CN109024071A - A kind of preparation method of face paper - Google Patents

A kind of preparation method of face paper Download PDF

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Publication number
CN109024071A
CN109024071A CN201810727113.XA CN201810727113A CN109024071A CN 109024071 A CN109024071 A CN 109024071A CN 201810727113 A CN201810727113 A CN 201810727113A CN 109024071 A CN109024071 A CN 109024071A
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Prior art keywords
mass ratio
face paper
preparation
mixing
take
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王建东
陈建春
卢星
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Individual
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Priority to CN201810727113.XA priority Critical patent/CN109024071A/en
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212—Face masks
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55—Phosphorus compounds
    • A61K8/553—Phospholipids, e.g. lecithin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73—Polysaccharides
    • A61K8/733—Alginic acid; Salts thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21F—PAPER-MAKING MACHINES; METHODS OF PRODUCING PAPER THEREON
    • D21F13/00—Making discontinuous sheets of paper, pulpboard or cardboard, or of wet web, for fibreboard production
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/02—Material of vegetable origin
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/03—Non-macromolecular organic compounds
    • D21H17/05—Non-macromolecular organic compounds containing elements other than carbon and hydrogen only
    • D21H17/10—Phosphorus-containing compounds
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/24—Polysaccharides
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
    • D21H17/24—Polysaccharides
    • D21H17/30—Alginic acid or alginates
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/20—Macromolecular organic compounds
    • D21H17/33—Synthetic macromolecular compounds
    • D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D21H17/37—Polymers of unsaturated acids or derivatives thereof, e.g. polyacrylates
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63—Inorganic compounds
    • D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/675—Oxides, hydroxides or carbonates
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/18—Reinforcing agents
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/36—Biocidal agents, e.g. fungicidal, bactericidal, insecticidal agents
    • D—TEXTILES; PAPER
    • D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14—Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/38—Corrosion-inhibiting agents or anti-oxidants
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/10—General cosmetic use

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  • Animal Behavior & Ethology (AREA)
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  • Oil, Petroleum & Natural Gas (AREA)
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Abstract

The invention discloses a kind of preparation methods of face paper, belong to skincare product field.Technical solution of the present invention is by adding a small amount of carbomer, a large amount of acid groups are had in carbomer molecular structure, hydrogen bond can be formed with the glycosyl group in system, generate gel network, to improve the mechanical property of product, in addition, acid groups therein can be in conjunction with the schiff bases that fructose and amino acid react, make schiff bases in rearrangement process, it is arranged in gel network structure and is fixed, improve the stability of face paper and easy to use, avoid just user, the possibility torn to shreds unintentionally, gel network can also preferably be enriched with nutrient solution, improve the activity ratio of facial mask.The present invention solves the problems, such as that current face paper is not strong to the preservation effect of nutrient solution.

Description

A kind of preparation method of face paper
Technical field
The invention discloses a kind of preparation methods of face paper, belong to skincare product field.
Background technique
Traditional face paper is the facial mask articles with non-woven fabrics Jing Guo machine-shaping, also needs to deploy nutrition when making facial mask Water is immersed in face paper in nutritive water, then takes out, and is covered in face, removes after several minutes, so that the part in nutritive water Nutrition is by facial percutaneous absorption.
The material of common face paper has silk, cotton, a terylene or blended etc., the face paper cost of silk and cotton compared with Height, therefore face paper is mostly that terylene and blended non-woven fabrics are made.Face paper tensile property made of terylene and blended non-woven fabrics is good, But hygroscopicity is poor, it is difficult to lock a large amount of nutritive water, nutritive water is largely oozed out and flowed down when being attached on the face, and waste is serious, drop The low using effect of facial mask needs to improve water absorbing capacity on the basis of guaranteeing tensile property.
Summary of the invention
The technical problems to be solved by the invention: for the not strong problem of preservation effect of the current face paper to nutrient solution, A kind of preparation method of face paper is provided.
In order to solve the above technical problems, the present invention is using technical solution as described below:
A kind of preparation method of face paper includes the following steps:
(1) it takes shrimp shell to wash, dry, pulverize sieving, take sieving particle at 40 ~ 55 DEG C, it is mixed that solvent is added in 1:3 in mass ratio ~ 6 Stirring is closed, the fructose of sieving granular mass 5 ~ 10%, mashing is added, homogenization must pre-process shrimp shell slurry；
(2) take pretreatment shrimp shell slurry 5:1:1 in mass ratio that adjuvant, sodium alginate mixing is added, concentrated by rotary evaporation must be concentrated Liquid, it is spare；
(3) it takes thickener to mix with water for 1:40 ~ 50 in mass ratio, stands swelling, obtain swelling solution, take swelling solution in 70 ~ 85 DEG C, Heating stirring dissolution, it is cooling, the plants essential oil of thickener qualities 2 ~ 5%, the phosphatide of thickener qualities 8 ~ 12%, thickener matter is added Mixing is mixed in the amino acid of the carbomer of amount 1 ~ 4%, thickener qualities 5 ~ 8%, obtains mucus；
(4) take spare concentrate, mucus, log paper pulp, auxiliary agent is that 2:3 ~ 5:10:0.2 ~ 0.5 is mixed in mass ratio, shearing point It dissipating, vacuum defoamation, film liquid must be mixed into, coating is mixed into film liquid, controls coating thickness, and film is taken off in vacuum drying, it is freeze-dried, Film base is obtained, then is cut, is wound to get face paper.
Shrimp shell in the step (1) is freshwater shrimp shell, prawn shell, any one in grass shrimp shell.
1:4 ~ 8 in mass ratio in the step (1) take Dopamine hydrochloride that sodium carbonate liquor mixing, ultrasonic wavelength-division is added It dissipates to get solvent.
Adjuvant in the step (2): 4:2 ~ 3 take chitosan, collagen peptide mixing to get adjuvant in mass ratio.
Thickener in the step (3): 5:1:1 ~ 2 take peach gum, guar gum, lac mixing to get thickening in mass ratio Agent.
Plants essential oil in the step (3): Lavender, peach blossom essential oil, any one in jasmine essential oil.
Phosphatide in the step (3): 5:1 ~ 2 take soybean lecithin, cuorin mixing to get phosphatide in mass ratio.
Carbomer in the step (3): carbomer 934, Acritamer 940, any one in Carbopol 941.
Amino acid in the step (3): 2 ~ 4:1:1:1 ~ 2 in mass ratio take leucine, glutamic acid, cysteine, sweet Propylhomoserin mixes to get amino acid.
Auxiliary agent in the step (4): 6:1:0.2 ~ 0.5 takes carboxymethyl cellulose, pearl powder, calcium hypochlorite in mass ratio Mixing is to get auxiliary agent.
The present invention is compared with other methods, and advantageous effects are:
(1) present invention is crushed cooperation fructose high speed and is beaten, chitin, astaxanthin can be leached in slurry, is mentioned using shrimp shell as raw material For good inoxidizability, it is sustained during face paper system absorbs nutrient solution, is greatly improved skin of face vigor, Immunity, sodium bicarbonate, fructose and amino acid are improved, sodium bicarbonate is generated carbon dioxide and water by thermal decomposition, there is aqueous condition Under, condensation reaction occurs for free amino acid in carbonyl and system in fructose, forms schiff bases, then can partially occur virtue draw it is anti- It answers, so that schiff bases form all sharp product of stable Armagh after rearranging, and with Covalent bonding together, it is excellent to assign face paper system The different performances such as anti-oxidant, antibacterial, to improve facial mask paper product to the preservation effect of nutrient solution, amino acid used can part shape At tripeptides, i.e. glutathione, it is possible to provide inoxidizability reduces facial melanin pigmentation, improves smoothness and the reduction of skin The appearance of blackhead；
(2) technical solution of the present invention, which passes through, adds a small amount of carbomer, has a large amount of acid groups in carbomer molecular structure, can be with body Glycosyl group in system forms hydrogen bond, gel network is generated, so that the mechanical property of product is improved, in addition, acid groups therein can In conjunction with the schiff bases that fructose and amino acid react, makes schiff bases in rearrangement process, be arranged in gel network structure And fixed, the stability of face paper and easy to use is improved, avoids just user, it is not intended to the possibility torn to shreds, gel network It can also be preferably enriched with nutrient solution, improve the activity ratio of facial mask.
Specific embodiment
Shrimp shell: freshwater shrimp shell, prawn shell, any one in grass shrimp shell.
Solvent: 1:4 ~ 8 take Dopamine hydrochloride to be added in the sodium carbonate liquor that mass fraction is 15% and mix in mass ratio, with 250W ultrasonic wave disperses 5 ~ 10min to get solvent.
Adjuvant: 4:2 ~ 3 take chitosan, collagen peptide mixing to get adjuvant in mass ratio.
Thickener: 5:1:1 ~ 2 take peach gum, guar gum, lac mixing to get thickener in mass ratio.
Phosphatide: 5:1 ~ 2 take soybean lecithin, cuorin mixing to get phosphatide in mass ratio.
Carbomer: carbomer 934, Acritamer 940, any one in Carbopol 941.
Amino acid: 2 ~ 4:1:1:1 ~ 2 in mass ratio take leucine, glutamic acid, cysteine, glycine mixing to get ammonia Base acid.
Plants essential oil: Lavender, peach blossom essential oil, any one in jasmine essential oil.
Auxiliary agent: 6:1:0.2 ~ 0.5 takes carboxymethyl cellulose, pearl powder, calcium hypochlorite mixing to get auxiliary agent in mass ratio.
A kind of preparation method of face paper, includes the following steps:
(1) it takes shrimp shell to be washed with deionized, after moving to 60 ~ 80 DEG C of oven dryings, crushed 80 meshes, take sieving particle in water At 40 ~ 55 DEG C of bath, 1:3 in mass ratio ~ 6 is added solvent mixing and pours into container, and the fructose of sieving granular mass 5 ~ 10% is added, After being beaten 8 ~ 15min of processing with beater with 3000 ~ 4000r/min revolving speed, colloid mill is moved into, with 2000 ~ 2500r/min revolving speed Under the conditions of, homogenization 10min must pre-process shrimp shell slurry；
(2) take pretreatment shrimp shell slurry 5:1:1 in mass ratio that adjuvant, sodium alginate mixing is added, with 300 ~ 400r/min stirring After 20 ~ 40min, Rotary Evaporators are put in, under the conditions of 45 ~ 55 DEG C, 600kPa, 3 ~ 5h of concentrated by rotary evaporation obtains concentrate, spare；
(3) after taking thickener to mix with water for 1:40 ~ 50 in mass ratio, 10 ~ 12h of swelling is stood at room temperature, swelling solution is obtained, takes Swelling solution is in 70 ~ 85 DEG C of water-bath, under the conditions of 600 ~ 800r/min, heating stirring 40 ~ 55min of dissolution, and cooled to room temperature, The carbomer of the plants essential oil of thickener qualities 2 ~ 5%, the phosphatide of thickener qualities 8 ~ 12%, thickener qualities 1 ~ 4% is added, The amino acid of thickener qualities 5 ~ 8% mixes, and is stirred 40 ~ 60min with 600 ~ 800r/min, obtains mucus；
(4) take spare concentrate, mucus, log paper pulp, auxiliary agent is that 2:3 ~ 5:10:0.2 ~ 0.5 is mixed in mass ratio, with 2000 After ~ 3000r/min shearing dispersion, then through vacuum defoamation, it must be mixed into film liquid, take and be mixed into film liquid and be coated on glass pane surface, Control coating thickness is 0.05 ~ 0.1mm, is dried in vacuo in 25 ~ 40 DEG C, takes off film, and under -35 DEG C, 30Pa pressure condition, freezing is dry Dry 3 ~ 5h obtains film base, then is cut, and winds to get face paper.
Embodiment 1
Shrimp shell: freshwater shrimp shell.
Solvent: 1:4 in mass ratio takes Dopamine hydrochloride to be added in the sodium carbonate liquor that mass fraction is 15% and mixes, with 250W ultrasonic wave disperses 5min to get solvent.
Adjuvant: 4:2 in mass ratio takes chitosan, collagen peptide mixing to get adjuvant.
Thickener: 5:1:1 in mass ratio takes peach gum, guar gum, lac mixing to get thickener.
Phosphatide: 5:1 in mass ratio takes soybean lecithin, cuorin mixing to get phosphatide.
Carbomer: carbomer 934.
Amino acid: 2:1:1:1 in mass ratio takes leucine, glutamic acid, cysteine, glycine mixing to get amino Acid.
Plants essential oil: Lavender.
Auxiliary agent: 6:1:0.2 in mass ratio takes carboxymethyl cellulose, pearl powder, calcium hypochlorite mixing to get auxiliary agent.
A kind of preparation method of face paper, includes the following steps:
(1) it takes shrimp shell to be washed with deionized, after moving to 60 DEG C of oven dryings, crushed 80 meshes, take sieving particle in water-bath At 40 DEG C, 1:3 in mass ratio be added solvent mixing pour into container, and be added sieving granular mass 5% fructose, with beater with After 3000r/min revolving speed mashing processing 8min, colloid mill is moved into, under 2000r/min speed conditions, homogenization 10min is obtained Pre-process shrimp shell slurry；
(2) it takes pretreatment shrimp shell slurry 5:1:1 in mass ratio that adjuvant, sodium alginate mixing is added, 20min is stirred with 300r/min Afterwards, Rotary Evaporators are put in, under the conditions of 45 DEG C, 600kPa, concentrated by rotary evaporation 3h obtains concentrate, spare；
(3) after taking thickener to mix with water for 1:40 in mass ratio, swelling 10h is stood at room temperature, swelling solution is obtained, takes swelling solution In 70 DEG C of water-bath, under the conditions of 600r/min, heating stirring dissolves 40min, and cooled to room temperature adds thickener qualities 2% plants essential oil, the phosphatide of thickener qualities 8%, thickener qualities 1% carbomer, the amino acid-mixed of thickener qualities 5% It closes, 40min is stirred with 600r/min, obtains mucus；
(4) take spare concentrate, mucus, log paper pulp, auxiliary agent is 2:3:10:0.2 mixing in mass ratio, with 2000r/min After shearing dispersion, then through vacuum defoamation, it must is mixed into film liquid, take and be mixed into film liquid and be coated on glass pane surface, control coating thickness Degree is 0.05mm, is dried in vacuo in 25 DEG C, takes off film, under -35 DEG C, 30Pa pressure condition, is freeze-dried 3h, obtains film base, then pass through Cutting winds to get face paper.
Embodiment 2
Shrimp shell: prawn shell.
Solvent: 1:6 in mass ratio takes Dopamine hydrochloride to be added in the sodium carbonate liquor that mass fraction is 15% and mixes, with 250W ultrasonic wave disperses 7min to get solvent.
Adjuvant: 4:2.5 in mass ratio takes chitosan, collagen peptide mixing to get adjuvant.
Thickener: 5:1:1.5 in mass ratio takes peach gum, guar gum, lac mixing to get thickener.
Phosphatide: 5:1.5 in mass ratio takes soybean lecithin, cuorin mixing to get phosphatide.
Carbomer: Acritamer 940.
Amino acid: 3:1:1:1.5 in mass ratio takes leucine, glutamic acid, cysteine, glycine mixing to get amino Acid.
Plants essential oil: peach blossom essential oil.
Auxiliary agent: 6:1:0.3 in mass ratio takes carboxymethyl cellulose, pearl powder, calcium hypochlorite mixing to get auxiliary agent.
A kind of preparation method of face paper, includes the following steps:
(1) it takes shrimp shell to be washed with deionized, after moving to 70 DEG C of oven dryings, crushed 80 meshes, take sieving particle in water-bath At 50 DEG C, 1:4 in mass ratio be added solvent mixing pour into container, and be added sieving granular mass 7% fructose, with beater with After 3500r/min revolving speed mashing processing 12min, colloid mill is moved into, under 2200r/min speed conditions, homogenization 10min, Shrimp shell slurry must be pre-processed；
(2) it takes pretreatment shrimp shell slurry 5:1:1 in mass ratio that adjuvant, sodium alginate mixing is added, 30min is stirred with 350r/min Afterwards, Rotary Evaporators are put in, under the conditions of 50 DEG C, 600kPa, concentrated by rotary evaporation 4h obtains concentrate, spare；
(3) after taking thickener to mix with water for 1:45 in mass ratio, swelling 11h is stood at room temperature, swelling solution is obtained, takes swelling solution In 80 DEG C of water-bath, under the conditions of 700r/min, heating stirring dissolves 50min, and cooled to room temperature adds thickener qualities 3% plants essential oil, the phosphatide of thickener qualities 10%, thickener qualities 2% carbomer, the amino acid-mixed of thickener qualities 6% It closes, 50min is stirred with 700r/min, obtains mucus；
(4) take spare concentrate, mucus, log paper pulp, auxiliary agent is 2:4:10:0.3 mixing in mass ratio, with 2500r/min After shearing dispersion, then through vacuum defoamation, it must is mixed into film liquid, take and be mixed into film liquid and be coated on glass pane surface, control coating thickness Degree is 0.08mm, is dried in vacuo in 30 DEG C, takes off film, under -35 DEG C, 30Pa pressure condition, is freeze-dried 4h, obtains film base, then pass through Cutting winds to get face paper.
Embodiment 3
Shrimp shell: grass shrimp shell.
Solvent: 1:8 in mass ratio takes Dopamine hydrochloride to be added in the sodium carbonate liquor that mass fraction is 15% and mixes, with 250W ultrasonic wave disperses 10min to get solvent.
Adjuvant: 4:3 in mass ratio takes chitosan, collagen peptide mixing to get adjuvant.
Thickener: 5:1:2 in mass ratio takes peach gum, guar gum, lac mixing to get thickener.
Phosphatide: 5:2 in mass ratio takes soybean lecithin, cuorin mixing to get phosphatide.
Carbomer: Carbopol 941.
Amino acid: 4:1:1:2 in mass ratio takes leucine, glutamic acid, cysteine, glycine mixing to get amino Acid.
Plants essential oil: jasmine essential oil.
Auxiliary agent: 6:1:0.5 in mass ratio takes carboxymethyl cellulose, pearl powder, calcium hypochlorite mixing to get auxiliary agent.
A kind of preparation method of face paper, includes the following steps:
(1) it takes shrimp shell to be washed with deionized, after moving to 80 DEG C of oven dryings, crushed 80 meshes, take sieving particle in water-bath At 55 DEG C, 1:6 in mass ratio be added solvent mixing pour into container, and be added sieving granular mass 10% fructose, with beater with After 4000r/min revolving speed mashing processing 15min, colloid mill is moved into, under 2500r/min speed conditions, homogenization 10min, Shrimp shell slurry must be pre-processed；
(2) it takes pretreatment shrimp shell slurry 5:1:1 in mass ratio that adjuvant, sodium alginate mixing is added, 40min is stirred with 400r/min Afterwards, Rotary Evaporators are put in, under the conditions of 55 DEG C, 600kPa, concentrated by rotary evaporation 5h obtains concentrate, spare；
(3) after taking thickener to mix with water for 1:50 in mass ratio, swelling 12h is stood at room temperature, swelling solution is obtained, takes swelling solution In 85 DEG C of water-bath, under the conditions of 800r/min, heating stirring dissolves 55min, and cooled to room temperature adds thickener qualities 5% plants essential oil, the phosphatide of thickener qualities 12%, thickener qualities 4% carbomer, the amino acid-mixed of thickener qualities 8% It closes, 60min is stirred with 800r/min, obtains mucus；
(4) take spare concentrate, mucus, log paper pulp, auxiliary agent is 2:5:10:0.5 mixing in mass ratio, with 3000r/min After shearing dispersion, then through vacuum defoamation, it must is mixed into film liquid, take and be mixed into film liquid and be coated on glass pane surface, control coating thickness Degree is 0.1mm, is dried in vacuo in 40 DEG C, takes off film, under -35 DEG C, 30Pa pressure condition, is freeze-dried 5h, obtains film base, then through cutting It cuts, winds to get face paper.
Comparative example: the face paper of Guangzhou company production.
Face paper prepared by embodiment 1,2,3 and comparative example is filled into 30g nutrient solution, tile 12h at 25 DEG C, to facial mask Paper carries out the test of nutrient solution preservation effect, test result record such as table 1.
Table 1:
In conclusion as shown in Table 1, face paper prepared by the present invention is significant to the preservation effect of nutrient solution, it is worth advocating energetically It uses.

Claims (10)

1. a kind of preparation method of face paper, which is characterized in that the preparation method includes the following steps:
(1) it takes shrimp shell to wash, dry, pulverize sieving, take sieving particle at 40 ~ 55 DEG C, it is mixed that solvent is added in 1:3 in mass ratio ~ 6 Stirring is closed, the fructose of sieving granular mass 5 ~ 10%, mashing is added, homogenization must pre-process shrimp shell slurry；
(2) take pretreatment shrimp shell slurry 5:1:1 in mass ratio that adjuvant, sodium alginate mixing is added, concentrated by rotary evaporation must be concentrated Liquid, it is spare；
(3) it takes thickener to mix with water for 1:40 ~ 50 in mass ratio, stands swelling, obtain swelling solution, take swelling solution in 70 ~ 85 DEG C, Heating stirring dissolution, it is cooling, the plants essential oil of thickener qualities 2 ~ 5%, the phosphatide of thickener qualities 8 ~ 12%, thickener matter is added Mixing is mixed in the amino acid of the carbomer of amount 1 ~ 4%, thickener qualities 5 ~ 8%, obtains mucus；
(4) take spare concentrate, mucus, log paper pulp, auxiliary agent is that 2:3 ~ 5:10:0.2 ~ 0.5 is mixed in mass ratio, shearing point It dissipating, vacuum defoamation, film liquid must be mixed into, coating is mixed into film liquid, controls coating thickness, and film is taken off in vacuum drying, it is freeze-dried, Film base is obtained, then is cut, is wound to get face paper.
2. a kind of preparation method of face paper according to claim 1, which is characterized in that the shrimp shell in the step (1) is Freshwater shrimp shell, prawn shell, any one in grass shrimp shell.
3. a kind of preparation method of face paper according to claim 1, which is characterized in that press quality in the step (1) Take Dopamine hydrochloride that sodium carbonate liquor mixing is added than 1:4 ~ 8, ultrasonic wave disperses to get solvent.
4. a kind of preparation method of face paper according to claim 1, which is characterized in that the adjuvant in the step (2): press Mass ratio 4:2 ~ 3 take chitosan, collagen peptide mixing to get adjuvant.
5. a kind of preparation method of face paper according to claim 1, which is characterized in that the thickener in the step (3): 5:1:1 ~ 2 take peach gum, guar gum, lac mixing to get thickener in mass ratio.
6. a kind of preparation method of face paper according to claim 1, which is characterized in that the plant essence in the step (3) Oil: Lavender, peach blossom essential oil, any one in jasmine essential oil.
7. a kind of preparation method of face paper according to claim 1, which is characterized in that the phosphatide in the step (3): press Mass ratio 5:1 ~ 2 take soybean lecithin, cuorin mixing to get phosphatide.
8. a kind of preparation method of face paper according to claim 1, which is characterized in that the carbomer in the step (3): Carbomer 934, Acritamer 940, any one in Carbopol 941.
9. a kind of preparation method of face paper according to claim 1, which is characterized in that the amino acid in the step (3): 2 ~ 4:1:1:1 ~ 2 in mass ratio take leucine, glutamic acid, cysteine, glycine mixing to get amino acid.
10. a kind of preparation method of face paper according to claim 1, which is characterized in that the auxiliary agent in the step (4): 6:1:0.2 ~ 0.5 takes carboxymethyl cellulose, pearl powder, calcium hypochlorite mixing to get auxiliary agent in mass ratio.
CN201810727113.XA 2018-07-05 2018-07-05 A kind of preparation method of face paper Pending CN109024071A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110063918A (en) * 2019-06-13 2019-07-30 优牌生物科技有限公司 It is a kind of to stablize the facial mask base-material coexisted and preparation method with chitin film cloth
CN111265426A (en) * 2020-03-18 2020-06-12 陈健江 Stripping type mask composition and preparation method thereof
CN112655717A (en) * 2020-12-11 2021-04-16 成都瑰奎弘生物科技有限公司 Preparation method of organic-inorganic composite medical antibacterial film
CN114182571A (en) * 2020-09-15 2022-03-15 刘训林 Pearl amino acid paper towel and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110063918A (en) * 2019-06-13 2019-07-30 优牌生物科技有限公司 It is a kind of to stablize the facial mask base-material coexisted and preparation method with chitin film cloth
CN111265426A (en) * 2020-03-18 2020-06-12 陈健江 Stripping type mask composition and preparation method thereof
CN114182571A (en) * 2020-09-15 2022-03-15 刘训林 Pearl amino acid paper towel and preparation method thereof
CN112655717A (en) * 2020-12-11 2021-04-16 成都瑰奎弘生物科技有限公司 Preparation method of organic-inorganic composite medical antibacterial film

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Application publication date: 20181218