CN108887461A - Peony seeds albumen and its extracting method - Google Patents

Peony seeds albumen and its extracting method Download PDF

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Publication number
CN108887461A
CN108887461A CN201810512444.1A CN201810512444A CN108887461A CN 108887461 A CN108887461 A CN 108887461A CN 201810512444 A CN201810512444 A CN 201810512444A CN 108887461 A CN108887461 A CN 108887461A
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CN
China
Prior art keywords
peony
peony seeds
albumen
extracting method
separated
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810512444.1A
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Chinese (zh)
Inventor
邹平
张迎阳
李丽娟
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Changzhou University
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Changzhou University
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Publication date
Application filed by Changzhou University filed Critical Changzhou University
Priority to CN201810512444.1A priority Critical patent/CN108887461A/en
Publication of CN108887461A publication Critical patent/CN108887461A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23JPROTEIN COMPOSITIONS FOR FOODSTUFFS; WORKING-UP PROTEINS FOR FOODSTUFFS; PHOSPHATIDE COMPOSITIONS FOR FOODSTUFFS
    • A23J1/00Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites
    • A23J1/14Obtaining protein compositions for foodstuffs; Bulk opening of eggs and separation of yolks from whites from leguminous or other vegetable seeds; from press-cake or oil-bearing seeds

Abstract

The invention belongs to field of deep processing of farm products, in particular to peony seeds albumen and its extracting method:Peony seeds albumen and its extracting method:After peony seeds shelling, shell is separated with benevolence, then by benevolence by broken, after preheating, peony seed oil is separated using supercritical extraction, remainder is the peony seeds dregs of rice, the peony seeds dregs of rice powder separated is dried, it crushes, the distilled water of certain mass ratio is then added, after high-speed homogenization, NaOH solution is added and is adjusted to suitable ph, stirring and leaching certain time under the conditions of 40-60 DEG C, leaching liquor is centrifuged, collect supernatant, obtain tree peony protein solution, then tree peony protein solution pH value is adjusted to acidity with HCl solution again, the tree peony albumen precipitated, it is centrifuged and washs to neutrality, it is dried to obtain peony seeds albumen.This method extracting method is simple and fast, at low cost, is conducive to industrialization production, the molecular weight of gained peony seeds albumen is mainly in 10-30ku, it is necessary to which amino acid content is high, and nutritive value is high.

Description

Peony seeds albumen and its extracting method
Technical field
The invention belongs to field of deep processing of farm products, in particular to peony seeds albumen and its extracting method.
Background technique
Tree peony has permanent plantation history in China, and oil has good economic, ecology and social benefit with tree peony, energetically Development oil can not only make full use of forest land resource abundant with tree peony industry, effectively increase in the case where not striving ground with peasant Food plant oil yield, maintenance national food and oil safety optimize national diet structure, improve health conditions.And life can be improved State environment promotes economic development, increases farmers' income.Oil can produce 3000~3500kg/hm of seed with tree peony2, peony seed oil 600 out ~700kg/hm2, benefit per mu is more than 5000 yuan, and compared with traditional grain and oil crop, benefit is plant cereal crops 8~10 Times.Oil is an important economic tree with tree peony, and development oil is with tree peony industry for improving farmers' income, peasant being helped to shake off poverty It gets rich and is of great significance.However it is also less to the comprehensive utilization of peony seeds at present, peony seeds mention the grouts after oil, contain high egg It is white, it is a kind of novel plant albumen leaved for development.
Summary of the invention
The present invention provides peony seeds albumen and its extracting methods, and steps are as follows:
(1) after peony seeds shelling, shell is separated with benevolence, then by benevolence after broken, preheating, using overcritical extraction Separation peony seed oil is followed the example of, remainder is the peony seeds dregs of rice, and the peony seeds dregs of rice powder separated is dried, and is crushed;
(2) distilled water of 10-15 times of mass ratio, high-speed homogenization are added in the tree peony benevolence powder that step (1) obtains;
(3) NaOH solution is added in the homogenate obtained by step (2) to be adjusted to pH is 8.8-10.0, under the conditions of 40-60 DEG C Stirring leaching 1-2h, collects filtrate;
(4) dilute HCl solution is added in step (3) by tree peony protein solution pH value to 4.5-5.5, the tree peony precipitated Albumen;
(5) mixture obtained by step (4) is centrifuged, sub-cloud precipitating, and washed to neutrality, be dried to obtain peony seeds Albumen.
The beneficial effects of the present invention are:This method extracting method is simple and fast, at low cost, is conducive to industrialization production, institute The molecular weight of peony seeds albumen is obtained mainly in 10-30ku, it is necessary to which amino acid content is high, and nutritive value is high.
Detailed description of the invention
Fig. 1 is influence of the pH to peony seeds protein extracting ratio in the embodiment of the present invention 1.
Fig. 2 is the amino acid analysis result of peony seeds albumen in the embodiment of the present invention 1.

Claims (7)

1. peony seeds albumen and its extracting method, it is characterised in that:The step of the method is,
Peony seeds albumen and its extracting method:After peony seeds shelling, shell is separated with benevolence, then by benevolence by broken, pre- After heat, peony seed oil is separated using supercritical extraction, remainder is the peony seeds dregs of rice, the peony seeds dregs of rice powder that will be separated It is dried, crushes, then the distilled water of addition certain mass ratio, after high-speed homogenization, NaOH solution is added and is adjusted to suitable pH Value, stirring and leaching certain time, leaching liquor is centrifuged under the conditions of 40-60 DEG C, is collected supernatant, is obtained tree peony protein Solution, is then adjusted to acidity for tree peony protein solution pH value with HCl solution again, and the tree peony albumen precipitated is centrifuged and washs To neutrality, freeze-drying obtains peony seeds albumen.This method extracting method is simple and fast, at low cost, is conducive to industrialization production, institute The molecular weight of peony seeds albumen is obtained mainly in 10-30ku, it is necessary to which amino acid content is high, and nutritive value is high.
(1) after peony seeds shelling, shell is separated with benevolence, then by benevolence after broken, preheating, using supercritical extraction Peony seed oil is separated, remainder is the peony seeds dregs of rice, and the peony seeds dregs of rice powder separated is dried, and is crushed;
(2) distilled water of certain mass ratio is added in the peony seeds powder that step (1) obtains, after high-speed homogenization, it is molten that NaOH is added Liquid is adjusted to suitable ph, stirring and leaching certain time under the conditions of 40-60 DEG C, collects filtrate;
(3) dilute HCl solution is added in step (2) and tree peony protein solution pH value is adjusted to acidity, the tree peony albumen precipitated;
(4) mixture obtained by step (3) is centrifuged, sub-cloud precipitating, and washed to neutrality, be dried to obtain peony seeds egg It is white.
2. peony seeds albumen as described in claim 1 and its extracting method, it is characterised in that:In step (1), in peony seeds Edible oil separation uses supercritical extraction.
3. peony seeds albumen as described in claim 1 and its extracting method, it is characterised in that:Distillation described in step (2) Water adding proportion is in 10-15 times of peony seeds dregs of rice powder weight.
4. peony seeds albumen as described in claim 1 and its extracting method, it is characterised in that:In step (2), it is molten that NaOH is added It is 8.8-10.0 that liquid, which is adjusted to pH,.
5. peony seeds albumen as described in claim 1 and its extracting method, it is characterised in that:In step (2), extraction is being stirred It is carried out under state, extraction time 1-2h.
6. peony seeds albumen as described in claim 1 and its extracting method, it is characterised in that:In step (3), dilute HCl is added Tree peony protein solution pH value is adjusted to 4.5-5.5 by solution.
7. peony seeds albumen as described in claim 1 and its extracting method, it is characterised in that:In step (4), albumen can lead to The modes such as vacuum drying, drying, microwave drying, vacuum freeze drying are closed to obtain.
CN201810512444.1A 2018-05-25 2018-05-25 Peony seeds albumen and its extracting method Pending CN108887461A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810512444.1A CN108887461A (en) 2018-05-25 2018-05-25 Peony seeds albumen and its extracting method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810512444.1A CN108887461A (en) 2018-05-25 2018-05-25 Peony seeds albumen and its extracting method

Publications (1)

Publication Number Publication Date
CN108887461A true CN108887461A (en) 2018-11-27

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Family Applications (1)

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CN201810512444.1A Pending CN108887461A (en) 2018-05-25 2018-05-25 Peony seeds albumen and its extracting method

Country Status (1)

Country Link
CN (1) CN108887461A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113383851A (en) * 2021-07-02 2021-09-14 山东省科学院菏泽分院 Method for extracting peony protein isolate for oil

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103497822A (en) * 2013-10-14 2014-01-08 铜陵瑞璞牡丹产业发展有限公司 Method of extracting protein and dietary fibers from peony seeds or peony seed meal
CN106281659A (en) * 2016-08-30 2017-01-04 铜陵亚通牡丹产业发展有限公司 Method for extracting protein in a kind of seed of Flos Moutan dregs of rice
CN106467855A (en) * 2015-08-17 2017-03-01 洛阳健特生物科技有限公司 Peony seed oil supercritical CO 2 extraction technology
CN108060012A (en) * 2017-12-19 2018-05-22 贵州航天乌江机电设备有限责任公司 A kind of extracting method of peony seed oil

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103497822A (en) * 2013-10-14 2014-01-08 铜陵瑞璞牡丹产业发展有限公司 Method of extracting protein and dietary fibers from peony seeds or peony seed meal
CN106467855A (en) * 2015-08-17 2017-03-01 洛阳健特生物科技有限公司 Peony seed oil supercritical CO 2 extraction technology
CN106281659A (en) * 2016-08-30 2017-01-04 铜陵亚通牡丹产业发展有限公司 Method for extracting protein in a kind of seed of Flos Moutan dregs of rice
CN108060012A (en) * 2017-12-19 2018-05-22 贵州航天乌江机电设备有限责任公司 A kind of extracting method of peony seed oil

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113383851A (en) * 2021-07-02 2021-09-14 山东省科学院菏泽分院 Method for extracting peony protein isolate for oil
CN113383851B (en) * 2021-07-02 2023-09-01 山东省科学院菏泽分院 Method for extracting peony isolated protein for oil

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