CN108947644A - A kind of preparation method of flower planting liquid medicine fertilizer - Google Patents

A kind of preparation method of flower planting liquid medicine fertilizer Download PDF

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Publication number
CN108947644A
CN108947644A CN201810674653.6A CN201810674653A CN108947644A CN 108947644 A CN108947644 A CN 108947644A CN 201810674653 A CN201810674653 A CN 201810674653A CN 108947644 A CN108947644 A CN 108947644A
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China
Prior art keywords
additive amount
liquid medicine
medicine fertilizer
preparation
solution
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CN201810674653.6A
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Chinese (zh)
Inventor
肖忠
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ANHUI RUIRAN BIOLOGICAL FERTILIZER TECHNOLOGY CO LTD
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ANHUI RUIRAN BIOLOGICAL FERTILIZER TECHNOLOGY CO LTD
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Priority to CN201810674653.6A priority Critical patent/CN108947644A/en
Publication of CN108947644A publication Critical patent/CN108947644A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C11/00Other nitrogenous fertilisers
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05FORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
    • C05F3/00Fertilisers from human or animal excrements, e.g. manure

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses a kind of flower planting preparation methods of liquid medicine fertilizer comprising following steps: (1) excrement takes fermentation liquid through anaerobic fermentation, is filtered by vacuum to obtain filtrate after precipitating;(2) concentrate is concentrated to get using reverse osmosis membrane to filtrate;(3) it takes a certain amount of concentrate, ethoxy is added and replaces ethylenediamine triacetic acid, stirs to being completely dissolved, add microelement and stir to dissolution and obtain solution A;(4) a certain amount of concentrate is taken, powder of amino acids is added, stirring obtains solution B to dissolving;(5) solution A and solution B are mixed, adds Folium Artemisiae Argyi extract;(6) it is eventually adding ascorbic acid and adjusts PH to 6.3-6.6, obtain liquid medicine fertilizer.It is an advantage of the current invention that concentration biogas slurry is equipped with amino acid, microelement and plant extracts and obtains meeting the Ministry of Agriculture to fertilizer nutrient required standard, can also kill various pathogens, reduce a possibility that flowers are by disease as base manure.

Description

A kind of preparation method of flower planting liquid medicine fertilizer
Technical field
The invention belongs to technical field of agricultural fertilizers, and in particular to a kind of preparation method of flower planting liquid medicine fertilizer.
Background technique
Biogas slurry is used for flower planting fertilizer, at flower planting initial stage as base manure, or as subsequent top dressing apply, Usually show enchashment to use, and the nutrient in biogas slurry stoste, the content of especially some macroelement fertilizers are lower, can not reach To the Ministry of Agriculture for the relevant regulations of liquid fertilizer, therefore other fertilizer must also be cooperated to be used in conjunction with.
Summary of the invention
Technical problem to be solved by the present invention lies in: when biogas slurry is directly used in flower planting, a great number of elements in stoste Fertilizer nutrient content is lower, needs to use with other fertilizers.
The present invention solves above-mentioned technical problem using following technical scheme:
A kind of preparation method of flower planting liquid medicine fertilizer comprising following steps:
(1) human or animal's excrement takes fermentation liquid through anaerobic fermentation, is filtered by vacuum to obtain filtrate after precipitating;
(2) 7-10 times is concentrated using reverse osmosis membrane to the filtrate that step (1) obtains, obtains concentrate;
(3) a certain amount of concentrate is taken, is heated to 30-40 DEG C, ethoxy is added and replaces ethylenediamine triacetic acid, is stirred to completely molten Solution, adds microelement and stirs to dissolution and obtain solution A;
(4) a certain amount of concentrate is taken, powder of amino acids is added, stirring obtains solution B to dissolving;
(5) solution A and solution B are mixed, then Folium Artemisiae Argyi extract is added thereto;
(6) ascorbic acid is added in the solution obtained to step (5) and adjusts PH to 6.3-6.6, obtain liquid medicine fertilizer;
Wherein, every configuration 1L liquid medicine fertilizer, the ethoxy are 2.70-3.0g for the additive amount of ethylenediamine triacetic acid;Institute The additive amount for stating powder of amino acids is 115-130g;The additive amount of the Folium Artemisiae Argyi extract is 0.7-1g.
Preferably, the preparation method of a kind of flower planting liquid medicine fertilizer, every configuration 1L liquid medicine fertilizer, the ethoxy replace The additive amount of ethylenediamine triacetic acid is 2.8g;The additive amount of the powder of amino acids is 120g;The addition of the Folium Artemisiae Argyi extract Amount is 0.8g.
Preferably, the preparation method of a kind of flower planting liquid medicine fertilizer, the microelement be Fe element, Mn element, Cu element, Zn element and B element.
Preferably, the preparation method of a kind of flower planting liquid medicine fertilizer, every configuration 1L liquid medicine fertilizer, the Fe element Additive amount is 0.6-0.8g;The additive amount of the Mn element is 0.3-0.4g;The additive amount of the Cu element is 0.06-0.08g; The additive amount of the Zn element is 0.01-0.03g;The additive amount of the B element is 0.10-0.16g.
Preferably, the preparation method of a kind of flower planting liquid medicine fertilizer, every configuration 1L liquid medicine fertilizer, the Fe element Additive amount is 0.7g;The additive amount of the Mn element is 0.35g;The additive amount of the Cu element is 0.07g;The Zn element Additive amount is 0.02g;The additive amount of the B element is 0.14g.
Preferably, the preparation method of a kind of flower planting liquid medicine fertilizer, the Folium Artemisiae Argyi extract the preparation method comprises the following steps: will Extracting solution is obtained using water extraction extraction method after folium artemisiae argyi is broken, then is concentrated, is spray-dried and obtains solid extract.
Preferably, the preparation method of a kind of flower planting liquid medicine fertilizer, the temperature of the anaerobic fermentation are that 20-40 is Celsius Degree.
The technology of the present invention the utility model has the advantages that
Biogas slurry is concentrated by reverse osmosis membrane for technical solution of the present invention, improves the concentration of nutrient contained therein, and thereto Amino acid and inorganic microelement is added, microelement is complexed for ethylenediamine triacetic acid using ethoxy, more so as to it Good ground cover plant absorbs;Folium artemisiae argyi is a kind of natural bactericidal agent, and wide sterilization spectrum can effectively kill various pathogens, reduces flowers and meets with A possibility that by disease.
Specific embodiment
For convenient for those skilled in the art understand that technical solution of the present invention, now in conjunction with specific embodiment to the technology of the present invention side Case is described further.
The invention discloses a kind of flower planting preparation methods of liquid medicine fertilizer comprising following steps:
(1) human or animal's excrement takes fermentation liquid, is filtered by vacuum to obtain after precipitating through anaerobic fermentation at 20-40 DEG C Filtrate.
(2) filtrate that step (1) obtains is concentrated using reverse osmosis membrane, obtains concentrate.
For the suitable cycles of concentration of determination, the present invention is by obtaining 2-10 times of concentrate first with reverse osmosis membrane, so Nutrient in the concentrate of different multiples is measured respectively afterwards.It is triumphant using semimicro after sample is disappeared and boiled using the concentrated sulfuric acid-water The formula way of distillation measures full nitrogen, and molybdenum blue colorimetric method measures full phosphorus, and flare photometer measures full potassium.Concrete operation method is existing Technology can refer to water and effluent monitoring analysis method.7-10 times is concentrated into biogas slurry stoste by analysis of experimental results determination.
(3) a certain amount of concentrate is taken, is heated to 30-40 DEG C, ethoxy is added and replaces ethylenediamine triacetic acid (HEEDTA), stirring To being completely dissolved, adds microelement and stir to dissolution and obtain solution A;The microelement is Fe element, Mn element, Cu member Element, Zn element and B element.HEEDTA is used as chelating agent, and the chelate reacted with minor metallic element is more steady It is fixed.
(4) a certain amount of concentrate is taken, powder of amino acids is added, stirring obtains solution B to dissolving;
(5) solution A and solution B are mixed, then Folium Artemisiae Argyi extract is added thereto;The Folium Artemisiae Argyi extract, which refers to, to end Extracting solution is obtained using water extraction extraction method after leaf is broken, then is concentrated, is spray-dried and obtains solid.Extract folium artemisiae argyi is as a kind of Natural bactericidal agent, wide sterilization spectrum can kill a variety of pathogens and fungi, endanger to avoid flowers by disease pest,.
(6) ascorbic acid is added in the solution obtained to step (5) and adjusts PH to 6.3-6.6, supply concentrate and obtain liquid Body medicine fertilizer.The PH that ascorbic acid is not only used to adjust liquid medicine fertilizer is weakly acidic, is more suitable for absorption of the flowers for nutriment; On the other hand, ascorbic acid has reproducibility, can be oxidized to avoid part nutriment, in favor of the absorption of flowers.
The liquid medicine fertilizer that come that the present invention will be described in detail below by specific embodiment described.Each original in following specific embodiments The dosage of material each means additive amount when configuration 1L liquid medicine fertilizer.
Embodiment one
1L liquid medicine fertilizer is configured in the present embodiment, the cycles of concentration of the biogas slurry concentrate is 7 times;The HEEDTA's Additive amount is 2.8g;The additive amount of the powder of amino acids is 120g;The additive amount of the Folium Artemisiae Argyi extract is 0.8g;The Fe The additive amount of element is 0.7g;The additive amount of the Mn element is 0.35g;The additive amount of the Cu element is 0.07g;The Zn The additive amount of element is 0.02g;The additive amount of the B element is 0.14g.Ascorbic acid is finally added into mixture by its PH 6.6 are adjusted to, medicine fertilizer finished product is obtained.
Embodiment two
Medicine fertilizer 1L is configured in the present embodiment, the cycles of concentration of the biogas slurry concentrate is 10 times;The HEEDTA's adds Dosage is 3.0g;The additive amount of the powder of amino acids is 130g;The additive amount of the Folium Artemisiae Argyi extract is 1g;The Fe element Additive amount be 0.6g;The additive amount of the Mn element is 0.40g;The additive amount of the Cu element is 0.08g;The Zn element Additive amount be 0.01g;The additive amount of the B element is 0.10g.Finally ascorbic acid is added into mixture to be adjusted to its PH 6.3, obtain medicine fertilizer finished product.
Embodiment three
Medicine fertilizer 1L is configured in the present embodiment, the cycles of concentration of the biogas slurry concentrate is 9 times;The addition of the HEEDTA Amount is 2.7g;The additive amount of the powder of amino acids is 115g;The additive amount of the Folium Artemisiae Argyi extract is 0.75g;The Fe member The additive amount of element is 0.8g;The additive amount of the Mn element is 0.30g;The additive amount of the Cu element is 0.06g;The Zn member The additive amount of element is 0.03g;The additive amount of the B element is 0.16g.Ascorbic acid is finally added into mixture by its PH tune To 6.5, medicine fertilizer finished product is obtained.
Technical solution of the present invention is exemplarily described invention above in conjunction with specific embodiment, it is clear that present invention tool Body realization is not subject to the restrictions described above, as long as using the various non-realities that the inventive concept and technical scheme of the present invention carry out Matter improve, or it is not improved the conception and technical scheme of invention are directly applied into other occasions, in guarantor of the invention Within the scope of shield.

Claims (7)

1. a kind of flower planting preparation method of liquid medicine fertilizer, which comprises the following steps:
(1) human or animal's excrement takes fermentation liquid through anaerobic fermentation, is filtered by vacuum to obtain filtrate after precipitating;
(2) 7-10 times is concentrated using reverse osmosis membrane to the filtrate that step (1) obtains, obtains concentrate;
(3) take a certain amount of concentrate, be heated to 30-40 DEG C, ethoxy is added and replaces ethylenediamine triacetic acid, stirring to being completely dissolved, It adds microelement and stirs to dissolution and obtain solution A;
(4) a certain amount of concentrate is taken, powder of amino acids is added, stirring obtains solution B to dissolving;
(5) solution A and solution B are mixed, then Folium Artemisiae Argyi extract is added thereto;
(6) ascorbic acid is added in the solution obtained to step (5) and adjusts PH to 6.3-6.6, obtain liquid medicine fertilizer;
Wherein, every configuration 1L liquid medicine fertilizer, the ethoxy are 2.70-3.0g for the additive amount of ethylenediamine triacetic acid;The ammonia The additive amount of base acid powder is 115-130g;The additive amount of the Folium Artemisiae Argyi extract is 0.7-1g.
2. a kind of flower planting according to claim 1 preparation method of liquid medicine fertilizer, which is characterized in that every configuration 1L Liquid medicine fertilizer, the ethoxy are 2.8g for the additive amount of ethylenediamine triacetic acid;The additive amount of the powder of amino acids is 120g; The additive amount of the Folium Artemisiae Argyi extract is 0.8g.
3. a kind of flower planting according to claim 1 preparation method of liquid medicine fertilizer, which is characterized in that described micro Element is Fe element, Mn element, Cu element, Zn element and B element.
4. a kind of flower planting according to claim 3 preparation method of liquid medicine fertilizer, which is characterized in that every configuration 1L Liquid medicine fertilizer, the additive amount of the Fe element are 0.6-0.8g;The additive amount of the Mn element is 0.3-0.4g;The Cu element Additive amount be 0.06-0.08g;The additive amount of the Zn element is 0.01-0.03g;The additive amount of the B element is 0.10- 0.16g。
5. a kind of flower planting according to claim 4 preparation method of liquid medicine fertilizer, which is characterized in that every configuration 1L Liquid medicine fertilizer, the additive amount of the Fe element are 0.7g;The additive amount of the Mn element is 0.35g;The addition of the Cu element Amount is 0.07g;The additive amount of the Zn element is 0.02g;The additive amount of the B element is 0.14g.
6. a kind of flower planting according to claim 1 or 2 preparation method of liquid medicine fertilizer, which is characterized in that described Folium Artemisiae Argyi extract the preparation method comprises the following steps: by folium artemisiae argyi it is broken after extracting solution obtained using water extraction extraction method, then be concentrated, be spray-dried Obtain solid extract.
7. a kind of flower planting according to claim 1 preparation method of liquid medicine fertilizer, which is characterized in that the anaerobism The temperature of fermentation is 20-40 degrees Celsius.
CN201810674653.6A 2018-06-27 2018-06-27 A kind of preparation method of flower planting liquid medicine fertilizer Pending CN108947644A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109627111A (en) * 2019-02-26 2019-04-16 刘立军 A kind of liquid compound organic fertilizer and preparation method thereof

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CN103626575A (en) * 2013-11-06 2014-03-12 湖北中化东方肥料有限公司 Method for preparing high-efficient organic-inorganic compound fertilizer from biogas slurry
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CN107417467A (en) * 2017-08-05 2017-12-01 周维民 A kind of green upgrading water soluble fertilizer and preparation method thereof
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CN103626575A (en) * 2013-11-06 2014-03-12 湖北中化东方肥料有限公司 Method for preparing high-efficient organic-inorganic compound fertilizer from biogas slurry
CN105085082A (en) * 2015-09-17 2015-11-25 郭云征 Organic and inorganic cooperation fertilizer and application thereof
CN105948986A (en) * 2016-05-06 2016-09-21 南宁绿智环保科技有限公司 Amino acid containing liquid fertilizer and preparation method thereof
CN106242820A (en) * 2016-08-23 2016-12-21 铜仁市万山区米贡山高效农业科技有限公司 A kind of Rhizoma Gastrodiae special fertilizer
CN106748268A (en) * 2017-01-22 2017-05-31 陆川县众联种植农民专业合作社 A kind of aniseed fertilizer material
CN106927958A (en) * 2017-04-28 2017-07-07 宁夏农林科学院农业资源与环境研究所 Special amino acid composite liquid fertilizer of calacareous soil and preparation method thereof
CN107417467A (en) * 2017-08-05 2017-12-01 周维民 A kind of green upgrading water soluble fertilizer and preparation method thereof
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Publication number Priority date Publication date Assignee Title
CN109627111A (en) * 2019-02-26 2019-04-16 刘立军 A kind of liquid compound organic fertilizer and preparation method thereof

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