CN109056187A - Utilize the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material - Google Patents
Utilize the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material Download PDFInfo
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- CN109056187A CN109056187A CN201810682877.1A CN201810682877A CN109056187A CN 109056187 A CN109056187 A CN 109056187A CN 201810682877 A CN201810682877 A CN 201810682877A CN 109056187 A CN109056187 A CN 109056187A
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- denim
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Classifications
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- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/44—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling
- D04H1/46—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres
- D04H1/48—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres in combination with at least one other method of consolidation
- D04H1/485—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties the fleeces or layers being consolidated by mechanical means, e.g. by rolling by needling or like operations to cause entanglement of fibres in combination with at least one other method of consolidation in combination with weld-bonding
Abstract
The invention discloses the methods using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material, and steps are as follows: ornament is first removed, by denim shredding at fleeces;Polypropylene fibre is cut into feeding roller formula carding machine after staple fiber mixes in proportion with denim fleeces again, it cleans, mix through cylinder, doffer, working roll and angle stripper, uniformly at single fiber shape, secondly, single fiber shape is combed into thin net, web is made in thin net;Needle thorn finally is carried out to fibre web film, obtains Nomex, then Nomex is placed on hot-press solidifying on hot press.Preparation method of the invention, the thinking that traditional-handwork is laid with enhancing composite material is abandoned, waste and old cowboy's fiber/polypropylene fiber needled felt is prepared using a kind of nonwoven needled technique, and use hot-forming rapid curing, this kind of Nomex enhancing composite materials property is uniform, and interlayer and in-plane mechanical properties are high.
Description
Technical field
The invention belongs to fibre reinforced composites technical fields, and in particular to a kind of to utilize waste and old denim and polypropylene
The method of fiber preparation cowboy's fiber reinforced polypropylene composite material.
Background technique
The whole world generates more than 4,000 ten thousand tons of waste textiles every year at present, wherein China is annual about to generate 20,000,000 tons.And
As the improvement of people's living standards, the consumption figure to clothes is being continuously increased, the quantity of corresponding waste textile is also being held
It is continuous to increase, 895,000,000 tons will be reached to the year two thousand fifty waste textile.Chemical fibre textile accounts in the waste textile of China
70%, Nature Fibre Textile product account for 30%, and wherein cotton fiber waste textile has accounted for 15% or so.The use that these cotton fibers have
Come with other chemical fibre hybrid woven clothes, such as polyester-cotton blend blending product, some is used directly to do Pure cotton Product, as we are several
Everyone is owned by least one two jeans, and most of is woven drill material, and ingredient almost 100% is cotton fibre
Dimension.With the diversification of the Aesthetic Style of people, denim replacement period is shorter and shorter, and a large amount of waste and old denim is eliminated down
Come.These waste textiles 97% can be theoretically recycled, but the waste textile ratio actually recycled is very
It is low.The processing means of current waste textile are mainly still burned or are buried.Burning can generate a large amount of toxic gases, pollute
Atmospheric environment, buries the dyestuff that can be allowed on denim and chemical substance is discharged into soil, and soil pollution is caused in turn result in water
Pollution.
Due to the deterioration of shortage of resources and environment, people gradually recognize effective use to resource and protection environment to working as
The important meaning of the preceding sustainable development of socio-economy.Therefore, the recycling to waste and old denim is all increased all over the world.It is useless
The way of recycling of old textile has chemical recovery and mechanical recycling two major classes.Chemical recovery will consider asking for dyestuff on textile
Topic, and mechanical recycling possesses lower cost than chemical recovery.The mechanical performance of reinforcing material is than fiber in the composite
Color and appearance are more important.The replacement time of present jean is short, in waste and old jean fibre strength reduce and it is few, therefore
Some researchers are dedicated to the reinforcement that waste and old jean is processed into fiber product as composite material.At present with waste and old cowboy
Most of the method for cloth enhancing composite material is using waste and old denim direct hand pasting forming or hot-forming.However, at present
Most of fashion jeans pass through old-imitating treatment, the jeans that many young men wear have many holes, are difficult direct shearing use
Make the reinforcement material of composite material.In addition, the surface density of denim is very high, resin is obstructed in mobility wherein, is difficult benefit
Composite material is produced with resin transfer molding (RTM) process (RTM) or vacuum-bag process technique.Therefore, some scholars or enterprise will
Denim is processed into threadiness to enhance composite material.This method solve it is above-mentioned directly with denim enhancing composite material deposit
The problem of, but the main at present method using craft laying cowboy's fiber enhances composite material, is difficult that laying is uniform, this is just
It causes composite property to differ greatly, can not be used as structural member.
In textile processing technology, the raw material that non-woven processing technology needs is exactly chopped strand, waste and old jean warp
The cowboy's fibre length obtained after planting-opener shredding (is concentrated mainly within the scope of 30-45mm) between 23-71mm, meets non-knit
It makes and combs requirement of the networking to fibre length 20-150mm in processing technology.Mixed and disorderly fiber, which carries out combing, can become very
Even web can form Nomex using needling treatment.Therefore using nonwoven needled technique can produce it is each to
The Nomex of the same sex, this method can solve that the not uniform mechanical property of current fibre reinforced composites performance is low to ask
Topic.
Matrix resin has and can be divided into thermosetting resin and thermoplastic resin two major classes.Wherein, polypropylene is that a kind of property is excellent
Inexpensive, widely used resins for universal use, have high heat distortion temperature, excellent rigidity, electrical insulating property, density it is small, it is corrosion-resistant,
The features such as humidity, fire-retardant, brilliant folding resistance and easy processing form.The fields such as plastics, fiber thus are widely used in, the whole world
1 year output is about 30,000,000 tons.In recent years, being continuously increased with polypropylene product yield and consumption, it is waste and old poly-
Propylene is also more and more, has been further exacerbated by the environmental problem and social concern got worse.The processing of waste and old polypropylene in the past
Method is mainly burned and landfill, and in recent years, due to petroleum resources growing tension, polypropylene price is also floated.Therefore, it gives up
Extensive concern and great attention of the old polyacrylic recycling by countries in the world.Therefore some researchers are by waste and old polypropylene
Recycling carries out spinning, but the decline of this fibrous mechanical property is larger, should not make high-grade product, therefore application is limited.
But if this fiber is used into the disadvantage that can avoid mechanical property deficiency as the matrix of reinforcing material.This will
It greatly improves the added value of polypropylene product, while reasonable utilization waste polypropylene plastic, reduces production cost, also avoid
Waste polypropylene plastic environmental pollution.
The decomposition temperature of cotton fiber between 240 DEG C -400 DEG C, and be more than 90% decomposable process occur 300 DEG C with
On.Polyacrylic fusing point is 176 DEG C, therefore the present invention will be to carry out mixing comb for waste and old cowboy's fiber and waste and old polypropylene fiber
Networking is managed, then passes through needle felting, is then being lower than waste and old cowboy's fiber/waste and old polypropylene fiber needled felt on press
It is hot-forming under conditions of 240 DEG C to prepare waste and old cowboy's fiber reinforcement waste polypropylene composite material.Waste and old cowboy's fiber reinforcement
Waste polypropylene composite material possesses low-density and high specific strength feature, therefore can be widely applied with its composite material enhanced
In multiple fields such as automobile, furniture, buildings, there is vast potential for future development.
Summary of the invention
Polypropylene enhancing composite material is prepared using denim and polypropylene fibre the object of the present invention is to provide a kind of
It is uneven to solve the enhancing composite materials property existing in the prior art directly prepared by waste and old cowboy's fiber for method
Problem even, mechanical property is lower, while improving the utilization rate of waste and old cowboy's clothing.
The technical scheme adopted by the invention is that poly- using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforcement
The method of acrylic composite, specifically includes the following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved makes its shredding at fiber using planting-opener
Wadding;
Polypropylene fibre is cut into feeding roller formula comb after staple fiber mixes in proportion with denim fleeces by step 2
Reason machine cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber shape, combing by single fiber shape
At thin net;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains with a thickness of 1-4mm and cohesive force being 5-20N's
Nomex;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5.
The features of the present invention also characterized in that
The fibre length of the waste and old cowboy's fleeces obtained after shredding in step 1 is 20-80mm.
The length of polypropylene fibre after cutting in step 2 is 30-45mm.
The quality of waste and old cowboy's fiber accounts for the 30%- of waste and old cowboy's fiber and polypropylene fibre quality sum in step 2
70%.
Needling density in step 4 is 1-15 thorn/cm2。
The temperature of hot-press solidifying is 176-240 DEG C, pressure 3-20MPa, time 2-10min in step 5.
The invention has the advantages that
(1) present invention prepares the side of cowboy's fiber reinforced polypropylene composite material using waste and old denim and polypropylene fibre
Method has abandoned the thinking that traditional-handwork is laid with enhancing composite material, using a kind of nonwoven needled technique compared with prior art
Waste and old cowboy's fiber/polypropylene fiber needled felt is prepared, and uses hot-forming rapid curing for waste and old fibre reinforced polypropylene
Composite material;
(2) present invention prepares the side of cowboy's fiber reinforced polypropylene composite material using waste and old denim and polypropylene fibre
The enhancing composite materials property of method preparation is uniform, and interlayer and in-plane mechanical properties are high, is the system of waste and old composite material for weaving
Offer new method is provided;
(3) present invention prepares the side of cowboy's fiber reinforced polypropylene composite material using waste and old denim and polypropylene fibre
Method, the main component of waste and old denim are cotton fiber, good spinnability, and cotton fiber natural convolution makes it have certain obvolvent
Power.And polypropylene fibre favorable rates it is honest and clean, with high heat distortion temperature, excellent rigidity, electrical insulating property, density it is small, it is corrosion-resistant,
Special, the composite woods prepared by two kinds of waste and old fibre mixing networkings such as humidity, fire-retardant, brilliant folding resistance and easy processing molding
The advantages of material can play two kinds of fibers simultaneously, makes its performance learn from other's strong points to offset one's weaknesses, the excellent composite material of forming properties;
(4) present invention prepares the side of cowboy's fiber reinforced polypropylene composite material using waste and old denim and polypropylene fibre
Method, the denim of selection are textile waste, and waste and old polypropylene polypropylene fibre is secondary use fiber, it is possible to reduce the wave of resource
Take, improves the utilization rate of textile waste, while the pollution to environment can also be caused to avoid the landfill of textile waste and burning.
Specific embodiment
The present invention is described in detail With reference to embodiment.
The method that the present invention prepares cowboy's fiber reinforced polypropylene composite material using waste and old denim and polypropylene fibre,
Specifically includes the following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved keeps its shredding long at fiber using planting-opener
Degree is 20-80mm fleeces;
Step 2, polypropylene fibre is cut into fibre length be 30-45mm staple fiber and denim fleeces in proportion
Feeding roller formula carding machine after mixing cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber
Single fiber shape is being combed into thin net by shape, wherein the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and waste and old polypropylene is poly-
The 30%-70% of tacryl quality sum;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains with a thickness of 1-4mm and cohesive force being 5-20N's
Nomex;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5, wherein the temperature of hot-press solidifying
It is 176-240 DEG C, pressure 3-20MPa, time 2-10min.
Embodiment 1
It is specific to wrap using the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material
Include following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved keeps its shredding long at fiber using planting-opener
Degree is 20mm fleeces;
Step 2, polypropylene fibre is cut into fibre length be 30mm staple fiber and denim fleeces mix in proportion
Feeding roller formula carding machine after conjunction cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber shape,
Single fiber shape is being combed into thin net, wherein the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and polypropylene fibre quality
The sum of 30%;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains piercing with a thickness of the needle that 1mm and cohesive force are 5N
Felt;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5, wherein the temperature of hot-press solidifying
It is 176 DEG C, pressure 3MPa, time 2min.
Embodiment 2
It is specific to wrap using the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material
Include following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved keeps its shredding long at fiber using planting-opener
Degree is 40mm fleeces;
Step 2, polypropylene fibre is cut into fibre length be 35mm staple fiber and denim fleeces mix in proportion
Feeding roller formula carding machine after conjunction cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber shape,
Single fiber shape is being combed into thin net, wherein the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and polypropylene fibre quality
The sum of 40%;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains piercing with a thickness of the needle that 2mm and cohesive force are 15N
Felt;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5, wherein the temperature of hot-press solidifying
It is 200 DEG C, pressure 15MPa, time 8min.
Embodiment 3
It is specific to wrap using the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material
Include following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved keeps its shredding long at fiber using planting-opener
Degree is 80mm fleeces;
Step 2, polypropylene fibre is cut into fibre length be 45mm staple fiber and denim fleeces mix in proportion
Feeding roller formula carding machine after conjunction cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber shape,
Single fiber shape is being combed into thin net, wherein the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and polypropylene fibre quality
The sum of 70%;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains piercing with a thickness of the needle that 4mm and cohesive force are 20N
Felt;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5, wherein the temperature of hot-press solidifying
It is 240 DEG C, pressure 20MPa, time 10min.
Embodiment 4
It is specific to wrap using the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material
Include following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved keeps its shredding long at fiber using planting-opener
Degree is 25mm fleeces;
Step 2, polypropylene fibre is cut into fibre length be 35mm staple fiber and denim fleeces mix in proportion
Feeding roller formula carding machine after conjunction cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber shape,
Single fiber shape is being combed into thin net, wherein the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and polypropylene fibre quality
The sum of 50%;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains piercing with a thickness of the needle that 3mm and cohesive force are 10N
Felt;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5, wherein the temperature of hot-press solidifying
It is 210 DEG C, pressure 18MPa, time 5min.
Embodiment 5
It is specific to wrap using the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material
Include following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved keeps its shredding long at fiber using planting-opener
Degree is 40mm fleeces;
Step 2, polypropylene fibre is cut into fibre length be 35mm staple fiber and denim fleeces mix in proportion
Feeding roller formula carding machine after conjunction cleans through cylinder, doffer, working roll and angle stripper, mixes, uniformly at single fiber shape,
Single fiber shape is being combed into thin net, wherein the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and polypropylene fibre quality
The sum of 60%;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains piercing with a thickness of the needle that 2mm and cohesive force are 18N
Felt;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5, wherein the temperature of hot-press solidifying
It is 180 DEG C, pressure 18MPa, time 9min.
Side using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material of the invention
Method has abandoned the thinking that traditional-handwork is laid with enhancing composite material, using a kind of nonwoven needled technique compared with prior art
Waste and old cowboy's fiber/polypropylene fiber needled felt is prepared, and uses hot-forming rapid curing for waste and old fibre reinforced polypropylene
Composite material, and the material mechanical performance prepared is uniform, interlayer and in-plane mechanical properties are high, are the system of waste and old composite material for weaving
Offer new method is provided;Meanwhile the main component of waste and old denim is cotton fiber, good spinnability, cotton fiber natural convolution makes it
With certain cohesive force, and the denim selected is textile waste, and waste and old polypropylene polypropylene fibre is secondary use fiber,
The waste that resource can be reduced improves the utilization rate of textile waste, while can also make to avoid the landfill of textile waste and burning
The pollution of pairs of environment, and polypropylene fibre favorable rates it is honest and clean, with high heat distortion temperature, excellent rigidity, electrical insulating property, close
It is special to spend small, corrosion-resistant, humidity, fire-retardant, brilliant folding resistance and easy processing molding etc., by two kinds of waste and old fibre mixing networkings
The composite material of preparation can play the advantages of two kinds of fibers simultaneously, its performance is made to learn from other's strong points to offset one's weaknesses, excellent compound of forming properties
Material.
Claims (6)
1. using the method for waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene composite material, feature exists
In, specifically includes the following steps:
Ornament in step 1, the waste and old denim of removal, denim is paved makes its shredding at fleeces using planting-opener;
Polypropylene fibre is cut into feeding roller formula carding machine after staple fiber is mixed with denim fleeces by step 2, through tin
Woods, doffer, working roll and angle stripper clean, mix, uniformly at single fiber shape, and single fiber shape is being combed into thin net;
Using cross-lapped machine fiber membrane is made in thin net by step 3;
Step 4 reinforces fiber membrane progress repeated puncture, obtains piercing with a thickness of the needle that 1-4mm and cohesive force are 5-20N
Felt;
Nomex obtained in step 4 is placed on hot-press solidifying on hot press by step 5.
2. according to claim 1 compound using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene
The method of material, which is characterized in that the fibre length of the waste and old cowboy's fleeces obtained after shredding in the step 1 is 20-
80mm。
3. according to claim 1 compound using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene
The method of material, which is characterized in that the length of the polypropylene fibre after cutting after cutting in the step 2 is 30-45mm.
4. according to claim 1 compound using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene
The method of material, which is characterized in that the quality of waste and old cowboy's fiber accounts for waste and old cowboy's fiber and polypropylene fibre in the step 2
The 30%-70% of quality sum.
5. according to claim 1 compound using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene
The method of material, which is characterized in that the density that needle pierces in the step 4 is 1-15 thorn/cm2。
6. according to claim 1 compound using waste and old denim and polypropylene fibre preparation cowboy's fiber reinforced polypropylene
The method of material, which is characterized in that the temperature of hot-press solidifying is 176-240 DEG C, pressure 3-20MPa in the step 5, the time
For 2-10min.
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Cited By (3)
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CN110343314A (en) * | 2019-06-28 | 2019-10-18 | 中塑联新材料科技湖北有限公司 | A method of plastics activeness and quietness agent is prepared with waste textile opening fiber |
CN110512436A (en) * | 2019-08-30 | 2019-11-29 | 大连工业大学 | A kind of pigment or coating and its preparation method and application based on discarded denim powder |
CN111809276A (en) * | 2020-06-03 | 2020-10-23 | 艾达索高新材料芜湖有限公司 | Face-shaped fiber leftover material recycling method |
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