CN108822660A - Insulating mold coating of transparent glass and preparation method thereof - Google Patents
Insulating mold coating of transparent glass and preparation method thereof Download PDFInfo
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- CN108822660A CN108822660A CN201810533465.1A CN201810533465A CN108822660A CN 108822660 A CN108822660 A CN 108822660A CN 201810533465 A CN201810533465 A CN 201810533465A CN 108822660 A CN108822660 A CN 108822660A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/04—Homopolymers or copolymers of esters
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/004—Reflecting paints; Signal paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/32—Radiation-absorbing paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Inorganic Chemistry (AREA)
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Abstract
The invention proposes a kind of insulating mold coating of transparent glass and preparation method thereof, according to the number of parts by weight, including following components：70~90 parts of epoxy modified silicone resin, 10~20 parts of polyvinyl resin, 5~15 parts of nano-titanium dioxide, 5~15 parts of thermal insulating filling, 1~3 part of wetting dispersing agent, 0.5~1 part of mould inhibitor, 4~8 parts of thickener, 1~3 part of defoaming agent, 6~12 parts of coalescing agent and 40~60 parts of deionized water, the thermal insulating filling is modified crystal whisker of hexa potassium titanate, and the modified crystal whisker of hexa potassium titanate is mainly prepared by expanded perlite, indium trichloride and basic zirconium chloride.The coating not only reflectivity with higher and emissivity, good heat-insulation effect, thermal coefficient is low, can be applied to indoor heat-insulated.
Description
Technical field
The invention belongs to technical field of coatings, and in particular to a kind of insulating mold coating of transparent glass and preparation method thereof.
Background technique
Insulating mold coating of transparent glass is the new type functional building coating centainly applied and be taken seriously in recent years.?
The excessively high hot summer and warm winter zone of China's summer temperature, hot summer and warm winter area area, the coating are imitated in addition to the decoration with common exterior coating
Outside fruit, additionally it is possible to which reflected solar radiation is warm and reduces film coated surface temperature, and mitigates band due to summer, film coated surface temperature was excessively high
The a series of problems come.Although there are many insulating mold coating of transparent glass research, in practical applications there is also problems,
Such as：Performance is unstable, patent 200510028388.7 report reflective heat-insulation paint although have fairly good solar reflectivity,
But infrared emittance is poor；Color is single, mainly based on white or light-colored coating, limitation is larger etc..
In the prior art, the products such as pad pasting, sheathing paper, metal coating heat-protecting glass are generallyd use realize windowpane every
Heat problem, but usually there is the problems such as light transmittance is low, heat insulation is bad, complex process in these products.Nowadays people are to building
The pay attention to day by day of power saving, the enhancing of environmental protection ideas and the raising of safe sex consciousness are built, insulating mold coating is as a kind of new
Type, thermal insulation, environmental protection, insulation product are more and more concerned.
Summary of the invention
The present invention proposes a kind of insulating mold coating of transparent glass, the coating not only reflectivity with higher and emissivity, every
Thermal effect is good, and thermal coefficient is low, can be applied to indoor heat-insulated.
The technical proposal of the invention is realized in this way：
A kind of insulating mold coating of transparent glass, according to the number of parts by weight, including following components：
70~90 parts of epoxy modified silicone resin, 10~20 parts of polyvinyl resin, 5~15 parts of nano-titanium dioxide, every
5~15 parts of hot filler, 1~3 part of wetting dispersing agent, 0.5~1 part of mould inhibitor, 4~8 parts of thickener, 1~3 part of defoaming agent, film forming
6~12 parts of auxiliary agent and 40~60 parts of deionized water, the thermal insulating filling are modified crystal whisker of hexa potassium titanate, six metatitanic acid of modification
Potassium whisker is mainly prepared by crystal whisker of hexa potassium titanate, silicon nitride and silane coupling agent.
Preferably, the preparation method of the modified crystal whisker of hexa potassium titanate：
Crystal whisker of hexa potassium titanate and silicon nitride are added in acetone, ultrasonic disperse is carried out, dispersion liquid is obtained, by dispersion liquid liter
Then temperature sequentially adds silane coupling agent, water and polyamide, stirs evenly to 75~82 DEG C, dry after reaction.
Preferably, the mass ratio of the silicon nitride and the crystal whisker of hexa potassium titanate is 1:5~7, the silane coupling agent
Mass ratio with the crystal whisker of hexa potassium titanate is 1:20~25, the mass ratio of the polyamide and the silicon nitride is 1:15
~20.
Preferably, the silane coupling agent is KH550 or KH560.
Preferably, the wetting dispersing agent be ammonium acrylate dipersant, the mould inhibitor be termil or
Person's Kathon.
Preferably, the thickener is non-ionic polyurethane compound, modified polyacrylic acid ammonium or modified polyacrylic acid
Sodium；The defoaming agent is dimethyl silicone polymer solution or mineral oil；The coalescing agent is alcohol ester 12, ethylene glycol only son
Ether, ethylene glycol, propylene-glycol ethyl ether or propandiol butyl ether.
It is a further object to provide a kind of preparation methods of insulating mold coating of transparent glass, include the following steps：
1) wetting dispersing agent, mould inhibitor, 1/2~3/5 defoaming agent are added in deionized water according to formula ratio, 300~
Stirring is sufficiently mixed under the revolving speed of 500r/min；
2) be added into the mixture of step 1) nano-titanium dioxide, polyvinyl resin and thermal insulating filling 1000~
Disperse under the revolving speed of 2000r/min；
3) epoxy modified silicone resin, thickener, coalescing agent are added into the dispersion liquid of step 2) and remaining disappears
Infusion stirs evenly.
Beneficial effects of the present invention：
1, the preparation method of modified crystal whisker of hexa potassium titanate is in the component of coating of the invention：By crystal whisker of hexa potassium titanate and nitrogen
SiClx is added in acetone, is carried out ultrasonic disperse, is obtained dispersion liquid, dispersion liquid is warming up to 75~82 DEG C, is then sequentially added
Silane coupling agent, water and polyamide, stir evenly, and dry after reaction.The modification potassium hexatitanate that this method obtains is brilliant
Palpus stability with higher and high temperature resistance, to make crystal whisker of hexa potassium titanate that there is high temperature sound-absorbing, chemical stability, insulation
Property, reflection infrared ray, excellent antiseptic property etc., moreover it is possible to improve the rigidity for applying coating, solve potassium hexatitanate crystalline substance individually
The problem of bring stability difference and temperature tolerance difference must be modified.
2, the present invention has higher shielding rate in infrared light district, has good transmissivity in visible region, in ultraviolet region
There is significant absorption effect, it is seen that light transmission > 85%, infrared light shielding rate >=63%, energy-saving effect is significant, heat insulation and heat control
15~20 DEG C, energy conservation 20~30%.
Specific embodiment
Embodiment 1
The preparation method of modified crystal whisker of hexa potassium titanate：
Crystal whisker of hexa potassium titanate and silicon nitride are added in acetone, ultrasonic disperse is carried out, dispersion liquid is obtained, by dispersion liquid liter
Then temperature sequentially adds KH560, water and polyamide, stirs evenly to 75 DEG C, dry after reaction.Silicon nitride and six
The mass ratio of potassium titanate crystal whisker is 1:5, KH560 and crystal whisker of hexa potassium titanate mass ratio be 1:23, polyamide and silicon nitride
Mass ratio be 1:17.
Embodiment 2
The preparation method of modified crystal whisker of hexa potassium titanate：
Crystal whisker of hexa potassium titanate and silicon nitride are added in acetone, ultrasonic disperse is carried out, dispersion liquid is obtained, by dispersion liquid liter
Then temperature sequentially adds KH550, water and polyamide, stirs evenly to 82 DEG C, dry after reaction.Silicon nitride and institute
The mass ratio for stating crystal whisker of hexa potassium titanate is 1:5, KH550 and crystal whisker of hexa potassium titanate mass ratio be 1:20, polyamide and nitrogen
The mass ratio of SiClx is 1:20.
Embodiment 3
A kind of insulating mold coating of transparent glass, according to the number of parts by weight, including following components：
Acrylic emulsion and 10 parts of 15 parts of 80 parts of mixture, polyvinyl resin, the nano-titanium dioxide of silica solution, embodiment
1 10 parts of modification crystal whisker of hexa potassium titanate, 2 parts of ammonium acrylate dipersant, 0.8 part of termil, modified polyacrylic acid
6 parts of ammonium, 2 parts of mineral oil, 9 parts of propylene-glycol ethyl ether and 50 parts of deionized water.
Preparation method：
1) deionized water is added in ammonium acrylate dipersant, termil, 1/2 mineral oil according to formula ratio
In, it stirs and is sufficiently mixed under the revolving speed of 300r/min；
2) six metatitanic acid of modification of nano-titanium dioxide, polyvinyl resin and embodiment 1 is added into the mixture of step 1)
Potassium whisker disperses under the revolving speed of 1000r/min；
3) mixture, the modified polyacrylic acid ammonium, third of acrylic emulsion and silica solution are added into the dispersion liquid of step 2)
Glycol ether and remaining termil stir evenly.
Embodiment 4
A kind of insulating mold coating of transparent glass, according to the number of parts by weight, including following components：
Acrylic emulsion and 5 parts of 20 parts of 70 parts of mixture, polyvinyl resin, the nano-titanium dioxide of silica solution, embodiment 2
5 parts of modification crystal whisker of hexa potassium titanate, 1 part of ammonium acrylate dipersant, 0.5 part of Kathon, modified
8 parts of Sodium Polyacrylate, 1 part of dimethyl silicone polymer solution, 12 parts of alcohol ester and 60 parts of deionized water.
Preparation method includes the following steps：
1) according to formula ratio by ammonium acrylate dipersant, Kathon, 3/5 poly dimethyl silicon
Oxygen alkane solution is added in deionized water, stirs and is sufficiently mixed under the revolving speed of 500r/min；
2) six metatitanic acid of modification of nano-titanium dioxide, polyvinyl resin and embodiment 2 is added into the mixture of step 1)
Potassium whisker disperses under the revolving speed of 2000r/min；
3) mixture, modified polyacrylate sodium, the alcohol of acrylic emulsion and silica solution are added into the dispersion liquid of step 2)
Ester 12 and remaining dimethyl silicone polymer solution stir evenly.
Embodiment 5
A kind of insulating mold coating of transparent glass, according to the number of parts by weight, including following components：
Acrylic emulsion and 15 parts of 10 parts of 90 parts of mixture, polyvinyl resin, the nano-titanium dioxide of silica solution, embodiment
2 15 parts of modification crystal whisker of hexa potassium titanate, 3 parts of ammonium acrylate dipersant, 1 part of termil, modified polyacrylic acid ammonium 4
Part, 3 parts of mineral oil, 12 parts of ethylene glycol monobutyl ether and 40 parts of deionized water
Preparation method：
1) deionized water is added in ammonium acrylate dipersant, termil, 1/2 mineral oil according to formula ratio
In, it stirs and is sufficiently mixed under the revolving speed of 400r/min；
2) six metatitanic acid of modification of nano-titanium dioxide, polyvinyl resin and embodiment 2 is added into the mixture of step 1)
Potassium whisker disperses under the revolving speed of 1600r/min；
3) mixture, the modified polyacrylic acid ammonium, second of acrylic emulsion and silica solution are added into the dispersion liquid of step 2)
Glycol monobutyl ether and remaining mineral oil stir evenly.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent replacement, improvement and so on be should all be included in the protection scope of the present invention.
Claims (7)
1. a kind of insulating mold coating of transparent glass, which is characterized in that according to the number of parts by weight, including following components：
70~90 parts of epoxy modified silicone resin, 5~15 parts of nano-titanium dioxide, heat-insulated is filled out 10~20 parts of polyvinyl resin
Expect 5~15 parts, 1~3 part of wetting dispersing agent, 0.5~1 part of mould inhibitor, 4~8 parts of thickener, 1~3 part of defoaming agent, coalescing agent 6
~12 parts and 40~60 parts of deionized water, the thermal insulating filling is modified crystal whisker of hexa potassium titanate, and the modified potassium hexatitanate is brilliant
It must be mainly prepared by crystal whisker of hexa potassium titanate, silicon nitride and silane coupling agent.
2. insulating mold coating of transparent glass according to claim 1, which is characterized in that the system of the modified crystal whisker of hexa potassium titanate
Preparation Method：
Crystal whisker of hexa potassium titanate and silicon nitride are added in acetone, ultrasonic disperse is carried out, obtains dispersion liquid, dispersion liquid is warming up to
75~82 DEG C, silane coupling agent, water and polyamide are then sequentially added, is stirred evenly, dried after reaction.
3. insulating mold coating of transparent glass according to claim 2, which is characterized in that the silicon nitride and the potassium hexatitanate
The mass ratio of whisker is 1:5~7, the mass ratio of the silane coupling agent and the crystal whisker of hexa potassium titanate is 1:20~25,
The mass ratio of the polyamide and the silicon nitride is 1:15~20.
4. insulating mold coating of transparent glass according to claim 2, which is characterized in that the silane coupling agent be KH550 or
Person KH560.
5. insulating mold coating of transparent glass according to claim 1, which is characterized in that the wetting dispersing agent is ammonium acrylate
Dipersant, the mould inhibitor are termil or Kathon.
6. insulating mold coating of transparent glass according to claim 1, which is characterized in that the thickener is non-ionic polyurethane
Compound, modified polyacrylic acid ammonium or modified polyacrylate sodium；The defoaming agent is dimethyl silicone polymer solution or mineral
Oil；The coalescing agent is alcohol ester 12, ethylene glycol monobutyl ether, ethylene glycol, propylene-glycol ethyl ether or propandiol butyl ether.
7. the preparation method of insulating mold coating of transparent glass as described in claim 1, which is characterized in that include the following steps：
1) wetting dispersing agent, mould inhibitor, 1/2~3/5 defoaming agent are added in deionized water according to formula ratio, in 300~500r/
Stirring is sufficiently mixed under the revolving speed of min；
2) nano-titanium dioxide, polyvinyl resin and thermal insulating filling are added into the mixture of step 1) in 1000~2000r/
Disperse under the revolving speed of min；
3) epoxy modified silicone resin, thickener, coalescing agent and remaining defoaming agent are added into the dispersion liquid of step 2)
It stirs evenly.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201810533465.1A CN108822660A (en) | 2018-05-29 | 2018-05-29 | Insulating mold coating of transparent glass and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810533465.1A CN108822660A (en) | 2018-05-29 | 2018-05-29 | Insulating mold coating of transparent glass and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109896754A (en) * | 2019-03-21 | 2019-06-18 | 南京汉旗新材料股份有限公司 | A kind of glass fungus-proof liquid |
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| CN103602263A (en) * | 2013-12-07 | 2014-02-26 | 北京顺缘天和新材料技术有限公司 | Transparent heat-insulation energy-saving nano paint and preparation method thereof |
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| CN107325663A (en) * | 2017-08-03 | 2017-11-07 | 合肥泓定科技有限公司 | Architectural reflective heat-insulation paint and preparation method thereof |
| CN107325720A (en) * | 2017-08-03 | 2017-11-07 | 合肥泓定科技有限公司 | Aqueous glass heat insulation paint and preparation method thereof |
| CN107573844A (en) * | 2017-08-18 | 2018-01-12 | 宏建中玻（高碑店）玻璃科技有限公司 | A kind of transparent nano insulating moulding coating |
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2018
- 2018-05-29 CN CN201810533465.1A patent/CN108822660A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101982514A (en) * | 2010-11-01 | 2011-03-02 | 秦如新 | Nano transparent thermal insulation coating |
| CN103602263A (en) * | 2013-12-07 | 2014-02-26 | 北京顺缘天和新材料技术有限公司 | Transparent heat-insulation energy-saving nano paint and preparation method thereof |
| CN104231917A (en) * | 2014-10-13 | 2014-12-24 | 北京国泰瑞华精藻硅特种材料有限公司 | Nanometer high temperature resistant thermal insulation and prevention coating |
| CN107325663A (en) * | 2017-08-03 | 2017-11-07 | 合肥泓定科技有限公司 | Architectural reflective heat-insulation paint and preparation method thereof |
| CN107325720A (en) * | 2017-08-03 | 2017-11-07 | 合肥泓定科技有限公司 | Aqueous glass heat insulation paint and preparation method thereof |
| CN107573844A (en) * | 2017-08-18 | 2018-01-12 | 宏建中玻（高碑店）玻璃科技有限公司 | A kind of transparent nano insulating moulding coating |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109896754A (en) * | 2019-03-21 | 2019-06-18 | 南京汉旗新材料股份有限公司 | A kind of glass fungus-proof liquid |
| CN109896754B (en) * | 2019-03-21 | 2021-07-27 | 南京汉旗新材料股份有限公司 | Glass mildew-proof liquid |
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Application publication date: 20181116 |
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| RJ01 | Rejection of invention patent application after publication |