CN109115383A - The Prediction method for fatigue life of cold extrusion Strengthening Hole - Google Patents

The Prediction method for fatigue life of cold extrusion Strengthening Hole Download PDF

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Publication number
CN109115383A
CN109115383A CN201710492275.5A CN201710492275A CN109115383A CN 109115383 A CN109115383 A CN 109115383A CN 201710492275 A CN201710492275 A CN 201710492275A CN 109115383 A CN109115383 A CN 109115383A
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China
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cold
extrusion
fatigue life
finite element
cold extrusion
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CN201710492275.5A
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CN109115383B (en
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邹成
李汝鹏
凡志磊
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Commercial Aircraft Corp of China Ltd
Shanghai Aircraft Manufacturing Co Ltd
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Commercial Aircraft Corp of China Ltd
Shanghai Aircraft Manufacturing Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L5/00Apparatus for, or methods of, measuring force, work, mechanical power, or torque, specially adapted for specific purposes
    • G01L5/0047Apparatus for, or methods of, measuring force, work, mechanical power, or torque, specially adapted for specific purposes measuring forces due to residual stresses
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/41Refractivity; Phase-affecting properties, e.g. optical path length
    • G01N21/45Refractivity; Phase-affecting properties, e.g. optical path length using interferometric methods; using Schlieren methods
    • GPHYSICS
    • G06COMPUTING; CALCULATING OR COUNTING
    • G06FELECTRIC DIGITAL DATA PROCESSING
    • G06F30/00Computer-aided design [CAD]
    • G06F30/20Design optimisation, verification or simulation
    • G06F30/23Design optimisation, verification or simulation using finite element methods [FEM] or finite difference methods [FDM]

Abstract

The invention discloses a kind of Prediction method for fatigue life of cold extrusion Strengthening Hole.The Prediction method for fatigue life of cold extrusion Strengthening Hole of the invention comprises steps of determining that cold extrusion operating condition;According to identified cold extrusion operating condition, finite element analysis model is established using finite element analysis software;Setting cold-extrusion technology parameter simultaneously carries out Finite Element Simulation Analysis, obtains the simulation result of residual stress distribution and amount of interference;Cold extrusion test piece is made based on cold extrusion operating condition and cold-extrusion technology parameter;The residual stress distribution and amount of interference of cold extrusion test piece are measured;Finite element analysis model is modified according to comparing;Based on modified finite element analysis model, forecast analysis is carried out to fatigue life.The present invention can accurately and efficiently predict the fatigue life of the Cold-Expanded Hole under different cold-extrusion technology methods, and the selection and optimization for cold-extrusion technology method provides reliable basis.

Description

The Prediction method for fatigue life of cold extrusion Strengthening Hole
Technical field
The present invention relates to the fatigue life of the technical field of Prediction method for fatigue life more particularly to cold extrusion Strengthening Hole is pre- Survey method.
Background technique
According to statistics, the fatigue failure of aircraft structure service phase investigation statistics analysis shows, 70% or more structural fatigue Problem occurs in junction, it has also become one of most important root of aviation aircraft structural failure.It can using cold-extrusion technology Achieve the purpose that improve fatigue life in the form of by improving residual stress, but different processes is to the shadow of fatigue life Difference is rung, needs to obtain optimal process by analysis of experiments.
Fatigue life under specific cold-extrusion technology can be obtained by the method for test, but this method is in actual production In the process, it needs to spend a large amount of manpower, financial resources and time.Therefore, it is necessary to the methods predicted using analysis of Fatigue-life to subtract Few tested number, traditional Prediction method for fatigue life can be analyzed under different structure form with using software progress simulation analysis Fatigue life, but influence of the different process to fatigue life can not be usually analyzed, there are still deficiencies for accuracy.
Therefore, need a kind of new simulating analysis, can be set up using less test cold-extrusion technology with it is tired Relationship between the labor service life, efficiently to realize accurate, the reliable prediction for different cold-extrusion technology method fatigue lives.
Summary of the invention
The technical problem to be solved by the present invention is in order to overcome Prediction method for fatigue life in the prior art to be difficult to consider It is influenced brought by different cold-extrusion technologies, and uses the cost of test method test fatigue life excessively high, excessive cycle scarce It falls into, proposes a kind of Prediction method for fatigue life of cold extrusion Strengthening Hole.
The present invention is to solve above-mentioned technical problem by following technical proposals:
The present invention provides a kind of Prediction method for fatigue life of cold extrusion Strengthening Hole, it is characterized in that comprising it is following Step:
Step 1: determining cold extrusion operating condition;
Step 2: establishing finite element analysis mould using finite element analysis software according to the identified cold extrusion operating condition Type;
Step 3: cold-extrusion technology parameter is arranged and carries out finite element and imitates on the basis of the finite element analysis model True analysis, obtains the simulation result of corresponding with the cold-extrusion technology parameter residual stress distribution and amount of interference;
Step 4: making cold extrusion test piece based on the cold extrusion operating condition and the cold-extrusion technology parameter;
Step 5: using residual stress measurement instrument and amount of interference measuring instrument, to the residual stress point of the cold extrusion test piece Cloth and amount of interference measure;
Step 6: the simulation result of residual stress distribution and amount of interference that comparison step three obtains obtained with step 5 it is residual The measurement result of residue stress distribution and amount of interference, and the finite element analysis model is modified according to comparison result, so that It obtains the simulation result and approaches the measurement result;
Step 7: being made based on modified finite element analysis model using analysis of Fatigue-life software with residual stress distribution Forecast analysis is carried out for fatigue life of the input quantity to cold extrusion Strengthening Hole.
Preferably, the cold extrusion operating condition includes aperture and/or the material properties of cold extrusion Strengthening Hole.
Preferably, the finite element analysis model established in step 2 includes test piece part and extruded rod part.
Preferably, the cold-extrusion technology parameter includes press ratio and/or extruding rate.
Preferably, including pair to the measurement that the residual stress distribution and amount of interference of the cold extrusion test piece carry out in step 5 The measurement of at least eight reference point.
Preferably, being executed respectively based on multiple groups cold-extrusion technology parameter Step 3: four, five to obtain the multiple groups cold extrusion The simulation result and measurement result of the corresponding residual stress distribution of technological parameter and amount of interference, and according to institute in step 6 State the simulation result of the corresponding residual stress distribution of multiple groups cold-extrusion technology parameter and amount of interference and the comparison of measurement result As a result the finite element analysis model is modified.
Preferably, the analysis of Fatigue-life software used in step 7 is MSC.fatigue.
Preferably, the forecast analysis in step 7 to the fatigue life of cold extrusion Strengthening Hole, is analyzed using fatigue life S-N Method.
Preferably, also being adopted to mean stress in step 7 in the forecast analysis of the fatigue life of cold extrusion Strengthening Hole It is corrected with goodman equation.
On the basis of common knowledge of the art, above-mentioned each optimum condition, can any combination to get each preferable reality of the present invention Example.
The positive effect of the present invention is that:
The Prediction method for fatigue life of cold extrusion Strengthening Hole of the invention, can overcome the shortcomings of existing methods, using having The test of limit helps to improve the validity of simulation and accuracy of established limit element artificial module, can accurately and efficiently predict The fatigue life of Cold-Expanded Hole under different cold-extrusion technology methods provides reliably for the selection and optimization of cold-extrusion technology method Foundation.Compared to existing method, the present invention can efficiently reduce test period and experimentation cost, reach rapid comparison analysis Purpose.
Detailed description of the invention
Fig. 1 is a preferred embodiment of the present invention the flow chart of the Prediction method for fatigue life of cold extrusion Strengthening Hole.
Specific embodiment
With reference to the accompanying drawings of the specification, further the preferred embodiment of the present invention is described in detail, description below To be illustrative, not limitation of the present invention, any other similar situation are still fallen among protection scope of the present invention.
In specific descriptions below, the term of directionality, such as "left", "right", "upper", "lower", "front", "rear", etc., The direction with reference to described in attached drawing uses.The component of the embodiment of the present invention can be placed in a variety of different directions, directionality Term is for illustrative purposes and not restrictive.
Refering to what is shown in Fig. 1, the Prediction method for fatigue life of the cold extrusion Strengthening Hole of a preferred embodiment according to the present invention, The following steps are included:
Step 1: determining cold extrusion operating condition, it is preferable that the cold extrusion operating condition includes aperture and the material of cold extrusion Strengthening Hole Expect property;
Step 2: establishing finite element analysis mould using finite element analysis software according to the identified cold extrusion operating condition Type, finite element analysis model preferably include test piece part and extruded rod part;
Step 3: cold-extrusion technology parameter is arranged and carries out finite element and imitates on the basis of the finite element analysis model True analysis, obtains the simulation result of corresponding with the cold-extrusion technology parameter residual stress distribution and amount of interference, wherein described Cold-extrusion technology parameter preferably includes press ratio and extruding rate;
Step 4: making cold extrusion test piece based on the cold extrusion operating condition and the cold-extrusion technology parameter;
Step 5: using residual stress measurement instrument and amount of interference measuring instrument, to the residual stress point of the cold extrusion test piece Cloth and amount of interference measure;
Step 6: the simulation result of residual stress distribution and amount of interference that comparison step three obtains obtained with step 5 it is residual The measurement result of residue stress distribution and amount of interference, and the finite element analysis model is modified according to comparison result, so that It obtains the simulation result and approaches the measurement result;
Step 7: being made based on modified finite element analysis model using analysis of Fatigue-life software with residual stress distribution Forecast analysis is carried out for fatigue life of the input quantity to cold extrusion Strengthening Hole.
Some preferred embodiments according to the present invention in the above-mentioned methods can be based on multiple groups cold-extrusion technology parameter point It Zhi Hang not be Step 3: four, five to obtain the corresponding residual stress distribution of the multiple groups cold-extrusion technology parameter and amount of interference Simulation result and measurement result, and according to the corresponding residual stress of the multiple groups cold-extrusion technology parameter in step 6 The comparison result of the simulation result and measurement result of distribution and amount of interference is modified the finite element analysis model.
Some preferred embodiments according to the present invention, to the residual stress distribution of the cold extrusion test piece in step 5 The measurement carried out with amount of interference includes the measurement at least eight reference point.
MSC.fatigue fatigue life can be used in the above method in further preferred embodiment according to the present invention Software is analyzed, wherein fatigue life S-N analysis method specifically can be used, and mean stress is corrected using goodman equation.
The Prediction method for fatigue life of cold extrusion Strengthening Hole of the invention is illustrated for an application example again below.
Cold extrusion operating condition in this application example is, using the slotted liner bushing of Cr15Ni7Mo2Al to 1 piece of 4mm's 2060T8E30 aluminium lithium alloy plate carries out cold extrusion, and the final nominal diameter aperture in the hole of institute's cold extrusion is 4.420mm.
Firstly, being modeled using finite element emulation software ABAQUS, the technological parameter of use includes first hole aperture 4.530mm, duration 0.2s is squeezed, Finite Element Simulation Analysis is carried out to Cold Extrusion Process with this technological parameter, obtains residual stress Distribution.
Secondly, carrying out cold extrusion specimen preparation with above-mentioned emulation operating condition, the 2060T8E30 aluminium lithium alloy plate of 4mm is carried out Drilling, and the nominal value of 4.420mm is made up to using cold-extrusion technology, and using residual stress measurement instrument to residual stress into Row test.For the adequacy for guaranteeing data, it is proposed that measured to no less than 10 holes, each hole takes no less than 8 measurement points. Measurement result and simulation result are compared after completing measurement, and carry out certain amendment to simulation model.It just obtains as a result, Modified finite element analysis model.It, can Cold-Expanded Hole under forecast analysis different technical parameters based on this analysis model Fatigue life.
Different technological parameters is inputted, different residual stress point can be obtained using modified finite element analysis model Cloth.Residual stress distribution is imported in analysis of Fatigue-life software MSC.fatigue again, establishes same forecasting fatigue operating condition, And fatigue life S-N analysis method is chosen, processing is modified using Goodman equation for mean stress, and select maximum Principal stress mode analyzes the multiaxis of stress, and the confidence level of fatigue life can for example be taken as 50%, just can predict to obtain different works The fatigue life of Cold-Expanded Hole under skill parameter.
Although specific embodiments of the present invention have been described above, it will be appreciated by those of skill in the art that these It is merely illustrative of, protection scope of the present invention is defined by the appended claims.Those skilled in the art is not carrying on the back Under the premise of from the principle and substance of the present invention, many changes and modifications may be made, but these are changed Protection scope of the present invention is each fallen with modification.

Claims (9)

1. a kind of Prediction method for fatigue life of cold extrusion Strengthening Hole, which is characterized in that itself the following steps are included:
Step 1: determining cold extrusion operating condition;
Step 2: establishing finite element analysis model using finite element analysis software according to the identified cold extrusion operating condition;
Step 3: cold-extrusion technology parameter is arranged and carries out finite element simulation point on the basis of the finite element analysis model Analysis, obtains the simulation result of corresponding with the cold-extrusion technology parameter residual stress distribution and amount of interference;
Step 4: making cold extrusion test piece based on the cold extrusion operating condition and the cold-extrusion technology parameter;
Step 5: using residual stress measurement instrument and amount of interference measuring instrument, residual stress distribution to the cold extrusion test piece and Amount of interference measures;
Step 6: the remnants that the simulation result of residual stress distribution and amount of interference that comparison step three obtains is obtained with step 5 are answered The measurement result of power distribution and amount of interference, and the finite element analysis model is modified according to comparison result, so that institute It states simulation result and approaches the measurement result;
Step 7: be based on modified finite element analysis model, using analysis of Fatigue-life software, using residual stress distribution as defeated Enter amount and forecast analysis is carried out to the fatigue life of cold extrusion Strengthening Hole.
2. Prediction method for fatigue life as described in claim 1, which is characterized in that the cold extrusion operating condition includes cold-extruded pressure Change aperture and/or the material properties in hole.
3. Prediction method for fatigue life as described in claim 1, which is characterized in that the finite element analysis established in step 2 Model includes test piece part and extruded rod part.
4. Prediction method for fatigue life as described in claim 1, which is characterized in that the cold-extrusion technology parameter includes squeezing Rate and/or extruding rate.
5. Prediction method for fatigue life as described in claim 1, which is characterized in that the cold extrusion test piece in step 5 The measurement that residual stress distribution and amount of interference carry out includes the measurement at least eight reference point.
6. the Prediction method for fatigue life as described in any one of claim 1-5, which is characterized in that be based on multiple groups cold extrusion Technological parameter executes respectively Step 3: four, five to obtain the corresponding residual stress point of the multiple groups cold-extrusion technology parameter The simulation result and measurement result of cloth and amount of interference, and respectively corresponded in step 6 according to the multiple groups cold-extrusion technology parameter Residual stress distribution and amount of interference simulation result and measurement result comparison result to the finite element analysis model carry out Amendment.
7. Prediction method for fatigue life as described in claim 1, which is characterized in that the analysis of Fatigue-life used in step 7 Software is MSC.fatigue.
8. Prediction method for fatigue life as claimed in claim 7, which is characterized in that the tired of cold extrusion Strengthening Hole in step 7 The forecast analysis in labor service life, using fatigue life S-N analysis method.
9. Prediction method for fatigue life as claimed in claim 8, which is characterized in that cold extrusion Strengthening Hole in step 7 In the forecast analysis of fatigue life, also mean stress is corrected using goodman equation.
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110765549A (en) * 2019-10-16 2020-02-07 昆山六丰机械工业有限公司 Method and system for analyzing structural stress of automobile casting
CN111209702A (en) * 2020-01-02 2020-05-29 中车青岛四方机车车辆股份有限公司 Method and device for simulating and testing alignment of rail train body strength
CN111241741A (en) * 2020-03-25 2020-06-05 南京市特种设备安全监督检验研究院 Crane wheel rail abrasion monitoring method based on residual stress influence interval correction
CN111737812A (en) * 2020-05-13 2020-10-02 南京航空航天大学 Fatigue life prediction method for secondary extrusion reinforced hole
CN112100766A (en) * 2020-08-28 2020-12-18 北京航空航天大学 Fatigue life prediction method for cold extrusion reinforced hole structure
CN112214846A (en) * 2020-09-09 2021-01-12 浙江意动科技股份有限公司 Method for reducing stress concentration
CN112906269A (en) * 2021-02-08 2021-06-04 南通中远海运船务工程有限公司 Method for prolonging fatigue life of complex structure of crude oil transfer barge

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102175511A (en) * 2010-12-24 2011-09-07 深圳市大族激光科技股份有限公司 Method and system for estimating material property
CN103455671A (en) * 2013-08-27 2013-12-18 西北工业大学 Method for predicting fatigue life of electromagnetically-riveted joint
CN104268335A (en) * 2014-09-23 2015-01-07 工业和信息化部电子第五研究所 Vibration fatigue life predication method and system for micro-packaging assembly
CN104809311A (en) * 2015-05-14 2015-07-29 东南大学 Structural part remaining life predicting method based on multi-factor fusion correction
CN106547999A (en) * 2016-12-08 2017-03-29 湖南大学 Drawing die structure based on Explicit Dynamics Finite Element Method is analyzed

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102175511A (en) * 2010-12-24 2011-09-07 深圳市大族激光科技股份有限公司 Method and system for estimating material property
CN103455671A (en) * 2013-08-27 2013-12-18 西北工业大学 Method for predicting fatigue life of electromagnetically-riveted joint
CN104268335A (en) * 2014-09-23 2015-01-07 工业和信息化部电子第五研究所 Vibration fatigue life predication method and system for micro-packaging assembly
CN104809311A (en) * 2015-05-14 2015-07-29 东南大学 Structural part remaining life predicting method based on multi-factor fusion correction
CN106547999A (en) * 2016-12-08 2017-03-29 湖南大学 Drawing die structure based on Explicit Dynamics Finite Element Method is analyzed

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
王彩勇等: "开缝衬套冷挤压孔疲劳寿命仿真模型建立及验证", 《兵器材料科学与工程》 *

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110765549A (en) * 2019-10-16 2020-02-07 昆山六丰机械工业有限公司 Method and system for analyzing structural stress of automobile casting
CN111209702A (en) * 2020-01-02 2020-05-29 中车青岛四方机车车辆股份有限公司 Method and device for simulating and testing alignment of rail train body strength
CN111241741A (en) * 2020-03-25 2020-06-05 南京市特种设备安全监督检验研究院 Crane wheel rail abrasion monitoring method based on residual stress influence interval correction
CN111241741B (en) * 2020-03-25 2023-04-28 南京市特种设备安全监督检验研究院 Crane wheel rail abrasion monitoring method based on residual stress influence interval correction
CN111737812A (en) * 2020-05-13 2020-10-02 南京航空航天大学 Fatigue life prediction method for secondary extrusion reinforced hole
CN112100766A (en) * 2020-08-28 2020-12-18 北京航空航天大学 Fatigue life prediction method for cold extrusion reinforced hole structure
CN112214846A (en) * 2020-09-09 2021-01-12 浙江意动科技股份有限公司 Method for reducing stress concentration
CN112906269A (en) * 2021-02-08 2021-06-04 南通中远海运船务工程有限公司 Method for prolonging fatigue life of complex structure of crude oil transfer barge
CN112906269B (en) * 2021-02-08 2023-09-26 南通中远海运船务工程有限公司 Method for prolonging fatigue life of complex structure of crude oil-to-barge

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