CN105199882A - Natural handmade soap - Google Patents

Natural handmade soap Download PDF

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Publication number
CN105199882A
CN105199882A CN201510631199.2A CN201510631199A CN105199882A CN 105199882 A CN105199882 A CN 105199882A CN 201510631199 A CN201510631199 A CN 201510631199A CN 105199882 A CN105199882 A CN 105199882A
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China
Prior art keywords
handmade soap
sepiolite
weight
natural handmade
seed
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CN201510631199.2A
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CN105199882B (en
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肖长根
石海信
肖远财
王爱荣
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Ming Liangchangfu Petrochemical Industry Science And Technology Ltd Of Tourist Resources
Qinzhou University
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Ming Liangchangfu Petrochemical Industry Science And Technology Ltd Of Tourist Resources
Qinzhou University
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Abstract

The invention discloses natural handmade soap. The natural handmade soap is made from, by weight, 70-80 parts of soap grains, 10-15 parts of sapindus extract solution, 3-8 parts of aged sepiolite and 2-6 parts of cocamidopropyl betaine. The sapindus extract solution is prepared by steps: soaking dry sapindus fruits in warm water 5-10 times of the dry sapindus fruits in weight, boiling, extracting until specific gravity of the obtained extract solution is 1.0-1.2, and filtering to obtain the sapindus extract solution. The aged sepiolite is prepared by steps: grinding alpha sepiolite, adding water to ageing for 7-10 days, filtering, adding lime solution with the mass concentration being 1-1.5% into filter residues to soak for 7-10 days, filtering, drying filter residues and grinding to obtain the aged sepiolite. The natural handmade soap has the advantages of effectiveness in skin cleaning and bactriostasis and low skin irritation.

Description

A kind of natural handmade soap
Technical field
The present invention relates to a kind of daily articles for washing, be specifically related to a kind of natural handmade soap.
Background technology
Conventional toilet soaps is main component mainly with sodium soap, and the general pH value of soap body is higher, although there is higher cleaning capacity, too large to the pungency of skin, washes that rear skin is dry, skinfeel is poor, not resistance to hard water, and washes rear skin and can produce tight sense.
Seed of Chinese Soapberry tree has another name called soap tree, and main product is in Southeast Asian countries, and all there is cultivation in the Yangtze valley of China, southern each province and Hainan Island.Sapindoside can reduce the surface tension of water, has good whipability, strong detergency, and has the features such as sterilization, antipruritic, fragrance is pure, also has certain radiation resistance.Brighten in emulsion the effective constituent that can be used as restraint of tyrosinase activity, also can be used on the effective constituent as natural active matter in natural shampoo and various cleaning and protecting skin makeup (as cleansing milk, brightening emulsion).
Publication number is the patent of invention of CN102199500A, disclose a kind of formula and making method of Sapindus handmade soap, specifically fat acyloxy ethylsulfonic acid sodium, neat soap, AMONYL 380LC, fat acyloxy ethylsulfonic acid sodium and Seed of Chinese Soapberry water are extracted concentrated solution mix and blend to dissolve, add stearic acid, TETRADECONIC ACID, laurostearic acid dissolving again, add the sweet amino proline of methyl, Flos Rosae Rugosae quintessence oil stirs, fully dissolve after fixing and obtain.Publication number is that the patent of invention of CN102533479A also discloses similar technical scheme.These two inventions are all the main source of extracting solution as saponin(e in handmade soap of Seed of Chinese Soapberry pericarp, have streptococcus aureus, Salmonellas and colibacillus and kill and restraining effect,, foaming exquisiteness very gentle to skin, effectively alleviate chemical substance to injure the stimulation of skin, reduce the degree of aging of skin.But they with to play the clay that Adsorption of Heavy Metal Ions etc. acts on composite, cannot not reach better cleaning skin effect.
Summary of the invention
The technical problem to be solved in the present invention is to provide one can play effective cleaning skin and bacteriostatic action, and the natural handmade soap few to skin irritation.
Natural handmade soap of the present invention, by weight, comprises the component of following weight parts:
Sepiolite 3-8 part after neat soap 70-80 part, Seed of Chinese Soapberry extracting solution 10-15 part, ripening, AMONYL 380LC 2-6 part; Wherein,
Described Seed of Chinese Soapberry extracting solution is prepared by the following method: get dry Seed of Chinese Soapberry fruit, adds and is equivalent to its weight 5-10 warm water soaking doubly, then boil extraction, until the proportion of gained extracting solution is 1.0-1.2, stop extracting, filter, namely obtain Seed of Chinese Soapberry extracting solution;
Sepiolite after described ripening is prepared by the following method: get α sepiolite, pulverizes, soaks 7-10 days, filters, and adds the lime solution immersion 7-10 days that mass concentration is 1-1.5%, filter, filter residue and drying, pulverize, to obtain final product in gained filter residue.
Sepiolite after Seed of Chinese Soapberry extracting solution and ripening carries out composite by the present invention, necessary neat soap and AMONYL 380LC is coordinated to obtain handmade soap again, wherein contain forulic acid in Seed of Chinese Soapberry extracting solution, nicotinic acid, the effective constituents such as phenolic acid etc. tens seed amino acid and natural beauty capacity factor, utilize sepiolite surface-area large, special crystalline structure, heterogeneity charge distribution and characterization of adsorption, the organic substance in Seed of Chinese Soapberry extracting solution is made to be adsorbed in sepiolite, sustained release in follow-up use procedure, not only effectively can remove the grease on skin, dust etc., the heavy metal ion of skin surface attachment can also be removed, reach effective cleaning skin, antibacterial object, and skin is not stimulated, use rear skin wet, not tight.
In technique scheme, the weight proportion of each component is preferably: neat soap 75-80 part, Seed of Chinese Soapberry extracting solution 12-15 part, sepiolite 3-5 part, AMONYL 380LC 2-4 part.
In technique scheme, in the preparation method of described Seed of Chinese Soapberry extracting solution, warm water is generally the water that temperature is 40-60 DEG C, and the time that warm water is soaked is generally 12-24h.
In technique scheme, in the preparation method of the sepiolite after described ripening, the add-on of water is soaking the water yield required for 7-10 days for meeting α sepiolite, generally, the α sepiolite of 1kg needs the water adding 10-15kg could meet 1kg α sepiolite to soak 7-10 days under normal temperature condition.The add-on of lime solution is after water soaking, filter the 1-3% of gained filter residue weight.Described lime solution be by according to concentration requirement a certain amount of unslaked lime is placed in water dissolve should and obtain.
In order to make natural handmade soap of the present invention have better humidity-holding effect, a certain amount of wetting Agent for Printing Inks can also be added in formula.Preferably, natural handmade soap of the present invention also comprises the wetting Agent for Printing Inks of 2-5 weight part, and the preferred consumption of described wetting Agent for Printing Inks is 2-3 weight part.The selection of described wetting Agent for Printing Inks is same as the prior art, can be specifically one or more the combination be selected from glycerine, propylene glycol and sorbyl alcohol.
In order to make natural handmade soap of the present invention have better skin effect, a certain amount of skin-protecting agent can also be added in formula.Preferably, natural handmade soap of the present invention also comprises the skin-protecting agent of 2-5 weight part, and the preferred consumption of described skin-protecting agent is 2-3 weight part.The selection of described skin-protecting agent is same as the prior art, can be specifically one or more the combination be selected from glycerine, honey and milk.
According to the demand of reality, natural handmade soap of the present invention can also comprise the essential oil of 0.1-1 weight part again, preferably includes the essential oil of 0.3-0.7 weight part.The selection of described essential oil is same as the prior art, can be specifically to be selected from one or more the combination in Flos Rosae Rugosae quintessence oil, osmanthus essential oil, jasmin quintessence oil and peppermint essence wet goods.
In technical scheme of the present invention, the granularity of the sepiolite after described ripening is preferably 80-120 order, is more preferably 100-120 order.
The preparation method of natural handmade soap of the present invention is same as the prior art.Preferably be prepared by the following method:
1) get dry Seed of Chinese Soapberry fruit, add and be equivalent to its weight 5-10 warm water soaking doubly, then boil extraction, until the proportion of gained extracting solution is 1.0-1.2, stops extracting, filter, obtain Seed of Chinese Soapberry extracting solution, for subsequent use;
2) get α sepiolite, pulverize, soak 7-10 days, filter, in gained filter residue, add the lime solution immersion 7-10 days that mass concentration is 1-1.5%, filter, filter residue and drying, pulverize, namely obtain the sepiolite after ripening, for subsequent use;
3) by weight, take the sepiolite 3-8 part after neat soap 70-80 part, Seed of Chinese Soapberry extracting solution 10-15 part, ripening and AMONYL 380LC 2-6 part (if also having the words of other component to take in the lump) and be placed in container, pour into after stirring in mould, complete curing and demolding, to obtain final product.
Compared with prior art, feature of the present invention is:
1, sepiolite after Seed of Chinese Soapberry extracting solution and ripening is carried out composite, necessary neat soap and AMONYL 380LC is coordinated to obtain handmade soap again, wherein contain forulic acid in Seed of Chinese Soapberry extracting solution, nicotinic acid, the effective constituents such as phenolic acid etc. tens seed amino acid and natural beauty capacity factor, utilize sepiolite surface-area large, special crystalline structure, heterogeneity charge distribution and characterization of adsorption, the organic substance in Seed of Chinese Soapberry extracting solution is made to be adsorbed in sepiolite, sustained release in follow-up use procedure, not only effectively can remove the grease on skin, dust etc., the heavy metal ion of skin surface attachment can also be removed, reach effective cleaning skin, antibacterial object, and it is few to skin irritation, use rear skin wet, not tight,
2, by the obtained handmade soap pH value of formula of the present invention between 7.0-8.0, foaming is fine and smooth.
Embodiment
Below in conjunction with specific embodiment, the present invention is described in further detail, and to understand content of the present invention better, but the present invention is not limited to following examples.
Embodiment 1
1) get dry Seed of Chinese Soapberry fruit, add the warm water (40-50 DEG C) being equivalent to its weight 9 times and soak 24h, then boil extraction, until the proportion of gained extracting solution is 1.1, stops extracting, filter, obtain Seed of Chinese Soapberry extracting solution, for subsequent use;
2) α sepiolite is got, be crushed to 100-120 order, add the water soaking 10 days being equivalent to its weight 10 times, filter, add in gained filter residue mass concentration be 1.5% lime solution (add-on of lime solution is 2% of aforementioned filter residue weight) soak 7 days, filter, filter residue and drying, be crushed to 100-120 order, namely obtain the sepiolite after ripening, for subsequent use;
3) by weight, take the sepiolite 3 parts after neat soap 75 parts, Seed of Chinese Soapberry extracting solution 15 parts, ripening and AMONYL 380LC 4 parts is placed in container, pour in mould after stirring, the demoulding after solidification 12h, to obtain final product.
After testing, the handmade soap pH value that the present embodiment is obtained is between 7.0-7.3.
Embodiment 2
1) with the step 1 of embodiment 1);
2) with the step 2 of embodiment 1);
3) by weight, take the sepiolite 6 parts after neat soap 80 parts, Seed of Chinese Soapberry extracting solution 10 parts, ripening, AMONYL 380LC 6 parts and glycerine 3 parts and be placed in container, pour in mould after stirring, the demoulding after solidification 12h, to obtain final product.
After testing, the handmade soap pH value that the present embodiment is obtained is between 7.2-7.5.
Embodiment 3
1) with the step 1 of embodiment 1);
2) with the step 2 of embodiment 1);
3) by weight, take the sepiolite 8 parts after neat soap 70 parts, Seed of Chinese Soapberry extracting solution 12 parts, ripening, AMONYL 380LC 2 parts, sorbyl alcohol 5 parts and honey 3 parts and be placed in container, pour into after stirring in mould, the demoulding after solidification 12h, to obtain final product.
After testing, the handmade soap pH value that the present embodiment is obtained is between 7.2-7.5.
Embodiment 4
1) get dry Seed of Chinese Soapberry fruit, add the warm water (50-55 DEG C) being equivalent to its weight 10 times and soak 12h, then boil extraction, until the proportion of gained extracting solution is 1.2, stops extracting, filter, obtain Seed of Chinese Soapberry extracting solution, for subsequent use;
2) α sepiolite is got, be crushed to 80-100 order, add the water soaking 7 days being equivalent to its weight 15 times, filter, add in gained filter residue mass concentration be 1% lime solution (add-on of lime solution is 3% of aforementioned filter residue weight) soak 10 days, filter, filter residue and drying, be crushed to 100-120 order, namely obtain the sepiolite after ripening, for subsequent use;
3) by weight, take the sepiolite 5 parts after neat soap 78 parts, Seed of Chinese Soapberry extracting solution 14 parts, ripening, AMONYL 380LC 3 parts, propylene glycol 2 parts, honey 2 parts and Flos Rosae Rugosae quintessence oil 0.5 part and be placed in container, pour into after stirring in mould, the demoulding after solidification 12h, to obtain final product.
After testing, the handmade soap pH value that the present embodiment is obtained is between 7.6-8.0.
Embodiment 5
1) get dry Seed of Chinese Soapberry fruit, add the warm water (40-45 DEG C) being equivalent to its weight 6 times and soak 20h, then boil extraction, until the proportion of gained extracting solution is 1.0, stops extracting, filter, obtain Seed of Chinese Soapberry extracting solution, for subsequent use;
2) α sepiolite is got, be crushed to 80-100 order, add the water soaking 8 days being equivalent to its weight 12 times, filter, add in gained filter residue mass concentration be 1.2% lime solution (add-on of lime solution is 1% of aforementioned filter residue weight) soak 9 days, filter, filter residue and drying, be crushed to 100-120 order, namely obtain the sepiolite after ripening, for subsequent use;
3) by weight, take the sepiolite 4 parts after neat soap 72 parts, Seed of Chinese Soapberry extracting solution 15 parts, ripening, AMONYL 380LC 5 parts, propylene glycol 4 parts, honey 5 parts and jasmin quintessence oil 1 part and be placed in container, pour into after stirring in mould, the demoulding after solidification 12h, to obtain final product.
After testing, the handmade soap pH value that the present embodiment is obtained is between 7.0-7.2.
The handmade soap obtained by method described in embodiment 1-5 is sent Guangxi Zhuang Autonomous Region light industrial goods quality monitoring testing station with QB/T2485-2008 " perfumed soap " for according to detecting, result as described in Table 1:
Table 1:

Claims (8)

1. a natural handmade soap, by weight, comprises the component of following weight parts:
Sepiolite 3-8 part after neat soap 70-80 part, Seed of Chinese Soapberry extracting solution 10-15 part, ripening, AMONYL 380LC 2-6 part; Wherein,
Described Seed of Chinese Soapberry extracting solution is prepared by the following method: get dry Seed of Chinese Soapberry fruit, adds and is equivalent to its weight 5-10 warm water soaking doubly, then boil extraction, until the proportion of gained extracting solution is 1.0-1.2, stop extracting, filter, namely obtain Seed of Chinese Soapberry extracting solution;
Sepiolite after described ripening is prepared by the following method: get α sepiolite, and pulverize, add water ageing 7-10 days, filters, and adds the lime solution immersion 7-10 days that mass concentration is 1-1.5%, filter, filter residue and drying, pulverize, to obtain final product in gained filter residue.
2. natural handmade soap according to claim 1, is characterized in that: the weight proportion of each component is:
Neat soap 75-80 part, Seed of Chinese Soapberry extracting solution 12-15 part, sepiolite 3-5 part, AMONYL 380LC 2-4 part.
3. natural handmade soap according to claim 1 and 2, is characterized in that: this natural handmade soap also comprises the wetting Agent for Printing Inks of 2-5 weight part.
4. natural handmade soap according to claim 3, is characterized in that: described wetting Agent for Printing Inks is selected from one or more the combination in glycerine, propylene glycol and sorbyl alcohol.
5. natural handmade soap according to claim 3, is characterized in that: this natural handmade soap also comprises the skin-protecting agent of 2-5 weight part.
6. natural handmade soap according to claim 5, is characterized in that: described skin-protecting agent is one or more the combination be selected from glycerine, honey and milk.
7. natural handmade soap according to claim 3, is characterized in that: this natural handmade soap also comprises the essential oil of 0.1-1 weight part.
8. natural handmade soap according to claim 7, is characterized in that: described essential oil is one or more the combination in Flos Rosae Rugosae quintessence oil, osmanthus essential oil, jasmin quintessence oil and Peppermint essential oil.
CN201510631199.2A 2015-09-29 2015-09-29 A kind of natural handmade soap Active CN105199882B (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106398878A (en) * 2016-08-19 2017-02-15 跨越生物科技(滁州)有限公司 Congealed fat essential oil handmade soap with effects of skin soothing and convergence
CN107603779A (en) * 2017-09-22 2018-01-19 广西巧恩茶业有限公司 A kind of jasmine essential oil soap
CN108102824A (en) * 2017-12-18 2018-06-01 郭舒洋 A kind of preparation method of Multifunctional fancy soap
CN109777676A (en) * 2019-03-18 2019-05-21 惠州市旭东实业有限公司 A kind of craft facial soap

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010016083A (en) * 2000-10-31 2001-03-05 채장식 soap components containing sepiolite, talc and wood tar
CN102199500A (en) * 2011-04-22 2011-09-28 江西金乔园林有限公司 Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20010016083A (en) * 2000-10-31 2001-03-05 채장식 soap components containing sepiolite, talc and wood tar
CN102199500A (en) * 2011-04-22 2011-09-28 江西金乔园林有限公司 Formula of Chinese soapberry fruit handmade soap and method for preparing Chinese soapberry fruit handmade soap

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
邓庚凤等: "海泡石的性能及其应用", 《江西科学》 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106398878A (en) * 2016-08-19 2017-02-15 跨越生物科技(滁州)有限公司 Congealed fat essential oil handmade soap with effects of skin soothing and convergence
CN107603779A (en) * 2017-09-22 2018-01-19 广西巧恩茶业有限公司 A kind of jasmine essential oil soap
CN108102824A (en) * 2017-12-18 2018-06-01 郭舒洋 A kind of preparation method of Multifunctional fancy soap
CN109777676A (en) * 2019-03-18 2019-05-21 惠州市旭东实业有限公司 A kind of craft facial soap

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