CN108914570A - A kind of cashmere softening agent and preparation method thereof with bacteria resistance function - Google Patents
A kind of cashmere softening agent and preparation method thereof with bacteria resistance function Download PDFInfo
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- CN108914570A CN108914570A CN201810809928.2A CN201810809928A CN108914570A CN 108914570 A CN108914570 A CN 108914570A CN 201810809928 A CN201810809928 A CN 201810809928A CN 108914570 A CN108914570 A CN 108914570A
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- softening agent
- sorbitan fatty
- fatty acid
- bacteria
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/328—Amines the amino group being bound to an acyclic or cycloaliphatic carbon atom
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/05—Cellulose or derivatives thereof
- D06M15/09—Cellulose ethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/285—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acid amides or imides
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/10—Animal fibres
- D06M2101/12—Keratin fibres or silk
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/50—Modified hand or grip properties; Softening compositions
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of cashmere softening agent and preparation method thereof with bacteria resistance function, is made of the raw material of following weight:20-30 parts of double octyl methyl tertiary amines, 12-20 parts of trimethylamine, 2~4 parts of ASAP bacteriostatic agent, 18~24 parts of polyacrylamide amine emulsifier, 15~22 parts of OSP solubilizer, 3-6 parts of sodium carboxymethylcellulose pyce, 8-10 parts of potassium chloride, 1-2 parts of sorbitan fatty acid ester, 0.1~0.5 part of essence, 0.05~0.3 part of citric acid, 3-5 parts of epoxychloropropane, 30~50 parts of ternary polymerization amido silicon oil, 25~45 parts of methyl methacrylate, 2-3 parts of polypropylene glycol, 550 parts of distilled water.Technical solution formula provided by the invention rationally, has good bacteriostasis rate to walsh staphylococcus and Escherichia coli, and can make fabrics feel soft.
Description
Technical field
The invention belongs to the antibacterial finish agent technical fields of textile fabric, and in particular to a kind of mixing anti-bacteria cashmere is soft
Agent and preparation method thereof.
Background technique
In recent years, stepping up due to living standards of the people, the clothing that people couple are closely connected with daily life are wanted
It asks also higher and higher, is embodied in:Clothing just develops towards functionalization aspect.In order to improve the feel and comfort level of clothing,
Hydrophilic amino silicone oil is usually added to the finishing agent for being used as fabric after water emulsification, uses and assigns the better flexibility of fabric, smooth
Property, hydrophily and yellowing resistance.But cashmere finishing agent is not yet seen in report.
Summary of the invention
It is a kind of not only with excellent fungistatic effect task of the invention lies in providing, but also with ideal color inhibition effect
Mix anti-bacteria cashmere softening agent and preparation method thereof.
The task of the present invention is in this way to complete,
A kind of cashmere softening agent with bacteria resistance function, is made of the raw material of following weight:
20-30 parts of double octyl methyl tertiary amines;
Trimethylamine:12-20 parts;
2~4 parts of ASAP bacteriostatic agent;
18~24 parts of polyacrylamide amine emulsifier;
15~22 parts of OSP solubilizer;
3-6 parts of sodium carboxymethylcellulose pyce;
8-10 parts of potassium chloride;
1-2 parts of sorbitan fatty acid ester;
0.1~0.5 part of essence;
0.05~0.3 part of citric acid;
3-5 parts of epoxychloropropane;
30~50 parts of ternary polymerization amido silicon oil;
25~45 parts of methyl methacrylate;
2-3 parts of polypropylene glycol;
550 parts of distilled water.
Preferably, the polyacrylamide amine emulsifier is aliphatic acid polyethenoxy ether, sorbitan fatty acid, nonyl phenol
One of polyoxyethylene ether or combinations thereof.
Further, a kind of preparation method mixing anti-bacteria cashmere softening agent, steps are as follows:By double octyls of formula ratio
Methyl tertiary amine, trimethylamine, sodium carboxymethylcellulose pyce, potassium chloride, sorbitan fatty acid ester, citric acid, epoxychloropropane, ternary
Copolymerization amido silicon oil, methyl methacrylate, polypropylene glycol, distilled water mixing are heated to 90-95 DEG C, stir 1-2 hours, then
ASAP bacteriostatic agent is added, polyacrylamide amine emulsifier, OSP solubilizer, essence mixing, 90-95 DEG C of temperature holding, stirring 1-2 is small
When, it is cooled to room temperature obtained.
Technical solution formula provided by the invention is reasonable, to walsh staphylococcus bacteriostasis rate up to 99% or more, to large intestine bar
The bacteriostasis rate of bacterium can make fabrics feel soft up to 99.2% or more.
Specific embodiment
It is described further With reference to embodiment:
Embodiment
A kind of cashmere softening agent with bacteria resistance function, is made of the raw material of following weight:
20-30 parts of double octyl methyl tertiary amines;
Trimethylamine:12-20 parts;
2~4 parts of ASAP bacteriostatic agent;
18~24 parts of polyacrylamide amine emulsifier;
15~22 parts of OSP solubilizer;
3-6 parts of sodium carboxymethylcellulose pyce;
8-10 parts of potassium chloride;
1-2 parts of sorbitan fatty acid ester;
0.1~0.5 part of essence;
0.05~0.3 part of citric acid;
3-5 parts of epoxychloropropane;
30~50 parts of ternary polymerization amido silicon oil;
25~45 parts of methyl methacrylate;
2-3 parts of polypropylene glycol;
550 parts of distilled water.
Polyacrylamide amine emulsifier is aliphatic acid polyethenoxy ether, sorbitan fatty acid, nonylphenol polyoxyethylene ether
One of or combinations thereof.
The invention also discloses a kind of preparation methods for mixing anti-bacteria cashmere softening agent, and steps are as follows:By the double of formula ratio
Octyl methyl tertiary amine, trimethylamine, sodium carboxymethylcellulose pyce, potassium chloride, sorbitan fatty acid ester, citric acid, epoxy chloropropionate
Alkane, ternary polymerization amido silicon oil, methyl methacrylate, polypropylene glycol, distilled water mixing are heated to 90-95 DEG C, stir 1-2
Hour, add ASAP bacteriostatic agent, polyacrylamide amine emulsifier, OSP solubilizer, essence mixing, temperature keeps for 90-95 DEG C, stirred
It mixes 1-2 hours, is cooled to room temperature obtained.
Technical solution formula provided by the invention is reasonable, to walsh staphylococcus bacteriostasis rate up to 99% or more, to large intestine bar
The bacteriostasis rate of bacterium can make fabrics feel soft up to 99.2% or more.
Obtained fabric had both had good hand after being handled using mixing anti-bacteria cashmere softening agent of the invention
Sense and yellowing resistance, and there is good fungistatic effect, preferably realize the purpose of the present invention.
Claims (3)
1. a kind of cashmere softening agent with bacteria resistance function, it is characterised in that:It is to be made of the raw material of following weight:
20-30 parts of double octyl methyl tertiary amines;
Trimethylamine:12-20 parts;
2~4 parts of ASAP bacteriostatic agent;
18~24 parts of polyacrylamide amine emulsifier;
15~22 parts of OSP solubilizer;
3-6 parts of sodium carboxymethylcellulose pyce;
8-10 parts of potassium chloride;
1-2 parts of sorbitan fatty acid ester;
0.1~0.5 part of essence;
0.05~0.3 part of citric acid;
3-5 parts of epoxychloropropane;
30~50 parts of ternary polymerization amido silicon oil;
25~45 parts of methyl methacrylate;
2-3 parts of polypropylene glycol;
550 parts of distilled water.
2. a kind of mixing anti-bacteria cashmere softening agent according to claim 1, it is characterised in that:The polyacrylamide cream
Agent is one of aliphatic acid polyethenoxy ether, sorbitan fatty acid, nonylphenol polyoxyethylene ether or combinations thereof.
3. a kind of preparation method for mixing anti-bacteria cashmere softening agent according to claim 1, it is characterised in that:Step is such as
Under:By double octyl methyl tertiary amines of formula ratio, trimethylamine, sodium carboxymethylcellulose pyce, potassium chloride, sorbitan fatty acid ester,
Citric acid, epoxychloropropane, ternary polymerization amido silicon oil, methyl methacrylate, polypropylene glycol, distilled water mixing are heated to
It 90-95 DEG C, stirs 1-2 hours, adds ASAP bacteriostatic agent, polyacrylamide amine emulsifier, OSP solubilizer, essence mixing, temperature
It is kept for 90-95 DEG C, stirs 1-2 hours, be cooled to room temperature obtained.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201810809928.2A CN108914570A (en) | 2018-07-23 | 2018-07-23 | A kind of cashmere softening agent and preparation method thereof with bacteria resistance function |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201810809928.2A CN108914570A (en) | 2018-07-23 | 2018-07-23 | A kind of cashmere softening agent and preparation method thereof with bacteria resistance function |
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Publication Number | Publication Date |
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CN108914570A true CN108914570A (en) | 2018-11-30 |
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CN201810809928.2A Withdrawn CN108914570A (en) | 2018-07-23 | 2018-07-23 | A kind of cashmere softening agent and preparation method thereof with bacteria resistance function |
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Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102877293A (en) * | 2011-07-11 | 2013-01-16 | 李晓梅 | Softener suitable for plurality of fabrics |
CN103061147A (en) * | 2011-10-21 | 2013-04-24 | 江苏白玉兰纺织印染有限公司 | Composite antibacterial softening agent |
CN103614908A (en) * | 2013-12-02 | 2014-03-05 | 湖州金塔地纺织厂 | Fabric softener |
CN103696270A (en) * | 2013-12-18 | 2014-04-02 | 江苏波波熊纺织品有限公司 | Mixed anti-bacteria cashmere softening agent |
CN104372618A (en) * | 2013-08-13 | 2015-02-25 | 杨林贵 | Wrinkle-resistant textile softening agent |
CN105671224A (en) * | 2016-03-04 | 2016-06-15 | 季资朝 | Leather softening agent and preparing method thereof |
-
2018
- 2018-07-23 CN CN201810809928.2A patent/CN108914570A/en not_active Withdrawn
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102877293A (en) * | 2011-07-11 | 2013-01-16 | 李晓梅 | Softener suitable for plurality of fabrics |
CN103061147A (en) * | 2011-10-21 | 2013-04-24 | 江苏白玉兰纺织印染有限公司 | Composite antibacterial softening agent |
CN104372618A (en) * | 2013-08-13 | 2015-02-25 | 杨林贵 | Wrinkle-resistant textile softening agent |
CN103614908A (en) * | 2013-12-02 | 2014-03-05 | 湖州金塔地纺织厂 | Fabric softener |
CN103696270A (en) * | 2013-12-18 | 2014-04-02 | 江苏波波熊纺织品有限公司 | Mixed anti-bacteria cashmere softening agent |
CN105671224A (en) * | 2016-03-04 | 2016-06-15 | 季资朝 | Leather softening agent and preparing method thereof |
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Application publication date: 20181130 |
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WW01 | Invention patent application withdrawn after publication |