CN109044917A - Low deuterium rose and preparation method thereof - Google Patents
Low deuterium rose and preparation method thereof Download PDFInfo
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- CN109044917A CN109044917A CN201811192677.4A CN201811192677A CN109044917A CN 109044917 A CN109044917 A CN 109044917A CN 201811192677 A CN201811192677 A CN 201811192677A CN 109044917 A CN109044917 A CN 109044917A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/965—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
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- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The present invention relates to technical field of skin care to provide a kind of low deuterium rose for the general problem of the effect of anti-aging, comprising: rose 15%-25%, preservative 0.2%-1%, surplus are low deuterium-oxide;Low deuterium-oxide deuterium content is 15ppm-25ppm.A kind of preparation method of low deuterium rose, comprising: (1) disinfector;(2) low deuterium-oxide disinfection;(3) initial mixture is prepared;(4) final mixture is prepared;(5) discharging.Low deuterium-oxide can be with activating human body cells, effective protection DNA repair enzyme, promote enzyme reaction, reduce the mistake of life entity DNA replication dna, furthermore low deuterium environment also can exciting human epiphysin generation, it is possible to reduce senile plaque makes the more pale gloss of skin.
Description
Technical field
The present invention relates to technical field of skin care, more particularly, to a kind of low deuterium rose and preparation method thereof.
Background technique
In skin care item, water occupies very main status, by the nutrition in skin care item while human body is by absorbing water
Ingredient draws are into skin, the effect of to play U.S. face skin care.
With social development, demand of the people to skin care item is higher and higher, is that consumer is outstanding by skin care item anti-aging
For one of the function of concern.
Caused by aging mainly passes through superoxide radical, this is the monster that occurs on the cell Mitochondria of people, it is specially
Door eats up DNA, RNA gene or destroys cell membrane, hinders normal cell division, makes one to cannot get fresh cells and aging is dead
It dies.
In general, existing skin care item majority is usually delayed senescence by the member that supplement human body is lost, such as replenishing collagen
Deng, fail to tackle the problem at its root, cause delay senescence effect it is general, therefore, there are also improve space.
Summary of the invention
In view of the deficiencies of the prior art, the present invention intends to provide a kind of low deuterium rose and its preparation side
Method has the advantages that anti-aging effect is preferable.
To achieve the above object, the present invention provides the following technical scheme that
A kind of low deuterium rose, includes the following components'mass percentage:
Rose 15%-25%
Preservative 0.2%-1%
Surplus is low deuterium-oxide;
The deuterium content of the low deuterium-oxide is 15ppm-25ppm.
By using above-mentioned technical proposal, by the way that the low deuterium-oxide of 15ppm-25ppm is added, due to low deuterium-oxide molecule very
It is active, it will drive all corners that life power element aquo ion goes to human body, by the energy that itself appraises at the current rate of life power element
Power comes the electronics attraction of superoxide radical, so that superoxide radical is become normal oxygen molecule, delay senescence;Low deuterium-oxide is also
It can promote enzyme reaction with activating human body cells, effective protection DNA repair enzyme, reduce the mistake of life entity DNA replication dna, it is furthermore low
Deuterium environment also can exciting human epiphysin generation, it is possible to reduce senile plaque makes the more pale gloss of skin;Due to the life of low deuterium-oxide
Higher cost is produced, the deuterium in pure water is extracted into low deuterium-oxide deuterium content and is reduced to 15ppm-25ppm, can be played extraordinary
Anti-aging effects control the production cost of skin care item, promote convenient for skin care item;Make shelf life of products longer by preservative;
Skin care item are made to have preferable anti-inflammatory, skin of releiving, calm skin, antiallergic, bright color equivalent by the way that rose is added
Fruit, while rose taste is fragrant, improves consumer's usage experience;Have small light molecular structure by low deuterium-oxide, has extremely strong
Penetration, can carry more oxonium ions and nutriment, minerals penetrate narrow cell membrane aquaporin and enter cell, can mention
The effect that high rose is absorbed by the body.
In the present invention, rose uses rose generally in the art;Preservative uses anti-corrosion generally in the art
Agent, such as parahydroxyacet-ophenone, benzaldehyde, salicylic acid, 1.2- hexylene glycol.
The present invention is further arranged to: the preservative includes the 1.2- hexylene glycol that mass percent is 0.1%-0.5%.
Have using it preferable anti-by using above-mentioned technical proposal by using 1.2- hexylene glycol as preservative
Bacterium effect plays preferable antisepsis, so that extending the better effect of shelf life of products.
The present invention is further arranged to: the preservative further includes the para hydroxybenzene that mass percent is 0.1%-0.5%
Ethyl ketone.
It is preferable water-soluble using it by using parahydroxyacet-ophenone as preservative by using above-mentioned technical proposal
Property so that preservative preferably disperse with low deuterium-oxide in so that the anti-corrosion effect of skin care item is preferable, while para hydroxybenzene second
Ketone has the effect of preferable anti-oxidant, anti-irritant so that skin care item to the nursing efficacy of skin more preferably;Pass through para hydroxybenzene second
The preferable antibacterial effect of ketone, so that its effect for extending the skin care item shelf-life is preferable.
In view of the deficienciess of the prior art, the second object of the present invention is to provide a kind of sodium hyaluronate skin care item and its system
Preparation Method has the advantages that anti-aging effect is preferable.
A kind of preparation method according to above-mentioned low deuterium rose, comprising the following steps:
(1) disinfector;
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is warming up to 85 DEG C -95 DEG C;
(3) initial mixture is prepared, specific as follows:
Rose is added in 40 DEG C -50 DEG C of low deuterium-oxide and is stirred evenly;
(4) final mixture is prepared, specific as follows:
Preservative is added in 40 DEG C -50 DEG C of initial mixture and is stirred evenly;
(5) discharging.
By using above-mentioned technical proposal, disappeared by the way that low deuterium-oxide is warming up to 85 DEG C -95 DEG C with carrying out high temperature to low deuterium-oxide
Poison sterilizing;By, to carry out disinfection sterilizing to rose, while avoiding temperature is excessively high from leading in 40 DEG C of -50 DEG C of addition roses
The structure of destruction rose is caused, the case where rose inactivation causes the effect of skin care item nursing skin to decline to a great extent is reduced;
By protecting the activity of each component in 40 DEG C of -50 DEG C of addition preservatives, avoid temperature is excessively high each component inactivation is caused to lead to skin care
The case where product effect disappears, so that skin care item have preferable anti-aging effects.
The present invention is further arranged to: discharge temp is 35 DEG C -40 DEG C in the step (5).
It is 35 DEG C -40 DEG C by discharge temp, so that moisture is not easy Yin Wen in skin care item by using above-mentioned technical proposal
It spends higher and evaporates, the ratio of each component in skin care item is preferably kept, so that preferable the effect of skin care item.
The present invention is further arranged to: passing through 500 mesh filter-cloth filterings in the step (5) when discharging.
By using above-mentioned technical proposal, after 500 mesh filter-cloth filterings, so that it is impure less in skin care item, it improves
Skin care quality.
In conclusion the invention has the following advantages:
1. internal enzyme element activity can be promoted by the low deuterium-oxide that 20ppm is added, reach several times even more than ten of general water
Times, body immunity can be enhanced, improve internal SOD enzyme element vigor, effectively remove the acidic waste in blood, prevent and treat anaphylaxis disease
Disease is effectively improved vivo environment, and Skin Cell keeps young healthy state, delaying human body caducity;
2. deuterium in pure water is extracted into low deuterium-oxide deuterium content and is reduced to since the production cost of low deuterium-oxide is higher
15ppm-25ppm can play extraordinary anti-aging effects, control the production cost of skin care item, promote convenient for skin care item;
3. by the way that low deuterium-oxide is warming up to 85 DEG C -95 DEG C to carry out high-temp sterilizing to low deuterium-oxide, by 40 DEG C -50
DEG C rose is added to carry out disinfection sterilizing to rose, while rose being avoided to inactivate, by adding at 40 DEG C -50 DEG C
Enter preservative, protects the activity of each component.
Specific embodiment
With reference to embodiments, invention is further described in detail.
Embodiment 1
A kind of low deuterium rose, includes the following components'mass percentage:
Rose 15%;1.2- hexylene glycol 0.1%;Parahydroxyacet-ophenone 0.1%;The low deuterium-oxide of surplus;
Wherein deuterium content is 15ppm in low deuterium-oxide.
In the present embodiment, rose uses and field rose (kind: Desert Rose), manufacturer: Huocheng County five
Color river valley agricultural development Co., Ltd.
Low deuterium rose the preparation method is as follows:
(1) disinfecting utensils, specific as follows:
Utensil is put into emulsion pot, and water is added, is heated to 100 DEG C, boiling water sterilizes 10 minutes, and taking-up utensil is simultaneously cold
But, the water in emulsion pot and drying are drawn off.
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is added in emulsion pot, revolving speed 10r/min is stirred and heated to 90 DEG C, and heat preservation cools down after twenty minutes.
(3) initial mixture is prepared, specific as follows:
After low deuterium-oxide is cooled to 45 DEG C, rose is added in emulsion pot, 45 DEG C of constant temperature, revolving speed 60r/min stirring
10min forms initial mixture.
(4) final mixture is prepared, specific as follows:
Initial mixture heat up to 50 DEG C, 1.2- hexylene glycol and parahydroxyacet-ophenone are added in emulsion pot, constant temperature 50
DEG C, revolving speed 45r/min stirs 5min, and revolving speed 60r/min stirs Temperature fall after 5min, forms final mixture.
(5) discharging, specific as follows:
After final mixture is cooled to 38 DEG C, with 500 mesh filter-cloth filterings and discharge, bottling storage.
Embodiment 2
The difference of embodiment 1 is:
Low deuterium rose includes the following components'mass percentage:
Rose 25%;1.2- hexylene glycol 0.5%;Parahydroxyacet-ophenone 0.5%;The low deuterium-oxide of surplus;
Wherein deuterium content is 25ppm in low deuterium-oxide.
Embodiment 3
The difference of embodiment 1 is:
Low deuterium rose includes the following components'mass percentage:
Rose 15%;1.2- hexylene glycol 0.1%;Parahydroxyacet-ophenone 0.1%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 20ppm.
Embodiment 4
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 17.5%;1.2- hexylene glycol 0.2%;Parahydroxyacet-ophenone 0.2%;The low deuterium-oxide of surplus;Wherein low deuterium
Deuterium content is 20ppm in water.
Embodiment 5
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 20%;1.2- hexylene glycol 0.3%;Parahydroxyacet-ophenone 0.3%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 20ppm.
Embodiment 6
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 22.5%;1.2- hexylene glycol 0.4%;Parahydroxyacet-ophenone 0.4%;The low deuterium-oxide of surplus;Wherein low deuterium
Deuterium content is 20ppm in water.
Embodiment 7
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 25%;1.2- hexylene glycol 0.5%;Parahydroxyacet-ophenone 0.5%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 20ppm.
Embodiment 8
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 20%;1.2- hexylene glycol 0.3%;Parahydroxyacet-ophenone 0.3%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 15ppm.
Embodiment 9
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 20%;1.2- hexylene glycol 0.3%;Parahydroxyacet-ophenone 0.3%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 17.5ppm.
Embodiment 10
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 20%;1.2- hexylene glycol 0.3%;Parahydroxyacet-ophenone 0.3%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 22.5ppm.
Embodiment 11
It is with the difference for implementing 1:
Low deuterium rose includes the following components'mass percentage:
Rose 20%;1.2- hexylene glycol 0.3%;Parahydroxyacet-ophenone 0.3%;The low deuterium-oxide of surplus;Wherein low deuterium-oxide
Middle deuterium content is 25ppm.
Embodiment 12
Difference with embodiment 5 is:
Low deuterium rose the preparation method is as follows:
(1) disinfecting utensils, specific as follows:
Utensil is put into emulsion pot, and water is added, is heated to 100 DEG C, boiling water sterilizes 10 minutes, and taking-up utensil is simultaneously cold
But, the water in emulsion pot and drying are drawn off.
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is added in emulsion pot, revolving speed 10r/min is stirred and heated to 85 DEG C, and heat preservation cools down after twenty minutes.
(3) initial mixture is prepared, specific as follows:
After low deuterium-oxide is cooled to 40 DEG C, rose is added in emulsion pot, 40 DEG C of constant temperature, revolving speed 60r/min stirring
10min forms initial mixture.
(4) final mixture is prepared, specific as follows:
Initial mixture heat up to 45 DEG C, 1.2- hexylene glycol and parahydroxyacet-ophenone are added in emulsion pot, constant temperature 45
DEG C, revolving speed 45r/min stirs 5min, and revolving speed 60r/min stirs Temperature fall after 5min, forms final mixture.
(5) discharging, specific as follows:
After final mixture is cooled to 40 DEG C, with 500 mesh filter-cloth filterings and discharge, bottling storage.
Embodiment 13
Difference with embodiment 5 is:
Low deuterium rose the preparation method is as follows:
(1) disinfecting utensils, specific as follows:
Utensil is put into emulsion pot, and water is added, is heated to 100 DEG C, boiling water sterilizes 10 minutes, and taking-up utensil is simultaneously cold
But, the water in emulsion pot and drying are drawn off.
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is added in emulsion pot, revolving speed 10r/min is stirred and heated to 95 DEG C, and heat preservation cools down after twenty minutes.
(3) initial mixture is prepared, specific as follows:
After low deuterium-oxide is cooled to 50 DEG C, rose is added in emulsion pot, 50 DEG C of constant temperature, revolving speed 60r/min stirring
10min forms initial mixture.
(4) final mixture is prepared, specific as follows:
Initial mixture is cooled to 40 DEG C, 1.2- hexylene glycol and parahydroxyacet-ophenone is added in emulsion pot, constant temperature 40
DEG C, revolving speed 45r/min stirs 5min, and revolving speed 60r/min stirs Temperature fall after 5min, forms final mixture.
(5) discharging, specific as follows:
After final mixture is cooled to 35 DEG C, with 500 mesh filter-cloth filterings and discharge, bottling storage.
Comparative example 1
Difference with embodiment 5 is:
Low deuterium rose includes the following components'mass percentage:
Rose 20%;1.2- hexylene glycol 0.3%;Parahydroxyacet-ophenone 0.3%;Surplus pure water;
Wherein deuterium content is 150ppm in pure water.
Comparative example 2
Difference with embodiment 5 is:
Low deuterium rose the preparation method is as follows:
(1) disinfecting utensils, specific as follows:
Utensil is put into emulsion pot, and water is added, is heated to 100 DEG C, boiling water sterilizes 10 minutes, and taking-up utensil is simultaneously cold
But, the water in emulsion pot and drying are drawn off.
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is added in emulsion pot, revolving speed 10r/min is stirred and heated to 80 DEG C, and heat preservation cools down after twenty minutes.
(3) initial mixture is prepared, specific as follows:
After low deuterium-oxide is cooled to 55 DEG C, rose is added in emulsion pot, 55 DEG C of constant temperature, revolving speed 60r/min stirring
10min forms initial mixture.
(4) final mixture is prepared, specific as follows:
Keeping initial mixture is 55 DEG C, 1.2- hexylene glycol and parahydroxyacet-ophenone is added in emulsion pot, constant temperature 55
DEG C, revolving speed 45r/min stirs 5min, and revolving speed 60r/min stirs Temperature fall after 5min, forms final mixture.
(5) discharging, specific as follows:
After 38 DEG C of final mixture cooling, with 500 mesh filter-cloth filterings and discharge, bottling storage.
Comparative example 3
Difference with embodiment 5 is:
Low deuterium rose the preparation method is as follows:
(1) disinfecting utensils, specific as follows:
Utensil is put into emulsion pot, and water is added, is heated to 100 DEG C, boiling water sterilizes 10 minutes, and taking-up utensil is simultaneously cold
But, the water in emulsion pot and drying are drawn off.
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is added in emulsion pot, revolving speed 10r/min is stirred and heated to 75 DEG C, and heat preservation cools down after twenty minutes.
(3) initial mixture is prepared, specific as follows:
After low deuterium-oxide is cooled to 60 DEG C, rose is added in emulsion pot, 60 DEG C of constant temperature, revolving speed 60r/min stirring
10min forms initial mixture.
(4) final mixture is prepared, specific as follows:
Keeping initial mixture is 60 DEG C, 1.2- hexylene glycol and parahydroxyacet-ophenone is added in emulsion pot, constant temperature 60
DEG C, revolving speed 45r/min stirs 5min, and revolving speed 60r/min stirs Temperature fall after 5min, forms final mixture.
(5) discharging, specific as follows:
After 38 DEG C of final mixture cooling, with 500 mesh filter-cloth filterings and discharge, bottling storage.
Specific test data is shown in Table 1-5
Experiment 1
The product that the production of each embodiment obtains is applied on small white mouse skin of back, once in the morning and once at night, after seven days,
By detecting luminous intensity by fluorescent quantitative detection device in small white mouse dorsal injection luminol reagent.
Luminol reagent concentration is 0.2%, and injection rate 10ml is injected using hypodermic injection.
First small white mouse is anaesthetized to improve detection accuracy before test.
Experiment 2
Supernatant water is dripped on slide, and the product sampling 1g that the production of each embodiment obtains is instilled in clear water, dyestuff is added.It is logical
Optical microphotograph sem observation is crossed, amplification factor is 800 times, and heart position takes 3 points of observation at random in a liquid, records in range of observation
Bacterial number living is simultaneously averaged.
Experiment 3
20 users are invited to carry out using test, practical embodiment 5 product of embodiment 5 and comparative example 1 at random
Number each ten of 1 product of product and comparative example, before use, user's facial skin moisture is detected by moisture detector,
User's facial skin moisture, and statistical experiment data are detected again by moisture detector using after five minutes.
Table 1
Table 2
Table 3
Embodiment 8 | Embodiment 9 | Embodiment 10 | Embodiment 11 | |
Luminous intensity | 1721 | 1769 | 2185 | 2463 |
Bacterial number living | 21 | 17 | 19 | 20 |
Appearance | It is transparent | It is transparent | It is transparent | It is transparent |
Table 4
Embodiment 12 | Embodiment 13 | Comparative example 2 | Comparative example 3 | |
Luminous intensity | 1863 | 1849 | 1857 | 1852 |
Bacterial number living | 31 | 12 | 57 | 89 |
Appearance | It is transparent | It is transparent | Muddy, suspension | Muddy, precipitating |
Table 5
It can be obtained by table 1, after low deuterium-oxide is added, can obviously reduce luminous intensity, when being detected using chemoluminescence method, shone
Intensity is lower, it was demonstrated that superoxide radical concentration is lower, it is clear that after low deuterium-oxide is added, the superoxide radical in biology can be made dense
Degree is decreased obviously, and then reduces the case where superoxide radical destroys cell, realizes the effect of anti-aging.
It can be obtained by table 2, each component is added and each component content changes, superoxide radical is eliminated to low deuterium-oxide
Effect without obvious negative effect, that is, low deuterium-oxide, which is added, to act synergistically with the various function ingredients of addition, improve skin care item shield
Skin effect guarantees the effect that low deuterium-oxide promotes rose to be absorbed by the skin.
It can be obtained by table 3, when the deuterium content in low deuterium-oxide is greater than 20ppm, increase the deuterium content for reducing low deuterium-oxide, help
In being substantially reduced luminous intensity, and after the deuterium content of low deuterium-oxide is less than 20ppm, the amplitude for reducing luminous intensity is greatly decreased,
As it can be seen that the effect for eliminating superoxide radical is preferable and sexual valence is relatively high when the deuterium content of low deuterium-oxide is 20ppm, control at
This, so that product is easy to spread.
It can be obtained by table 4, after low deuterium-oxide sterilisation temp is lower than 85 DEG C, bacterial number of living in product is significantly increased, so that
Disinfection Effect is decreased obviously, and reduces product quality.
After the processing temperature of initial mixture is higher than 50 DEG C and final mixture processing temperature is greater than 50 DEG C, skin care item
Significant change occurs for appearance, muddy even precipitating occurs, loses this is because deactivation phenomenom especially rose occurs in each component
Caused by living, decline the quality of skin care item.
Therefore low deuterium-oxide sterilisation temp control is controlled in the processing temperature of 85 DEG C -95 DEG C, initial mixture at 40 DEG C -50
DEG C, the processing temperature of final mixture control at 40 DEG C -50 DEG C, the skin care quality produced is preferable.
Can be obtained according to table 5, using the user face moisture content incrementss after 5 product of embodiment be substantially better than use than
Compared with the user face moisture content incrementss after 1 product of example, it was demonstrated that will obviously be had in low deuterium rose using low deuterium-oxide
Help improve the effect of skin care item.
The embodiment of present embodiment is presently preferred embodiments of the present invention, not limits protection of the invention according to this
Range, therefore: the equivalence changes that all structures under this invention, shape, principle are done, should all be covered by protection scope of the present invention it
It is interior.
Claims (6)
1. a kind of low deuterium rose, it is characterized in that: including the following components'mass percentage:
Rose 15%-25%
Preservative 0.2%-1%
Surplus is low deuterium-oxide;
The deuterium content of the low deuterium-oxide is 15ppm-25ppm.
2. low deuterium rose according to claim 1, it is characterized in that: the preservative includes 1.2- hexylene glycol.
3. low deuterium rose according to claim 2, it is characterized in that: the preservative further includes parahydroxyacet-ophenone.
4. a kind of preparation method of low deuterium rose according to claim 1 to 3, it is characterized in that: including following step
It is rapid:
(1) disinfector;
(2) low deuterium-oxide disinfection, specific as follows:
Low deuterium-oxide is warming up to 85 DEG C -95 DEG C;
(3) initial mixture is prepared, specific as follows:
Rose is added in 40 DEG C -50 DEG C of low deuterium-oxide and is stirred evenly;
(4) final mixture is prepared, specific as follows:
Preservative is added in 40 DEG C -50 DEG C of initial mixture and is stirred evenly;
(5) discharging.
5. the preparation method according to claim 4, it is characterized in that: discharge temp is 35 DEG C -40 DEG C in the step (5).
6. the preparation method according to claim 4, it is characterized in that passing through 500 mesh filter cloth mistakes in the step (5) when discharging
Filter.
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