CN103445283A - Processing method of tobacco raw materials for heating non-combustion tobacco products - Google Patents
Processing method of tobacco raw materials for heating non-combustion tobacco products Download PDFInfo
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- CN103445283A CN103445283A CN2013104523390A CN201310452339A CN103445283A CN 103445283 A CN103445283 A CN 103445283A CN 2013104523390 A CN2013104523390 A CN 2013104523390A CN 201310452339 A CN201310452339 A CN 201310452339A CN 103445283 A CN103445283 A CN 103445283A
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Abstract
A processing method of tobacco raw materials for heating non-combustion tobacco products sequentially includes: adjusting moisture of the tobacco raw materials, heating at 100-300 DEG C for 0.5-8 hours; cooling at room temperature; balancing at 22 DEG C and 60% of moisture for 24-120 hours, applying glycoside aroma precursors, and standing for 48-120 hours to guarantee that the aroma precursors are fully absorbed by the raw materials; applying polyol to the raw materials after perfuming, and standing for 48-120 hours under a seal state to guarantee that the polyol is fully absorbed by the raw materials; balancing at 22 DEG C and 60% of moisture for 24-120 hours to obtain the tobacco raw materials for heating the non-combustion tobacco products. The tobacco raw materials processed by the method has the advantages that smoke releasing performance of the tobacco raw materials during heating of the non-combustion tobacco products is increased evidently, sensory quality of the released smoke is improved evidently, and good satisfaction and comfortableness are achieved.
Description
Technical field
The invention belongs to technical field of tobacco, be specifically related to a kind of processing method that heats non-burning type tobacco product tobacco material.
Background technology
Heating non-burning type tobacco product is a kind of novel tobacco product, can add and impel contained tobacco-containing material to produce the smog of sucking for the consumer under non-fired state by heat, with traditional cigarette, compare, the release of side-stream smoke and part harmful substance obviously reduces.Heating non-burning type tobacco product is released by company of R. J. Reynolds Tobacco the earliest, although this series products not yet obtains the extensive approval in market, but due to the lasting increase of global range Tobacco Control dynamics with and reducing aspect the healthy potential risk of environmental pollution and smoking the clear superiority existed, international Field of Tobacco thinks that this series products is the important directions of following tobacco product development always.
Chinese patent CN02826243.3, the CN200980159916.9 of Chinese patent CN88101196, the 89108679.X of the application of company of R. J. Reynolds Tobacco and Japan Tobacco Inc's application discloses carbon and heated product composition and the relevant technologies that class heats non-burning type tobacco product.The electrical heating class that discloses Chinese patent CN94102530.6, CN96194107.3, CN96195594.5, CN200380102439.5, the CN200580036230.2 of Fei Mo tobacco company application heats product composition and the relevant technologies of non-burning type tobacco product.But by the anatomy to existing product, find, the burst size that carbon heating class heats CO in non-burning type tobacco product main flume is high, and the organoleptic quality of flue gas also not yet reaches gratifying degree; The electrical heating class heats non-burning type tobacco product and is heated down and can effectively discharges the flue gas with tobacco characteristic chicken flavor, after heating, obvious charing phenomenon has appearred in tobacco-containing material, but burning has to a certain degree also occurred, illustrate that existing product also need further optimize aspect fire-retardant, could really accomplish that tobacco-containing material is to discharge flue gas under the on-fuel state of heating, and the organoleptic quality of flue gas is also to await further improvement.
Therefore, in order further to improve the flue gas quality of the non-burning type tobacco product of heating, need on the one hand to optimize heater and control parameter, on the other hand used tobacco material is carried out to suitable processing, it is also vital improving flue gas release performance and the flue gas quality of cigarette core under the non-fired state of heating that adopts the designed preparation of this tobacco material.
Summary of the invention
The processing method of a kind of tobacco material that purpose of the present invention provides for above-mentioned prior art situation just, after processing by the method, in heating, the flue gas release performance under non-fired state obviously improves tobacco material, discharge flue gas organoleptic quality obviously improve.
The objective of the invention is to be achieved through the following technical solutions:
A kind of processing method that heats non-burning type tobacco product tobacco material comprises the following steps successively:
(1) heat treated of tobacco material: after the moisture of tobacco material is adjusted to 10 %～25 %, be placed in enclosed system, 100 ℃～300 ℃ lower heat treated 0.5 h～8 h; After heating finishes, keep cooling 12 h of airtight condition room temperature～48 h, obtain the tobacco material after heat treated.The tobacco material adopted can be one or more mixing of the dissimilar tobacco leaves such as flue-cured tobacco, burley tobaccos, Turkish tobaccos.
(2) perfuming of tobacco material is processed: by the tobacco material after heat treated 22 ℃ of temperature, in the environment of relative humidity 60 % after balance 24 h～120 h, applying wherein mass ratio is the glucosides class fragrance precursor of 50 ppm～1000 ppm, and place 48 h～120 h under sealing state, guarantee the abundant absorption of raw material to fragrance precursor.The glucosides class fragrance precursor adopted can be one or more mixing of 3-oxo ionol glucoside, ionol glucoside, benzyl carbinol glucoside, menthol glucoside, geraniol glucoside etc.
(3) the reinforced processing of tobacco material: after the tobacco material perfuming is processed, apply wherein the polyalcohol of mass ratio 5 %～20 %, and place 48 h～120 h under sealing state, guarantee the abundant absorption of tobacco material to polyalcohol.The tobacco material that then will feed in raw material after processing is 22 ℃ of temperature, and balance 24 h～120 h in the environment of relative humidity 60 % obtain being applicable to heat the tobacco material of non-burning type tobacco product.The polyalcohol adopted can be one or both mixing of propane diols, glycerine.
The invention has the advantages that:
1. tobacco material is carried out in certain temperature range to heat treated, can play good maturation, improve the content of tobacco material fragrance matter, heat treated also can cause the Partial digestion of the macromolecular substances such as polysaccharide in tobacco material simultaneously, and whole processing procedure is carried out in enclosed system, can again by tobacco material, be adsorbed again in the material cooling procedure gone out due to heated volatile, can not lose.Therefore, heat treated favourable improve tobacco material in heating the flue gas release performance under non-fired state and discharge the organoleptic quality of flue gas.
2. have good stability under glucosides class fragrance precursor normal temperature of the present invention, temperature is the glycosidic bond fracture during higher than 200 ℃, generates corresponding fragrance matter.Adopt such material to carry out the perfuming processing to tobacco material, can the Stable Release fragrance matter under the non-fired state of heating, thus improve the organoleptic quality of discharge flue gas.Especially the 3-oxo ionol glucoside heating pyrolyze that adopted can Stable Release tobacco characteristic chicken flavor material Megastigmatrienone, the tobacco feature of flue gas that obviously strengthening discharges.
3. adopt propane diols or glycerine to the tobacco material processing of feeding in raw material, can strengthen the flue gas release performance of tobacco material under the non-fired state of heating, improve flue gas concentration, simultaneously because its volatilization in heating process can effectively absorb heat, thereby also can play good fire retardation to tobacco material, guarantee that tobacco material is to discharge flue gas under the on-fuel state of heating.
4. after tobacco material is adopted method processing of the present invention, its flue gas release performance heated under non-fired state obviously improves with the organoleptic quality of discharge flue gas, and the applicability in the non-burning type tobacco product of heating obviously strengthens.
5. operating procedure of the present invention is simple, cost is low, has good industrial prospect.
The specific embodiment
The present invention is described further below in conjunction with embodiment:
Embodiment 1
Take 100 g flue-cured tobacco pipe tobaccos, its humidification, to moisture content 15 %, is added in 500 mL stainless steel enclosed high pressure reaction vessels, the reaction vessel that then pipe tobacco will be housed is placed in Muffle furnace, heating 2 h under 180 ℃.After heating finishes, take out reaction vessel, keep cooling 24 h of air-tight state room temperature, then take out pipe tobacco, and 22 ℃ of temperature, balance 72 h in the environment of relative humidity 60 %.In the heat treatment pipe tobacco after balance, by the addition of 100 ppm, apply 3-oxo ionol glucoside.After pipe tobacco after perfuming is placed 72 h under sealing state, the addition by 10% applies propane diols wherein, and again places 72 h under sealing state.Then by it 22 ℃ of temperature, balance 72 h in the environment of relative humidity 60 %, obtain being applicable to heat the tobacco material of non-burning type tobacco product.
Thermogravimetric analysis shows, this tobacco material heats and obvious combustion phenomena can not occur under 300 ℃, the thermal weight loss rate is 45 %, before flue gas release performance under the non-fired state of heating after tobacco material is processed obviously is better than processing, and the flue gas discharged presents obvious flue-cured tobacco style and features, there is good satisfaction and comfortableness.
Embodiment 2
Taking 60 g flue-cured tobacco pipe tobaccos, 20 g burley tobaccos pipe tobaccos and 20 Turkish tobaccos pipe tobaccos mixes it, and humidification is to moisture content 20 %, add in 500 mL stainless steel enclosed high pressure reaction vessels, the reaction vessel that then pipe tobacco will be housed is placed in Muffle furnace, under 220 ℃, heats 1h.After heating finishes, take out reaction vessel, keep cooling 36 h of air-tight state room temperature, then take out pipe tobacco, and 22 ℃ of temperature, balance 96 h in the environment of relative humidity 60 %.In the heat treatment pipe tobacco after balance, apply 3-oxo ionol glucoside, benzyl carbinol glucoside and menthol glucoside, addition is 100 ppm.After pipe tobacco after perfuming is placed 96 h under sealing state, by the addition of 15 %, apply wherein glycerine, and again place 96 h under sealing state.Then by it 22 ℃ of temperature, balance 96 h in the environment of relative humidity 60 %, obtain being applicable to heat the tobacco material of non-burning type tobacco product.
Thermogravimetric analysis shows, this tobacco material heats and obvious combustion phenomena can not occur under 300 ℃, the thermal weight loss rate is 51 %, before flue gas release performance under the non-fired state of heating after tobacco material is processed obviously is better than processing, and the flue gas discharged presents obvious mixed type style feature, there is good satisfaction and comfortableness.
Claims (4)
- One kind the heating non-burning type tobacco product tobacco material processing method, it is characterized in that: comprise the following steps successively:(1) heat treated: after the moisture of tobacco material is adjusted to 10 %～25 %, be placed in enclosed system, 100 ℃～300 ℃ lower heat treated 0.5 h～8 h; After heating finishes, keep cooling 12 h of airtight condition room temperature～48 h, obtain the tobacco material after heat treated;(2) perfuming is processed: by the tobacco material after heat treated 22 ℃ of temperature, in the environment of relative humidity 60 % after balance 24 h～120 h, applying wherein addition is the glucosides class fragrance precursor of 50 ppm～1000 ppm, and place 48 h～120 h under sealing state, guarantee the abundant absorption of raw material to fragrance precursor;(3) the reinforced processing: after the tobacco material perfuming is processed, apply wherein the polyalcohol of mass ratio 5 %～20 %, and place 48 h～120 h under sealing state, guarantee the abundant absorption of tobacco material to polyalcohol, the tobacco material that then will feed in raw material after processing is 22 ℃ of temperature, balance 24 h～120 h in the environment of relative humidity 60 %, obtain being applicable to heat the tobacco material of non-burning type tobacco product.
- 2. the processing method of the non-burning type tobacco product of heating according to claim 1 tobacco material, it is characterized in that: the tobacco material adopted is any one or a few mixing in flue-cured tobacco, burley tobaccos, Turkish tobaccos.
- 3. the processing method of the non-burning type tobacco product of heating according to claim 1 tobacco material is characterized in that: the glucosides class fragrance precursor adopted is any one or a few the mixing in 3-oxo ionol glucoside, ionol glucoside, benzyl carbinol glucoside, menthol glucoside, geraniol glucoside.
- 4. the processing method of the non-burning type tobacco product of heating according to claim 1 tobacco material is characterized in that: the mixing of any one or two kinds that the polyalcohol adopted is propane diols, glycerine.
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| CN104366687A (en) * | 2014-09-15 | 2015-02-25 | 云南中烟新材料科技有限公司 | Smoking material for low-temperature nonflammable cigarette and preparing method thereof |
| CN105559133A (en) * | 2016-03-09 | 2016-05-11 | 江苏中烟工业有限责任公司 | Treatment method for heating cigarette core material of non-combustible cigarettes |
| CN105595399A (en) * | 2016-02-04 | 2016-05-25 | 江苏中烟工业有限责任公司 | Treatment method applicable to tobacco raw material of heated non-burning cigarette |
| CN105686071A (en) * | 2016-03-09 | 2016-06-22 | 江苏中烟工业有限责任公司 | Method for treating tobacco raw material for heating non-burning cigarettes |
| CN107574016A (en) * | 2017-10-20 | 2018-01-12 | 云南中烟工业有限责任公司 | One kind heats do not burn the savory extract formula of the special peppermint of cigarette and preparation method |
| CN108835714A (en) * | 2018-05-12 | 2018-11-20 | 深圳市大咖威普科技有限公司 | Dual-purpose type cigarette and its tobacco filler |
| CN109275946A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A kind of dynamic extraction processing method suitable for heating pipe tobacco under not combustion state |
| CN109275947A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A kind of supercritical extract processing method suitable for heating pipe tobacco under not combustion state |
| CN109275934A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A kind of processing method suitable for heating pipe tobacco under not combustion state |
| CN109275945A (en) * | 2018-09-27 | 2019-01-29 | 浙江中烟工业有限责任公司 | It is a kind of to heat the pipe tobacco microwave handling method that do not burn |
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| CN109554225A (en) * | 2018-11-29 | 2019-04-02 | 四川中烟工业有限责任公司 | A kind of fragrance functional additive increasing cigarette " profit sweet tea sense " |
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| CN109554225A (en) * | 2018-11-29 | 2019-04-02 | 四川中烟工业有限责任公司 | A kind of fragrance functional additive increasing cigarette " profit sweet tea sense " |
| CN109730352A (en) * | 2019-01-15 | 2019-05-10 | 湖南环境生物职业技术学院 | A kind of tobacco-containing material preparation method suitable for heating non-combustion-type tobacco product |
| CN110464043A (en) * | 2019-07-09 | 2019-11-19 | 河南中烟工业有限责任公司 | For heating the faint scent essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
| CN110464043B (en) * | 2019-07-09 | 2022-01-11 | 河南中烟工业有限责任公司 | Fragrant essence for heating non-combustible cigarette, tobacco sheet and non-combustible cigarette |
| CN111109639A (en) * | 2020-03-05 | 2020-05-08 | 中国烟草总公司郑州烟草研究院 | Addition process of glycerol in silk making process |
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