CN109056305A - A kind of postfinishing process of water-fastness type dacron - Google Patents
A kind of postfinishing process of water-fastness type dacron Download PDFInfo
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- CN109056305A CN109056305A CN201810705496.0A CN201810705496A CN109056305A CN 109056305 A CN109056305 A CN 109056305A CN 201810705496 A CN201810705496 A CN 201810705496A CN 109056305 A CN109056305 A CN 109056305A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/003—Treatment with radio-waves or microwaves
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
- D06L1/16—Multi-step processes
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/46—Compounds containing quaternary nitrogen atoms
- D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
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- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a kind of postfinishing process of water-fastness type dacron, it is related to fabric post-treatment technical field, the following steps are included: the preparation of (1) post-finishing liquid, (2) it pads, (3) preliminary drying, (4) microwave is fixed, (5) washing, (6) drying.Post-finishing liquid is made using chitosan quaternary ammonium salt, Cocoamidopropyl betaine, softening agent and antistatic agent SN as raw material by the present invention, by the effect endowing terylene soft fabric feel of the post-finishing liquid and excellent washable, yellowing-resistant and antistatic property, to improve the use quality of dacron.
Description
Technical field:
The present invention relates to fabric post-treatment technical fields, and in particular to a kind of rear finishing duplex of water-fastness type dacron
Skill.
Background technique:
Terylene is an important species in synthetic fibers, is the product name of China's polyester fiber.It is with poly- to benzene
Dioctyl phthalate or dimethyl terephthalate (DMT) and ethylene glycol are raw material, through high at fibre prepared by esterification or transesterification and polycondensation reaction
Polymers-polyethylene terephthalate (PET) through spinning and post-processes manufactured fiber.
Softening agent is a major class in post-finishing agent, and major function is the different feel/wind for meeting Polyester Textiles
The requirement of lattice.Polyester Textiles softening agent is broadly divided into two major classes, and the aliphatic type and organic silicon type of non-silicon are most widely used at present
General is organic silicon type.
The development of silicone softening agent substantially experienced three phases, and the first generation is methyl-silicone oil emulsion, this kind of softening agent
Disadvantage be it is poor with the binding force of fiber, it is not washable；It can be in conjunction with fiber although second generation silicone softening agent contains
Hydroxyl, but binding ability is poor, treatment effect is bad；Third generation silicone softening agent can be divided into simple function group according to functional group and change
Property silicone oil and polyfunctional group modified silicon oil can improve the washability, soft of fabric by the affinity of active group enhancing and fiber
Toughness, hydrophily etc..Therefore, how by postfinishing process being used cooperatively for softening agent and other function auxiliary agent improve
The service performance of dacron becomes current research hotspot.
Summary of the invention:
Technical problem to be solved by the present invention lies in a kind of postfinishing process of water-fastness type dacron is provided, through this
Not only flexibility is good for dacron after process, but also with excellent washable, yellowing-resistant and antistatic property, to mention
The use quality of high dacron.
The following technical solution is employed for the technical problems to be solved by the invention to realize:
A kind of postfinishing process of water-fastness type dacron, comprising the following steps:
(1) preparation of post-finishing liquid: into water be added chitosan quaternary ammonium salt, Cocoamidopropyl betaine, softening agent and
Antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) it pads: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:30-50, second dipping and rolling, every time
Impregnate 15-30min, pick-up rate 70-80%；
(3) preliminary drying: by the dacron after above-mentioned pad in 100-110 DEG C of preliminary drying 1-3min；
(4) microwave is fixed: will utilize microwave reactor microwave treatment 30-90s through pre-baked dacron；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 40-50 DEG C of warm water,
Second using 10-20 DEG C of cold water washing, water washing bath ratio 1:15-30；
(6) it dries: by 45-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
Water in the step (1), chitosan quaternary ammonium salt, Cocoamidopropyl betaine, softening agent and antistatic agent SN
Mass ratio is 100:10-20:3-8:1-5:0.5-1.
The operating condition of microwave reactor is microwave frequency 2450MHz, output power 700W in the step (4).
The softening agent is prepared from the following raw materials in parts by weight:
35-45 parts of terpolymer block amido silicon oil, 5-10 parts of PEG-60 rilanit special, acrylic acid-acrylic ester-phosphine
Acid -1-5 parts of sulfonate quadripolymer, white 1-5 parts of aluminium polychloride, 0.5-2 parts of nano-titanium dioxide, 1-hydroxy ethylene-1,1-diphosphonic
Sour 0.5-2 parts of four sodium, 100-200 parts of deionized water.
The nano-titanium dioxide passes through modification, method of modifying are as follows: nano-titanium dioxide is first placed in 100-110
Dry in DEG C baking oven to constant weight, add hydrolysis of polymaleic anhydride, be warming up to 125-135 DEG C of insulated and stirred 5-15min, then plus
Enter trihydroxymethylpropanyltri diglycidyl ether, continues at 125-135 DEG C of insulated and stirred 15-30min, and with the cooling of 5 DEG C/min
Speed is cooled to 0-5 DEG C of heat preservation and stands 0.5-1h, finally crushes obtained solid and nanometer powder is made in milled processed.
The mass ratio of the nano-titanium dioxide, hydrolysis of polymaleic anhydride and trihydroxymethylpropanyltri diglycidyl ether is 1:
0.01-0.05:0.05-0.5。
The beneficial effects of the present invention are:
(1) present invention is using chitosan quaternary ammonium salt, Cocoamidopropyl betaine, softening agent and antistatic agent SN as raw material
Post-finishing liquid is made, by the effect endowing terylene soft fabric feel of the post-finishing liquid and excellent washable, yellowing-resistant and
Antistatic property, to improve the use quality of dacron；
(2) present invention realizes attachment of the post-finishing liquid component on polyester fiber by padding process, and by preliminary drying and
Microwave fixation process improves adhesive rate of the post-finishing liquid component on polyester fiber, and avoids long-time high-temperature process to terylene
Fiber causes irreversible damage；
(3) being used cooperatively come endowing terylene soft fabric feel by the softening agent of the invention, while improving terylene
The washability and yellowing resistance of fabric；And by improving its washability to the modification of nano-titanium dioxide, utilize
The distinctive permeability of nano-titanium dioxide enhances adhesive force of the softening agent functional component on polyester fiber, and then improves through soft
Soft dose of treated dacron wash durability, avoids fabric pliability rapid drawdown after washing.
Specific embodiment:
In order to be easy to understand the technical means, the creative features, the aims and the efficiencies achieved by the present invention, tie below
Specific embodiment is closed, the present invention is further explained.
Terpolymer block amido silicon oil in following embodiment and reference examples selects Jiaxing Ke Rui organosilicon Co., Ltd
The 815 of production, acrylic acid-acrylic ester-phosphonic acids-sulfonate quadripolymer select the calm and peaceful water process science and technology share in Shandong limited
The TH-241 of company's production.
Embodiment 1
Postfinishing process:
(1) preparation of post-finishing liquid: into 100g water be added 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine,
1.5g softening agent and 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) microwave is fixed: by through pre-baked dacron using microwave frequency 2450MHz, output power 700W it is micro-
Wave reactor microwave treatment 60s；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 45-50 DEG C of warm water,
Second using 15-20 DEG C of cold water washing, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
The preparation of softening agent:
40g terpolymer block amido silicon oil, 8g PEG-60 rilanit special, 5g third are added into 160g deionized water
Olefin(e) acid-acrylate-phosphonic acids-sulfonate quadripolymer, 3g white aluminium polychloride, 0.5g nano-titanium dioxide, 0.5g hydroxyl
Four sodium of base ethylene-diphosphonic acid, is uniformly mixed to get softening agent.
Embodiment 2
Postfinishing process:
(1) preparation of post-finishing liquid: into 100g water be added 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine,
2g softening agent and 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) microwave is fixed: by through pre-baked dacron using microwave frequency 2450MHz, output power 700W it is micro-
Wave reactor microwave treatment 60s；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 45-50 DEG C of warm water,
Second using 15-20 DEG C of cold water washing, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
The preparation of softening agent:
40g terpolymer block amido silicon oil, 8g PEG-60 rilanit special, 5g third are added into 160g deionized water
Olefin(e) acid-acrylate-phosphonic acids-sulfonate quadripolymer, 3g white aluminium polychloride, 0.5g nano-titanium dioxide, 0.5g hydroxyl
Four sodium of base ethylene-diphosphonic acid, is uniformly mixed to get softening agent.
Embodiment 3
Postfinishing process:
(1) preparation of post-finishing liquid: into 100g water be added 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine,
2g softening agent and 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) microwave is fixed: by through pre-baked dacron using microwave frequency 2450MHz, output power 700W it is micro-
Wave reactor microwave treatment 60s；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 45-50 DEG C of warm water,
Second using 15-20 DEG C of cold water washing, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
The preparation of softening agent:
40g terpolymer block amido silicon oil, 8g PEG-60 rilanit special, 5g third are added into 160g deionized water
Olefin(e) acid-acrylate-phosphonic acids-sulfonate quadripolymer, 3g white aluminium polychloride, 0.5g modified nano-titanium dioxide,
Four sodium of 0.5g 1-hydroxy ethylidene-1,1-diphosphonic acid, is uniformly mixed to get softening agent.
The preparation of modified nano-titanium dioxide: first 1g nano-titanium dioxide is placed in 105-110 DEG C of baking oven and is dried to perseverance
Weight, adds 0.05g hydrolysis of polymaleic anhydride, is warming up to 130-135 DEG C of insulated and stirred 10min, and tri- hydroxyl first of 0.25g is then added
Base propane triglycidyl ether continues at 130-135 DEG C of insulated and stirred 15min, and is cooled to 0- with the cooling rate of 5 DEG C/min
5 DEG C of heat preservations stand 30min, finally crush obtained solid and nanometer powder is made in milled processed.
Reference examples 1
Postfinishing process:
(1) preparation of post-finishing liquid: into 100g water be added 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine,
1.5g softening agent and 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) microwave is fixed: by through pre-baked dacron using microwave frequency 2450MHz, output power 700W it is micro-
Wave reactor microwave treatment 60s；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 45-50 DEG C of warm water,
Second using 15-20 DEG C of cold water washing, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
The preparation of softening agent:
40g terpolymer block amido silicon oil, 8g PEG-60 rilanit special, 5g third are added into 160g deionized water
Olefin(e) acid-acrylate-phosphonic acids-sulfonate quadripolymer, 0.5g nano-titanium dioxide, four sodium of 0.5g 1-hydroxy ethylidene-1,1-diphosphonic acid,
It is uniformly mixed to get softening agent.
Reference examples 2
Postfinishing process:
(1) preparation of post-finishing liquid: into 100g water be added 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine,
1.5g softening agent and 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) microwave is fixed: by through pre-baked dacron using microwave frequency 2450MHz, output power 700W it is micro-
Wave reactor microwave treatment 60s；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 45-50 DEG C of warm water,
Second using 15-20 DEG C of cold water washing, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
The preparation of softening agent:
It is white that 40g terpolymer block amido silicon oil, 8g PEG-60 rilanit special, 3g are added into 160g deionized water
Color aluminium polychloride, 0.5g nano-titanium dioxide, four sodium of 0.5g 1-hydroxy ethylidene-1,1-diphosphonic acid, are uniformly mixed to get softening agent.
Reference examples 3
Postfinishing process:
(1) preparation of post-finishing liquid: into 100g water be added 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine,
1.5g softening agent and 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) it washes: being washed twice to through pre-baked dacron, washed for the first time using 45-50 DEG C of warm water, the
It is secondary to be washed using 15-20 DEG C of cold water, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
The preparation of softening agent:
40g terpolymer block amido silicon oil, 8g PEG-60 rilanit special, 5g third are added into 160g deionized water
Olefin(e) acid-acrylate-phosphonic acids-sulfonate quadripolymer, 3g white aluminium polychloride, 0.5g nano-titanium dioxide, 0.5g hydroxyl
Four sodium of base ethylene-diphosphonic acid, is uniformly mixed to get softening agent.
Blank example
Postfinishing process:
(1) 15g chitosan quaternary ammonium salt, 5g Cocoamidopropyl betaine the preparation of post-finishing liquid: are added into 100g water
With 0.5g antistatic agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:40, second dipping and rolling impregnates every time
20min, pick-up rate 75%；
(3) preliminary drying: by the dacron after above-mentioned pad in 105-110 DEG C of preliminary drying 2min；
(4) microwave is fixed: by through pre-baked dacron using microwave frequency 2450MHz, output power 700W it is micro-
Wave reactor microwave treatment 60s；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 45-50 DEG C of warm water,
Second using 15-20 DEG C of cold water washing, water washing bath ratio 1:20；
(6) it dries: by 50-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
Embodiment 4
Based on embodiment 1, it is arranged in and does not add the reference examples 1 of white aluminium polychloride when preparing softening agent, making
Acrylic acid-acrylic ester-phosphonic acids-sulfonate quadripolymer reference examples 2 are not added when standby softening agent, without microwave fixation
The reference examples 3 of processing.
It is utilized respectively embodiment 1-3, reference examples 1-3, blank example and carries out final finishing to batch same specification dacron, to warp
Dacron after above-mentioned final finishing is tested for the property, and the results are shown in Table 1.
Stiffness: referring to GB/T 7689.4-2001 standard；
Washability: referring to GB/T 3921-2008 standard, stiffness after measurement is soaped 50 times；
Color inhibition: referring to ISO 105-X18；2007 standards.
The softening agent of the present invention of table 1 influences the performance of dacron
| Group | Stiffness | Washability | Color inhibition grade |
| Blank example | 4.85 | 5.93 | 2 |
| Embodiment 1 | 2.35 | 2.78 | 3 |
| Embodiment 2 | 2.21 | 2.56 | 3-4 |
| Embodiment 3 | 1.78 | 2.04 | 4 |
| Reference examples 1 | 2.49 | 3.07 | 3-4 |
| Reference examples 2 | 2.74 | 3.52 | 3 |
| Reference examples 3 | 3.18 | 3.86 | 2-3 |
The stiffness variation for being not added with the fabric of softening agent processing and the fabric of addition softening agent processing is bigger, illustrates to add
The fabric softness of softening agent processing is better；Stiffness variation is smaller after soaping 50 times, illustrates that washability is better；Color inhibition grade
It is higher, illustrate that yellowing resistance is better.
The above shows and describes the basic principles and main features of the present invention and the advantages of the present invention.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (4)
1. a kind of postfinishing process of water-fastness type dacron, which comprises the following steps:
(1) preparation of post-finishing liquid: chitosan quaternary ammonium salt, Cocoamidopropyl betaine, softening agent are added into water and resists quiet
Electric agent SN, stirring and dissolving is completely to get post-finishing liquid；
(2) pad: by dacron thorough impregnation in above-mentioned post-finishing liquid, bath raio 1:30-50, second dipping and rolling impregnates every time
15-30min, pick-up rate 70-80%；
(3) preliminary drying: by the dacron after above-mentioned pad in 100-110 DEG C of preliminary drying 1-3min；
(4) microwave is fixed: will utilize microwave reactor microwave treatment 30-90s through pre-baked dacron；
(5) it washes: the dacron through microwave fixation is washed twice, washed for the first time using 40-50 DEG C of warm water, second
It is secondary to be washed using 10-20 DEG C of cold water, water washing bath ratio 1:15-30；
(6) it dries: by 45-55 DEG C of hot-air seasoning of dacron after washing, i.e. completion final finishing.
2. the postfinishing process of water-fastness type dacron according to claim 1, it is characterised in that: the step (1)
Middle water, chitosan quaternary ammonium salt, Cocoamidopropyl betaine, softening agent and antistatic agent SN mass ratio be 100:10-20:3-
8:1-5:0.5-1。
3. the postfinishing process of water-fastness type dacron according to claim 1, it is characterised in that: the step (4)
The operating condition of middle microwave reactor is microwave frequency 2450MHz, output power 700W.
4. the postfinishing process of water-fastness type dacron according to claim 1, it is characterised in that: the softening agent by
The raw material of following parts by weight is made:
35-45 parts of terpolymer block amido silicon oil, 5-10 parts of PEG-60 rilanit special, acrylic acid-acrylic ester-phosphonic acids-
1-5 parts of sulfonate quadripolymer, white 1-5 parts of aluminium polychloride, 0.5-2 parts of nano-titanium dioxide, 1-hydroxy ethylidene-1,1-diphosphonic acid
Four 0.5-2 parts of sodium, 100-200 parts of deionized water.
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| CN114775193A (en) * | 2022-04-01 | 2022-07-22 | 深圳全棉时代科技有限公司 | Efficient drying process |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1584191A (en) * | 2004-05-28 | 2005-02-23 | 刘国平 | Nanometer softening smoothing agent and preparing method thereof |
| CN104404755A (en) * | 2014-11-04 | 2015-03-11 | 苏州经贸职业技术学院 | Anti-wrinkle silk fabric preparation method |
| CN106012545A (en) * | 2016-05-12 | 2016-10-12 | 浙江理工大学 | Aging, corrosion, bacterium and fouling resisting oiling agent for polyester fiber |
| CN106930108A (en) * | 2017-05-09 | 2017-07-07 | 深圳优普莱等离子体技术有限公司 | A kind of method of textile chitosan antibacterial finishing |
| CN107604661A (en) * | 2017-09-29 | 2018-01-19 | 安徽省创安体育用品有限公司 | A kind of method for lifting apocynum fibre tension failure performance |
| CN107938128A (en) * | 2017-11-30 | 2018-04-20 | 江苏圣澜服饰创意有限公司 | A kind of production technology of cotton soybean fiber polypropylene fibre rapid-curing cutback knitting fabric |
-
2018
- 2018-07-02 CN CN201810705496.0A patent/CN109056305A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1584191A (en) * | 2004-05-28 | 2005-02-23 | 刘国平 | Nanometer softening smoothing agent and preparing method thereof |
| CN104404755A (en) * | 2014-11-04 | 2015-03-11 | 苏州经贸职业技术学院 | Anti-wrinkle silk fabric preparation method |
| CN106012545A (en) * | 2016-05-12 | 2016-10-12 | 浙江理工大学 | Aging, corrosion, bacterium and fouling resisting oiling agent for polyester fiber |
| CN106930108A (en) * | 2017-05-09 | 2017-07-07 | 深圳优普莱等离子体技术有限公司 | A kind of method of textile chitosan antibacterial finishing |
| CN107604661A (en) * | 2017-09-29 | 2018-01-19 | 安徽省创安体育用品有限公司 | A kind of method for lifting apocynum fibre tension failure performance |
| CN107938128A (en) * | 2017-11-30 | 2018-04-20 | 江苏圣澜服饰创意有限公司 | A kind of production technology of cotton soybean fiber polypropylene fibre rapid-curing cutback knitting fabric |
Non-Patent Citations (4)
| Title |
|---|
| 何伟方: "《微波在纺织工业中的应用》", 31 May 1990, 纺织工业出版社 * |
| 刘江坚: "《染整节能减排新技术》", 31 May 2015, 中国纺织出版社 * |
| 周宏湘: "《染整新技术问答》", 30 April 1998, 中国纺织出版社 * |
| 杨继生: "《表面活性剂原理与应用》", 31 December 2012, 东南大学出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114775193A (en) * | 2022-04-01 | 2022-07-22 | 深圳全棉时代科技有限公司 | Efficient drying process |
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