CN110898247B - Super-concentrated deodorant gel and preparation method and application thereof - Google Patents
Super-concentrated deodorant gel and preparation method and application thereof Download PDFInfo
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- CN110898247B CN110898247B CN201911338420.XA CN201911338420A CN110898247B CN 110898247 B CN110898247 B CN 110898247B CN 201911338420 A CN201911338420 A CN 201911338420A CN 110898247 B CN110898247 B CN 110898247B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/012—Deodorant compositions characterised by being in a special form, e.g. gels, emulsions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/01—Deodorant compositions
- A61L9/013—Deodorant compositions containing animal or plant extracts, or vegetable material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2209/00—Aspects relating to disinfection, sterilisation or deodorisation of air
- A61L2209/20—Method-related aspects
- A61L2209/21—Use of chemical compounds for treating air or the like
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Botany (AREA)
- Zoology (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention discloses a super-concentrated deodorant gel and a preparation method and application thereof, wherein the super-concentrated deodorant gel comprises the following components in parts by weight: 50-80 parts of essence; 10-15 parts of polyvinyl chloride paste resin; 8-12 parts of benzyl benzoate; 0.1-10 parts of plant essential oil; 0.5-2 parts of zinc ricinoleate; 0.01 to 0.03 part of phenoxyethanol. The super-concentrated deodorizing gel overcomes the technical bottleneck that the highest proportion of essence addition in the prior balm and gel cannot exceed 10 percent, the essence addition can reach more than 50 percent, the product does not contain water or alcohol, the fragrance diffusing time is super-long, the gel structure is transparent and stable, the gel is not sticky and overflows, the use environment is not polluted, the transportation cost can be greatly reduced, and the super-concentrated deodorizing gel is a novel miniaturized gel capable of deodorizing and permanently diffusing fragrance.
Description
Technical Field
The invention relates to the technical field of air purification materials, in particular to a concentrated deodorant gel and a preparation method and application thereof.
Background
The perfume gel is a gel material which brings benefits or influences to the surrounding environment by diffusing active volatile substances and emitting perfume, the perfume is one of the main components in the perfume gel, the perfume is a concentrated perfume oil which imitates the smell of fruits and natural perfumes and is artificially synthesized, and the type and the addition amount of the perfume have great influence on the performance and the using effect of the perfume gel. In the existing fragrant gel or fragrant cream on the market, the highest proportion of essence addition cannot exceed 10 percent, because when the essence content is high, the fragrant gel or fragrant cream can be discharged, so that the fragrant gel and fragrant cream are easy to overflow, the environment is polluted, and the like.
Disclosure of Invention
The invention aims to overcome at least one defect of the prior art and provides the super-concentrated deodorant gel which has high essence content, lasting deodorant effect, no water discharge from the gel and no tank overflow.
The technical scheme adopted by the invention is as follows:
a super-concentrated deodorant gel comprises the following components in parts by weight:
50-80 parts of essence;
10-15 parts of polyvinyl chloride paste resin;
8-12 parts of benzyl benzoate;
0.1-10 parts of plant essential oil;
0.5-2 parts of zinc ricinoleate;
0.01-0.03 part of phenoxyethanol.
According to the invention, the polyvinyl chloride paste resin, the benzyl benzoate and the like are added into the essence and the plant essential oil, so that the essence content in the prepared super-concentrated deodorant gel can reach more than 50%, wherein the polyvinyl chloride paste resin is high-dispersity powder, has excellent paste forming performance and good dispersing performance, can be mixed with the essence and the plant essential oil to obtain a gel product, the benzyl benzoate can be used as a fixative of the essence, so that the essence and spice components are uniformly volatilized, rapid evaporation is prevented, the essence fragrance is more durable, zinc ricinoleate is used as a stabilizer of the polyvinyl chloride paste resin and is also used as a deodorant, phenoxyethanol has antibacterial and antiseptic effects, and the comprehensive performance of the super-concentrated deodorant gel can be further improved. The super-concentrated deodorizing gel overcomes the technical bottleneck that the highest proportion of essence addition in the prior balm and gel cannot exceed 10 percent, the essence addition can reach more than 50 percent, the product does not contain water or alcohol, the fragrance-dispersing time is super-long, the gel structure is transparent and stable, the gel is not sticky and overflows, the use environment is not polluted, the transportation cost is greatly reduced, and the super-concentrated deodorizing gel is a novel miniaturized gel capable of deodorizing and dispersing fragrance for a long time.
The main functions of the essence are to generate pleasant odor and to cover the odor of the product substrate, and the essence can be classified into floral, non-floral, fruity, liquor, tobacco and food flavors according to the flavor type. Preferably, the essence provided by the invention is a flower essence or a fruit essence.
The plant essential oil is an aromatic substance extracted from plants, has high volatility and small molecules, is easily absorbed by human bodies, can quickly permeate into internal organs of the human bodies, discharges redundant components out of the human bodies, has the fragrance of the plants, and can directly stimulate the secretion of pituitary gland, the secretion of enzymes, hormones and the like to balance internal functions. Preferably, the plant essential oil is rose essential oil, tea tree essential oil, lavender essential oil or rosemary essential oil.
Preferably, the essence is 50-60 parts by weight.
Preferably, the weight part of the plant essential oil is 5-10 parts.
Preferably, the preparation method of the super-concentrated deodorant gel comprises the following steps:
(1) fully mixing the plant essential oil, the essence and the benzyl benzoate, and then mixing and stirring the mixture with zinc ricinoleate and phenoxyethanol uniformly;
(2) and then adding the polyvinyl chloride paste resin, mixing and stirring, heating to 100-120 ℃, stirring while heating until the polyvinyl chloride paste resin is fully dissolved, stopping heating for 15min, filling the finished product, and cooling, condensing and forming the finished product within half an hour to obtain the super-concentrated deodorant aromatic gel.
The super-concentrated deodorant gel is applied to the field of air deodorization as a household deodorant and a vehicle deodorant.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, the high-dispersity powder polyvinyl chloride paste resin is added into the essence and the plant essential oil, so that the essence and the plant essential oil can be uniformly dispersed in the polyvinyl chloride paste resin to obtain a gel product, the content of the essence in the gel product can be up to more than 50%, the product does not contain water, does not contain alcohol, and the fragrance dispersing time is very long; the benzyl benzoate can be used as a fixative of the essence, so that the components of the essence are uniformly volatilized, rapid evaporation is prevented, and the fragrance of the essence is more durable.
Detailed Description
The invention is illustrated below with reference to specific embodiments.
The starting materials used in the following examples are all common commercial products.
Example 1
A super-concentrated deodorant gel comprises the following components:
60 parts of essence (floral essence);
10 parts of polyvinyl chloride paste resin;
10 parts of benzyl benzoate;
5 parts of plant essential oil (rose essential oil);
1 part of zinc ricinoleate;
0.02 part of phenoxyethanol.
The preparation method of the super-concentrated deodorant gel comprises the following steps:
(1) fully mixing the plant essential oil, the essence and the benzyl benzoate, and then mixing and stirring the mixture with zinc ricinoleate and phenoxyethanol uniformly;
(2) and then adding the polyvinyl chloride paste resin, mixing and stirring, heating to 100-120 ℃, stirring while heating until the polyvinyl chloride paste resin is fully dissolved, stopping heating for 15min, filling the finished product, and cooling, condensing and forming the finished product within half an hour to obtain the super-concentrated deodorant aromatic gel.
Example 2
A super-concentrated deodorant gel comprises the following components:
50 parts of essence (floral essence);
12 parts of polyvinyl chloride paste resin;
8 parts of benzyl benzoate;
10 parts of plant essential oil (rose essential oil);
0.5 part of zinc ricinoleate;
0.01 part of phenoxyethanol.
The preparation method of the super-concentrated deodorant gel is the same as that of example 1, and the description thereof is omitted.
Example 3
A super-concentrated deodorant gel comprises the following components:
80 parts of essence (floral essence);
15 parts of polyvinyl chloride paste resin;
12 parts of benzyl benzoate;
8 parts of plant essential oil (rose essential oil);
2 parts of zinc ricinoleate;
0.03 part of phenoxyethanol.
The preparation method of the super-concentrated deodorant gel is the same as that of example 1, and the description thereof is omitted.
Example 4
A super-concentrated deodorant gel comprises the following components:
60 parts of essence (fruity essence);
10 parts of polyvinyl chloride paste resin;
10 parts of benzyl benzoate;
5 parts of plant essential oil (lavender essential oil);
1 part of zinc ricinoleate;
0.02 part of phenoxyethanol.
The preparation method of the super-concentrated deodorant gel is the same as that of example 1, and the description thereof is omitted.
The prepared super-concentrated deodorant gel is subjected to performance test, and the specific test contents are as follows:
(1) testing the fragrance holding time:
opening 20 g of finished products, placing the finished products indoors at the average temperature of 26 ℃, smelling fragrance every day, and judging whether the fragrance belongs to the following conditions:
1-50 days, the fragrance is also strong, the fragrance is slightly reduced after 50 days, the fragrance still obviously exists at day 70, the fragrance-retaining time of the product is long, and the fragrance-retaining grade is excellent;
secondly, the fragrance is also strong for 1-30 days, and after 30 days, the fragrance is slightly reduced, so that the fragrance retention grade is good;
③ 1 to 10 days, the fragrance is also strong, and the grade is poor if the fragrance is slightly reduced after 10 days;
fourthly, the grade is poor when the fragrance is reduced within 1 to 10 days.
(2) Testing adhesion, transparency and shrinkage conditions:
the 20 g pack was opened, placed in a room with an average temperature of 26 ℃ and the surface morphology, adhesion morphology and shrinkage of the gel were observed every day, and the state was felt with fingers every day.
The experimental results show that: the hyperconcentration deodorant gel disclosed in the embodiments 1 to 4 of the invention has long lasting fragrance retention time and excellent fragrance retention grade, fragrance is also intense in 1-50 days, fragrance slightly decreases after 50 days, and fragrance still obviously exists at day 70. The super-concentrated deodorant gel described in examples 1 to 4 has high gel adhesion degree in days 1 to 30, is completely gelatinous, is soft to touch, does not break when being lightly pressed, and does not produce water, oil and hands; the super concentrated deodorant perfume gels described in examples 1 to 4 were clear within days 1 to 30 without any cloudy impurities; the super-concentrated deodorant gel described in examples 1 to 4 slightly shrinks overall around the gel after 30 days, the paste shrinks more after 50 days, the paste shrinks obviously to the middle after 70 days, the area is reduced by about two thirds, but the adhesion degree and the transparency are good, and the fragrance still remains obviously.
Therefore, the super-concentrated deodorant gel has the advantages of super-lasting fragrance emitting time, transparent and stable gel structure, no adhesion to hands, no overflow and no pollution to the use environment, and is a novel miniaturized fragrant gel capable of deodorizing and emitting fragrance for a long time.
It should be understood that the above-mentioned embodiments of the present invention are only examples for clearly illustrating the technical solutions of the present invention, and are not intended to limit the specific embodiments of the present invention. Any modification, equivalent replacement, and improvement made within the spirit and principle of the present invention claims should be included in the protection scope of the present invention claims.
Claims (3)
1. The super-concentrated deodorizing aromatic gel is characterized by comprising the following components in parts by weight:
50-60 parts of essence;
10-15 parts of polyvinyl chloride paste resin;
8-12 parts of benzyl benzoate;
5-10 parts of plant essential oil;
0.5-2 parts of zinc ricinoleate;
0.01-0.03 part of phenoxyethanol;
the essence is flower-fragrance type essence or fruit-fragrance type essence;
the plant essential oil is rose essential oil, tea tree essential oil, lavender essential oil or rosemary oil.
2. The method of preparing a super concentrated deodorant gel according to claim 1, comprising the steps of:
(1) fully mixing the plant essential oil, the essence and the benzyl benzoate, and then mixing and stirring the mixture with zinc ricinoleate and phenoxyethanol uniformly;
(2) and then adding the polyvinyl chloride paste resin, mixing and stirring, heating to 100-120 ℃, stirring while heating until the polyvinyl chloride paste resin is fully dissolved, stopping heating for 15min, filling the finished product, and cooling, condensing and forming the finished product within half an hour to obtain the super-concentrated deodorant aromatic gel.
3. Use of the super concentrated deodorant gel of claim 1 as a household deodorant, a car deodorant in the field of air deodorisation.
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CN201911338420.XA CN110898247B (en) | 2019-12-23 | 2019-12-23 | Super-concentrated deodorant gel and preparation method and application thereof |
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CN110898247A CN110898247A (en) | 2020-03-24 |
CN110898247B true CN110898247B (en) | 2022-02-18 |
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Citations (6)
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BE892021A (en) * | 1981-02-05 | 1982-05-27 | Firmenich & Cie | MULTI-COMPARTMENT PLASTIC PACKAGING FOR LIQUID AND SOLID PRODUCTS |
JPS62129183A (en) * | 1985-11-29 | 1987-06-11 | Dainichi Color & Chem Mfg Co Ltd | Deodorizing polyvinyl chloride sheet material |
CN101156956A (en) * | 2007-11-16 | 2008-04-09 | 张逸平 | Organism albumen gel aromatic and its preparing method |
CN102775537A (en) * | 2012-08-29 | 2012-11-14 | 沈阳化工股份有限公司 | High-strength PVC (polyvinyl chloride) paste resin and production method thereof |
CN103585654A (en) * | 2013-11-13 | 2014-02-19 | 东莞市日友汽车用品有限公司 | Paste-like air freshener with PVC (polyvinyl chloride) resin as main gel raw material |
CN104017225A (en) * | 2014-04-03 | 2014-09-03 | 高雷 | Improvement method of polyvinyl chloride paste resin |
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KR100744342B1 (en) * | 2001-12-28 | 2007-07-30 | 주식회사 엘지생활건강 | Deodorant composition |
US8318806B2 (en) * | 2007-10-03 | 2012-11-27 | Zorbx Inc. | Deodorizing composition and method of forming thereof |
CN108939118A (en) * | 2017-05-17 | 2018-12-07 | 东莞市腾美纳米新材料有限公司 | A kind of high-temp. resistant air aromatic gel and preparation method thereof |
CN107321170A (en) * | 2017-07-04 | 2017-11-07 | 广州市拓新化工科技有限公司 | A kind of odor scavenging agent and preparation method thereof |
CN107510859A (en) * | 2017-08-31 | 2017-12-26 | 广东爱车小屋实业发展股份有限公司 | Champignon and preparation method thereof |
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2019
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Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE892021A (en) * | 1981-02-05 | 1982-05-27 | Firmenich & Cie | MULTI-COMPARTMENT PLASTIC PACKAGING FOR LIQUID AND SOLID PRODUCTS |
JPS62129183A (en) * | 1985-11-29 | 1987-06-11 | Dainichi Color & Chem Mfg Co Ltd | Deodorizing polyvinyl chloride sheet material |
CN101156956A (en) * | 2007-11-16 | 2008-04-09 | 张逸平 | Organism albumen gel aromatic and its preparing method |
CN102775537A (en) * | 2012-08-29 | 2012-11-14 | 沈阳化工股份有限公司 | High-strength PVC (polyvinyl chloride) paste resin and production method thereof |
CN103585654A (en) * | 2013-11-13 | 2014-02-19 | 东莞市日友汽车用品有限公司 | Paste-like air freshener with PVC (polyvinyl chloride) resin as main gel raw material |
CN104017225A (en) * | 2014-04-03 | 2014-09-03 | 高雷 | Improvement method of polyvinyl chloride paste resin |
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