CN105559133B - One kind heats cigarette cigarette core material processing method of not burning - Google Patents
One kind heats cigarette cigarette core material processing method of not burning Download PDFInfo
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- CN105559133B CN105559133B CN201610131559.7A CN201610131559A CN105559133B CN 105559133 B CN105559133 B CN 105559133B CN 201610131559 A CN201610131559 A CN 201610131559A CN 105559133 B CN105559133 B CN 105559133B
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- Prior art keywords
- cigarette
- tobacco
- heating
- tobacco material
- core material
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/10—Roasting or cooling tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Abstract
Cigarette cigarette core material processing method of not burning is heated the invention discloses one kind,(1)Anaerobic glowing furnace is opened, it is 180 270 DEG C to set heating-up temperature, and is heated in inert gas atmosphere;(2)After anaerobic glowing furnace reaches the temperature of setting, tobacco material is put into rapidly in anaerobic glowing furnace and heats 3 20min;(3)Heating is finished, and stops heating, and tobacco material is cooled down in inert gas atmosphere;(4)The tobacco material of cooling is taken out after 24 48h of balance from anaerobic glowing furnace, applies the ethanol solution containing flavouring essence for tobacco and polyalcohol into tobacco material, and place 24 48h in sealed states;(5)Tobacco material after perfuming is handled was balanced after a period of time, obtained heating cigarette cigarette core material of not burning.By the tobacco material after present invention processing, flue gas can be effectively discharged under heating non-burning state, with good organoleptic quality, liking for suction fan can be preferably met.
Description
Technical field
Cigarette cigarette core material processing method of not burning is heated the present invention relates to one kind, belongs to technical field of tobacco.
Background technology
The heating cigarette that do not burn is current Field of Tobacco study hotspot, with " heating pipe tobacco or tobacco extract and it is non-combustible
Burn pipe tobacco " the characteristics of.Because tobacco product is not involved in burning, so as to avoid Pintsch process from producing substantial amounts of harmful components, simultaneously
Reduce the pollution of environment flue gas.In view of heating non-burning cigarette is to heat pipe tobacco rather than the burning pipe tobacco of traditional cigarette, flue gas
Organoleptic feature and regular-size cigarette flue gas there is larger difference.The sense organ matter that the cigarette that do not burn discharges flue gas is heated in order to improve
Amount, is extracted to cigarette core material about patent, is modified, flavoring and casing or mixed and match somebody with somebody with the progress of other functional materials.
The B of CN 103445283 disclose a kind of processing method for heating non-combustion-type tobacco product tobacco material, i.e., first adjust
Tobacco material moisture content is saved up to after 15%, then tobacco material is placed in stainless steel enclosed high pressure reaction vessel, in 100-300
Heat 0.5h-8h at DEG C, fed again after cooling tobacco material, perfuming is handled must be applied to heating non-burning cigarette
Tobacco-containing material.
The B of CN 103462210 disclose a kind of tobacco membrane preparation method for being applied to heating non-combustion-type tobacco product, should
Tobacco film is the solid tobacco extract and polyalcohol, filmogen and metallic hydrogen obtained after the alcohol steep thing of tobacco leaf is concentrated
The oxide gelatinization that adds water is carried out into obtained by film process.
CN103750535 B disclose a kind of preparation method for heating non-combustion type cigarette block, and the cigarette block is by tobacco slag
50-70%, offal end 5-20%, tobacco aromaticss 3-7%, deionized water 10-20%, alginates 7-11%, glycerine 1-2% mixing
Form.
The B of CN 103263072 are disclosed to be used for the preparation method of the tobacco-containing material without burning cigarette, is by former to tobacco
Material carries out perfuming processing gained.
The chemical composition identified in tobacco leaf and flue gas has kind more than 5000.The flue gas main component of the toasted release of pipe tobacco
It is the volatility and half volatile material in tobacco, species is various.Found in experimental study, the pipe tobacco baking of undressed processing
The flue gas of release inhales that taste is strong, excitant is relatively strong, have acid and strong tart flavour, miscellaneous gas heavier, and to inhale taste unstable for flue gas.
In order to further improve the flue gas release performance for heating cigarette cigarette core material of not burning, the preparation processing of tobacco-containing material is closed very much
Key.
Therefore, invention is a kind of can effectively improve the preparation side of the flue gas release performance under cigarette core material heating non-burning state
Method, is significantly for the exploitation for heating non-combustion-type tobacco product.
The content of the invention
The technical problems to be solved by the invention are that the defect for overcoming prior art heats the cigarette cigarette that do not burn there is provided one kind
Core material processing method, after being handled by this method, flue gas release performance of the tobacco material under heating non-burning state is obvious
Improve, the flue gas aesthetic quality discharged is obviously improved.
Technical scheme:In order to solve the above technical problems, the technical solution adopted by the present invention is:
One kind heats cigarette cigarette core material processing method of not burning, it is characterised in that comprise the following steps successively:
(1) anaerobic glowing furnace is opened, it is 180-270 DEG C to set heating-up temperature, and is heated in inert gas atmosphere;
(2) after anaerobic glowing furnace reaches the temperature of setting, tobacco material is put into rapidly in anaerobic glowing furnace and heats 3-
20min;
(3) heating is finished, and stops heating, and tobacco material is cooled down in inert gas atmosphere;
(4) tobacco material of cooling is taken out from anaerobic glowing furnace after balance 24-48h, applies into tobacco material and contain
The ethanol solution of flavouring essence for tobacco and polyalcohol, and 24-48h is placed in sealed states;
(5) tobacco material after perfuming is handled was balanced after a period of time, obtained heating cigarette cigarette core material of not burning.
It is preferred that, in step (1), heating-up temperature is 240-250 DEG C
It is preferred that, in step (1), the inert gas is selected from nitrogen or argon gas.
It is preferred that, in step (2), the tobacco material used is any one in flue-cured tobacco, Turkish tobaccos, burley tobaccos or several
Kind.
It is preferred that, in step (2), the tobacco material heat time is 6-7min.As more preferably scheme, when heating-up temperature is
240-250 DEG C, the heat time is 6-7min.
It is preferred that, in step (4), when tobacco material is balanced in 22 DEG C of temperature, the environment of relative humidity 60%.
It is preferred that, apply the ethanol solution containing flavouring essence for tobacco and polyalcohol, applied amount to tobacco material in step (4)
For MPipe tobacco:VEthanol=1.0~2g:1mL.It is furthermore preferred that applied amount is MPipe tobacco:VEthanol=1.5g:1mL.
It is preferred that, in step (4), flavouring essence for tobacco be β-caryophyllenol, nonyl lactone, 2- acetyl pyrroles, vanillic aldehyde,
One or more of mixing in acetophenone, 3- acetylpyridines.
It is preferred that, in step (4), polyalcohol for any one or two kinds of propane diols, glycerine mixing.
It is preferred that, in step (5), the tobacco material after perfuming is handled is placed in 22 DEG C of temperature, the ring of relative humidity 60%
48h is balanced in border.
Beneficial effect:The heating that the present invention is provided is not burnt cigarette cigarette core material processing method, relative to prior art, tool
Have the advantage that:
1st, tobacco material is heated under inert gas shielding using this method, tobacco can be effectively prevented from former
The high temperature cabonization of material.
2nd, tobacco material is heated under inert gas shielding using this method, can effectively reduces tobacco material
Acidity, alkaline components, making tobacco material, tart flavour is no longer shown in the flue gas that discharges under heating non-burning state, and flue gas
Excitant is reduced;
3rd, tobacco material is heated under inert gas shielding using this method, the acid of tobacco material release
Property, the amino acid in alkaline components and tobacco material decomposes generation amine by deaminizating and decarboxylic reaction and ammonia can be flowed
Dynamic inert gas discharge heating chamber, so that the material for avoiding tobacco material heating from volatilizing is adsorbed onto tobacco material surface to cigarette
Flue gas under the material heating non-burning state of grassland discharges the influence of aesthetic quality;
4th, the present invention carries out charging processing using the ethanol solution of propane diols or glycerine to tobacco material, increases cigarette
Flue gas release performance of the grassland material under heating non-burning state, improves flue gas concentration.
5th, the present invention adds β-caryophyllenol, nonyl lactone, 2- acetyl pyrroles, vanillic aldehyde, acetophenone, 3- acetyl group
The spices such as pyridine, can increase tobacco characteristic perfume, improve the organoleptic quality for discharging flue gas.
6th, tobacco material using the present invention method processing after, its heat non-burning state under flue gas release stability,
The organoleptic quality of discharged flue gas is substantially improved, and exhaust gas volumn is big, good flue gas matter, low miscellaneous gas, excitant and strength are moderate, cigarette
Gas satisfaction is strong, and the applicability in heating non-combustion-type tobacco product is remarkably reinforced.
7th, operating procedure of the invention is simple, cost is low, with good industrial prospect.
Embodiment
The present invention is further described with reference to specific embodiment.
Embodiment 1:
One kind heats cigarette cigarette core material processing method of not burning, comprises the following steps:Anaerobic glowing furnace is opened, sets and adds
Hot temperature is 240-250 DEG C, and heated in nitrogen atmosphere;After anaerobic glowing furnace reaches the temperature of setting, by tobacco material
Rapid be put into anaerobic glowing furnace heats 6-7min;Heating is finished, and stops heating, and tobacco material is cooled down in nitrogen atmosphere;Will
Tobacco material after cooling is taken out from anaerobic glowing furnace, and 48h is balanced in 22 DEG C of temperature, the environment of relative humidity 60%;To
Tobacco material after balance applies the ethanol solution containing flavouring essence for tobacco and polyalcohol, in placing 48h under sealing state, it is ensured that
Tobacco material is fully absorbed to flavouring essence for tobacco and polyalcohol;Tobacco material after perfuming is handled is placed in 22 DEG C of temperature, relatively
48h is balanced in the environment of humidity 60% and obtains heating cigarette cigarette core material of not burning.
The present invention does not have special limitation to the species of the flavouring essence for tobacco and source, is known using those skilled in the art
Flavouring essence for tobacco.In the present invention, the ethanol solution of the flavouring essence for tobacco and polyalcohol preferentially includes weight percent
The following composition of ratio:β-caryophyllenol 0.5 ‰, nonyl lactone 1 ‰, 2- acetyl pyrroles 2 ‰, vanillic aldehyde 2 ‰, acetophenone
3 ‰, 3- acetylpyridine 3 ‰, glycerine 5 ‰, remaining is absolute ethyl alcohol, and each component summation is 100, is mixed evenly to prepare.
Embodiment 2:
Be the same as Example 1, difference is, the ethanol solution of the flavouring essence for tobacco and polyalcohol includes percentage by weight
Following composition:β-caryophyllenol 0.5 ‰, nonyl lactone 1 ‰, 2- acetyl pyrroles 2 ‰, vanillic aldehyde 2 ‰, acetophenone 3 ‰, 3-
Acetylpyridine 3 ‰, propane diols 5 ‰, remaining is absolute ethyl alcohol, and each component summation is 100, is mixed evenly to prepare.
Application effect appraisal:
The cigarette core material prepared using embodiment 1, the method for embodiment 2 is added with undressed tobacco material (control sample)
It is added in heating non-burning smoking set and carries out sensory quality assessment, evaluation result is shown in Table 1.
Check problem:Sample and check table are provided to 6 experts that smoke panel test, it is desirable to which member of smoking refers to according to form requirement to items
Mark is smoked panel test.
The smoking result of the embodiment of the present invention of table 1
As shown in Table 1, released with flue gas of the treated tobacco material of the method for the present invention under heating non-burning state
Put performance is substantially improved with the organoleptic quality for discharging flue gas, and flue gas satisfaction is strong, and comfortableness is good, in heating non-combustion-type
Applicability in tobacco product is remarkably reinforced.
Described above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art
For member, without departing from the technical principles of the invention, some improvement and deformation can also be made, these improve and deformed
Also it should be regarded as protection scope of the present invention.
Claims (7)
- The cigarette cigarette core material processing method 1. one kind heating is not burnt, it is characterised in that comprise the following steps:(1)Anaerobic glowing furnace is opened, it is 240-250 DEG C to set heating-up temperature, and is heated in nitrogen or inert gas atmosphere;(2)After anaerobic glowing furnace reaches the temperature of setting, tobacco material is put into rapidly in anaerobic glowing furnace and heats 3- 20min;(3)Heating is finished, and stops heating, and tobacco material is cooled down in nitrogen or inert gas atmosphere;(4)The tobacco material of cooling is taken out after balance 24-48h from anaerobic glowing furnace, applies into tobacco material and is used containing cigarette The ethanol solution of essence and alcohol, the alcohol for any one or two kinds of propane diols, glycerine mixing, and in sealing shape 24-48h is placed under state;(5)Tobacco material after perfuming is handled was balanced after a period of time, obtained heating cigarette cigarette core material of not burning.
- The cigarette cigarette core material processing method 2. heating according to claim 1 is not burnt, it is characterised in that:Step(2)In, The tobacco material used is any one or a few in flue-cured tobacco, Turkish tobaccos, burley tobaccos.
- The cigarette cigarette core material processing method 3. heating according to claim 1 is not burnt, it is characterised in that:Step(2)In, The tobacco material heat time is 6-7min.
- The cigarette cigarette core material processing method 4. heating according to claim 1 is not burnt, it is characterised in that:Step(4)In, Tobacco material is balanced in 22 DEG C of temperature, the environment of relative humidity 60%.
- The cigarette cigarette core material processing method 5. heating according to claim 1 is not burnt, it is characterised in that:Step(4)In Apply the ethanol solution containing flavouring essence for tobacco and alcohol to tobacco material, applied amount is MPipe tobacco:VEthanol=1.0~2g:1mL.
- The cigarette cigarette core material processing method 6. heating according to claim 1 is not burnt, it is characterised in that:Step(4)In, Flavouring essence for tobacco is one in β-caryophyllenol, nonyl lactone, 2- acetyl pyrroles, vanillic aldehyde, acetophenone, 3- acetylpyridines Plant or several mixing.
- The cigarette cigarette core material processing method 7. heating according to claim 1 is not burnt, it is characterised in that:Step(5)In, Tobacco material after perfuming is handled is placed in 22 DEG C of temperature, the environment of relative humidity 60% and balances 48h.
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CN201610131559.7A CN105559133B (en) | 2016-03-09 | 2016-03-09 | One kind heats cigarette cigarette core material processing method of not burning |
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CN201610131559.7A CN105559133B (en) | 2016-03-09 | 2016-03-09 | One kind heats cigarette cigarette core material processing method of not burning |
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CN105559133B true CN105559133B (en) | 2017-08-11 |
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Families Citing this family (7)
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CN107699333A (en) * | 2017-11-08 | 2018-02-16 | 江苏恒森烟草机械有限公司 | A kind of high temperature extracts tobacco tar device |
CN110959893A (en) * | 2018-09-26 | 2020-04-07 | 浙江中烟工业有限责任公司 | Tobacco sheet added with functional incense raw materials and heating non-combustion cigarette adopting tobacco sheet |
CN110959888A (en) * | 2018-09-26 | 2020-04-07 | 浙江中烟工业有限责任公司 | Tobacco shred added with functional perfume raw material composition and heating non-combustion cigarette adopting tobacco shred |
CN110959901A (en) * | 2018-09-26 | 2020-04-07 | 浙江中烟工业有限责任公司 | Cigarette adopting tobacco-flavored cut tobacco functional incense raw material composition and being non-combustible by heating |
CN110946316A (en) * | 2018-09-27 | 2020-04-03 | 浙江中烟工业有限责任公司 | Method for treating non-burning tobacco shreds by heating |
CN109275934A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A kind of processing method suitable for heating pipe tobacco under not combustion state |
CN109275943A (en) * | 2018-10-08 | 2019-01-29 | 浙江中烟工业有限责任公司 | A method of moisture in cut tobacco being controlled under not combustion state suitable for heating |
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JPS51101199A (en) * | 1975-02-28 | 1976-09-07 | Takasago Perfumery Co Ltd | Tabakonokokitsumino kaizenhoho |
CN101061888A (en) * | 2006-04-27 | 2007-10-31 | 湖南中烟工业公司 | Device for carbonization and cracking at high temperature and the pyrolysis method |
CN101214086B (en) * | 2008-01-17 | 2010-06-16 | 云南瑞升烟草技术(集团)有限公司 | Method and equipment for pretreating cabo |
CN103445283B (en) * | 2013-09-29 | 2015-03-25 | 中国烟草总公司郑州烟草研究院 | Processing method of tobacco raw materials for heating non-combustion tobacco products |
CN103462213B (en) * | 2013-09-29 | 2015-07-29 | 中国烟草总公司郑州烟草研究院 | A kind of tobacco-containing material preparation method being applicable to heating non-combustion-type tobacco goods |
CN105249518B (en) * | 2015-09-25 | 2017-10-03 | 安徽中烟工业有限责任公司 | A kind of preparation method for heating the porous tobacco-containing material of non-combustion-type cigarette |
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