CN108913374A - A kind of detergent and preparation method thereof containing flat leaf thorn celery extract - Google Patents
A kind of detergent and preparation method thereof containing flat leaf thorn celery extract Download PDFInfo
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- CN108913374A CN108913374A CN201810758516.0A CN201810758516A CN108913374A CN 108913374 A CN108913374 A CN 108913374A CN 201810758516 A CN201810758516 A CN 201810758516A CN 108913374 A CN108913374 A CN 108913374A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/37—Mixtures of compounds all of which are anionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/14—Fillers; Abrasives ; Abrasive compositions; Suspending or absorbing agents not provided for in one single group of C11D3/12; Specific features concerning abrasives, e.g. granulometry or mixtures
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2082—Polycarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/37—Polymers
- C11D3/3746—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C11D3/3769—(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
- C11D3/3776—Heterocyclic compounds, e.g. lactam
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/382—Vegetable products, e.g. soya meal, wood flour, sawdust
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38618—Protease or amylase in liquid compositions only
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/386—Preparations containing enzymes, e.g. protease or amylase
- C11D3/38645—Preparations containing enzymes, e.g. protease or amylase containing cellulase
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3942—Inorganic per-compounds
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/39—Organic or inorganic per-compounds
- C11D3/3947—Liquid compositions
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
- C11D1/146—Sulfuric acid esters
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/30—Sulfonation products derived from lignin
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Abstract
The invention discloses a kind of detergent and preparation method thereof containing flat leaf thorn celery extract, the raw material of detergent of the preparation containing flat leaf thorn celery extract includes：Lignosulfonates, sldium lauryl sulfate, flat leaf thorn celery extract, lemon juice, PERFORMANCE OF MODIFIED VERMICULITE, protease, cellulase, sodium thiosulfate, succinic acid, sodium chloride, sodium cellulose glycolate, olive oil, essence, polyvinylpyrrolidone, bamboo charcoal powder, water.Detergent containing flat leaf thorn celery extract of the invention, expands the floristics of plant type detergent, and disclose preparation method, expands its occupation rate of market and the market influence.
Description
Technical field
The present invention relates to the technical fields of detergent composition, and in particular to a kind of cleaning containing flat leaf thorn celery extract
Agent and preparation method thereof.
Background technique
With advances in technology, the enhancing of environmental consciousness, requirement of the people for detergent product also from require cleaning imitate
Fruit, which rises to well, requires its environment-friendly high-efficiency.Major part detergent product is strong to the irritation of skin at present, can be to being washed when use
It washs article and brings chemical residual, and pollute the environment, cause the murder by poisoning to human body and environment.Therefore, exploitation environmental protection, it is mild,
Safe and effective detergent product be very it is necessary to.
Chinese Plants are resourceful, using the plant containing saponin prepare detergent can reach clean purpose and
Achieve the purpose that environmental protection, is a kind of effective method.Currently, existing plant type detergent mainly with soapberry, Chinese honey locust,
Tea seed etc. is used as raw material, and Exploitation degree is effective, needs to develop using other kind plants as the cleaning article of raw material, to increase
The kind of plant type detergent expands its occupation rate of market and the market influence.
Chinese patent CN201110342888.3 discloses detergent and its manufacture of a kind of fruit containing soapberry or pulp
The detergent of method, fruit containing soapberry or pulp includes detergent and soapberry fruit or pulp by purification, after purification
Soapberry fruit or pulp：The weight ratio of soapberry fruit or pulp after detergent and purification is 0.5/30~3/30, essence
Soapberry fruit or pulp after system refer to, and first soapberry fruit is dried, then by soapberry fruit or removes kernel
Soapberry pulp, cleaned with ethanol solution or aqueous isopropanol, or taken out after immersing ethanol solution or aqueous isopropanol, and make
It is dried.
Chinese patent CN201110453827.4 discloses a kind of pure plant type antibacterial cleanser and preparation method thereof, this is clear
In clean dose of raw material containing Chinese medicinal plant preparation, alkyl glycosides, cocoyl amphoteric surfactant, polyalcohol, acidity regulator,
Food flavor, deionized water.In the raw material of Chinese medicinal plant preparation containing climbing groundsel, flaccid knotweed herb, smilax, Common Leafflower Herb, Chinese wingnut leaf,
Frutus cnidii, kuh-seng.
Therefore, it is necessary in view of the above-mentioned problems, expand the floristics of plant type detergent, and open preparation method, with
Expand its occupation rate of market and the market influence.
Summary of the invention
The present invention is in view of the above-mentioned problems, provide a kind of detergent and preparation method thereof containing flat leaf thorn celery extract.
The present invention solve the above problems used by technical solution be：A kind of detergent containing flat leaf thorn celery extract,
Preparation containing flat leaf thorn celery extract detergent raw material and its parts by weight include：Lignosulfonates 10%~14%, the moon
Lauryl sulfate 8%~12%, flat leaf thorn celery extract 15%~20%, lemon juice 0.5%~1%, PERFORMANCE OF MODIFIED VERMICULITE 2%~
5%, protease 2%~3%, cellulase 1%~5%, sodium thiosulfate 0.2%~0.6%, succinic acid 0.2%~
0.4%, sodium chloride 0.1%~0.2%, sodium cellulose glycolate 0.5%~1%, olive oil 2.5%~4%, essence 0.5%
~1.5%, polyvinylpyrrolidone 0.5%~1%, bamboo charcoal powder 2%~4%, water complement to 100%.
Further, the raw material of detergent of the preparation containing flat leaf thorn celery extract and its parts by weight include：Sulfomethylated lignin
Hydrochlorate 12%~13%, sldium lauryl sulfate 9%~11%, flat leaf thorn celery extract 16%~18%, lemon juice 0.6%~
0.8%, PERFORMANCE OF MODIFIED VERMICULITE 3%~4%, protease 2.2%~2.8%, cellulase 2%~4%, sodium thiosulfate 0.3%~
0.5%, succinic acid 0.25%~0.35%, sodium chloride 0.12%~0.18%, sodium cellulose glycolate 0.6%~0.8%, olive
Olive oil 3%~3.5%, essence 1%~1.2%, polyvinylpyrrolidone 0.6%~0.8%, bamboo charcoal powder 2.5%~3.5%,
Water complements to 100%.
Further, the raw material of detergent of the preparation containing flat leaf thorn celery extract and its parts by weight include：Sulfomethylated lignin
Hydrochlorate 12.5%, sldium lauryl sulfate 10%, flat leaf thorn celery extract 17%, lemon juice 0.7%, PERFORMANCE OF MODIFIED VERMICULITE 3.5%, albumen
Enzyme 2.5%, cellulase 3%, sodium thiosulfate 0.4%, succinic acid 0.3%, sodium chloride 0.15%, sodium cellulose glycolate
0.7%, olive oil 3.2%, essence 1.1%, polyvinylpyrrolidone 0.7%, bamboo charcoal powder 3%, water complement to 100%.
Further, the extracting method of flat leaf thorn celery extract, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：
100 weight ratio adds water, ultrasound 15min~30min under the conditions of 40 DEG C~45 DEG C of temperature, then at 95 DEG C~105 DEG C
Water bath condition under extract 2h, taking-up is filtered, and filter cake I and filtrate I are obtained；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, in 40 DEG C~45 DEG C of temperature strip
Ultrasound 10min~20min under part, then extracts 1.5h under 95 DEG C~105 DEG C of water bath condition, and taking-up is filtered, obtained
Filter cake II and filtrate II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, in 40 DEG C~45 DEG C of temperature strip
Then ultrasound 5min~15min under part extracts 1h under 95 DEG C~105 DEG C of water bath condition, taking-up is filtered, and obtains filter cake
III and filtrate II I, merging filtrate I, filtrate II, filtrate II I, obtains merging filtrate；
Step S4, merging filtrate that step S3 is obtained is evaporated under reduced pressure be condensed into viscosity be 1500mPas~
The viscous body of 1800mPas；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, extracts 2h~4h, warp
Filtrate IV is obtained after suction filtration, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract.
Further, in step S4, operating temperature when reduction vaporization is 80 DEG C~85 DEG C.
Further, in step S5, the mass fraction of ethanol solution is 85%~95%.
Further, in step S5, operating temperature when reduction vaporization is 80 DEG C~85 DEG C
Further, the preparation method of PERFORMANCE OF MODIFIED VERMICULITE is：Vermiculite is crushed, 80 meshes is crossed, is transferred in the concentrated sulfuric acid and soaks
Bubble 4h~6h is transferred in Muffle furnace after gains are washed, dried, and is heat-treated under the conditions of 300 DEG C~350 DEG C of temperature
1h~1.5h, ground 200 mesh of mistake of products therefrom, obtains the PERFORMANCE OF MODIFIED VERMICULITE.
Another goal of the invention of the invention is to provide a kind of preparation of above-mentioned detergent containing flat leaf thorn celery extract
Method includes the following steps：
The flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil are added step A1
It is 35 DEG C~45 DEG C in temperature, under conditions of revolving speed is 400r/min~600r/min in the water of 50% mass percent
2h~4h is stirred, mixture I is obtained；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, fiber
The mixing that step A1 is obtained is added in plain enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 35 DEG C~45 DEG C in temperature in object I, revolving speed stirs 1h~3h under conditions of being 500r/min~700r/min, is mixed
Object II；
Step A3 the bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, and adds another
The water of 50% mass percent is 30 DEG C~40 DEG C in temperature, and revolving speed stirs under conditions of being 600r/min~800r/min
1h~2h is mixed, the detergent for containing flat leaf thorn celery extract is obtained.
Further, in step A3, the use temperature of the detergent containing flat leaf thorn celery extract is 25 DEG C~35 DEG C.
It is an advantage of the invention that：
1. detergent prepared by the present invention uses flat leaf thorn celery extract for raw material, green, environmental protection, there is good biology drop
Xie Xing, and add lignosulfonates, sldium lauryl sulfate, lemon juice, PERFORMANCE OF MODIFIED VERMICULITE, protease, cellulase, thiosulfuric acid
Sodium, succinic acid, sodium chloride, sodium cellulose glycolate, olive oil, essence, polyvinylpyrrolidone, bamboo charcoal powder, water are raw material,
Wash quick and easy, clean effect is significant, and mild to skin, is not easy to hurt hand；
2. the preparation method of the flat leaf thorn celery extract of the present invention is simple, convenient, efficient, its effective component can be sufficiently extracted,
Be conducive to expand its market competitiveness；
3. detergent prepared by the present invention uses PERFORMANCE OF MODIFIED VERMICULITE for one of raw material, by vermiculite it is engineered after, be conducive to improve
The surface-active and porosity of vermiculite improve the synergistic effect of vermiculite and surfactant, improve detergent cleaning effect；
4. the preparation method of detergent of the present invention preparation containing flat leaf thorn celery extract is simple, efficient, it is easy to scale
Mass production.
Specific embodiment
The embodiment of the present invention is described in detail below, but what the present invention can be defined by the claims and cover
Multitude of different ways is implemented.
Embodiment 1
A kind of detergent containing flat leaf thorn celery extract, preparation containing flat leaf thorn celery extract detergent raw material and
Its parts by weight includes：Lignosulfonates 10%, sldium lauryl sulfate 8%, flat leaf thorn celery extract 15%, lemon juice 0.5%,
PERFORMANCE OF MODIFIED VERMICULITE 2%, protease 2%, cellulase 1%, sodium thiosulfate 0.2%, succinic acid 0.2%, sodium chloride 0.1%, hydroxyl
Sodium carboxymethylcellulose pyce 0.5%, olive oil 2.5%, essence 0.5%, polyvinylpyrrolidone 0.5%, bamboo charcoal powder 2%, water are supplied
To 100%.
Wherein, the extracting method of flat leaf thorn celery extract, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：
100 weight ratio adds water, and ultrasound 15min, then extracts 2h under 95 DEG C of water bath condition, take under the conditions of 40 DEG C of temperature
It is filtered out, obtains filter cake I and filtrate I；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, surpasses under the conditions of 40 DEG C of temperature
Then sound 10min extracts 1.5h under 95 DEG C of water bath condition, taking-up is filtered, and obtains filter cake II and filtrate II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, surpasses under the conditions of 40 DEG C of temperature
Then sound 5min extracts 1h under 95 DEG C of water bath condition, taking-up is filtered, and filter cake III and filtrate II I are obtained, and merges filter
Liquid I, filtrate II, filtrate II I, obtain merging filtrate；
The merging filtrate that step S3 is obtained is evaporated under reduced pressure and is condensed into viscosity as the sticky of 1500mPas by step S4
Body；Wherein, operating temperature when reduction vaporization is 80 DEG C；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, 2h is extracted, through filtering
After obtain filtrate IV, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract；Wherein, ethanol solution
Mass fraction is 85%；Operating temperature when reduction vaporization is 80 DEG C；
Wherein, the preparation method of PERFORMANCE OF MODIFIED VERMICULITE is：Vermiculite is crushed, 80 meshes is crossed, is transferred in the concentrated sulfuric acid and impregnates 4h, institute
After object washed, dried, be transferred in Muffle furnace, 1h, products therefrom ground mistake be heat-treated under the conditions of 300 DEG C of temperature
200 meshes obtain the PERFORMANCE OF MODIFIED VERMICULITE.
The preparation method of the above-mentioned detergent containing flat leaf thorn celery extract, includes the following steps：
The flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil are added step A1
It is 35 DEG C in temperature in the water of 50% mass percent, revolving speed stirs 2h under conditions of being 400r/min, obtains mixture
I；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, fiber
The mixing that step A1 is obtained is added in plain enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 35 DEG C in temperature in object I, revolving speed stirs 1h under conditions of being 500r/min, obtains mixtures II；
Step A3 the bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, and adds another
The water of 50% mass percent is 30 DEG C in temperature, and revolving speed stirs 1h under conditions of being 600r/min, obtains described contain
The detergent of flat leaf thorn celery extract；Wherein, the use temperature of the detergent containing flat leaf thorn celery extract is 25 DEG C.
Embodiment 2
A kind of detergent containing flat leaf thorn celery extract, preparation containing flat leaf thorn celery extract detergent raw material and
Its parts by weight includes：Lignosulfonates 14%, sldium lauryl sulfate 12%, flat leaf thorn celery extract 20%, lemon juice 1%,
PERFORMANCE OF MODIFIED VERMICULITE 5%, protease 3 %, cellulase 5%, sodium thiosulfate 0.6%, succinic acid 0.4%, sodium chloride 0.2%, hydroxyl
Sodium carboxymethylcellulose pyce 1%, olive oil 4%, essence 1.5%, polyvinylpyrrolidone 1%, bamboo charcoal powder 4%, water complement to
100%.
Wherein, the extracting method of flat leaf thorn celery extract, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：
100 weight ratio adds water, and ultrasound 30min, then extracts 2h under 105 DEG C of water bath condition under the conditions of 45 DEG C of temperature,
Taking-up is filtered, and filter cake I and filtrate I are obtained；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, surpasses under the conditions of 45 DEG C of temperature
Then sound 20min extracts 1.5h under 105 DEG C of water bath condition, taking-up is filtered, and obtains filter cake II and filtrate II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, surpasses under the conditions of 45 DEG C of temperature
Then sound 15min extracts 1h under 105 DEG C of water bath condition, taking-up is filtered, and filter cake III and filtrate II I are obtained, and merges
Filtrate I, filtrate II, filtrate II I, obtain merging filtrate；
The merging filtrate that step S3 is obtained is evaporated under reduced pressure and is condensed into viscosity as the sticky of 1800mPas by step S4
Body；Wherein, operating temperature when reduction vaporization is 85 DEG C；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, 4h is extracted, through filtering
After obtain filtrate IV, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract；Wherein, ethanol solution
Mass fraction is 95%；Operating temperature when reduction vaporization is 85 DEG C；
Wherein, the preparation method of PERFORMANCE OF MODIFIED VERMICULITE is：Vermiculite is crushed, 80 meshes is crossed, is transferred in the concentrated sulfuric acid and impregnates 6h, institute
After object washed, dried, be transferred in Muffle furnace, be heat-treated 1.5h under the conditions of 350 DEG C of temperature, products therefrom is ground
200 meshes are crossed, the PERFORMANCE OF MODIFIED VERMICULITE is obtained.
The preparation method of the above-mentioned detergent containing flat leaf thorn celery extract, includes the following steps：
The flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil are added step A1
It is 45 DEG C in temperature in the water of 50% mass percent, revolving speed stirs 4h under conditions of being 600r/min, obtains mixture
I；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, fiber
The mixing that step A1 is obtained is added in plain enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 45 DEG C in temperature in object I, revolving speed stirs 3h under conditions of being 700r/min, obtains mixtures II；
Step A3 the bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, and adds another
The water of 50% mass percent is 40 DEG C in temperature, and revolving speed stirs 2h under conditions of being 800r/min, obtains described contain
The detergent of flat leaf thorn celery extract；Wherein, the use temperature of the detergent containing flat leaf thorn celery extract is 35 DEG C.
Embodiment 3
A kind of detergent containing flat leaf thorn celery extract, preparation containing flat leaf thorn celery extract detergent raw material and
Its parts by weight includes：Lignosulfonates 12%, sldium lauryl sulfate 9%, flat leaf thorn celery extract 16%, lemon juice 0.6%,
PERFORMANCE OF MODIFIED VERMICULITE 3%, protease 2.2%, cellulase 2%, sodium thiosulfate 0.3%, succinic acid 0.25%, sodium chloride
0.12%, sodium cellulose glycolate 0.6%, olive oil 3%, essence 1%, polyvinylpyrrolidone 0.6%, bamboo charcoal powder 2.5%,
Water complements to 100%.
Wherein, the extracting method of flat leaf thorn celery extract, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：
100 weight ratio adds water, and ultrasound 22min, then extracts 2h under 100 DEG C of water bath condition under the conditions of 43 DEG C of temperature,
Taking-up is filtered, and filter cake I and filtrate I are obtained；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, surpasses under the conditions of 43 DEG C of temperature
Then sound 15min extracts 1.5h under 100 DEG C of water bath condition, taking-up is filtered, and obtains filter cake II and filtrate II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, surpasses under the conditions of 43 DEG C of temperature
Then sound 10min extracts 1h under 100 DEG C of water bath condition, taking-up is filtered, and filter cake III and filtrate II I are obtained, and merges
Filtrate I, filtrate II, filtrate II I, obtain merging filtrate；
The merging filtrate that step S3 is obtained is evaporated under reduced pressure and is condensed into viscosity as the sticky of 1650mPas by step S4
Body；Wherein, operating temperature when reduction vaporization is 83 DEG C；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, 3h is extracted, through filtering
After obtain filtrate IV, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract；Wherein, ethanol solution
Mass fraction is 90%；Operating temperature when reduction vaporization is 83 DEG C；
Wherein, the preparation method of PERFORMANCE OF MODIFIED VERMICULITE is：Vermiculite is crushed, 80 meshes is crossed, is transferred in the concentrated sulfuric acid and impregnates 5h, institute
After object washed, dried, be transferred in Muffle furnace, be heat-treated 1.2h under the conditions of 325 DEG C of temperature, products therefrom is ground
200 meshes are crossed, the PERFORMANCE OF MODIFIED VERMICULITE is obtained.
The preparation method of the above-mentioned detergent containing flat leaf thorn celery extract, includes the following steps：
The flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil are added step A1
It is 40 DEG C in temperature in the water of 50% mass percent, revolving speed stirs 3h under conditions of being 500r/min, obtains mixture
I；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, fiber
The mixing that step A1 is obtained is added in plain enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 40 DEG C in temperature in object I, revolving speed stirs 2h under conditions of being 600r/min, obtains mixtures II；
Step A3 the bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, and adds another
The water of 50% mass percent is 35 DEG C in temperature, and revolving speed stirs 1.5h under conditions of being 700r/min, obtains described contain
There is the detergent of flat leaf thorn celery extract；Wherein, the use temperature of the detergent containing flat leaf thorn celery extract is 30 DEG C.
Embodiment 4
A kind of detergent containing flat leaf thorn celery extract, preparation containing flat leaf thorn celery extract detergent raw material and
Its parts by weight includes：Lignosulfonates 13%, sldium lauryl sulfate 11%, flat leaf thorn celery extract 18%, lemon juice
0.8%, PERFORMANCE OF MODIFIED VERMICULITE 4%, protease 2.8%, cellulase 4%, sodium thiosulfate 0.5%, succinic acid 0.35%, sodium chloride
0.18%, sodium cellulose glycolate 0.8%, olive oil 3.5%, essence 1.2%, polyvinylpyrrolidone 0.8%, bamboo charcoal powder
3.5%, water complements to 100%.
Wherein, the extracting method of flat leaf thorn celery extract, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：
100 weight ratio adds water, and ultrasound 18min, then extracts 2h under 98 DEG C of water bath condition, take under the conditions of 41 DEG C of temperature
It is filtered out, obtains filter cake I and filtrate I；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, surpasses under the conditions of 41 DEG C of temperature
Then sound 12min extracts 1.5h under 95 DEG C~105 DEG C of water bath condition, taking-up is filtered, and obtains filter cake II and filtrate
II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, surpasses under the conditions of 41 DEG C of temperature
Then sound 6min extracts 1h under 98 DEG C of water bath condition, taking-up is filtered, and filter cake III and filtrate II I are obtained, and merges filter
Liquid I, filtrate II, filtrate II I, obtain merging filtrate；
The merging filtrate that step S3 is obtained is evaporated under reduced pressure and is condensed into viscosity as the sticky of 1600mPas by step S4
Body；Wherein, operating temperature when reduction vaporization is 81 DEG C；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, 2.5h is extracted, through taking out
Filtrate IV is obtained after filter, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract；Wherein, ethanol solution
Mass fraction be 88%；Operating temperature when reduction vaporization is 81 DEG C；
Wherein, the preparation method of PERFORMANCE OF MODIFIED VERMICULITE is：Vermiculite is crushed, 80 meshes is crossed, is transferred in the concentrated sulfuric acid and impregnates 4.5h,
It after gains are washed, dried, is transferred in Muffle furnace, is heat-treated 1.2h under the conditions of 310 DEG C of temperature, products therefrom is through grinding
Honed 200 mesh, obtains the PERFORMANCE OF MODIFIED VERMICULITE.
The preparation method of the above-mentioned detergent containing flat leaf thorn celery extract, includes the following steps：
The flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil are added step A1
It is 36 DEG C in temperature in the water of 50% mass percent, revolving speed stirs 2.5h under conditions of being 420r/min, is mixed
Object I；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, fiber
The mixing that step A1 is obtained is added in plain enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 36 DEG C in temperature in object I, revolving speed stirs 1.5h under conditions of being 550r/min, obtains mixtures II；
Step A3 the bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, and adds another
The water of 50% mass percent is 31 DEG C in temperature, and revolving speed stirs 1.2h under conditions of being 650r/min, obtains described contain
There is the detergent of flat leaf thorn celery extract；Wherein, the use temperature of the detergent containing flat leaf thorn celery extract is 28 DEG C.
Embodiment 5
A kind of detergent containing flat leaf thorn celery extract, preparation containing flat leaf thorn celery extract detergent raw material and
Its parts by weight includes：Lignosulfonates 12.5%, sldium lauryl sulfate 10%, flat leaf thorn celery extract 17%, lemon juice
0.7%, PERFORMANCE OF MODIFIED VERMICULITE 3.5%, protease 2.5%, cellulase 3%, sodium thiosulfate 0.4%, succinic acid 0.3%, chlorination
Sodium 0.15%, sodium cellulose glycolate 0.7%, olive oil 3.2%, essence 1.1%, polyvinylpyrrolidone 0.7%, bamboo charcoal powder
3%, water complements to 100%.
Wherein, the extracting method of flat leaf thorn celery extract, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：
100 weight ratio adds water, and ultrasound 28min, then extracts 2h under 104 DEG C of water bath condition under the conditions of 44 DEG C of temperature,
Taking-up is filtered, and filter cake I and filtrate I are obtained；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, surpasses under the conditions of 43 DEG C of temperature
Then sound 16min extracts 1.5h under 102 DEG C of water bath condition, taking-up is filtered, and obtains filter cake II and filtrate II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, surpasses under the conditions of 42 DEG C of temperature
Then sound 8min extracts 1h under 99 DEG C of water bath condition, taking-up is filtered, and filter cake III and filtrate II I are obtained, and merges filter
Liquid I, filtrate II, filtrate II I, obtain merging filtrate；
The merging filtrate that step S3 is obtained is evaporated under reduced pressure and is condensed into viscosity as the sticky of 1700mPas by step S4
Body；Wherein, operating temperature when reduction vaporization is 84 DEG C；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, 3.5h is extracted, through taking out
Filtrate IV is obtained after filter, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract；Wherein, ethanol solution
Mass fraction be 94%；Operating temperature when reduction vaporization is 84 DEG C；
Wherein, the preparation method of PERFORMANCE OF MODIFIED VERMICULITE is：Vermiculite is crushed, 80 meshes is crossed, is transferred in the concentrated sulfuric acid and impregnates 5.5h,
It after gains are washed, dried, is transferred in Muffle furnace, is heat-treated 1.4h under the conditions of 340 DEG C of temperature, products therefrom is through grinding
Honed 200 mesh, obtains the PERFORMANCE OF MODIFIED VERMICULITE.
The preparation method of the above-mentioned detergent containing flat leaf thorn celery extract, includes the following steps：
The flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil are added step A1
It is 42 DEG C in temperature in the water of 50% mass percent, revolving speed stirs 3.5h under conditions of being 550r/min, is mixed
Object I；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, fiber
The mixing that step A1 is obtained is added in plain enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 44 DEG C in temperature in object I, revolving speed stirs 2.5h under conditions of being 660r/min, obtains mixtures II；
Step A3 the bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, and adds another
The water of 50% mass percent is 38 DEG C in temperature, and revolving speed stirs 1.6h under conditions of being 750r/min, obtains described contain
There is the detergent of flat leaf thorn celery extract；Wherein, the use temperature of the detergent containing flat leaf thorn celery extract is 32 DEG C.
Experimental example 1
Cleaning effect according to GB9985-2000 to the detergent for containing flat leaf thorn celery extract made from Examples 1 to 5
It is tested, test result is as shown in table 1.
The cleaning effect test result of 1 Examples 1 to 5 of the table detergent obtained containing flat leaf thorn celery extract
These are only the preferred embodiment of the present invention, is not intended to restrict the invention, for those skilled in the art
For member, the invention may be variously modified and varied.All within the spirits and principles of the present invention, it is made it is any modification,
Equivalent replacement, improvement etc., should all be included in the protection scope of the present invention.
Claims (10)
1. a kind of detergent containing flat leaf thorn celery extract, which is characterized in that containing flat leaf thorn celery extract described in preparation
The raw material and its parts by weight of detergent include：Lignosulfonates 10%~14%, sldium lauryl sulfate 8%~12%, flat leaf
Eryngo extract 15%~20%, lemon juice 0.5%~1%, PERFORMANCE OF MODIFIED VERMICULITE 2%~5%, protease 2%~3%, cellulose
Enzyme 1%~5%, sodium thiosulfate 0.2%~0.6%, succinic acid 0.2%~0.4%, sodium chloride 0.1%~0.2%, hydroxyl first
Base sodium cellulosate 0.5%~1%, olive oil 2.5%~4%, essence 0.5%~1.5%, polyvinylpyrrolidone 0.5%~
1%, bamboo charcoal powder 2%~4%, water complement to 100%.
2. the detergent according to claim 1 containing flat leaf thorn celery extract, which is characterized in that preparation is described containing flat
The raw material and its parts by weight of the detergent of leaf thorn celery extract include：Lignosulfonates 12%~13%, sldium lauryl sulfate
9%~11%, flat leaf thorn celery extract 16%~18%, lemon juice 0.6%~0.8%, PERFORMANCE OF MODIFIED VERMICULITE 3%~4%, protease
2.2%~2.8%, cellulase 2%~4%, sodium thiosulfate 0.3%~0.5%, succinic acid 0.25%~0.35%, chlorine
Change sodium 0.12%~0.18%, sodium cellulose glycolate 0.6%~0.8%, olive oil 3%~3.5%, essence 1%~
1.2%, polyvinylpyrrolidone 0.6%~0.8%, bamboo charcoal powder 2.5%~3.5%, water complement to 100%.
3. the detergent according to claim 1 containing flat leaf thorn celery extract, which is characterized in that preparation is described containing flat
The raw material and its parts by weight of the detergent of leaf thorn celery extract include：Lignosulfonates 12.5%, sldium lauryl sulfate 10%,
Flat leaf thorn celery extract 17%, lemon juice 0.7%, PERFORMANCE OF MODIFIED VERMICULITE 3.5%, protease 2.5%, cellulase 3%, thiosulfuric acid
Sodium 0.4%, sodium chloride 0.15%, sodium cellulose glycolate 0.7%, olive oil 3.2%, essence 1.1%, gathers succinic acid 0.3%
Vinylpyrrolidone 0.7%, bamboo charcoal powder 3%, water complement to 100%.
4. the detergent according to claim 1 containing flat leaf thorn celery extract, which is characterized in that the flat leaf thorn celery mentions
The extracting method for taking object, includes the following steps：
Flat leaf thorn celery is cleaned, is dry, crushed, crossing 200 meshes, the flat leaf thorn celery of crushing is then pressed 50 by step S1：100
Weight ratio adds water, ultrasound 15min~30min under the conditions of 40 DEG C~45 DEG C of temperature, then in 95 DEG C~105 DEG C of water-bath
Under the conditions of extract 2h, taking-up is filtered, and filter cake I and filtrate I are obtained；
Step S2, the filter cake I that step S1 is obtained is by 50：90 weight ratio adds water, under the conditions of 40 DEG C~45 DEG C of temperature
Then ultrasonic 10min~20min extracts 1.5h under 95 DEG C~105 DEG C of water bath condition, taking-up is filtered, and obtains filter cake
II and filtrate II；
Step S3, the filter cake II that step S2 is obtained is by 50：80 weight ratio adds water, under the conditions of 40 DEG C~45 DEG C of temperature
Then ultrasonic 5min~15min extracts 1h under 95 DEG C~105 DEG C of water bath condition, taking-up is filtered, and obtains filter cake III
Merging filtrate is obtained with filtrate II I, merging filtrate I, filtrate II, filtrate II I；
The merging filtrate that step S3 is obtained is evaporated under reduced pressure and is condensed into viscosity as 1500mPas~1800mPas by step S4
Viscous body；
Step S5, the viscous body that step S4 is obtained is by 60：100 weight ratio adds ethanol solution, 2h~4h is extracted, through filtering
After obtain filtrate IV, by filtrate IV through be evaporated under reduced pressure products therefrom be the flat leaf thorn celery extract.
5. the detergent according to claim 4 containing flat leaf thorn celery extract, which is characterized in that described in step S4
Operating temperature when reduction vaporization is 80 DEG C~85 DEG C.
6. the detergent according to claim 4 containing flat leaf thorn celery extract, which is characterized in that described in step S5
The mass fraction of ethanol solution is 85%~95%.
7. the detergent according to claim 4 containing flat leaf thorn celery extract, which is characterized in that described in step S5
Operating temperature when reduction vaporization is 80 DEG C~85 DEG C.
8. the detergent according to claim 1 containing flat leaf thorn celery extract, which is characterized in that the PERFORMANCE OF MODIFIED VERMICULITE
Preparation method is：Vermiculite is crushed, 80 meshes are crossed, is transferred to immersion 4h~6h in the concentrated sulfuric acid, after gains are washed, are dried,
It is transferred in Muffle furnace, 1h~1.5h, products therefrom ground 200 mesh of mistake is heat-treated under the conditions of 300 DEG C~350 DEG C of temperature
Sieve, obtains the PERFORMANCE OF MODIFIED VERMICULITE.
9. it is a kind of according to claim 1~any one of 8 described in the detergent containing flat leaf thorn celery extract preparation method,
It is characterized by comprising the following steps：
50% institute is added in the flat leaf thorn celery extract of the mass percent, PERFORMANCE OF MODIFIED VERMICULITE, sodium chloride, olive oil by step A1
It states in the water of mass percent, is 35 DEG C~45 DEG C in temperature, revolving speed stirs 2h under conditions of being 400r/min~600r/min
~4h obtains mixture I；
Step A2, by the lignosulfonates of the mass percent, sldium lauryl sulfate, lemon juice, protease, cellulose
The mixture that step A1 is obtained is added in enzyme, sodium thiosulfate, succinic acid, sodium cellulose glycolate, essence, polyvinylpyrrolidone
It is 35 DEG C~45 DEG C in temperature in I, revolving speed stirs 1h~3h under conditions of being 500r/min~700r/min, obtains mixture
II；
The bamboo charcoal powder of the mass percent is added in the mixtures II that step A2 is obtained, adds another 50% institute by step A3
The water for stating mass percent, temperature be 30 DEG C~40 DEG C, revolving speed be 600r/min~800r/min under conditions of stir 1h~
2h obtains the detergent for containing flat leaf thorn celery extract.
10. preparation method according to claim 9, which is characterized in that described to contain flat leaf thorn celery extract in step A3
Detergent use temperature be 25 DEG C~35 DEG C.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102559408A (en) * | 2011-12-30 | 2012-07-11 | 北京绿伞化学股份有限公司 | Pure plant type antibacterial cleanser and preparation method thereof |
| CN105349276A (en) * | 2015-12-08 | 2016-02-24 | 成都锦汇科技有限公司 | Disinfecting washing agent |
| CN108102794A (en) * | 2018-01-10 | 2018-06-01 | 深圳市芭格美生物科技有限公司 | A kind of Washine-machine chute detergent, preparation method and applications |
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2018
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102559408A (en) * | 2011-12-30 | 2012-07-11 | 北京绿伞化学股份有限公司 | Pure plant type antibacterial cleanser and preparation method thereof |
| CN105349276A (en) * | 2015-12-08 | 2016-02-24 | 成都锦汇科技有限公司 | Disinfecting washing agent |
| CN108102794A (en) * | 2018-01-10 | 2018-06-01 | 深圳市芭格美生物科技有限公司 | A kind of Washine-machine chute detergent, preparation method and applications |
Non-Patent Citations (1)
| Title |
|---|
| 程敏: "《中药药剂学实验指导》", 31 August 2016, 东南大学出版社 * |
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