CN108978270A - A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction - Google Patents
A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction Download PDFInfo
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- CN108978270A CN108978270A CN201810847259.8A CN201810847259A CN108978270A CN 108978270 A CN108978270 A CN 108978270A CN 201810847259 A CN201810847259 A CN 201810847259A CN 108978270 A CN108978270 A CN 108978270A
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- China
- Prior art keywords
- flaxen fiber
- biological stain
- polymerization reaction
- technique based
- laccase
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/02—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using organic solvents
- D06L1/06—De-sizing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06L—DRY-CLEANING, WASHING OR BLEACHING FIBRES, FILAMENTS, THREADS, YARNS, FABRICS, FEATHERS OR MADE-UP FIBROUS GOODS; BLEACHING LEATHER OR FURS
- D06L1/00—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods
- D06L1/12—Dry-cleaning or washing fibres, filaments, threads, yarns, fabrics, feathers or made-up fibrous goods using aqueous solvents
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction that the invention discloses a kind of, comprising the following steps: flaxen fiber A, is subjected to processing of singing；B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；F, flaxen fiber being finally subjected to soap boiling and washing, the dyeing that the present invention uses is easy to operate, and it is at low cost, it is environment friendly and pollution-free, it can be improved dyeing, the colour fixation of flaxen fiber.
Description
Technical field
The present invention relates to flaxen fiber staining technique field, specially a kind of flaxen fiber based on Laccase Catalyzed polymerization reaction is raw
Object dyeing.
Background technique
In recent years, increasingly strict with domestic and international environmental regulation, each fiber cleans dyeing process by height
Degree concern.Conventional coloring method and theory based on small molecule synthetic dyestuffs face lot of challenges, are mainly reflected in: synthetic dyestuffs
Preparation section is complicated, environmental pollution is big；Dyeing condition requires high (generally requiring harsh pH value and high temperature), dyeing multiple
Miscellaneous, water consume energy consumption height, modifying porcelain are difficult.Common dyes molecular weight is low, and dyeing product crock fastness is not good enough, tinting strength, tinting power
Low, dye utilization rate is low, and fast light, heat resistance also has a problem in various degree, and fiber is poor for applicability etc..The day of rising in recent years
Right dyestuff because chromatography is not complete, using heavy metal mordant pollution environment, dyefastness is poor the deficiencies of, practical application is greatly limited
System.
Summary of the invention
The flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction that the purpose of the present invention is to provide a kind of, with solution
Certainly the problems mentioned above in the background art.
To achieve the above object, the present invention provides the following technical solutions, and a kind of fiber crops based on Laccase Catalyzed polymerization reaction are fine
Vitamins dyeing the following steps are included:
A, flaxen fiber is subjected to processing of singing；
B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；
C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；
D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；
E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；
F, flaxen fiber is finally subjected to soap boiling and washing.
Preferably, it singes in the step A processing method are as follows: flaxen fiber is pressed using thermal insulation board, then in the gold heated
Metal surface slidably reciprocates 3-5 seconds.
Preferably, the step B neutral and alkali solution is warm width desizing enzyme 30g/L, caustic soda 15g/L, refining agent SR-
1206g/L, bath raio 1:10.
Preferably, clear water repeated flushing 3-5 times in the step C.
Preferably, low temperature drying temperature is 40-70 DEG C in the step C, drying time 30min-60min.
Preferably, laccase dosage is 200U/L, the dosage 40mmol/L of phenolic monomers, bath raio 1: 40 in the step D.
Preferably, color-fixing method in the step E are as follows: will immerse in reducing solution, reducing solution group is divided into sodium hydrosulfite 15-20
Part, 10-15 parts of caustic soda, 0.5-2 parts of salt, reduction temperature are 20-40 DEG C.
Preferably, it is 100-120 DEG C that gas, which steams temperature, in the step E, and gas steams the time for 40-60s.
Preferably, 60-80 DEG C of soap boiling temperature in the step F, soap boiling time are 3min-6min.
Compared with prior art, the beneficial effects of the present invention are:
(1) dyeing that the present invention uses is easy to operate, at low cost, environment friendly and pollution-free, can be improved the dye of flaxen fiber
Color, colour fixation.
(2) present invention use is singed, caustic dip is handled, and can effectively remove the impurity and leftover slurry on flaxen fiber surface,
Improve the dyeing effect of flaxen fiber.
(3) present invention steams step using fixation, gas, can be improved the colour fixation of flaxen fiber, further increases dyeing effect
Rate.
Specific embodiment
The following is a clear and complete description of the technical scheme in the embodiments of the invention, it is clear that described embodiment
Only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
Art personnel every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment one:
The present invention provides the following technical solutions, a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction,
The following steps are included:
A, flaxen fiber is subjected to processing of singing；
B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；
C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；
D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；
E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；
F, flaxen fiber is finally subjected to soap boiling and washing.
In the present embodiment, processing method of singing in step A are as follows: flaxen fiber is pressed using thermal insulation board, then in the gold heated
Metal surface slidably reciprocates 3 seconds.
In the present embodiment, step B neutral and alkali solution is warm width desizing enzyme 30g/L, caustic soda 15g/L, refining agent SR-
1206g/L, bath raio 1:10.
In the present embodiment, clear water repeated flushing 3 times in step C.
In the present embodiment, low temperature drying temperature is 40 DEG C in step C, drying time 30min.
In the present embodiment, laccase dosage is 200U/L, the dosage 40mmol/L of phenolic monomers, bath raio 1: 40 in step D.
In the present embodiment, color-fixing method in step E are as follows: will immerse in reducing solution, reducing solution group is divided into 15 parts of sodium hydrosulfite, burns
10 parts of alkali, 0.5 part of salt, reduction temperature are 20 DEG C.
It is 100 DEG C that gas, which steams temperature, in the present embodiment, in step E, and gas steams the time for 40s.
In the present embodiment, soap boiling temperature 60 C in step F, the soap boiling time is 3min.
Embodiment two:
A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction, comprising the following steps:
A, flaxen fiber is subjected to processing of singing；
B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；
C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；
D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；
E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；
F, flaxen fiber is finally subjected to soap boiling and washing.
In the present embodiment, processing method of singing in step A are as follows: flaxen fiber is pressed using thermal insulation board, then in the gold heated
Metal surface slidably reciprocates 5 seconds.
In the present embodiment, step B neutral and alkali solution is warm width desizing enzyme 30g/L, caustic soda 15g/L, refining agent SR-
1206g/L, bath raio 1:10.
In the present embodiment, clear water repeated flushing 5 times in step C.
In the present embodiment, low temperature drying temperature is 70 DEG C in step C, drying time 60min.
In the present embodiment, laccase dosage is 200U/L, the dosage 40mmol/L of phenolic monomers, bath raio 1: 40 in step D.
In the present embodiment, color-fixing method in step E are as follows: will immerse in reducing solution, reducing solution group is divided into 20 parts of sodium hydrosulfite, burns
15 parts of alkali, 2 parts of salt, reduction temperature are 40 DEG C.
It is 120 DEG C that gas, which steams temperature, in the present embodiment, in step E, and gas steams the time for 60s.
In the present embodiment, 80 DEG C of soap boiling temperature in step F, the soap boiling time is 6min.
Embodiment three:
A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction, comprising the following steps:
A, flaxen fiber is subjected to processing of singing；
B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；
C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；
D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；
E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；
F, flaxen fiber is finally subjected to soap boiling and washing.
In the present embodiment, processing method of singing in step A are as follows: flaxen fiber is pressed using thermal insulation board, then in the gold heated
Metal surface slidably reciprocates 3-5 seconds.
In the present embodiment, step B neutral and alkali solution is warm width desizing enzyme 30g/L, caustic soda 15g/L, refining agent SR-
1206g/L, bath raio 1:10.
In the present embodiment, clear water repeated flushing 3 times in step C.
In the present embodiment, low temperature drying temperature is 50 DEG C in step C, drying time 40min.
In the present embodiment, laccase dosage is 200U/L, the dosage 40mmol/L of phenolic monomers, bath raio 1: 40 in step D.
In the present embodiment, color-fixing method in step E are as follows: will immerse in reducing solution, reducing solution group is divided into 16 parts of sodium hydrosulfite, burns
11 parts of alkali, 1 part of salt, reduction temperature are 25 DEG C.
It is 105 DEG C that gas, which steams temperature, in the present embodiment, in step E, and gas steams the time for 45s.
In the present embodiment, 65 DEG C of soap boiling temperature in step F, the soap boiling time is 4min.
Example IV:
A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction, comprising the following steps:
A, flaxen fiber is subjected to processing of singing；
B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；
C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；
D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；
E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；
F, flaxen fiber is finally subjected to soap boiling and washing.
In the present embodiment, processing method of singing in step A are as follows: flaxen fiber is pressed using thermal insulation board, then in the gold heated
Metal surface slidably reciprocates 4 seconds.
In the present embodiment, step B neutral and alkali solution is warm width desizing enzyme 30g/L, caustic soda 15g/L, refining agent SR-
1206g/L, bath raio 1:10.
In the present embodiment, clear water repeated flushing 4 times in step C.
In the present embodiment, low temperature drying temperature is 55 DEG C in step C, drying time 45min.
In the present embodiment, laccase dosage is 200U/L, the dosage 40mmol/L of phenolic monomers, bath raio 1: 40 in step D.
In the present embodiment, color-fixing method in step E are as follows: will immerse in reducing solution, reducing solution group is divided into 17 parts of sodium hydrosulfite, burns
12 parts of alkali, 1 part of salt, reduction temperature are 30 DEG C.
It is 110 DEG C that gas, which steams temperature, in the present embodiment, in step E, and gas steams the time for 50s.
In the present embodiment, soap boiling temperature 70 C in step F, the soap boiling time is 5min.
Present invention use is singed, caustic dip is handled, and can effectively remove the impurity and leftover slurry on flaxen fiber surface, is improved
The dyeing effect of flaxen fiber；The present invention steams step using fixation, gas, can be improved the colour fixation of flaxen fiber, further mentions
High dyeing efficiency.
In conclusion the dyeing that the present invention uses is easy to operate, and it is at low cost, it is environment friendly and pollution-free, it can be improved numb fibre
The dyeing of dimension, colour fixation.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of variations, modification, replacement can be carried out to these embodiments without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (9)
1. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction, it is characterised in that: the following steps are included:
A, flaxen fiber is subjected to processing of singing；
B, the flaxen fiber after singing, which immerses in alkaline solution, to be handled, and surface impurity and leftover slurry are removed；
C, the flaxen fiber after alkali process is put into after repeated flushing is multiple in clear water and is put into drying in low temperature drying case；
D, the flaxen fiber after drying process is immersed in the buffer containing phenolic monomers and laccase and carries out biological stain；
E, the flaxen fiber after biological stain is subjected to fixation, gas steaming is handled；
F, flaxen fiber is finally subjected to soap boiling and washing.
2. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
Be: processing method of singing in the step A are as follows: using thermal insulation board press flaxen fiber, then the metal surface heated back and forth
Sliding 3-5 seconds.
3. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
Be: the step B neutral and alkali solution is warm width desizing enzyme 30g/L, caustic soda 15g/L, refining agent SR-1206g/L, bath raio 1:
10。
4. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
It is: clear water repeated flushing 3-5 times in the step C.
5. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
Be: low temperature drying temperature is 40-70 DEG C in the step C, drying time 30min-60min.
6. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
Be: laccase dosage is 200U/L, the dosage 40mmol/L of phenolic monomers, bath raio 1: 40 in the step D.
7. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
It is: color-fixing method in the step E are as follows: will immerse in reducing solution, reducing solution group is divided into 15-20 parts of sodium hydrosulfite, caustic soda 10-15
Part, 0.5-2 parts of salt, reduction temperature are 20-40 DEG C.
8. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
Be: it is 100-120 DEG C that gas, which steams temperature, in the step E, and gas steams the time for 40-60s.
9. a kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction according to claim 1, feature
Be: 60-80 DEG C of soap boiling temperature in the step F, soap boiling time are 3min-6min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810847259.8A CN108978270A (en) | 2018-07-27 | 2018-07-27 | A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810847259.8A CN108978270A (en) | 2018-07-27 | 2018-07-27 | A kind of flaxen fiber biological stain technique based on Laccase Catalyzed polymerization reaction |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109930395A (en) * | 2019-04-09 | 2019-06-25 | 中原工学院 | A kind of microbial staining method of cellulose-based fiber |
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| CN1420954A (en) * | 1999-12-14 | 2003-05-28 | 诺沃奇梅兹有限公司 | Enzymatic method for textile dyeing |
| CN101372763A (en) * | 2008-09-26 | 2009-02-25 | 绍兴中纺院江南分院有限公司 | Method for preparing bamboo primary fibre using composite biological enzyme |
| CN102702544A (en) * | 2012-05-18 | 2012-10-03 | 江南大学 | Method for improving compounding performance with resin by initiating hemp fiber grafted phenolic monomer with laccase |
| CN103952927A (en) * | 2014-04-30 | 2014-07-30 | 江南大学 | Linen fiber biologic dyeing process based on laccase catalysis polymerization color generation reaction |
-
2018
- 2018-07-27 CN CN201810847259.8A patent/CN108978270A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1420954A (en) * | 1999-12-14 | 2003-05-28 | 诺沃奇梅兹有限公司 | Enzymatic method for textile dyeing |
| CN101372763A (en) * | 2008-09-26 | 2009-02-25 | 绍兴中纺院江南分院有限公司 | Method for preparing bamboo primary fibre using composite biological enzyme |
| CN102702544A (en) * | 2012-05-18 | 2012-10-03 | 江南大学 | Method for improving compounding performance with resin by initiating hemp fiber grafted phenolic monomer with laccase |
| CN103952927A (en) * | 2014-04-30 | 2014-07-30 | 江南大学 | Linen fiber biologic dyeing process based on laccase catalysis polymerization color generation reaction |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109930395A (en) * | 2019-04-09 | 2019-06-25 | 中原工学院 | A kind of microbial staining method of cellulose-based fiber |
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