CN109052940A - A kind of heat-insulated compound glass material and preparation method thereof - Google Patents
A kind of heat-insulated compound glass material and preparation method thereof Download PDFInfo
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- CN109052940A CN109052940A CN201811277026.5A CN201811277026A CN109052940A CN 109052940 A CN109052940 A CN 109052940A CN 201811277026 A CN201811277026 A CN 201811277026A CN 109052940 A CN109052940 A CN 109052940A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B19/00—Other methods of shaping glass
- C03B19/12—Other methods of shaping glass by liquid-phase reaction processes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C14/00—Glass compositions containing a non-glass component, e.g. compositions containing fibres, filaments, whiskers, platelets, or the like, dispersed in a glass matrix
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- Chemical Kinetics & Catalysis (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Ceramic Engineering (AREA)
- Dispersion Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
The invention discloses a kind of heat-insulated compound glass materials and preparation method thereof, including following raw material by weight: 100-150 parts of base-material, 20-45 parts of pyrophillite, 25-50 parts of aluminium oxide, 10-30 parts of cosolvent, 15-25 parts of coagulator；Base-material processing, air-dries, then smash after base-material is cleaned, obtains coarse crushing base-material；Coarse crushing base-material is further smashed, is refiltered, base materials powder is obtained；Base materials powder is added in cosolvent and is stirred, while being heated, aluminium oxide is added after mixing, obtains mixing base fluid；Into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated compound glass material.The heat-insulated compound glass material of the present invention, aluminium oxide and pyrophillite are mixed into compound glass material, can reduce thermal conductivity, enhance heat insulation；The preparation method of heat-insulated compound glass material, manufacture craft is simple, at low cost.
Description
Technical field
The present invention relates to a kind of compound glass material and preparation method thereof, specifically a kind of heat-insulated compound glass material and
Preparation method.
Background technique
Glass is amorphous inorganic non-metallic material, is usually primary raw material with a variety of inorganic minerals, is additionally incorporated a small amount of
Made of auxiliary material.Its main component is silica and other oxides.The main component of simple glass is silicate
Double salt is a kind of non-crystalline solids of random structure.It is widely used in building, is used to belong to mixture every wind light transmission.Separately
Have the oxide for being mixed into certain metals perhaps salt and show color coloured glass and by physics or chemistry side
Tempered glass made from method etc..Sometimes some transparent plastics (such as polymethyl methacrylate) are also referred to as organic glass.
Compound glass material at present cannot reduce thermal conductivity well, and in turn resulting in cannot be heat-insulated well.
Summary of the invention
The purpose of the present invention is to provide a kind of heat-insulated compound glass materials and preparation method thereof, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the invention provides the following technical scheme:
A kind of heat-insulated compound glass material, including following raw material by weight: 100-150 parts of base-material, pyrophillite 20-
45 parts, 25-50 parts of aluminium oxide, 10-30 parts of cosolvent, 15-25 parts of coagulator.
As a further solution of the present invention: the heat-insulated compound glass material, including following raw material by weight:
105-130 parts of base-material, 25-40 parts of pyrophillite, 28-40 parts of aluminium oxide, 15-28 parts of cosolvent, 18-22 parts of coagulator.
As further scheme of the invention: the heat-insulated compound glass material, including following original by weight
Material: 120 parts of base-material, 28 parts of pyrophillite, 35 parts of aluminium oxide, 25 parts of cosolvent, 20 parts of coagulator.
As further scheme of the invention: the base-material is made of borax and feldspar.
As further scheme of the invention: the mass ratio that the borax and feldspar are added is 1-7:2-6.
As further scheme of the invention: the mass ratio that the borax and feldspar are added is 2-6:3-5.
As further scheme of the invention: the mass ratio that the borax and feldspar are added is 5:4.
As it is a further object to provide a kind of preparation method of heat-insulated compound glass material, including it is following
Step:
1) base-material is handled
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, added again after mixing
Enter aluminium oxide, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated
Compound glass material.
As further scheme of the invention: the mixing time in the step 2) is 30min.
Compared with prior art, the beneficial effects of the present invention are:
1, aluminium oxide and pyrophillite are mixed into compound glass material, can reduce thermal conductivity, enhance heat insulation；
2, the preparation method of heat-insulated compound glass material, manufacture craft is simple, at low cost.
Specific embodiment
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described,
Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention
Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, a kind of heat-insulated compound glass material, including following raw material by weight: base-material 100
Part, 20 parts of pyrophillite, 25 parts of aluminium oxide, 10 parts of cosolvent, 15 parts of coagulator.
Wherein, the base-material is made of borax and feldspar；The mass ratio that the borax and feldspar are added is 1:2.
A kind of preparation method of heat-insulated compound glass material, comprising the following steps:
1) base-material is handled
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, added again after mixing
Enter aluminium oxide, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated
Compound glass material.
Wherein, the mixing time in the step 2) is 30min.
Embodiment 2
In the embodiment of the present invention, a kind of heat-insulated compound glass material, including following raw material by weight: base-material 150
Part, 45 parts of pyrophillite, 50 parts of aluminium oxide, 30 parts of cosolvent, 25 parts of coagulator.
Wherein, the base-material is made of borax and feldspar；The mass ratio that the borax and feldspar are added is 7:6.
A kind of preparation method of heat-insulated compound glass material, comprising the following steps:
1) base-material is handled
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, added again after mixing
Enter aluminium oxide, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated
Compound glass material.
Wherein, the mixing time in the step 2) is 30min.
Embodiment 3
In the embodiment of the present invention, a kind of heat-insulated compound glass material, including following raw material by weight: base-material 105
Part, 25 parts of pyrophillite, 28 parts of aluminium oxide, 15 parts of cosolvent, 18 parts of coagulator.
Wherein, the base-material is made of borax and feldspar；The mass ratio that the borax and feldspar are added is 2:3.
A kind of preparation method of heat-insulated compound glass material, comprising the following steps:
1) base-material is handled
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, added again after mixing
Enter aluminium oxide, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated
Compound glass material.
Wherein, the mixing time in the step 2) is 30min.
Embodiment 4
In the embodiment of the present invention, a kind of heat-insulated compound glass material, including following raw material by weight: base-material 130
Part, 40 parts of pyrophillite, 40 parts of aluminium oxide, 28 parts of cosolvent, 22 parts of coagulator.
Wherein, the base-material is made of borax and feldspar；The mass ratio that the borax and feldspar are added is 6:5.
A kind of preparation method of heat-insulated compound glass material, comprising the following steps:
1) base-material is handled
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, added again after mixing
Enter aluminium oxide, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated
Compound glass material.
Wherein, the mixing time in the step 2) is 30min.
Embodiment 5
In the embodiment of the present invention, a kind of heat-insulated compound glass material, including following raw material by weight: base-material 120
Part, 28 parts of pyrophillite, 35 parts of aluminium oxide, 25 parts of cosolvent, 20 parts of coagulator.
Wherein, the base-material is made of borax and feldspar；The mass ratio that the borax and feldspar are added is 5:4.
A kind of preparation method of heat-insulated compound glass material, comprising the following steps:
1) base-material is handled
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, added again after mixing
Enter aluminium oxide, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated
Compound glass material.
Wherein, the mixing time in the step 2) is 30min.
Comparative example 1
A kind of nitride ceramics-glass ceramic composite of Chinese patent (Authorization Notice No. CN10554134B) and its
Glass composite material in preparation method.
Recipe ingredient such as the following table 1 of heat-insulated compound glass material in above-described embodiment 1-5:
Table 1
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| Base-material | 100 | 150 | 105 | 130 | 120 |
| Pyrophillite | 20 | 45 | 25 | 40 | 28 |
| Aluminium oxide | 25 | 50 | 28 | 40 | 35 |
| Cosolvent | 10 | 30 | 15 | 28 | 25 |
| Coagulator | 15 | 25 | 18 | 22 | 20 |
Test experience, the result of the thermal conductivity measured are carried out to product obtained in embodiment 1-5 and comparative example 1 respectively
Such as the following table 2:
Table 2
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (9)
1. a kind of heat-insulated compound glass material, which is characterized in that including following raw material by weight: 100-150 parts of base-material,
20-45 parts of pyrophillite, 25-50 parts of aluminium oxide, 10-30 parts of cosolvent, 15-25 parts of coagulator.
2. the heat-insulated compound glass material of one kind according to claim 1, which is characterized in that the heat-insulated compound glass
Material, including following raw material by weight: 105-130 parts of base-material, 25-40 parts of pyrophillite, 28-40 parts of aluminium oxide, cosolvent
15-28 parts, 18-22 parts of coagulator.
3. the heat-insulated compound glass material of one kind according to claim 1, which is characterized in that the heat-insulated compound glass
Material, including following raw material by weight: 120 parts of base-material, 28 parts of pyrophillite, 35 parts of aluminium oxide, 25 parts of cosolvent, coagulator
20 parts.
4. the heat-insulated compound glass material of one kind according to claim 1 to 3, which is characterized in that the base-material is by boron
Sand and feldspar composition.
5. the heat-insulated compound glass material of one kind according to claim 4, which is characterized in that the borax and feldspar are added
Mass ratio be 1-7:2-6.
6. the heat-insulated compound glass material of one kind according to claim 4, which is characterized in that the borax and feldspar are added
Mass ratio be 2-6:3-5.
7. the heat-insulated compound glass material of one kind according to claim 4, which is characterized in that the borax and feldspar are added
Mass ratio be 5:4.
8. a kind of preparation method of -7 any heat-insulated compound glass materials according to claim 1, which is characterized in that packet
Include following steps:
1) base-material is handled:
The first step is air-dried after cleaning base-material, then is smashed, and obtains coarse crushing base-material；
Coarse crushing base-material is further smashed, is refiltered, obtains base materials powder by second step；
2) it by the base materials powder in step 1), is added in cosolvent and is stirred, while being heated, oxygen is added after mixing
Change aluminium, continue to stir 20-40min, obtains mixing base fluid；
3) into mixing base fluid, coagulator and smashed pyrophillite is added in stirring, then is concentrated, and finally cooling obtains heat-insulated answer
Close glass material.
9. the preparation method of the heat-insulated compound glass material of one kind according to claim 8, which is characterized in that the step
2) mixing time in is 30min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811277026.5A CN109052940A (en) | 2018-10-30 | 2018-10-30 | A kind of heat-insulated compound glass material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201811277026.5A CN109052940A (en) | 2018-10-30 | 2018-10-30 | A kind of heat-insulated compound glass material and preparation method thereof |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1792919A (en) * | 2005-11-25 | 2006-06-28 | 中国洛阳浮法玻璃集团有限责任公司 | Sodium calcium silicon series fire-proofing glass |
| CN101460417A (en) * | 2006-06-01 | 2009-06-17 | 旭硝子欧洲平板玻璃股份有限公司 | Lime glass batch composition |
| CN101544467A (en) * | 2009-04-28 | 2009-09-30 | 陕西彩虹电子玻璃有限公司 | Crystal liquid substrate glass material and preparation method thereof |
| CN105948493A (en) * | 2016-04-27 | 2016-09-21 | 旌德县青川玻纤有限公司 | Production process for glass fiber yarn |
| CN107417093A (en) * | 2017-06-22 | 2017-12-01 | 合肥钢骨玻璃制品有限公司 | A kind of thermal resistance sound-absorbing glassware and preparation method thereof |
-
2018
- 2018-10-30 CN CN201811277026.5A patent/CN109052940A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1792919A (en) * | 2005-11-25 | 2006-06-28 | 中国洛阳浮法玻璃集团有限责任公司 | Sodium calcium silicon series fire-proofing glass |
| CN101460417A (en) * | 2006-06-01 | 2009-06-17 | 旭硝子欧洲平板玻璃股份有限公司 | Lime glass batch composition |
| CN101544467A (en) * | 2009-04-28 | 2009-09-30 | 陕西彩虹电子玻璃有限公司 | Crystal liquid substrate glass material and preparation method thereof |
| CN105948493A (en) * | 2016-04-27 | 2016-09-21 | 旌德县青川玻纤有限公司 | Production process for glass fiber yarn |
| CN107417093A (en) * | 2017-06-22 | 2017-12-01 | 合肥钢骨玻璃制品有限公司 | A kind of thermal resistance sound-absorbing glassware and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 程耀信等: "《非金属矿深加工与应用新技术》", 31 August 1995 * |
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