zinc according to claim 1 is for chlorophyll facial soap, which is characterized in that the lye be sodium hydroxide go from Sub- aqueous solution, solution concentration 20-40%wt.
5. zinc according to claim 1 is for chlorophyll facial soap, which is characterized in that the essential oil is Rosa Damascana, jasmine Essential oil, flores aurantii essential oil one of enter essential oil, Cananga odorata quintessence oil, Rosemary Oil, lavender essential oil, eucalyptus quintessence oil or several The mixture of kind.
6. zinc according to claim 1 is for chlorophyll facial soap, which is characterized in that the zinc for chlorophyll facial soap by The group of following parts by weight is grouped as: 50 parts of vegetable oil, 30 parts of lye, 10 parts of ethyl alcohol, 8 parts of sucrose, 2 parts of propylene glycol, zinc is green for leaf 0.3 part and 1 part of essential oil of element.
7. zinc according to claim 4 is for chlorophyll facial soap, which is characterized in that the vegetable oil is by following parts by weight Group be grouped as: 10 parts of castor oil, 15 parts of coconut oil, 15 parts of shea butter, 5 parts of SIMMONDSIA CHINENSIS SEED OIL and 5 parts of peanut oil.
8. zinc according to claim 1-7 is for chlorophyll facial soap, which is characterized in that the zinc is for chlorophyll Facial soap is made of following steps:
Step 1: by castor oil, coconut oil, shea butter, SIMMONDSIA CHINENSIS SEED OIL, peanut oil at 50-70 DEG C constant temperature 0.4-0.6h, add Enter lye, and be saponified 2-4h at 60-80 DEG C, obtains vegetable oil mixt；
Step 2: ethyl alcohol, propylene glycol, sucrose being added in step 1 gained vegetable oil mixt, after being sufficiently mixed, at 60-80 DEG C Lower constant temperature 2-4h；
Step 3: step 2 gained mixture being cooled to 40-50 DEG C, zinc is added for chlorophyll and essential oil, after being sufficiently mixed, is packed into Mold, it is cooling, it cures 2-4 days, packaging.
CN201810985045.7A 2018-08-28 2018-08-28 Zinc chlorophyll facial soap and preparation method thereof Active CN109135969B (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61190598A (en) * 1985-02-18 1986-08-25 株式会社　寺尾 Cosmetic soap and its production
CN1857192A (en) * 2006-03-28 2006-11-08 柳州两面针股份有限公司 Application of sodium zinc chlorophyllin in preparing oral cavity care article
US20080317836A1 (en) * 2007-06-19 2008-12-25 Discovery Partners Llc Topical compositions for anti-aging skin treatment
US20120283235A1 (en) * 2009-10-20 2012-11-08 Discovery Partners Llc Dermatologic and Cosmetic Compositions
CN106236687A (en) * 2016-08-26 2016-12-21 广东科玮生物技术股份有限公司 A kind of crease-resistant facial cream of chlorophyll and preparation method thereof
CN108384643A (en) * 2018-03-22 2018-08-10 徐州巨龙新材料科技有限公司 A kind of preparation method of kitchen greasy dirt cleaning agent

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61190598A (en) * 1985-02-18 1986-08-25 株式会社　寺尾 Cosmetic soap and its production
CN1857192A (en) * 2006-03-28 2006-11-08 柳州两面针股份有限公司 Application of sodium zinc chlorophyllin in preparing oral cavity care article
US20080317836A1 (en) * 2007-06-19 2008-12-25 Discovery Partners Llc Topical compositions for anti-aging skin treatment
US20120283235A1 (en) * 2009-10-20 2012-11-08 Discovery Partners Llc Dermatologic and Cosmetic Compositions
CN106236687A (en) * 2016-08-26 2016-12-21 广东科玮生物技术股份有限公司 A kind of crease-resistant facial cream of chlorophyll and preparation method thereof
CN108384643A (en) * 2018-03-22 2018-08-10 徐州巨龙新材料科技有限公司 A kind of preparation method of kitchen greasy dirt cleaning agent

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Effective date of registration: 20230407

Address after: Room 659, Building 7, Entrepreneurship Incubation Base, National University Science Park, Hainan Tropical Ocean University, No.1 Yucai Road, Jiyang District, Sanya City, Hainan Province, 572022

Patentee after: Sanya Rongxiang Technology Co.,Ltd.

Address before: 570100 No.1 Yucai Road, Sanya City, Hainan Province

Patentee before: HAINAN TROPICAL OCEAN University