CN109125115A - A kind of element face is spraying and preparation method thereof - Google Patents
A kind of element face is spraying and preparation method thereof Download PDFInfo
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- CN109125115A CN109125115A CN201811118040.0A CN201811118040A CN109125115A CN 109125115 A CN109125115 A CN 109125115A CN 201811118040 A CN201811118040 A CN 201811118040A CN 109125115 A CN109125115 A CN 109125115A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/24—Phosphorous; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4946—Imidazoles or their condensed derivatives, e.g. benzimidazoles
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/58—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing atoms other than carbon, hydrogen, halogen, oxygen, nitrogen, sulfur or phosphorus
- A61K8/585—Organosilicon compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
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Abstract
The present invention discloses that a kind of plain face is spraying and preparation method thereof, and the element face is spraying comprising following component: acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer, Xylitol-based glucoside/anhydro xylitol/xylitol and tourmaline.Acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer, Xylitol-based glucoside/anhydro xylitol/xylitol and tourmaline are arranged in pairs or groups simultaneously when using, spraying effect performance is best, not only has effects that preferable concealing and oil-control, also have effects that long-acting moisturizing and improve the colour of skin, and is good using skin sense.Plain face of the invention has atomization ejection effect well by spraying, will not reunite, and when being sprayed on skin, salubrious comfortable skin sense can be brought to user.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of element face is spraying and preparation method thereof.
Background technique
With social progress and development and the increasingly raising of people's living standard, cosmetics have more and more become existing
For indispensable a part in people's life.Currently, cosmetic industry has entered the high-speed developing period, along with various cosmetics
Type it is more and more, there is spraying (aerosol) the dosage form makeup pint grain husk of many advantages, such as easy to use, time saving, effect is good and
Out, increasingly by public approval and like, also more meet the compact modern Man's Demands of rhythm of life.
In recent years, the market share of global spray cosmetics continues solid growth, European spray alliance FEA in 2017
Data show that personal nursing spray accounts for the 61% of spray production, Chinese packaging federation spray professional committee member
The data of meeting show that Chinese personal nursing spray yield is about 3.5 hundred million tanks, it is contemplated that Chinese personal nursing in 5 years from now on is spraying
Agent market and product will exponentially increase.It can be seen that spray Cosmetic Market has good development prospect.However, mesh
There is also a little deficiencies for preceding spray cosmetics on the market, and if function is incomplete, skin-protecting function is single, is not met by use
The skin care demand at family is also left to be desired to user's bring usage experience sense.
Summary of the invention
It is an object of the invention to overcome above-mentioned shortcoming and defect of the existing technology, provide a kind of plain face it is spraying and its
Preparation method.
To achieve the above object, the technical scheme adopted by the invention is as follows:
A kind of element face is spraying comprising following component: acrylic acid (ester) class/C12-22 alkanol methacrylate copolymers
Object, Xylitol-based glucoside/anhydro xylitol/xylitol and tourmaline.
During plain face of the invention is spraying, the reasonable complementary synergistic component of a variety of proportions is used, this hair is effectively improved
The spraying effect performance of bright element face.
Wherein, acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer, trade name SP-7 thickener can
Purchased from the glad Chemical Industry Science Co., Ltd of upper oceanic rise.Acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer is spraying
It can be used as pseudoplastic behavior thickener in Material, spraying Material is enable to become diluter viscosity when being sheared by external force and can be atomized,
It can restore consistency under static state, solve the defect for having the Material of consistency that can not be atomized ejection in the market.Simultaneously as third
Olefin(e) acid (ester) class/C12-22 alkanol methacrylate copolymer is more sensitive to electrolyte, to make after being sprayed on skin by spraying
It can quickly melt, bring salubrious sense to user.In addition, acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer
It also will form one layer of uniform film in skin surface, to extend the spraying moistening effect to skin.
Xylitol-based glucoside/anhydro xylitol/xylitol, trade name AQUAXYL are purchased from hundred and win limited public affairs well
Department.Xylitol-based glucoside/anhydro xylitol/xylitol is the active constituent of natural botanical source, being capable of moisturizing and reconstruction skin
Skin structural system promotes the increase of hyaluronic acid and content of chondroitin sulfate, improves the moisture content of epidermis and corium, promotes mind
Synthesis through amide reinforces skin barrier effect, improves skin texture, reduces skin water loss.
Tourmaline also known as tourmaline are purchased from Guangzhou Ao Xue Chemical Co., Ltd..It can promote capillary blood is micro- to follow
Ring increases skin temperature, improves the colour of skin of skin, allows skin to restore honorable, shows the healthier more radiant colour of skin.
Inventor is by series of studies discovery, acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer, xylose
Alcohol radical glucoside/anhydro xylitol/xylitol and tourmaline are arranged in pairs or groups in use, spraying effect performance is best simultaneously, are not only had
Preferable concealing and oil-control effect also have effects that long-acting moisturizing and improve the colour of skin, and use skin sense good.Inventor is by system
Column research also found that acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer and Xylitol-based glucoside/dehydration are wooden
Sugar alcohol/xylitol compounding, can generate synergistic function, can significantly improve spraying moisturizing and oil-control effect.
Preferably, the plain face includes the component of following weight percentage: acrylic acid (ester) class/C12-22 alkanol by spraying
Methacrylate copolymer 0.1%~1%, Xylitol-based glucoside/anhydro xylitol/xylitol 1%~5%, Yi Jibi
Imperial or royal seal 0.5%~3%.
Preferably, acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer and Xylitol-based glucoside/
Anhydro xylitol/xylitol weight ratio is 0.5:3.Acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer with
When Xylitol-based glucoside/anhydro xylitol/xylitol is with proportion compounding, spraying moisturizing and oil-control effect are best.
Preferably, the plain face further includes the component of following weight percentage by spraying: emulsifier 2%~4% and helping cream
Agent 0.6%~4%；The assistant for emulsifying agent includes assistant for emulsifying agent A and assistant for emulsifying agent B.
The emulsifier, INCI entitled " PPG-10 cetyl ether phosphate, -8 phosphoric acid of two C12-15 Pareths
Ester ", No. CAS is " 6640-03-5 ", and trade name 94W is purchased from the glad Chemical Industry Science Co., Ltd of oceanic rise.94W has powder
Brilliant dispersion resistant to aggregation ability can effectively avoid product and generate agglomeration when smearing or being atomized and spray, meanwhile, also have
There is excellent anti-sweat water resistant to wash ability, can effectively extend and hold adornment effect.
The assistant for emulsifying agent A, INCI entitled " water, two (oleth -8) sodium phosphates, DMDM hydantoin ", commodity
Entitled APK-30 is purchased from the glad Chemical Industry Science Co., Ltd of oceanic rise.The assistant for emulsifying agent B, INCI entitled " water, acrylic acid
- 20 itaconate copolymeric of (ester) class/stereth, PEG-30 glycerol monolaurate, Phenoxyethanol, methyl hydroxybenzoate ", commodity
Entitled WD-4 is purchased from the glad Chemical Industry Science Co., Ltd of oceanic rise.APK-30 and WD-4 is conducive to the dispersion of powder and resists again
Aggregation, APK-30, WD-4 and 94W three and used time can make spraying atomization spray effect more preferable.
Preferably, the weight ratio of the assistant for emulsifying agent A and assistant for emulsifying agent B is 0.1~1:0.5~3.Assistant for emulsifying agent A with help
When emulsifier B is with proportion compounding, the dispersion of spraying Material and resistant to aggregation effect are preferable.
Most preferably, the weight ratio of the assistant for emulsifying agent A and assistant for emulsifying agent B is 1:2.Assistant for emulsifying agent A and assistant for emulsifying agent B with
When the proportion compounds, the dispersion of spraying Material and resistant to aggregation effect are best.
Preferably, the plain face further includes the component of following weight percentage: physical sunscreen agent 1%~8% by spraying.Institute
Stating physical sunscreen agent is siloxane treated titanium dioxide, INCI entitled " titanium dioxide (and) siloxanes ", trade name
SUNTITAN-AS is purchased from Guangzhou Hua Tu cosmetics Science and Technology Ltd..Spraying material of the SUNTITAN-AS in inventive formulation
There is excellent dispersibility in body, and titanium dioxide cohesion and light-catalyzed reaction will not occur, ultraviolet light can be reflected for a long time, had
There is good sun-proof result.
Preferably, the plain face further includes the component of following weight percentage: active additive 0.2%~3% by spraying.
The INCI of the active additive entitled " water/butanediol/pungent glycol/1,2- ethylene glycol/Margarita extract ", trade name is black
Margarita extract is purchased from hundred Hao Bo Co., Ltds.Black pearl extract is from Pinna pectinata mother-of-peal (identical as pearl component)
In the active constituent isolated, amino acid and organic principle rich in have moisturizing, whitening and anti-aging effects.
Preferably, the plain face further includes the component of following weight percentage: emollient 2%~20% by spraying, described
Emollient includes isobutyl palmitate and No. 15 white oils.Wherein, the trade name 2EHP of isobutyl palmitate, is purchased from Guangzhou
Wan Lu Chemical Co., Ltd., performance are stablized, and not oxidizable or generation peculiar smell can make skin soft soft without greasy feeling, seep
Permeability is good, also has antiperspirant effect, can also improve the dispersibility of other components.No. 15 white oils are cosmetics-stage, and INCI is entitled
" dormant oil " has moisturizing effect.Preferably, the weight ratio of the isobutyl palmitate and No. 15 white oils is 1~10:1~10.Most
Preferably, the weight ratio of isobutyl palmitate and No. 15 white oils is 1:1.
A kind of element face is spraying, is grouped as by the group of following weight percentage: acrylic acid (ester) class/C12-22 alkanol first
Base acrylate copolymer 0.1%~1%, Xylitol-based glucoside/anhydro xylitol/xylitol 1%~5%, tourmaline 0.5%
~3%, 94W emulsifier 2%~4%, APK-30 assistant for emulsifying agent 0.1%~1%, WD-4 assistant for emulsifying agent 0.5%~3%,
1%~10%, No. 15 SUNTITAN-AS 1%~8%, black pearl extract 0.2%~3%, isobutyl palmitate white oil 1%
~10%, pH adjusting agent 0.2%~1%, corrosion inhibiter 0.1%~2%, preservative 0.3%~1%, essence 0.005%~
0.02% and deionized water surplus.
Preferably, the plain face is spraying is grouped as by the group of following weight percentage: acrylic acid (ester) class/C12-22 alkane
Alcohol methacrylate copolymer 0.5%, Xylitol-based glucoside/anhydro xylitol/xylitol 3%, tourmaline 2.5%, 94W cream
Agent 3%, APK-30 assistant for emulsifying agent 0.5%, WD-4 assistant for emulsifying agent 1%, SUNTITAN-AS 4%, black pearl extract 1%,
5%, No. 15 white oil 5% of isobutyl palmitate, pH adjusting agent 0.5%, corrosion inhibiter 1%, preservative 0.5%, essence 0.01%, with
And deionized water surplus.
Preferably, the pH adjusting agent is triethanolamine.The INCI of the corrosion inhibiter entitled " phosphorus sodium calcium silicate, phosphoric acid
Ammonium dihydrogen ", trade name NTD-6A are purchased from the glad Chemical Industry Science Co., Ltd of oceanic rise.It is spraying that NTD-6A is added to the present invention
In formula, other component effects of formula will not be impacted, that is, will not influence the using effect of product, moreover it is possible to effectively prevent
Spraying in-tank corrosion.The INCI of the preservative entitled " Phenoxyethanol/methyl hydroxybenzoate/ethyl hydroxy benzoate/Sensiva SC50 ",
Trade name K350 is purchased from hundred Hao Bo Co., Ltds.
Preferably, the spraying preparation method of the plain face, includes the following steps:
(1) 94W emulsifier, APK-30 assistant for emulsifying agent, SUNTITAN-AS, isobutyl palmitate, tourmaline, No. 15 white oils
Mixing, and 75~80 DEG C are heated to, obtain mixture A；
(2) deionized water, acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer, WD-4 assistant for emulsifying agent
Mixing, and 75~80 DEG C are heated to, obtain mixture B；
(3) mixture A is added in mixture B, is stirred evenly, and 3~5min of high speed homogenization, pH is then added and adjusts
Agent, stirring cooling；
(4) it when the Material that step (3) obtains is cooled to 45 DEG C, is added in advance with water-soluble good corrosion inhibiter, then successively
Xylitol-based glucoside/anhydro xylitol/xylitol, black pearl extract, preservative, essence is added, stirs evenly, discharges,
It is spraying up to the plain face.
Compared with prior art, the beneficial effects of the present invention are: plain face of the invention to have atomization spray well by spraying
Effect out will not reunite, and when being sprayed on skin, salubrious comfortable skin sense can be brought to user.Plain face of the invention is spraying
Also there is preferable concealing and long-acting moisture-keeping efficacy, can control skin ingress of oil and improve the obscure phenomenon of skin.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further, but the present invention is not limited to following embodiments.It is worth noting that, unless otherwise indicated, it is used herein
Various components be this field current material, can by commercial channel buy obtain or by existing method be made.
The formula (weight percentage/%) of Examples 1 to 8 is as shown in the table:
Above embodiments 1~8 the preparation method is as follows:
(1) 94W, APK-30, SUNTITAN-AS, 2EHP, tourmaline, No. 15 white oil mixing, and 75~80 DEG C are heated to,
Obtain mixture A；
(2) deionized water, SP-7 thickener, WD-4 are mixed, and is heated to 75~80 DEG C, obtain mixture B；
(3) mixture A is added in mixture B, is stirred evenly, and 3~5min of high speed homogenization, pH is then added and adjusts
Agent, stirring cooling；
(4) it when the Material that step (3) obtains is cooled to 45 DEG C, is added in advance with water-soluble good NTD-6A, then successively
AQUAXYL, black pearl extract, K350, essence is added, stirs evenly, discharging is spraying to get plain face.
The formula (weight percentage/%) of comparative example 1~6 is as shown in the table:
The trade name SIMULGEL for the common thickener that comparative example usesTMFL (INCI title are as follows: hydroxy-ethyl acrylate/
Sodium acryloyldimethyl taurate copolymers (and) isohexadecane (and) polysorbate -60), it is good rich to be purchased from hundred.
Preparation method of the preparation method of comparative example 1~6 referring to above-described embodiment 1~8.
Experiment effect evaluation
One, measure of merit is sprayed
Method: respectively using the plain face of embodiment 1,2,3,4,7 and 8 and comparative example 1~4 by spraying as trial target.Examination
It tests product to put into respectively in binary spray bottle, claim the weight of first time respectively and records, this weight is total weight.Pressing two
The pump head of first spray bottle all ejects trial target, even if also can not spray thing until pressing pump head, claims second respectively
Secondary weight is simultaneously recorded, this weight is remaining weight.Emission rate is calculated, to evaluate the spraying ejection effect of plain face.
Emission rate=(total weight-remaining weight)/total weight × 100%
As a result as shown in the table:
The above results show: the plain face of embodiment all has preferable ejection effect by spraying, wherein the ejection effect of embodiment 1
Fruit is best.Comparing embodiment 1, embodiment 7 and embodiment 8 are it is found that when APK-30 is compounded with WD-4 with the proportion of 1:2, element
The spraying ejection effect of face is best, illustrates that the dispersion for being sprayed Material at this time and resistant to aggregation effect are best.Comparing embodiment 1, comparison
Example 1 and comparative example 4 are it is found that SP-7 thickener can obviously improve spraying ejection effect, with other common thickeners substitution SP-7
When thickener, spraying ejection effect is poor.Comparing embodiment 1, comparative example 2 and comparative example 3 are it is found that APK-30, WD-4 and 94W
Three and used time can make spraying atomization spray effect more preferable.
Two, efficacy test
Test one: respectively using the plain face of Examples 1 to 6 and comparative example 4~6 by spraying as trial target.Selection 270 is same
Area, age bracket were 18~35 one full year of life, the colour of skin is obscure, mixed type skin quality and the women white collar with freckle are as subject, were put down
It is divided into 9 groups, number is group 1~groups 9.For every group of subject in cleaning face and after smearing with a lotion, group 1 uses embodiment
1 trial target, organizes 2 trial targets for using embodiment 2, and group 3 organizes 4 tests for using embodiment 4 using the trial targets of embodiment 3
Product, group 5 use the trial target of embodiment 5, and group 6 is using the trial targets of embodiment 6, and using the trial target of comparative example 4, organize 8 makes group 7
With the trial target of comparative example 5, group 9 uses the trial target of comparative example 6, and the usage amount of each subject per is 0.5g.It applies
After having smeared, observe concealing effect, if concealing effect it is good and from then make 8~10 scores, if concealing effect it is preferable and relatively oneself then make a call to 5
~7, if concealing effect is bad and not enough certainly then makes a call to 1~4；Trial target is coated with using pressing lightly on respectively with a cotton pads
Skin surface, observe cotton pads on whether be stained with trial target, if hardly adhering to give a mark 8~10 points, if slight adhesion
Then give a mark 5~7 points；It gives a mark 1~4 point if adherency is more；Make smearing after the daily face cleaning on daytime of above-mentioned subject primary corresponding
Trial target, persistently using the health status for observing every group of subject's skin of face after one month, one month.
Test result is as follows shown in table:
| Group | Concealing, natural effect | Docile degree | One month rear face skin conditions |
| 1 (embodiment 1) of group | 9.5 | 9.3 | The colour of skin becomes ruddy and water moistens |
| 2 (embodiments 2) of group | 9.3 | 9.0 | The colour of skin becomes ruddy and water moistens |
| 3 (embodiments 3) of group | 9.1 | 8.8 | The colour of skin becomes ruddy and water moistens |
| 4 (embodiments 4) of group | 9.3 | 8.6 | The colour of skin becomes ruddy and water moistens |
| 5 (embodiments 5) of group | 9.2 | 9.1 | The colour of skin becomes ruddy and water moistens |
| 6 (embodiments 6) of group | 9.0 | 8.9 | The colour of skin becomes ruddy and water moistens |
| 7 (comparative examples 4) of group | 4.8 | 5.3 | The colour of skin becomes more ruddy, but water does not moisten |
| 8 (comparative examples 5) of group | 4.1 | 3.3 | The colour of skin becomes more ruddy, but water does not moisten |
| 9 (comparative examples 6) of group | 8.9 | 8.7 | The colour of skin is still obscure |
The above results show: the plain face of embodiment all have by spraying it is preferable cover freckle effect and concealing effect naturally,
Docile degree is high, and the plain face that embodiment is used for a long time is spraying, can also improve the obscure phenomenon of skin, so that skin is become water profit, especially
It is best with the effect of embodiment 1.
Comparing embodiment 1, embodiment 5 and embodiment 6 are it is found that SP-7 thickener is compounded with AQUAXYL with the proportion of 0.5:3
When, spraying using effect is best.
Comparing embodiment 1 and comparative example 4~6 are it is found that SP-7 thickener, AQUAXYL and tourmaline are arranged in pairs or groups simultaneously in use, spray
The effect of mist, performance was best, had natural concealing effect, and can improve the colour of skin.Comparative example 4 and comparative example 5 are due to lacking SP-7
Thickener or AQUAXYL cause spraying moistening effect to be affected, and skin cannot keep water profit, to also influence spraying
Concealing effect cannot reach good concealing, be easy picking.Comparative example 6 causes to be unable to improve the colour of skin by spraying due to lacking tourmaline
Obscure phenomenon.
Test two: respectively using the plain face of Examples 1 to 6 and comparative example 4~6 by spraying as trial target.Selection 270 is same
Area, age bracket were 18~35 one full year of life, the colour of skin is obscure, mixed type skin quality and the women white collar with freckle are as subject, were put down
It is divided into 9 groups, number is group 1~groups 9.Every group of subject carries out skin water after cleaning face, to every group of subject respectively
Divide and test, after average treatment, records every group of the initial moisture value of skin；Then trial target of the group 1 using embodiment 1,2 use of group
The trial target of embodiment 2, group 3 organize 4 trial targets for using embodiment 4 using the trial target of embodiment 3, and group 5 uses embodiment 5
Trial target, group 6 using embodiment 6 trial targets, group 7 using comparative example 4 trial targets, group 8 using comparative example 5 tests
Product, group 9 uses the trial target of comparative example 6, and the usage amount of each subject per is 0.5g, smears uniform.Smear 3h,
After 6h, 9h, the skin moisture content of every group of subject's same area is tested respectively, after average treatment, carry out recording every group respectively
Skin moisture content, and analyze；And when smearing 3h, 6h, 9h, it is respectively adopted with a oil-Absorbing Sheets, in the T of every subject
Area presses lightly on, and observes the oil suction situation of oil-Absorbing Sheets, if at least six people it is fuel-displaced it is serious if make 5 scores, if at least six people it is fuel-displaced compared with
To be serious, then 4 scores are made, makes 3 scores if at least six people is fuel-displaced generally, if at least six people is fuel-displaced relatively to make 2 scores less, at least six
People makes 1 score if not fuel-displaced, records and analyzes.
Test result is as follows for skin moisture content shown in table:
The above results show: using the subject of embodiment trial target after using 3h, 6h and 9h, the moisture content of skin
It is still higher by much than initial value, illustrates that the plain face of embodiment all has preferable long-acting moistening effect by spraying, skin can be made long
It keeps long wet, wherein the long-acting moistening effect of embodiment 1 is best.
Comparing embodiment 1, embodiment 5 and embodiment 6 are it is found that SP-7 thickener is compounded with AQUAXYL with the proportion of 0.5:3
When, spraying moistening effect is best.
Comparing embodiment 1 and comparative example 4~6 are sprayed it is found that when lacking SP-7 thickener, AQUAXYL or tourmaline in spraying
Moisture-keeping efficacy can all be decreased obviously, illustrate SP-7 thickener, AQUAXYL and tourmaline collocation in use, spraying moisture-keeping efficacy
It is best.Comparative example 4 and comparative example 5 cause spraying moistening effect to be decreased obviously due to lacking SP-7 thickener or AQUAXYL,
Moisture of skin scatters and disappears fast.
Skin ingress of oil situation statistical result is as shown in the table:
The above results show: using the subject of embodiment trial target using after 3h, 6h and 9h, skin ingress of oil it is less or
It is not fuel-displaced, illustrate that the plain face of embodiment has preferable oil-control effect by spraying, skin can be made to keep salubrious for a long time, wherein is real
The oil-control effect for applying example 1 is best.
Comparing embodiment 1, embodiment 5 and embodiment 6 are it is found that SP-7 thickener is compounded with AQUAXYL with the proportion of 0.5:3
When, spraying oil-control effect is best.
Comparing embodiment 1 and comparative example 4~6 are sprayed it is found that when lacking SP-7 thickener, AQUAXYL or tourmaline in spraying
Oil-control effect can all be decreased obviously, illustrate SP-7 thickener, AQUAXYL and tourmaline collocation in use, spraying oil-control effect
It is best.Comparative example 4 and comparative example 5 cause spraying oil-control effect to be decreased obviously due to lacking SP-7 thickener or AQUAXYL,
The reason is that spraying long-acting moisture-keeping efficacy declines, so that the moisture of skin is easy to scatter and disappear, institute uneven so as to cause skin water oil
To there is skin ingress of oil phenomenon serious situation.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than protects to the present invention
The limitation of range is protected, although the invention is described in detail with reference to the preferred embodiments, those skilled in the art should
Understand, it can be with modification or equivalent replacement of the technical solution of the present invention are made, without departing from the essence of technical solution of the present invention
And range.
Claims (10)
1. a kind of element face is spraying, which is characterized in that including following component: acrylic acid (ester) class/C12-22 alkanol methacrylic acid
Ester copolymer, Xylitol-based glucoside/anhydro xylitol/xylitol and tourmaline.
2. element face as described in claim 1 is spraying, which is characterized in that the element face includes following weight percentage by spraying
Component: acrylic acid (ester) class/C12-22 alkanol methacrylate copolymer 0.1%~1%, Xylitol-based glucoside/dehydration
Xylitol/xylitol 1%~5% and tourmaline 0.5%~3%.
3. element face as claimed in claim 2 is spraying, which is characterized in that acrylic acid (ester) class/C12-22 alkanol methyl-prop
Olefin(e) acid ester copolymer and Xylitol-based glucoside/anhydro xylitol/xylitol weight ratio are 0.5:3.
4. element face as claimed in any one of claims 1 to 3 is spraying, which is characterized in that the element face further includes following weight by spraying
Measure the component of percentage composition: emulsifier 2%~4% and assistant for emulsifying agent 0.6%~4%；The emulsifier is two C12-15 alkanes
The mixture of -8 phosphate of alcohol polyethers and PPG-10 cetyl ether phosphate；The assistant for emulsifying agent includes assistant for emulsifying agent A and helps cream
Agent B；The assistant for emulsifying agent A is the mixture of water, two (oleth -8) sodium phosphates and DMDM hydantoin；It is described to help cream
Agent B is water, -20 itaconate copolymeric of acrylic acid (ester) class/stereth, PEG-30 glycerol monolaurate, benzene oxygen second
The mixture of pure and mild methyl hydroxybenzoate.
5. element face as claimed in claim 4 is spraying, which is characterized in that the weight ratio of the assistant for emulsifying agent A and assistant for emulsifying agent B is
0.1~1:0.5~3.
6. element face as claimed in claim 5 is spraying, which is characterized in that the weight ratio of the assistant for emulsifying agent A and assistant for emulsifying agent B is
1:2。
7. element face as claimed in any one of claims 1 to 3 is spraying, which is characterized in that the element face further includes following weight by spraying
Measure the component of percentage composition: physical sunscreen agent 1%~8%；Preferably, the physical sunscreen agent be titanium dioxide (and) silicon oxygen
Alkane.
8. element face as claimed in any one of claims 1 to 3 is spraying, which is characterized in that the element face further includes following weight by spraying
Measure the component of percentage composition: active additive 0.2%~3%；Preferably, the active additive is water/butanediol/Xin Gan
Alcohol/1,2- ethylene glycol/Margarita extract.
9. element face as claimed in any one of claims 1 to 3 is spraying, which is characterized in that the element face further includes following weight by spraying
Measure the component of percentage composition: emollient 2%~20%, the emollient include isobutyl palmitate and No. 15 white oils.
10. a kind of element face is spraying, which is characterized in that be grouped as by the group of following weight percentage: acrylic acid (ester) class/C12-
22 alkanol methacrylate copolymers 0.1%~1%, Xylitol-based glucoside/anhydro xylitol/xylitol 1%~5%,
Tourmaline 0.5%~3%, emulsifier 2%~4%, assistant for emulsifying agent A0.1%~1%, assistant for emulsifying agent B 0.5%~3%, physics are anti-
Shine agent 1%~8%, active additive 0.2%~3%, isobutyl palmitate 1%~10%, No. 15 white oil 1%~10%, pH
It regulator 0.2%~1%, corrosion inhibiter 0.1%~2%, preservative 0.3%~1%, essence 0.005%~0.02% and goes
Ion water surplus；
The emulsifier is the mixture of two myristyl alcohol phosphates and PPG-10 cetyl ether phosphate；
The assistant for emulsifying agent A is the mixture of water, two (oleth -8) sodium phosphates and DMDM hydantoin；
The assistant for emulsifying agent B is water, -20 itaconate copolymeric of acrylic acid (ester) class/stereth, PEG-30 glycerol laurel
The mixture of acid esters, Phenoxyethanol and methyl hydroxybenzoate；
The physical sunscreen agent be titanium dioxide (and) siloxanes；
The active additive is water/butanediol/pungent glycol/1,2- ethylene glycol/Margarita extract；
The pH adjusting agent is triethanolamine；
The corrosion inhibiter is the mixture of phosphorus sodium calcium silicate and ammonium dihydrogen phosphate；
The preservative is Phenoxyethanol/methyl hydroxybenzoate/ethyl hydroxy benzoate/Sensiva SC50.
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| CN201811118040.0A CN109125115B (en) | 2018-09-25 | 2018-09-25 | Face-beautifying spray and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811118040.0A CN109125115B (en) | 2018-09-25 | 2018-09-25 | Face-beautifying spray and preparation method thereof |
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| CN109125115B CN109125115B (en) | 2021-04-16 |
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| CN201811118040.0A Active CN109125115B (en) | 2018-09-25 | 2018-09-25 | Face-beautifying spray and preparation method thereof |
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| Publication number | Publication date |
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| CN109125115B (en) | 2021-04-16 |
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