CN108948923A - A kind of reflective insulation lacquer and preparation method thereof - Google Patents
A kind of reflective insulation lacquer and preparation method thereof Download PDFInfo
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- CN108948923A CN108948923A CN201810904998.6A CN201810904998A CN108948923A CN 108948923 A CN108948923 A CN 108948923A CN 201810904998 A CN201810904998 A CN 201810904998A CN 108948923 A CN108948923 A CN 108948923A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D143/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
- C09D143/04—Homopolymers or copolymers of monomers containing silicon
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/70—Additives characterised by shape, e.g. fibres, flakes or microspheres
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2227—Oxides; Hydroxides of metals of aluminium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of reflective insulation lacquers, including below according to raw material: 160-180 parts of silicone acrylic emulsion, 20-30 parts of sol dispersion, 5-12 parts of propylene glycol, 0.2-0.5 parts of defoaming agent, 3-10 parts of cellulose, 0.3-0.7 parts of thickener, 5-10 parts of hollow glass micro-ball, 0-20 parts of silica 1,10-15 parts of aluminum oxide, 1-5 parts of dispersing agent, 2-6 parts of fungicide.The preparation method of the reflective insulation lacquer is also disclosed in the present invention.Reflective insulation lacquer of the invention is suitable for external wall, has effectively insulating effect, good soundproof effect, good insulating properties, it is ensured that the safety of exterior walls of buildings.
Description
Technical field
The present invention relates to structure material, specifically a kind of reflective insulation lacquer and preparation method thereof.
Background technique
External reflective heat-insulation paint starting is more early, and research is also more deep, makes great progress.Between multilayer aluminium film
The low air of thermal coefficient is introduced, composite material is made, has started the research of reflective heat-insulation paint.Phase late 1970s,
With the fast development of science and technology, radiation heat insulation and reflective insulation technology also achieve huge progress.
The watersoluble insulating mold coating for construction in China also has a large amount of research, and achieves biggish achievement.In the prior art
Using acrylic acid alkyd based resin as film forming matter, the filler of addition has rutile type titanium white, zinc oxide and mica powder, applies thickness
When degree is 20-30um, reflectivity can reach 80%, and also having a kind of can reflect the heat-insulated of various length ultraviolet lines and infrared ray
Coating, reflectivity can be high by 80%.
Lacquer is mainly used for roofing, plays the role of protecting roof waterpoof material and reducing temperature rising, but be used for
When exterior wall, good sound insulation, heat-insulated, insulation effect can not be played, existing lacquer manufacture craft is also more complex.
Summary of the invention
The purpose of the present invention is to provide a kind of reflective insulation lacquers and preparation method thereof, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the invention provides the following technical scheme:
A kind of reflective insulation lacquer, including below according to raw material: 160-180 parts of silicone acrylic emulsion, sol dispersion 20-
30 parts, 5-12 parts of propylene glycol, 0.2-0.5 parts of defoaming agent, 3-10 parts of cellulose, 0.3-0.7 parts of thickener, hollow glass micro-ball 5-
10 parts, 0-20 parts of silica 1,10-15 parts of aluminum oxide, 1-5 parts of dispersing agent, 2-6 parts of fungicide.
As a further solution of the present invention: the cellulose is sodium carboxymethylcellulose pyce, sodium citrate, apple fiber, mandarin orange
Any one in tangerine fiber.
As a further solution of the present invention: the thickener is one of starch, pectin, agar, starch derivatives.
As a further solution of the present invention: the dispersing agent is triethyl group hexyl phosphoric acid, lauryl sodium sulfate, methyl
Any one in amylalcohol, cellulose derivative.
As a further solution of the present invention: the preparation method of the reflective insulation lacquer, steps are as follows:
S1 makes cellulose dispersion liquid, weighs required raw material according to specific gravity, cellulose is placed in 11-16 times of deionized water,
Propylene glycol is added, keeps temperature in 45-55 degrees Celsius, persistently stirs 5-10 minutes, obtains cellulose dispersion liquid；
S2 takes sol dispersion, defoaming agent, thickener, aluminum oxide, dispersant, stirs under 45-50 degrees Celsius,
Revolving speed is 500-600 revs/min, obtains mixed solution；
The cellulose dispersion liquid that S1 is obtained is slowly added in the mixed solution that S2 is obtained, adds hollow glass micro-ball, two by S3
Silica, fungicide, it is 15-20 minutes ultrasonic, obtain sol dispersion；
S4, the sol dispersion that S3 is obtained, is placed in stirring container and stirs, and revolving speed is 1700-1900 revs/min, when stirring
Between for 25-30 minutes to get the reflective insulation lacquer.
Compared with prior art, the beneficial effects of the present invention are: manufacturing process of the present invention is simple, while there is following function
Can:
1, reflective insulation lacquer of the invention is suitable for external wall, and weatherability is splendid；
2, the present invention has effectively insulating effect, can reflect most of solar radiation, guarantee indoor temperature；
3, the present invention has good soundproof effect, is mixed with hollow glass micropearl, so that lacquer is imitated with good sound insulation
Fruit, and ensure that the low water absorption of the lacquer, building is preferably protected in the intensive Shelter in South China Cities of rainwater；
4 and the lacquer also there is good insulating properties, it is ensured that the safety of exterior walls of buildings.
Specific embodiment
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, this field is common
Technical staff's every other embodiment obtained without making creative work belongs to the model that the present invention protects
It encloses.
Embodiment 1
A kind of reflective insulation lacquer, including below according to raw material: 160 parts of silicone acrylic emulsion, 20 parts of sol dispersion, third
5 parts of glycol, 0.2 part of defoaming agent, 3 parts of cellulose, 0.3 part of thickener, 5 parts of hollow glass micro-ball, 0 part of silica 1, three oxidations
Two 10 parts of aluminium, 1 part of dispersing agent, 2 parts of fungicide.
In the present embodiment: the cellulose is sodium carboxymethylcellulose pyce.
In the present embodiment: the thickener is starch.
In the present embodiment: the dispersing agent is triethyl group hexyl phosphoric acid.
In the present embodiment: a kind of preparation method of reflective insulation lacquer, steps are as follows:
S1 makes cellulose dispersion liquid, weighs required raw material according to specific gravity, cellulose is placed in 11 times of deionized water, is added
Enter propylene glycol, keep temperature in 45 degrees Celsius, persistently stirs 5 minutes, obtain cellulose dispersion liquid；
S2 takes sol dispersion, defoaming agent, thickener, aluminum oxide, dispersant, stirs under 45 degrees Celsius, revolving speed
It is 500 revs/min, obtains mixed solution；
The cellulose dispersion liquid that S1 is obtained is slowly added in the mixed solution that S2 is obtained, adds hollow glass micro-ball, two by S3
Silica, fungicide, ultrasound 15 minutes, obtain sol dispersion；
S4, the sol dispersion that S3 is obtained, is placed in stirring container and stirs, and revolving speed is 1700 revs/min, mixing time 25
Minute is to get the reflective insulation lacquer.
Embodiment 2
A kind of reflective insulation lacquer, including below according to raw material: 168 parts of silicone acrylic emulsion, 24 parts of sol dispersion, third
7 parts of glycol, 0.3 part of defoaming agent, 5 parts of cellulose, 0.4 part of thickener, 7 parts of hollow glass micro-ball, 3 parts of silica 1, three oxidations
Two 13 parts of aluminium, 2 parts of dispersing agent, 4 parts of fungicide.
In the present embodiment: the cellulose is sodium citrate.
In the present embodiment: the thickener is one of pectin.
In the present embodiment: the dispersing agent is lauryl sodium sulfate.
In the present embodiment: a kind of preparation method of reflective insulation lacquer, steps are as follows:
S1 makes cellulose dispersion liquid, weighs required raw material according to specific gravity, cellulose is placed in 13 times of deionized water, is added
Enter propylene glycol, keep temperature in 48 degrees Celsius, persistently stirs 7 minutes, obtain cellulose dispersion liquid；
S2 takes sol dispersion, defoaming agent, thickener, aluminum oxide, dispersant, stirs under 46 degrees Celsius, revolving speed
It is 540 revs/min, obtains mixed solution；
The cellulose dispersion liquid that S1 is obtained is slowly added in the mixed solution that S2 is obtained, adds hollow glass micro-ball, two by S3
Silica, fungicide, ultrasound 16 minutes, obtain sol dispersion；
S4, the sol dispersion that S3 is obtained, is placed in stirring container and stirs, and revolving speed is 1750 revs/min, mixing time 27
Minute is to get the reflective insulation lacquer.
Embodiment 3
A kind of reflective insulation lacquer, including below according to raw material: 175 parts of silicone acrylic emulsion, 27 parts of sol dispersion, third
10 parts of glycol, 0.4 part of defoaming agent, 7 parts of cellulose, 0.6 part of thickener, 8 parts of hollow glass micro-ball, 7 parts of silica 1, three oxygen
Change 4 parts of two aluminium, 4 parts of dispersing agent, 5 parts of fungicide.
In the present embodiment: the cellulose is apple fiber.
In the present embodiment: the thickener is agar.
In the present embodiment: the dispersing agent is methyl anyl alcohol.
In the present embodiment: a kind of preparation method of reflective insulation lacquer, steps are as follows:
S1 makes cellulose dispersion liquid, weighs required raw material according to specific gravity, cellulose is placed in 15 times of deionized water, is added
Enter propylene glycol, keep temperature in 52 degrees Celsius, persistently stirs 8 minutes, obtain cellulose dispersion liquid；
S2 takes sol dispersion, defoaming agent, thickener, aluminum oxide, dispersant, stirs under 48 degrees Celsius, revolving speed
It is 580 revs/min, obtains mixed solution；
The cellulose dispersion liquid that S1 is obtained is slowly added in the mixed solution that S2 is obtained, adds hollow glass micro-ball, two by S3
Silica, fungicide, ultrasound 18 minutes, obtain sol dispersion；
S4, the sol dispersion that S3 is obtained, is placed in stirring container and stirs, and revolving speed is 1850 revs/min, mixing time 29
Minute is to get the reflective insulation lacquer.
Embodiment 4
A kind of reflective insulation lacquer, including below according to raw material: 180 parts of silicone acrylic emulsion, 30 parts of sol dispersion, third
12 parts of glycol, 0.5 part of defoaming agent, 10 parts of cellulose, 0.7 part of thickener, 10 parts of hollow glass micro-ball, 20 parts of silica, three
15 parts of Al 2 O, 5 parts of dispersing agent, 6 parts of fungicide.
In the present embodiment: the cellulose is citrus fruit fibres.
In the present embodiment: the thickener is starch derivatives.
In the present embodiment: the dispersing agent is cellulose derivative.
In the present embodiment: a kind of preparation method of reflective insulation lacquer, steps are as follows:
S1 makes cellulose dispersion liquid, weighs required raw material according to specific gravity, cellulose is placed in 16 times of deionized water, is added
Enter propylene glycol, keep temperature in 55 degrees Celsius, persistently stirs 10 minutes, obtain cellulose dispersion liquid；
S2 takes sol dispersion, defoaming agent, thickener, aluminum oxide, dispersant, stirs under 50 degrees Celsius, revolving speed
It is 600 revs/min, obtains mixed solution；
The cellulose dispersion liquid that S1 is obtained is slowly added in the mixed solution that S2 is obtained, adds hollow glass micro-ball, two by S3
Silica, fungicide, ultrasound 20 minutes, obtain sol dispersion；
S4, the sol dispersion that S3 is obtained, is placed in stirring container and stirs, and revolving speed is 1900 revs/min, mixing time 30
Minute is to get the reflective insulation lacquer.
It is obvious to a person skilled in the art that invention is not limited to the details of the above exemplary embodiments, Er Qie
In the case where without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the present invention is by appended power
Benefit requires rather than above description limits, it is intended that all by what is fallen within the meaning and scope of the equivalent elements of the claims
Variation is included within the present invention.
In addition, it should be understood that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
It considers the specification as a whole, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
The other embodiments being understood that.
Claims (7)
1. a kind of reflective insulation lacquer, which is characterized in that including below according to raw material: 160-180 parts of silicone acrylic emulsion,
20-30 parts of sol dispersion, 5-12 parts of propylene glycol, 0.2-0.5 parts of defoaming agent, 3-10 parts of cellulose, 0.3-0.7 parts of thickener,
5-10 parts of hollow glass micro-ball, 0-20 parts of silica 1,10-15 parts of aluminum oxide, 1-5 parts of dispersing agent, 2-6 parts of fungicide.
2. reflective insulation lacquer according to claim 1, which is characterized in that the cellulose be sodium carboxymethylcellulose pyce,
Sodium citrate, apple fiber, any one in citrus fruit fibres.
3. reflective insulation lacquer according to claim 2, which is characterized in that the thickener is starch, pectin, fine jade
Any one in rouge, starch derivatives.
4. reflective insulation lacquer according to claim 3, which is characterized in that the dispersing agent is triethyl group hexyl phosphorus
Acid, lauryl sodium sulfate, methyl anyl alcohol, any one in cellulose derivative.
5. a kind of paint preparation method of the true stone of reflective insulation a method as claimed in any one of claims 1 to 5, which is characterized in that steps are as follows
S1 makes cellulose dispersion liquid；
S2 takes sol dispersion, defoaming agent, thickener, aluminum oxide, dispersant, stirs under 45-50 degrees Celsius,
Revolving speed is 500-600 revs/min, obtains mixed solution；
The cellulose dispersion liquid that S1 is obtained is slowly added in the mixed solution that S2 is obtained, adds hollow glass micro-ball, two by S3
Silica, fungicide, it is 15-20 minutes ultrasonic, obtain sol dispersion；
S4, the sol dispersion that S3 is obtained, is placed in stirring container and stirs, and revolving speed is 1700-1900 revs/min, when stirring
Between for 25-30 minutes to get the reflective insulation lacquer.
6. the preparation method of reflective insulation lacquer according to claim 6, which is characterized in that in step S1, cellulose
Dispersion liquid the preparation method comprises the following steps: weigh required raw material according to specific gravity, cellulose is placed in 11-16 times of deionized water, is added
Propylene glycol keeps temperature in 45-55 degrees Celsius, persistently stirs 5-10 minutes, obtains cellulose dispersion liquid.
7. purposes of the lacquer in preparation reflective insulation lacquer product as described in claim 1-4 is any.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810904998.6A CN108948923A (en) | 2018-08-09 | 2018-08-09 | A kind of reflective insulation lacquer and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810904998.6A CN108948923A (en) | 2018-08-09 | 2018-08-09 | A kind of reflective insulation lacquer and preparation method thereof |
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| Publication Number | Publication Date |
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| CN108948923A true CN108948923A (en) | 2018-12-07 |
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| CN201810904998.6A Pending CN108948923A (en) | 2018-08-09 | 2018-08-09 | A kind of reflective insulation lacquer and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111393077A (en) * | 2020-03-24 | 2020-07-10 | 上海凡瑞得新型建材有限公司 | Reflective heat-insulation stone-like paint and preparation method thereof |
| CN113583531A (en) * | 2021-08-16 | 2021-11-02 | 广东涂百年新型材料有限公司 | Reflective heat-insulation real stone paint material and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106349855A (en) * | 2016-08-31 | 2017-01-25 | 铃鹿复合建材（上海）有限公司 | Reflective thermal insulating really stone paint |
| CN107903749A (en) * | 2017-11-12 | 2018-04-13 | 佛山市嘉柏丽涂料有限公司 | A kind of reflective insulation lacquer and preparation method thereof |
-
2018
- 2018-08-09 CN CN201810904998.6A patent/CN108948923A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106349855A (en) * | 2016-08-31 | 2017-01-25 | 铃鹿复合建材（上海）有限公司 | Reflective thermal insulating really stone paint |
| CN107903749A (en) * | 2017-11-12 | 2018-04-13 | 佛山市嘉柏丽涂料有限公司 | A kind of reflective insulation lacquer and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111393077A (en) * | 2020-03-24 | 2020-07-10 | 上海凡瑞得新型建材有限公司 | Reflective heat-insulation stone-like paint and preparation method thereof |
| CN113583531A (en) * | 2021-08-16 | 2021-11-02 | 广东涂百年新型材料有限公司 | Reflective heat-insulation real stone paint material and preparation method thereof |
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Application publication date: 20181207 |