CN108888553A - A kind of perfume atmosphere is spraying and preparation method thereof - Google Patents
A kind of perfume atmosphere is spraying and preparation method thereof Download PDFInfo
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- CN108888553A CN108888553A CN201810820839.8A CN201810820839A CN108888553A CN 108888553 A CN108888553 A CN 108888553A CN 201810820839 A CN201810820839 A CN 201810820839A CN 108888553 A CN108888553 A CN 108888553A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/042—Gels
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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Abstract
The invention belongs to cosmetic field, in particular to a kind of fragrant atmosphere is spraying and preparation method thereof.Hydrogel moulder 1-50%, chelating agent 0.01-1%, Sodium Hyaluronate 0.001-5%, surplus is deionized water.The hydrogel moulder, the raw material comprising following weight percent number meter：Gelatinizing agent 0.01-3%, rheology control agent 0.1-5%, polyalcohol 0.5-30%, aromatic oil 0.5-30%, emulsifier 0.05-8%, pigment 0.001-5%, surplus are deionized water.The perfume atmosphere has slow releasing function by spraying, and essence/essential oil is wrapped in tridimensional network by hydrogel, and it is lasting to press the fragrant atmosphere of release in the shear history of spray head, lasting.The spraying mild safety, does not add ethyl alcohol or solubilizer, so more comfortable when being sprayed directly on skin surface.And its safety is also all substantially increased in production, transport, storage.
Description
Technical field
The invention belongs to cosmetic field, in particular to a kind of fragrant atmosphere is spraying and preparation method thereof.
Background technique
At present in cosmetic technical field, perfume is that the alcoholic solution of essence adds a certain amount of fixastive, is sprayed on skin
The positions such as skin, the hem, handkerchief and hairline distribute pleasant fragrance.It is to lean on solubilization technique by essence solubilising into water there are also minority,
To achieve the purpose that assign perfume products perfume (or spice) atmosphere.
But it is existing make solvent using a large amount of purification denatured ethyl alcohol, be on the one hand directly sprayed on skin can bring it is larger
Irritation, on the other hand due to the presence of a large amount of alcohol, this kind of perfume belongs to dangerous material, in production, transport, storing process
Specific condition is required, production and circulation cost are increased.And the perfume products of solubilization technique exploitation are utilized, essence additive amount is few,
Solubilizer brings sticky skin sense, and experience sense is poor, while having certain irritation.
So developing, a kind of not spirituosity, skin sense be salubrious, the non-hazardous fragrant atmosphere of transport and storage is highly desirable by spraying
's.
Summary of the invention
The object of the present invention is to provide a kind of fragrant atmosphere to be sprayed, and the spraying mild, safety, skin sense is salubrious, brings pleasant perfume atmosphere
While lasting it is lasting.
It is a further object to provide the spraying preparation methods of above-mentioned fragrant atmosphere.
The purpose of the present invention can be achieved through the following technical solutions
A kind of perfume atmosphere is spraying, which is characterized in that the raw material comprising following weight percent number meter：
Hydrogel moulder 1-50%
Chelating agent 0.01-1%
Sodium Hyaluronate 0.001-5%
Surplus is deionized water；
The hydrogel moulder, the raw material comprising following weight percent number meter：
Preferably,
A kind of perfume atmosphere is spraying, which is characterized in that the raw material comprising following weight percent number meter：
Hydrogel moulder 5-15%
Chelating agent 0.05-0.1%
Sodium Hyaluronate 0.01-0.3%
Surplus is deionized water；
The hydrogel moulder, the raw material comprising following weight percent number meter：
Preferably, the chelating agent is ethylenediamine tetra-acetic acid (EDTA), aminotriacetic acid (NTA), hydroxyethyl ethylenediamine three
Acetic acid (HEDTA), ethylenediamine disuccinic acid and its salt.It is further preferred that the chelating agent is EDETATE SODIUM or EDTA trisodium.
Preferably, the rheology control agent is locust bean gum, xanthan gum, pectin, gum arabic, isinglass, biology sugar
The combination of one or more of glue, Sodium Hyaluronate.
The polyalcohol is one of glycerol, butanediol, propylene glycol, dipropylene glycol, sorbierite, pentanediol, hexylene glycol
Or several combinations.
The aromatic oil is essence or essential oil.It is further preferred that the essence is natural essence used for cosmetic or conjunction
At essence；The essential oil is natural essential oil or synthesis essential oil used for cosmetic.
The HLB value 4-10 of the emulsifier, using the emulsifier, it can be achieved that small molecule essence or stablizing for essential oil coat.
Beneficial effect is can to wrap up aromatic oil into the network structure of hydrogel and containing these small molecule essence/essences
The hydrogel moulder of oil can be stable be present in fragrant atmosphere spray formula, be unlikely to leak, make to become cloudy forfeiture sustained release by spraying
Effect.
Preferably, the emulsifier is polyglyceryl fatty acid ester class, fatty acid glyceride, methyl glycol fatty acid ester class, Portugal
Grape sugar fatty acid ester, sucrose stearate, sucrose distearate, anhydrous sorbitol palmitate, anhydrous sorbitol stearic acid
The combination of one or more of ester, stereth -6.
The gelatinizing agent is in monovalence/divalent metal salt of agar, gellan gum, alginic acid divalent metal salt, carragheen
The combination of one or more of metal salts.It is further preferred that the alginic acid divalent metal salt is calcium alginate；The carragheen
Monovalence/divalent metal salt be carragheen sylvite.
It is further preferred that the gelatinizing agent is agar, gellan gum, calcium alginate are proportionally 1-3：1：1-5 is carried out
Compounding.It ensure that the softness of gel, moisture retention have certain toughness again.
The spraying preparation method of above-mentioned perfume atmosphere, step include：
(1) preparation of hydrogel moulder：
(A) water phase weighs deionized water according to the ratio, polyalcohol, gelatinizing agent, rheology control agent, stirs evenly, is heated to
85-95 DEG C, insulated and stirred 25-35min；Preferably, the heating temperature is 90 DEG C, insulated and stirred 30 minutes, suitable to heat
Temperature and soaking time can guarantee that gelatinizing agent can be sufficiently swollen.
(B) oily phase, weighs aromatic oil, emulsifier is heated to 75-85 DEG C, heating time 5-10min according to the ratio；It is preferred that
, the heating temperature is 80 DEG C, guarantees the effect of emulsification package；Heating time is 5min, guarantees that small molecule aromatic oil will not
Excessively volatilization, while certain solid state emulsifying agents being enable to melt.
(C) under homogeneous, during the oil phase is added to the aqueous phase, homogeneous 3-6min is kept the temperature；Preferably, heat preservation homogenizing time is
5min。
(D) pigment is added while stirring, stirs evenly；
(E) stirring is maintained, is cooled to 68 DEG C -72 DEG C, is fabricated to certain moulding, 18-25min plastic is stood, obtains water-setting
Glue moulder；
(2) according to the proportion, by the stirring of chelating agent, Sodium Hyaluronate and deionized water, dissolution, the water in step (1) is added
Gel moulder.
In fragrant atmosphere spray formula system listed by the present invention, the addition of Sodium Hyaluronate is not only moisture retention effect, more
It is important to soften hydrogel moulder, while chelating agent is also to play the role of softening hydrogel moulder, only this
Sample just can guarantee that moulder is smoothly sheared when passing through spraying pump head, discharge fragrant atmosphere, otherwise can holddown.
Compared with prior art, the beneficial effects of the present invention are：
1, the fragrant atmosphere has slow releasing function by spraying, and essence/essential oil is wrapped in its tridimensional network by hydrogel,
It presses and discharges fragrant atmosphere in the shear history of spray head, since special three-dimensional structure exists, make essence/essential oil slow release, lasting
Persistently.
2, the spraying mild safety of the fragrant atmosphere, does not add ethyl alcohol or solubilizer, so when being sprayed directly on skin surface
It is more comfortable.And its safety is also all substantially increased in production, transport, storage.
3, the fragrant atmosphere is spraying is rich in aesthetic feeling because having the presence of the hydrogel of certain moulding, more fitting people
When using cosmetics to the original original intention of the pursuit of beauty, increase added value of product.
Specific embodiment
Below with reference to embodiment, the invention will be further described：
Embodiment 1
1, the spraying preparation of fragrant atmosphere,
Weigh the raw material of following weight percent number meter：
Hydrogel moulder 10%
EDETATE SODIUM 0.1%
Sodium Hyaluronate 0.03%
Surplus is water.
EDETATE SODIUM, Sodium Hyaluronate and water are successively weighed into container, stirring and dissolving, finally by hydrogel moulder
In addition system.
2, the preparation of hydrogel moulder,
Weigh the raw material of following weight percent number meter：
(1) it is added to the water after dispersing agar, xanthan gum, gellan gum glycerol, to 90 DEG C, heat preservation is stirred for warming while stirring
30min is mixed, guarantees sufficiently dissolution；
(2) -4 isostearate of oily phase flavoring rose essence and polyglycereol is weighed, stirring is warming up to 80 DEG C, and heating time is
5min；
(3) homogeneous is opened, becomes homogeneous side during the oil phase is added to the aqueous phase, maintains homogeneous 5min.
(4) pigment is added while stirring, stirs evenly；
(5) stirring is maintained, greenhouse cooling is fabricated to various moulding to 70 DEG C ± 2 DEG C, stands 20min plastic, obtains water-setting
Glue moulder.
Test content：The contrast test of fragrant atmosphere lasting is assessed with certain commercially available brand perfume.
Test result：The commercially available spirituosity rose scent perfume of sprinkling same amount and nothing of the present invention on the fragrant paper of examination of standard
Alcohol perfume (or spice) atmosphere is spraying, and the aromatic flavour for finding commercially available perfume is assessed after one minute or even some are pungent, and alcohol-free fragrant atmosphere is spraying
Rose scent is milder, and commercially available perfume fragrance is obviously thin out after 2 hours, and fragrant atmosphere of the invention is sprayed fragrance without significant change.4 is small
When after when perfume fragrance volatilize completely, still there is obvious rose fragrance to remain on the spraying examination perfume (or spice) paper of fragrant atmosphere of the invention.
Therefore illustrate that the alcohol-free fragrant atmosphere that the present invention develops has the characteristics that be sustained fragrance lasting and advantage by spraying.
Embodiment 2：
1, the spraying preparation of fragrant atmosphere,
Weigh the raw material of following weight percent number meter：
Hydrogel moulder 10%
EDETATE SODIUM 0.05%
Sodium Hyaluronate 0.1%
Surplus is water.
EDTA, Sodium Hyaluronate and water are successively weighed into container, stirring and dissolving, finally hydrogel moulder is added
In system.
2, the preparation of hydrogel moulder,
Weigh the raw material of following weight percent number meter：
(1) it will be added to the water after the dispersion of gellan gum, locust bean gum, carragheen butanediol and propylene glycol, rise while stirring
For temperature to 90 DEG C, insulated and stirred 30min, KCl is added in guarantee after completely dissolution；
(2) three isostearate of oily phase Lavender and polyglycereol -2, Span60 are weighed, stirring rises
Temperature is to 80 DEG C, heating time 10min；
(3) homogeneous is opened, becomes homogeneous side during the oil phase is added to the aqueous phase, maintains homogeneous 5min.
(4) pigment is added while stirring, stirs evenly；
(5) stirring is maintained, greenhouse cooling is fabricated to various moulding to 70 DEG C ± 2 DEG C, stands 20min plastic, obtains water-setting
Glue moulder.
Test content：The contrast test of fragrant atmosphere lasting is assessed with certain commercially available brand perfume.
Test result：The commercially available spirituosity lavender flavor type perfume of sprinkling same amount and nothing of the present invention on the fragrant paper of the examination of standard
Alcohol perfume (or spice) atmosphere is spraying, and assessment finds the aromatic flavour of commercially available perfume after one minute, and the spraying examination perfume (or spice) paper of the fragrant atmosphere of the present invention have it is soft
The lavender of sum；Commercially available perfume fragrance is obviously thin out after 2 hours, and alcohol-free perfume atmosphere is sprayed fragrance without significant change；4 hours
Perfume fragrance volatilizees completely when afterwards, still has obvious lavender fragrance to remain on the spraying examination perfume (or spice) paper of fragrant atmosphere of the invention.
Therefore illustrate that the alcohol-free fragrant atmosphere that the present invention develops is made using the tridimensional network of hydrogel and special packing technology by spraying
Lavender sustained release, and lasting is lasting.
Embodiment 3：
1, the spraying preparation of fragrant atmosphere,
Weigh the raw material of following weight percent number meter：
Hydrogel moulder 10%
Ethylenediamine succinic acid trisodium 0.05%
Sodium Hyaluronate 0.1%
Surplus is water.
Ethylenediamine succinic acid trisodium, Sodium Hyaluronate and water are successively weighed into container, stirring and dissolving, finally by water-setting
In glue moulder addition system.
2, the preparation of hydrogel moulder,
Weigh the raw material of following weight percent number meter：
(1) it will be added after the dispersion of agar, gellan gum, locust bean gum, xanthan gum, sodium alginate hexylene glycol and dipropylene glycol
In water, to 90 DEG C, insulated and stirred 30min, CaCl is added in guarantee after completely dissolution for warming while stirring2；
(2) oily phase refined jasmine oil and sucrose stearate are weighed, stirring is warming up to 80 DEG C, heating time 10min；
(3) homogeneous is opened, becomes homogeneous side during the oil phase is added to the aqueous phase, maintains homogeneous 5min.
(4) pigment is added while stirring, stirs evenly；
(5) stirring is maintained, greenhouse cooling is fabricated to various moulding to 70 DEG C ± 2 DEG C, stands 20min plastic, obtains water-setting
Glue moulder.
Test content：The contrast test of fragrant atmosphere lasting is assessed with certain commercially available brand perfume.
Test result：Commercially available spirituosity jasmine fragrance perfume and the present invention that same amount is sprayed on the fragrant paper of examination of standard are fragrant
Atmosphere is spraying, and assessment finds that the fragrance smell of commercially available perfume is dense strongly fragrant after one minute, and to be sprayed jasmine fragrance more clear for the fragrant atmosphere of the present invention
Light, commercially available perfume fragrance is very light after 2 hours, and fragrant atmosphere of the invention is sprayed fragrance without significant change.Perfume is fragrant when after 4 hours
Gas volatilizees completely, still has obvious jasmine fragrance to remain on the spraying examination perfume (or spice) paper of fragrant atmosphere of the invention, after 6 hours, the present invention
The spraying examination perfume (or spice) paper of fragrant atmosphere on still there is obvious jasmine fragrance to remain, still have Jasmine fragrance residual after 8 hours.Therefore
Illustrate that the fragrant atmosphere that the present invention develops has the characteristics that be sustained fragrance lasting and advantage by spraying, and after use compounding gelatinizing agent, because
It is more soft for gel, and just have certain toughness, so that fragrant atmosphere is more longlasting, using pump head will not be blocked.
The above is presently preferred embodiments of the present invention, but the present invention should not be limited to disclosed in the embodiment
Content.So all do not depart from the lower equivalent or modification completed of spirit disclosed in this invention, the model that the present invention protects is both fallen within
It encloses.
Claims (9)
1. a kind of perfume atmosphere is spraying, which is characterized in that the raw material comprising following weight percent number meter：
The hydrogel moulder, the raw material comprising following weight percent number meter：
2. perfume atmosphere according to claim 1 is spraying, it is characterised in that：The chelating agent is ethylenediamine tetra-acetic acid, amino three
Acetic acid, hydroxyethylethylene diamine tri-acetic acid, ethylenediamine disuccinic acid and its salt.
3. perfume atmosphere according to claim 1 is spraying, it is characterised in that：The rheology control agent be locust bean gum, xanthan gum,
The combination of one or more of pectin, gum arabic, isinglass, biological carbohydrate gum, Sodium Hyaluronate.
4. perfume atmosphere according to claim 1 is spraying, it is characterised in that：The polyalcohol be glycerol, butanediol, propylene glycol,
The combination of one or more of dipropylene glycol, sorbierite, pentanediol, hexylene glycol.
5. perfume atmosphere according to claim 1 is spraying, it is characterised in that：The aromatic oil is essence or essential oil.
6. perfume atmosphere according to claim 1 is spraying, it is characterised in that：The HLB value of the emulsifier is 4-10.
7. perfume atmosphere according to claim 6 is spraying, it is characterised in that：The emulsifier is polyglyceryl fatty acid ester class, sweet
Oil and fat acid esters, methyl glycol fatty acid ester class, glucose fatty acid ester, sucrose stearate, sucrose distearate, dehydration mountain
The combination of one or more of pears alcohol palmitate, Span60, stereth -6.
8. perfume atmosphere according to claim 1 is spraying, it is characterised in that：The gelatinizing agent is agar, gellan gum, alginic acid two
One or more of valence metal salt, monovalence/divalent metal salt of carragheen combine.
9. a kind of preparation method that fragrant atmosphere described in claim 1 is spraying, step include：
(1) preparation of hydrogel moulder：
(A) water phase weighs deionized water according to the ratio, polyalcohol, gelatinizing agent, rheology control agent, stirs evenly, is heated to 85-95
DEG C, insulated and stirred 25-35min；
(B) oily phase, weighs aromatic oil, emulsifier is heated to 75-85 DEG C according to the ratio, and heating time is no more than 5-10min；
(C) under homogeneous, during the oil phase is added to the aqueous phase, homogeneous 3-6min is kept the temperature；
(D) pigment is added while stirring, stirs evenly；
(E) stirring is maintained, is cooled to 68 DEG C -72 DEG C, is fabricated to certain moulding, 18-25min plastic is stood, obtains hydrogel and make
Type object；
(2) according to the proportion, it by the stirring of metal ion chelation agent, Sodium Hyaluronate and deionized water, dissolution, is added in step (1)
Hydrogel moulder.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109453091A (en) * | 2019-01-02 | 2019-03-12 | 广东美宝化妆品有限公司 | A kind of perfume and preparation method thereof based on compound fresh flower extracting solution |
| CN110354024A (en) * | 2019-07-19 | 2019-10-22 | 深圳市越昌科技有限公司 | Suitable for underclothes fragrant atmosphere scented tea and be applicable in the personal clothing of scented tea |
| CN110507552A (en) * | 2019-09-19 | 2019-11-29 | 义乌市为你美化妆品有限公司 | A kind of ethanol-free perfume and preparation method thereof |
| CN113599348A (en) * | 2021-09-02 | 2021-11-05 | 上海菲珂尔化妆品有限公司 | Spray composition, preparation method thereof and spray cosmetic |
| CN115023215A (en) * | 2020-02-04 | 2022-09-06 | 弗门尼舍有限公司 | Formulations providing long-lasting fragrance performance |
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| CN109453091A (en) * | 2019-01-02 | 2019-03-12 | 广东美宝化妆品有限公司 | A kind of perfume and preparation method thereof based on compound fresh flower extracting solution |
| CN109453091B (en) * | 2019-01-02 | 2021-08-24 | 广东美宝化妆品有限公司 | Perfume based on composite flower extracting solution and preparation method thereof |
| CN110354024A (en) * | 2019-07-19 | 2019-10-22 | 深圳市越昌科技有限公司 | Suitable for underclothes fragrant atmosphere scented tea and be applicable in the personal clothing of scented tea |
| CN110354024B (en) * | 2019-07-19 | 2020-09-25 | 深圳市越昌科技有限公司 | Fragrance sheet suitable for underwear and underwear suitable for fragrance sheet |
| CN110507552A (en) * | 2019-09-19 | 2019-11-29 | 义乌市为你美化妆品有限公司 | A kind of ethanol-free perfume and preparation method thereof |
| CN115023215A (en) * | 2020-02-04 | 2022-09-06 | 弗门尼舍有限公司 | Formulations providing long-lasting fragrance performance |
| CN113599348A (en) * | 2021-09-02 | 2021-11-05 | 上海菲珂尔化妆品有限公司 | Spray composition, preparation method thereof and spray cosmetic |
| CN113599348B (en) * | 2021-09-02 | 2024-02-13 | 上海菲珂尔化妆品有限公司 | Spray composition, preparation method thereof and spray cosmetic |
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Application publication date: 20181127 |