CN109123752A - A kind of low-temperature atomizing tobacco aromaticss and its application - Google Patents
A kind of low-temperature atomizing tobacco aromaticss and its application Download PDFInfo
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- CN109123752A CN109123752A CN201811237346.8A CN201811237346A CN109123752A CN 109123752 A CN109123752 A CN 109123752A CN 201811237346 A CN201811237346 A CN 201811237346A CN 109123752 A CN109123752 A CN 109123752A
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- tobacco
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- temperature atomizing
- aromaticss
- glucoside
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses a kind of low-temperature atomizing tobacco aromaticss and its applications, the low-temperature atomizing tobacco aromaticss include the component of following mass percent: compound tobacco reactant 18~30%, fragrance precursor object 0.05%~0.1%, tobacco spice 10~15%, mouthfeel modifying agent 55~70%.A kind of application of low-temperature atomizing tobacco aromaticss, after aforementioned low-temperature atomizing tobacco aromaticss are mixed with tobacco stem shred concentrate according to weight ratio 5~7:2~4, it is applied in paper process sheets of fibres chip base as coating fluid, obtains low-temperature atomizing reconstituted tobacoo after dry.The low-temperature atomizing reconstituted tobacoo has the beneficial effects such as aromatic strongly fragrant, the improvement throat drying of amount of smoke abundance, tobacco and excitement.
Description
Technical field
Do not burn tobacco product technical field the present invention relates to low temperature, and in particular to a kind of low-temperature atomizing tobacco aromaticss and its
Using.
Background technique
Low-temperature atomizing cigarette is to be heated by external heating element to tobacco material, and non-tobacco directly burning generates
Smog can reduce the harmful smoke of known type caused by the result of combustion of tobacco and thermal degradation in conventional cigarette significantly in this way
Ingredient.Low-temperature atomizing cigarette usually issues atomizing in 200~400 DEG C of temperature condition, and low-temperature atomizing cigarette is subtracted with its tar reduction
The advantages such as harmful, environmental-friendly, satisfaction is strong are becoming most promising new tobacco products.
Novel tobacco-low temperature tobacco product form of not burning is rich and varied in the world now, such as luxuriant and rich with fragrance IQOS, Great Britain and America not
The GLO of tobacco, the charcoal that Reynolds is released heat cigarette CORE, and the PLOOMTECH etc. that Japan Tobacco goes out, low temperature incombustible material is all
Use reconstituted tobacco for carrier, only technology is not quite similar.In general, low-temperature atomizing cigarette filler is mainly reconstituted tobacco
With a small amount of pipe tobacco and other adjunct ingredients, the physiology such as nicotine meet ingredient and discharge insufficient, shadow under the conditions of lower temperature
Ring suction satisfaction；On the other hand, generation smog is relatively slow and smokescope is insufficient, it is difficult to reach traditional low-coke tar cigarette product
Suction impression；Furthermore in practical heating process, local temperature is excessively high to will lead to reconstituted tobacco and pipe tobacco glows problem, generates
Other harmful substances matter and the smell of burning.As it can be seen that improving low-temperature atomizing cigarette drawbacks described above existing at present has become this field urgently
It solves the problems, such as.
The disclosure of background above technology contents is only used for auxiliary and understands inventive concept and technical solution of the invention, not
The prior art for necessarily belonging to present patent application shows above content in the applying date of present patent application in no tangible proof
Before have disclosed in the case where, above-mentioned background technique should not be taken to evaluation the application novelty and creativeness.
Summary of the invention
It is a primary object of the present invention to propose in a kind of low-temperature atomizing tobacco aromaticss and coat containing cigarette perfume
The reconstituted tobacoo of material, to solve, cigarette perfume present in existing low-temperature atomizing cigarette is insufficient, mist amount is few, mouthfeel is bad and easy
There is the technical issues of smoke grenade is glowed.
The present invention proposes following technical scheme for the above-mentioned purpose:
A kind of low-temperature atomizing tobacco aromaticss, the component comprising following mass percent: compound tobacco reactant 18~30%,
Fragrance precursor object 0.05%~0.1%, tobacco spice 10~15%, mouthfeel modifying agent 55~70%.
Low-temperature atomizing tobacco aromaticss provided by above-mentioned technical proposal are used to prepare low-temperature atomizing reconstituted tobacoo, prepared
Obtained reconstituted tobacoo, in low temperature tobacco heater tool using upper, it can be achieved that reducing tar and reducing harm, amount of smoke abundance, tobacco are aromatic
Strongly fragrant, improvement throat drying and excitement and other effects, have the market prospects of substitution traditional cigarette.
Preferably, the compound tobacco reactant is prepared by the following method:
(1) tobacco material is crushed to 200~300 mesh, the ammonium phosphate salt and tobacco material weight of tobacco material weight 5% is added
5 times of deionized water, soak at room temperature is for 24 hours；
(2) filter: filter residue is dried in vacuo to obtain solid tobacco powder, spare；Methylene chloride extraction is added in supernatant, obtains dichloro
Methane layer；
(3) lactic acid of tobacco material weight 5% is added toward dichloromethane layer, reacts 1h, concentration and recovery two after cooling at the boil
Chloromethanes obtains tobacco extract；
(4) the solid tobacco powder is mixed with the tobacco extract, obtains the compound tobacco reactant.
Preferably, the tobacco material is the mixture of Fo Jiniya flue-cured tobacco, Turkey's Turkish tobaccos and Malawi's burley tobaccos.
It is highly preferred that the mass ratio of Fo Jiniya flue-cured tobacco, Turkey's Turkish tobaccos and Malawi's burley tobaccos is 7 in the tobacco material:
1.5:1.5。
Preferably, the fragrance precursor object is the mixture of sugar ester and glucosides, wherein the weight ratio of sugar ester and glucosides is
1~2:2.It is highly preferred that the sugar ester includes butyric acid fructose ester, 2-Methyl Butyric Acid fructose ester, isovaleric acid fructose ester, 3- methylpent
At least one of tart fruit sugar ester, 3 Methylbutanoic acid glucose ester, lactic acid fructose ester and lactic acid glucose ester；The glucosides includes
Ethyl vanillin glucoside, vanillic aldehyde glucoside, benzyl carbinol glucoside, ionol glucoside, trans- 2- hexenol
At least one of glucoside, geraniol glucoside, menthol glucoside and raspberry ketone glucoside.
Preferably, the tobacco spice is fractionation component of the pure tobacco oil between 150 DEG C~300 DEG C.
Preferably, the mouthfeel modifying agent be glycerine, propylene glycol and water mixture, wherein glycerine, propylene glycol with
The mass ratio of water is 6:1.5:1.
Preferably, the low-temperature atomizing tobacco aromaticss also include 5% yunyan extract, the tobacco spice of tobacco spice weight
1% Zimbabwe's tobacco extract of the sunning smoke-dipping paste and tobacco spice weight of the 2% of weight.
The present invention separately also provides a kind of application of low-temperature atomizing tobacco aromaticss, comprising: low-temperature atomizing cigarette above-mentioned is fragrant
After material is mixed with tobacco stem shred concentrate according to weight ratio 5~7:2~4, paper process sheets of fibres is applied to as coating fluid
In chip base, low-temperature atomizing reconstituted tobacoo is obtained after dry.
Aforementioned low-temperature atomizing tobacco aromaticss are applied to preparation low-temperature atomizing reconstituted tobacoo, acquired reconstituted tobacoo has drop
Burnt harm reduction, amount of smoke are sufficient, tobacco it is aromatic it is strongly fragrant, improve that throat is dry and the beneficial effects such as excitement, and preparation process it is simple,
It is at low cost.
Specific embodiment
Below with reference to specific embodiment, the invention will be further described.
A wherein specific embodiment of the invention provides a kind of low-temperature atomizing tobacco aromaticss, includes following mass percent
Component: compound tobacco reactant 18~30%, fragrance precursor object 0.05%~0.1%, tobacco spice 10~15%, mouthfeel changes
Good dose 55~70%.In some embodiments, the low-temperature atomizing tobacco aromaticss are made of above four kinds of components；In other realities
It applies in example, the low-temperature atomizing tobacco aromaticss also include 5% yunyan extract of tobacco spice weight, tobacco spice weight
1% Zimbabwe's tobacco extract of 2% sunning smoke-dipping paste and tobacco spice weight.
In a preferred embodiment, compound tobacco reactant is prepared via a method which: first by tobacco material powder
200~300 mesh are broken to, the ammonium phosphate salt and 5 times of tobacco material weight of deionized water of tobacco material weight 5%, room temperature is added
It impregnating for 24 hours, is filtered later, the filter residue of filtering is dried in vacuo to obtain solid tobacco powder, and it is spare, and dichloro is added in supernatant
Methane extraction, obtains dichloromethane layer；The lactic acid of tobacco material weight 5% is added toward dichloromethane layer, reacts 1h at the boil,
Concentration and recovery methylene chloride after cooling, obtains tobacco extract；The solid tobacco powder will be mixed with the tobacco extract
It closes, obtains required compound tobacco reactant.Tobacco material used in it is Fo Jiniya flue-cured tobacco, Turkey's Turkish tobaccos and horse
The mixture of dimension burley tobaccos is drawn, and the mass ratio of three is 7:1.5:1.5.
In a preferred embodiment, the fragrance precursor object is the mixture of sugar ester and glucosides, wherein sugar ester and glucosides
Weight ratio is 1~2:2.Wherein, sugar ester used include butyric acid fructose ester, 2-Methyl Butyric Acid fructose ester, isovaleric acid fructose ester,
At least one of 3 methylvaleric acid fructose ester, 3 Methylbutanoic acid glucose ester, lactic acid fructose ester and lactic acid glucose ester；It is used
Glucosides include Ethyl vanillin glucoside, vanillic aldehyde glucoside, benzyl carbinol glucoside, ionol glucoside,
At least one in trans- 2- hexenol glucoside, geraniol glucoside, menthol glucoside and raspberry ketone glucoside
Kind.
In a preferred embodiment, the tobacco spice is fractionation component of the pure tobacco oil between 150 DEG C~300 DEG C.
Required pure tobacco oil component is prepared by molecular distillation technique, wherein vacuum condition is 300~1000Pa, and scraping plate temperature is
50~80 DEG C.
Mouthfeel modifying agent used is the mixture of glycerine, propylene glycol and water.In a preferred embodiment, the mouthfeel
Modifying agent is mixed by glycerine, propylene glycol and the water that mass ratio is 6:1.5:1.
Another specific embodiment of the present invention provides a kind of application of low-temperature atomizing tobacco aromaticss, comprising: by aforementioned tool
After the low-temperature atomizing tobacco aromaticss that body embodiment provides are mixed with tobacco stem shred concentrate according to weight ratio 5~7:2~4,
It is applied in paper process sheets of fibres chip base as coating fluid, obtains low-temperature atomizing reconstituted tobacoo after dry.
Beneficial effects of the present invention are verified below by specific embodiment and reference examples.
Embodiment 1, a kind of low-temperature atomizing tobacco aromaticss include compound tobacco reactant 25%, tobacco spice 15%, mouthfeel
Modifying agent 59.9% and fragrance precursor object 0.1%, percentage indicate mass percent.Wherein, tobacco spice is using Jin Babu
Wei pure tobacco oil scrapes what plate temperature was prepared for 68 DEG C by being 500Pa in vacuum degree；Tobacco aromaticss contain 0.05%
The arbitrary proportion mixture of butyric acid fructose ester and isovaleric acid fructose ester and 0.05% Ethyl vanillin glucoside, purple sieve
Blue alcohol glucoside, geraniol glucoside, any 2 kinds of menthol glucoside or 4 kinds arbitrary proportion mixture.It will be upper
State component low-temperature atomizing tobacco aromaticss mixed with tobacco stem shred concentrate according to weight ratio 6:4 after, as coating fluid be coated with
Onto traditional paper process sheets of fibres chip base, low-temperature atomizing reconstituted tobacoo A is obtained after dry.
Compared with Example 1, only component ratio is different for embodiment 2, low-temperature atomizing tobacco aromaticss provided in this embodiment,
Specially compound tobacco reactant 30%, tobacco spice 10%, mouthfeel modifying agent 59.9%, fragrance precursor object 0.1%.This is low
After temperature atomization tobacco aromaticss are mixed with tobacco stem shred concentrate according to weight ratio 6:4, traditional papermaking is applied to as coating fluid
In method sheets of fibres chip base, low-temperature atomizing reconstituted tobacoo B is obtained after dry.
Compared with Example 1, only component ratio is different for embodiment 3, low-temperature atomizing tobacco aromaticss provided in this embodiment,
Specially compound tobacco reactant 30%, tobacco spice 13%, mouthfeel modifying agent 56.95%, fragrance precursor object 0.05%.It should
After low-temperature atomizing tobacco aromaticss are mixed with tobacco stem shred concentrate according to weight ratio 6:4, tradition is applied to as coating fluid and is made
In paper method sheets of fibres chip base, low-temperature atomizing reconstituted tobacoo C is obtained after dry.
Embodiment 4, a kind of low-temperature atomizing tobacco aromaticss include compound tobacco reactant 25%, tobacco spice 15%, mouthfeel
Modifying agent 59.9% and fragrance precursor object 0.1%.Wherein, which contains 0.05% lactic acid glucose ester and 0.05%
Raspberry ketone glucoside.After the tobacco aromaticss are mixed with tobacco stem shred concentrate according to weight ratio 6:4, as coating
Liquid is applied in traditional paper process sheets of fibres chip base, obtains low-temperature atomizing reconstituted tobacoo D after dry.
Embodiment 5, a kind of low-temperature atomizing tobacco aromaticss include compound tobacco reactant 25%, tobacco spice 15%, mouthfeel
Modifying agent 59.9% and fragrance precursor object 0.1%.Wherein, tobacco spice is to use Brazilian pure tobacco oil in vacuum degree for 800Pa,
Scrape what plate temperature was prepared for 80 DEG C.After the tobacco aromaticss are mixed with tobacco stem shred concentrate according to weight ratio 6:4, make
It is applied in traditional paper process sheets of fibres chip base for coating fluid, obtains low-temperature atomizing reconstituted tobacoo E after dry.
Reference examples: not adding low-temperature atomizing tobacco aromaticss of the invention, is applied to tradition only with tobacco stem shred concentrate
In paper process sheets of fibres chip base, low-temperature atomizing reconstituted tobacoo control sample, referred to as blank sample are obtained after dry.
Low-temperature atomizing reconstituted tobacoo A~E of embodiment 1 to 5 is used in the electronic apparatus of low-temperature atomizing tobacco feel
Official's performance rating, by comparing with blank sample, smoking result is as follows:
| Sample | Smoking result |
| Blank sample | Amount of smoke is small, and flue gas is weaker, and fragrance is insufficient, and irritation is big, and cigarette perfume is light.Simulation suction feels poor |
| Sample A | Amount of smoke is big, and satisfaction is strong, and tobacco sheet is aromatic strongly fragrant, and simulation suction effect is preferable |
| Sample B | Amount of smoke is big, and satisfaction is preferable, and throat is comfortable, and tobacco aroma is preferable, and simulation suction effect is preferable |
| Sample C | Amount of smoke is big, and satisfaction is preferable, and throat is relatively comfortable, and tobacco perfume (or spice) is abundant, and simulation suction effect is preferable |
| Sample D | Amount of smoke is big, and satisfaction is preferable, and throat's stimulation reduces, and tobacco aroma is preferable, and simulation suction effect is preferable |
| Sample E | Amount of smoke is medium, and satisfaction is good, and throat is relatively comfortable, and tobacco aroma is preferable, and simulation suction effect is good |
By upper table, it can be concluded that, low-temperature atomizing tobacco aromaticss provided by the invention are applied in reconstituted tobacoo preparation, warp
Experimental verification is crossed, there are the beneficial effects such as aromatic strongly fragrant, the improvement throat drying of amount of smoke abundance, tobacco and excitement, there is substitution
The market prospects of traditional cigarette.
The above content is a further detailed description of the present invention in conjunction with specific preferred embodiments, and it cannot be said that
Specific implementation of the invention is only limited to these instructions.For those skilled in the art to which the present invention belongs, it is not taking off
Under the premise of from present inventive concept, several equivalent substitute or obvious modifications can also be made, and performance or use is identical, all answered
When being considered as belonging to protection scope of the present invention.
Claims (10)
1. a kind of low-temperature atomizing tobacco aromaticss, which is characterized in that the component comprising following mass percent: compound tobacco reactant
18~30%, fragrance precursor object 0.05%~0.1%, tobacco spice 10~15%, mouthfeel modifying agent 55~70%.
2. low-temperature atomizing tobacco aromaticss as described in claim 1, which is characterized in that the compound tobacco reactant passes through following
Method is prepared:
(1) tobacco material is crushed to 200~300 mesh, the ammonium phosphate salt and tobacco material weight of tobacco material weight 5% is added
5 times of deionized water, soak at room temperature is for 24 hours；
(2) filter: filter residue is dried in vacuo to obtain solid tobacco powder, spare；Methylene chloride extraction is added in supernatant, obtains dichloro
Methane layer；
(3) lactic acid of tobacco material weight 5% is added toward dichloromethane layer, reacts 1h, concentration and recovery two after cooling at the boil
Chloromethanes obtains tobacco extract；
(4) the solid tobacco powder is mixed with the tobacco extract, obtains the compound tobacco reactant.
3. low-temperature atomizing tobacco aromaticss as claimed in claim 2, it is characterised in that: the tobacco material is roasting for Fo Jiniya
The mixture of cigarette, Turkey's Turkish tobaccos and Malawi's burley tobaccos.
4. low-temperature atomizing tobacco aromaticss as claimed in claim 3, it is characterised in that: Fo Jiniya is roasting in the tobacco material
The mass ratio of cigarette, Turkey's Turkish tobaccos and Malawi's burley tobaccos is 7:1.5:1.5.
5. low-temperature atomizing tobacco aromaticss as described in claim 1, it is characterised in that: the fragrance precursor object is sugar ester and glucosides
Mixture, wherein the weight ratio of sugar ester and glucosides be 1~2:2.
6. low-temperature atomizing tobacco aromaticss as claimed in claim 5, it is characterised in that: the sugar ester includes butyric acid fructose ester, 2-
Methylbutanoic acid fructose ester, isovaleric acid fructose ester, 3 methylvaleric acid fructose ester, 3 Methylbutanoic acid glucose ester, lactic acid fructose ester and
At least one of lactic acid glucose ester；The glucosides includes Ethyl vanillin glucoside, vanillic aldehyde glucoside, benzyl carbinol
Glucoside, ionol glucoside, trans- 2- hexenol glucoside, geraniol glucoside, menthol glucoside and
At least one of raspberry ketone glucoside.
7. low-temperature atomizing tobacco aromaticss as described in claim 1, it is characterised in that: the tobacco spice is that pure tobacco oil exists
Fractionation component between 150 DEG C~300 DEG C.
8. low-temperature atomizing tobacco aromaticss as described in any one of claim 1 to 7, it is characterised in that: the mouthfeel modifying agent is
The mixture of glycerine, propylene glycol and water, wherein the mass ratio of glycerine, propylene glycol and water is 6:1.5:1.
9. low-temperature atomizing tobacco aromaticss as described in claim 1, it is characterised in that: also include the 5% of tobacco spice weight
The 2% 1% Zimbabwe's tobacco extract for drying smoke-dipping paste and tobacco spice weight of yunyan extract, tobacco spice weight.
10. a kind of application of low-temperature atomizing tobacco aromaticss characterized by comprising claim 1 to 9 is described in any item
After low-temperature atomizing tobacco aromaticss are mixed with tobacco stem shred concentrate according to weight ratio 5~7:2~4, it is applied to as coating fluid
In paper process sheets of fibres chip base, low-temperature atomizing reconstituted tobacoo is obtained after dry.
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| CN110464043A (en) * | 2019-07-09 | 2019-11-19 | 河南中烟工业有限责任公司 | For heating the faint scent essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
| CN110477439A (en) * | 2019-07-09 | 2019-11-22 | 河南中烟工业有限责任公司 | For heating the sugar ester essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
| CN111713730A (en) * | 2020-07-17 | 2020-09-29 | 杨伟祖 | Aroma-enhancing and harm-reducing particle for cigarettes and preparation method and application thereof |
| CN112155249A (en) * | 2020-10-16 | 2021-01-01 | 河南中烟工业有限责任公司 | Essence for improving sense comfort and cigarette paper |
| CN113100469A (en) * | 2021-03-15 | 2021-07-13 | 云南中烟工业有限责任公司 | Method for improving aroma of cigarette products by using raspberry glycosides |
| CN115005488A (en) * | 2022-06-24 | 2022-09-06 | 湖北中烟工业有限责任公司 | Atomizing agent for cigarettes and electronic cigarette liquid |
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| CN110464043A (en) * | 2019-07-09 | 2019-11-19 | 河南中烟工业有限责任公司 | For heating the faint scent essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
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| CN115005488A (en) * | 2022-06-24 | 2022-09-06 | 湖北中烟工业有限责任公司 | Atomizing agent for cigarettes and electronic cigarette liquid |
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| CN109123752B (en) | 2019-10-11 |
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